CN114652631A - Composition and cosmetic for removing dark eye circles and preparation method thereof - Google Patents
Composition and cosmetic for removing dark eye circles and preparation method thereof Download PDFInfo
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Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to a composition for removing dark circles, a cosmetic and a preparation method thereof. The composition for removing dark eye circles comprises the following components in parts by weight: 0.05-0.7 part of glucosyl hesperidin, 0.005-0.1 part of carboxymethyl chitosan, 0.001-0.1 part of glabridin, 0.0001-0.05 part of palmitoyl tripeptide-5 and 0.0001-0.06 part of passion fruit extract. The composition for removing dark under-eye circles provided by the invention has interaction and all-round coordination, plays an optimal role in repairing eye skin, reduces the area of serious pigmentation, improves the strength of capillary vessels and lymphatic vessels, reduces capillary vessel penetration and blood stasis, and finally achieves the effect of reducing dark under-eye circles.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a composition for removing dark circles, a cosmetic and a preparation method of the cosmetic.
Background
The black eye, commonly known as panda' is an annular eye which is located in the infraorbital areas on both sides and appears dark green or dark tea, which is a common eye problem. The eye skin has the following characteristics: the thickness of the eye skin is 0.6-4.0mm, which is 1/3-1/5 of the thickness of the face skin; secondly, the skin is continuously stretched when the eye blinks every day; thirdly, only sebaceous glands and abnormal sweat glands are arranged around the eyes, so the water-fat membrane has small protective effect on the skin of the eyes; fourthly, the skin at the eyes has low fat content and lacks elastic fiber and collagen structure, so that the skin at the eyes easily loses elasticity and even has the phenomenon of premature senility; the nerve fibers and capillary vessels around the eyes are high in distribution density, and poor blood circulation easily causes dim and fatigue of the eyes. Therefore, the phenomena of dim skin and loose skin at the eyes easily occur due to irregular daily work and rest, improper use of the eyes and the like, and the problems of black eye circles, under-eye bags, fish tail lines, fat particles and the like occur.
Studies have shown that the formation of dark circles is mainly associated with pigmentation and vascular changes. The black eye can be divided into four types, namely a vascular type, a pigment type, a relaxation type and a compound type according to the formation mechanism of the black eye. The blood vessel type black eye ring is usually in a black and dark color, the blood flow speed in the microvascular is slow due to factors such as insufficient sleep, eye fatigue and the like, the blood volume is increased, the oxygen consumption is increased, the hypoxia heme is greatly increased, the phenomena of blood stasis and edema of the skin around the eyes are caused, and the black eye ring is displayed after light reflection; the pigment type black eye is dark brown, and is mainly characterized in that pigment deposits around eyes caused by long-term sun exposure, excessive skin dryness and blood retention; the loose black eye is a depression generated by aging and thinning of eye skin and loss of collagen, and a cyan shadow is formed at the bottom of an eye socket; the fourth composite black eye is a mixed black eye, which is the case that 2-3 black eyes exist in the first three types at the same time.
At present, more and more people are deeply troubled by dark circles. Therefore, in recent years, the cosmetic products for the black eye repair and the eye care are increasingly popularized, and the demand for the eye repair care is also greatly increased. However, although there are a number of black eye removing products in the market at present, the mechanism and function of the products are single, and the products cannot achieve a good black eye removing effect due to the fact that the comprehensive cause of the black eye is not considered, so people have strong demands for development of novel black eye removing products.
For example, patent CN112656745A discloses an eye anti-aging nutrient solution, and a preparation method and application thereof. The nutrient solution is prepared by using seaweed extract, wheat extract and oat extract rich in anions and skin hematopoiesis function to improve skin texture; and whitening by cherry extract, grape seed extract, pomegranate extract and yeast extract. For another example, patent CN113181103A discloses an eye essence for fading black eye circles and eye wrinkles, which is prepared from the following raw materials, by weight, 3-5 parts of glycerol, 2-4 parts of butanediol, 0.5 part of p-hydroxyacetophenone, 0.2 part of sodium polyacrylate, 0.05 part of allantoin, 2-5 parts of deionized water, 2-5 parts of lactobacillus strain extract, 2-5 parts of tea leaf extract, 2-5 parts of pomegranate peel extract, 2-5 parts of small fruit coffee seed extract, 2-5 parts of euglena gracilis polysaccharide, 2-5 parts of hydrolyzed collagen, 0.5-1 part of placental protein, 0.5 part of 1, 2-hexanediol, and 0.05-0.1 part of acetyl hexapeptide.
However, the technical scheme has a single mechanism and function, and does not have a good black eye removing effect because the comprehensive cause of the black eye is not considered. Therefore, there is a strong need for the development of new eye products for removing dark circles.
Disclosure of Invention
The invention provides a composition and a cosmetic for removing dark circles and a preparation method thereof, and aims to overcome the defects in the prior art. The composition for removing dark eye circles provided by the invention has interaction and all-round coordination, plays the best role of repairing eye skin, reduces the area of serious pigmentation, improves the strength of capillary vessels and lymphatic vessels, reduces the capillary vessel penetration and blood stasis, and finally achieves the effect of reducing dark eye circles.
The technical scheme of the invention is as follows:
the composition for removing dark eye circles comprises the following components in parts by weight: 0.05-0.7 part of glucosyl hesperidin, 0.005-0.1 part of carboxymethyl chitosan, 0.001-0.1 part of glabridin, 0.0001-0.05 part of palmitoyl tripeptide-5 and 0.0001-0.06 part of passion fruit extract. The composition starts from the formation mechanism of dark eye circles, and is a product with stronger black eye circle removing effect by reducing pigmentation, inhibiting inflammation, improving vasodilation, promoting lymphatic circulation, enhancing collagen to compact eye skin and the like.
Further, the composition for removing dark circles comprises the following components in parts by weight: 0.3 part of glucosyl hesperidin, 0.05 part of carboxymethyl chitosan, 0.07 part of glabridin, 0.015 part of palmitoyl tripeptide-5 and 0.04 part of passion fruit extract. The fructus Plumeriae Acutifoliae extract is fructus Plumeriae Acutifoliae (PASSIFLORA EDULIS) extract.
In addition, the invention also provides a cosmetic for removing black eye circles, which comprises the composition for removing black eye circles and an auxiliary agent.
Further, the black eye removing cosmetic comprises the following auxiliary agents: the composition for removing dark circles under the eyes, EDTA disodium, propylene glycol, 1, 2-hexanediol, p-hydroxyacetophenone and water.
Moreover, the invention also provides a preparation method of the cosmetic for removing dark circles, which comprises the following steps:
(1) accurately weighing the components in proportion:
component 1: EDTA disodium, propylene glycol, 1, 2-hexanediol and p-hydroxyacetophenone;
and (2) component: glucosyl hesperidin, carboxymethyl chitosan, glabridin, palmitoyl tripeptide-5, and fructus Plumeriae Acutifoliae extract;
(2) adding the components of the component 1 and water into a pot, heating, homogenizing, stirring, defoaming, and then continuously stirring and cooling;
(3) maintaining the temperature of the material in the pot; dissolving and dispersing the component 2 uniformly, adding into a pot, homogenizing, stirring, cooling, and discharging. Some raw materials in the component 2 are powder, some raw materials are liquid, and the powder is dissolved after the raw materials are mixed together.
Further, the heating temperature in the step (2) is 80-85 ℃.
Further, the homogenization speed in the step (2) is 2000-3000rpm, and the time is 2-5 min; the homogenization speed in the step (3) is 2000-3000rpm, and the time is 2-4 min.
Further, the stirring speed before the foaming operation in the step (2) is 10-25rpm, and the time is 3-5 min.
Further, in the step (2), vacuum defoaming is adopted for defoaming.
Further, the stirring is continued in the step (2) to reduce the temperature: stirring at 10-25rpm, and cooling to 45 deg.C; in the step (3), the stirring speed is 10-25rpm, and the temperature is reduced to 30 ℃.
The invention starts from the formation mechanism of dark eye circles, comprehensively considers the aspects of reducing pigmentation, inhibiting inflammation, improving vasodilation, promoting lymphatic circulation, strengthening collagen and compacting eye skin and the like, and finally develops the composition for removing the dark eye circles.
By matching of multiple efficacy mechanisms, the carboxymethyl chitosan is adopted to effectively inhibit the activity of inflammatory factors; the glabridin can effectively reduce melanin deposition around eyes, resist external invasion and free radicals and reduce skin moisture loss, so that dark eye circles are effectively relieved and removed, skin aging is delayed, and skin luster is improved; moreover, as the skin elasticity is reduced due to the decrease of the expression of tissue growth factor beta due to the aging, the palmitoyl tripeptide-5 promotes the synthesis of collagen I by activating the tissue growth factor beta and acts on the hyaluronic acid synthesis of aged fibroblasts; promoting collagen synthesis and protecting collagen from degradation; in addition, glucosyl hesperidin can reduce the amount of liquid accumulated in the area to eliminate edema and improve the metabolism of skin by reducing the permeability of blood vessels in the area and promoting the regeneration of lymphatic vessels. It is noted that the glucosyl hesperidin, glabridin, palmitoyl tripeptide-5 and the eggnum fruit extract are compounded, so that the effect is obviously superior to that of single or simple combination, and the effects of reducing eye edema, resisting inflammation, enhancing skin elasticity, calming, strongly moistening skin and fading dark circles are realized.
Compared with the prior art, the composition and the cosmetic for removing dark circles and the preparation method thereof provided by the invention have the following advantages:
the composition for removing dark under-eye circles provided by the invention comprehensively considers the aspects of reducing pigmentation, inhibiting inflammation, improving vasodilation, promoting lymphatic circulation, strengthening collagen and tightening eye skin and the like, and realizes the effects of reducing eye edema, resisting inflammation, strengthening skin elasticity, calming and strongly moistening skin and lightening dark under-eye circles. Wherein glucosyl hesperidin, carboxymethyl chitosan, glabridin, palmitoyl tripeptide-5 and the passion fruit extract interact to cooperatively play a role in effectively repairing eye skin, improving the strength of capillary vessels and lymphatic vessels while reducing the area of serious pigmentation, reducing the permeation and blood stasis of the capillary vessels, finally realizing the change of skin pigmentation and effectively eliminating dark circles.
Detailed Description
The present invention is further illustrated by the following description of specific embodiments, which are not intended to limit the invention, and various modifications and improvements can be made by those skilled in the art based on the basic idea of the invention, but the invention is within the protection scope of the invention.
Wherein glucosyl hesperidin used in the invention is purchased from Hayashibara co, Ltd; carboxymethyl chitosan was purchased from shanghai chunlu biochemistry ltd; glabridin was purchased from Shanghai Orly practice Co., Ltd; extracts of passion fruit (PASSIFLORA EDULIS) fruits were purchased from ichima PHARCOS co., LTD; the other reagents are common reagents and can be purchased from conventional reagent production and sale companies.
Example 1
A preparation method of a cosmetic for removing dark circles comprises the following steps:
(1) accurately weighing the components in proportion:
component 1: EDTA disodium, propylene glycol, 1, 2-hexanediol and p-hydroxyacetophenone;
and (2) component: glucosyl hesperidin, carboxymethyl chitosan, glabridin, palmitoyl tripeptide-5, and fructus Plumeriae Acutifoliae extract;
(2) adding the components of the component 1 and water into a pot, and heating to 80 ℃; homogenizing at 2000rpm for 2 min; stirring at 10rpm for 3 min; defoaming in vacuum; stirring at the speed of 10rpm, and then continuously stirring and cooling to 45 ℃;
(3) maintaining the temperature of the material in the pot, dissolving and dispersing the component 2 uniformly, adding into the pot, homogenizing at 2000rpm for 2 min; stirring at 10rpm, cooling to 30 deg.C, and discharging.
The dosage ratio of the component 1 to the component 2 is 1: 6.38; wherein, the component 1 comprises the following components in parts by weight: 0.03 part of EDTA disodium, 2.0 parts of propylene glycol, 0.5 part of 1, 2-hexanediol and 0.5 part of p-hydroxyacetophenone. The dosage of the component 1, the component 2 and the water in the cosmetic for removing the dark circles is 100 parts by weight. Wherein the components of component 2 are shown in Table 1.
Example 2
A preparation method of a cosmetic for removing dark circles comprises the following steps:
(1) accurately weighing the components in proportion:
component 1: EDTA disodium, propylene glycol, 1, 2-hexanediol and p-hydroxyacetophenone;
and (2) component: glucosyl hesperidin, carboxymethyl chitosan, glabridin, palmitoyl tripeptide-5, and fructus Plumeriae Acutifoliae extract;
(2) adding the components of the component 1 and water into a pot, and heating to 85 ℃; homogenizing at 3000rpm for 5 min; stirring at 25rpm for 5 min; defoaming in vacuum; stirring at the speed of 25rpm, and then continuously stirring and cooling to 45 ℃;
(3) maintaining the temperature of the material in the pot; dissolving and dispersing the component 2 uniformly, adding into a pot, and homogenizing at 3000rpm for 4 min; stirring at 25rpm, cooling to 30 deg.C, and discharging.
The dosage ratio of the component 1 to the component 2 is 1: 6.38; wherein, the component 1 comprises the following components in parts by weight: 0.03 part of EDTA disodium, 2.0 parts of propylene glycol, 0.5 part of 1, 2-hexanediol and 0.5 part of p-hydroxyacetophenone. The dosage of the component 1, the component 2 and the water in the cosmetic for removing the dark circles is 100 parts by weight. Wherein the components of component 2 are shown in Table 1.
Example 3
A preparation method of a cosmetic for removing dark circles comprises the following steps:
(1) accurately weighing the components in proportion:
component 1: EDTA disodium, propylene glycol, 1, 2-hexanediol and p-hydroxyacetophenone;
and (2) component: glucosyl hesperidin, carboxymethyl chitosan, glabridin, palmitoyl tripeptide-5, and fructus Plumeriae Acutifoliae extract;
(2) adding the components of the component 1 and water into a pot, and heating to 80 ℃; homogenizing at 2500rpm for 3 min; stirring at 15rpm for 4 min; defoaming in vacuum; stirring at the speed of 15rpm, and then continuously stirring and cooling to 45 ℃;
(3) maintaining the temperature of the material in the pot; dissolving and dispersing the components 2 uniformly, adding into a pan, homogenizing at 2500rpm for 2min at stirring speed of 20rpm, cooling to 30 deg.C, stirring at 10rpm, and discharging.
The dosage ratio of the component 1 to the component 2 is 1: 6.38; wherein, the component 1 comprises the following components in parts by weight: 0.03 part of EDTA disodium, 2.0 parts of propylene glycol, 0.5 part of 1, 2-hexanediol and 0.5 part of p-hydroxyacetophenone. The dosage of the component 1, the component 2 and the water in the cosmetic for removing the dark circles is 100 parts by weight. Wherein the components of component 2 are shown in Table 1.
Example 4
The preparation method of the embodiment 4 is similar to that of the embodiment 3, wherein the using ratio of the component 1 to the component 2 is 1: 6.38; wherein, the component 1 comprises the following components in parts by weight: 0.03 part of EDTA disodium, 2.0 parts of propylene glycol, 0.5 part of 1, 2-hexanediol and 0.5 part of p-hydroxyacetophenone. The dosage of the component 1, the component 2 and the water in the cosmetic for removing the dark circles is 100 parts by weight. Wherein the components of component 2 are shown in Table 1.
Comparative examples 1 to 5
Comparative examples 1 to 5 provide black eye removing cosmetics prepared in the same manner as in example 3 except that the component 2 is different in composition, and the composition of the component 2 in comparative examples 1 to 5 is shown in Table 1.
Table 1 formula table
Note: the amounts of the components in the table are "parts by weight"; the fructus Plumeriae Acutifoliae extract is fructus Plumeriae Acutifoliae (PASSIFLORA EDULIS) extract.
Test examples: evaluation of efficacy
1. Instrument and sample:
the instrument comprises the following steps: skin elasticity tester MPA 580; skin melanin and heme test probe MX 18; skin color test probe CL 400.
Sample preparation: the black eye removing cosmetic samples obtained in examples 1 to 4 and comparative examples 1 to 5 are 9 types in total.
2. Selection of subjects:
qualified volunteers are selected and signed with an informed consent, and finally 90 persons are completed, and 10 volunteers are tried on each sample.
And (3) inclusion standard: healthy female volunteers with a habit of daily use of skin care products, Chinese, 35-45 years old; the face of the volunteer has fine lines/wrinkles around eyes and is not sensitive to common cosmetics; the compliance of the subjects is high.
Exclusion criteria: those who have used antihistamines for the last week or immunosuppressants for the last month; those who have used any anti-inflammatory drug on the test site in approximately two months; insulin dependent diabetes mellitus patients; patients suffering from respiratory diseases undergoing treatment; people with allergic constitution, allergic dermatitis and the like have a skin disease history; people who are receiving dermatology treatment or people who take light basic acids, whitening and anti-aging medicines within one month; the tested area has large area of birthmarks, scratch marks, leukoplakia, pigmented nevi, keloids and other skin characterizers which influence the test.
3. And (3) testing environmental conditions: the test environment temperature is 20-22 ℃, the humidity is 40-60%, and real-time dynamic monitoring is carried out.
4. The product using method comprises the following steps: the samples obtained in the examples and comparative examples were used in groups 9. The test samples were applied at a frequency of 0.2 g/application, 2 times/day (1 time each in the morning and evening), and periocular skin (under the eyes and the lines of the corners of the eyes) was used. During the test, subjects were protected from excessive uv exposure.
5. The testing process comprises the following steps:
(1) skin color test
Before use and at the 4 th week after use, the face cleaning standard is used for cleaning, after standing in a constant temperature and humidity chamber for 20min, the skin color test probe, the skin melanin test probe and the heme test probe are used for measuring the L, a, b and MI values of the skin at the test positions respectively, each test area is tested for three times, and the ITA DEG value (the increase of the ITA DEG value indicates the skin lightening) is recorded and calculated.
(2) Skin elasticity test
Opening the software of the current meter Q, clicking the Measurement of a toolbar or directly clicking a Measurement button at the upper right corner, taking down the probe cover after the pump is started, clicking OK, vertically and lightly contacting the probe with the skin after being cleaned or smeared with a sample and the like within 5s of reciprocal time, starting the test by properly retracting all springs at the top end of the probe, and moving the probe away until the test cycle time is over, and covering the probe cover.
(3) Skin moisture test
A. Skin moisture content testing procedure
Opening MPA5 software, clicking Corneometer10030770 button on the upper right corner, taking off the probe cover, vertically and lightly pressing the probe on the skin after cleaning or sample smearing treatment, etc., sensing that the spring is inside the probe to stretch and contract, displaying the test result and the average value in a window after 1s, optionally selecting not less than 3 points at the test skin part, testing, taking the average value, and covering the probe cover.
(4) Skin moisture loss test procedure
Opening MPA5 software, clicking Tewameter10041249 button at the upper right corner, taking off the probe cover, vertically and lightly pressing the shorter end of the probe cylindrical hollow cavity against the skin after cleaning or sample smearing treatment, lightly pressing handle white button, displaying a test value in the window every 1s, when the 5 th time is tested, starting to display an average value, requiring the test to take the average value for no less than 6 times, lightly pressing the handle white button, ending the test, and covering the probe cover.
And (4) calculating and analyzing results:
a data arrangement mode: the data output is the average of 10 people per group.
6. And (3) testing results:
ITA ° value variation amount:
TABLE 2ITA DEG value variation amount
Skin elasticity test:
the value of the elasticity R2 represents the ratio of the amount of springback of the skin in the absence of negative pressure to the maximum amount of stretch in the presence of negative pressure, and a ratio closer to 1 indicates better skin elasticity.
Table 3 skin elasticity test
| Before use | After 4 weeks of use | Rate of improvement/%) | |
| Example 1 | 0.654 | 0.756 | 15.59 |
| Example 2 | 0.65 | 0.754 | 16 |
| Example 3 | 0.655 | 0.795 | 21.37 |
| Example 4 | 0.64 | 0.75 | 17.18 |
| Comparative example 1 | 0.642 | 0.715 | 11.37 |
| Comparative example 2 | 0.652 | 0.711 | 9.05 |
| Comparative example 3 | 0.655 | 0.732 | 11.75 |
| Comparative example 4 | 0.645 | 0.732 | 13.48 |
| Comparative example 5 | 0.655 | 0.733 | 11.91 |
Skin moisture test results:
table 4 skin moisture test
Transdermal water loss test data:
TABLE 5 transdermal Water loss test
| Before use | After 4 weeks of use | Rate of improvement/%) | |
| Example 1 | 12.12 | 9.93 | 18.07 |
| Example 2 | 11.81 | 8.85 | 25.06 |
| Example 3 | 12 | 8.64 | 28 |
| Example 4 | 12.51 | 9.86 | 21.18 |
| Comparative example 1 | 12.33 | 10.85 | 12 |
| Comparative example 2 | 11.93 | 10.73 | 10.06 |
| Comparative example 3 | 11.77 | 10 | 15.04 |
| Comparative example 4 | 12.12 | 10.12 | 16.5 |
| Comparative example 5 | 12 | 10.2 | 15 |
According to the data of the groups, the skin brightness near the eye circumference is effectively improved after the tester uses the test sample for four weeks, namely the black eye is faded; it is also shown by elasticity data and skin moisture data that the elasticity of the skin is extracted and a repair is obtained. The results show that the effect combination of glucosyl hesperidin, carboxymethyl chitosan, glabridin, palmitoyl tripeptide-5 and the passion fruit extract in the invention is added into the essence, so that the comprehensive interaction can be realized, the optimal eye skin repairing effect can be coordinately played, the skin pigmentation can be changed, the dark eye circles can be eliminated, the area with serious pigmentation can be reduced, the strength of capillary vessels and lymphatic vessels can be improved, the capillary vessel penetration and blood siltation can be reduced, and the dark eye circles can be reduced.
Wherein, the composition described in the embodiment 3 is a preferable component, and the proportion of each component of the component 2 is as follows: glucosyl hesperidin 0.3%, carboxymethyl chitosan 0.05%, glabridin 0.07%, palmitoyl tripeptide-5% in 0.015% and plumeria rubra extract 0.04%.
The foregoing embodiments are merely illustrative of the principles and utilities of the present invention and are not intended to limit the invention. Any person skilled in the art can modify or change the above-mentioned embodiments without departing from the spirit and scope of the present invention. Accordingly, it is intended that all equivalent modifications or changes which can be made by those skilled in the art without departing from the spirit and technical spirit of the present invention be covered by the claims of the present invention.
Claims (10)
1. The composition for removing dark eye circles is characterized by comprising the following components in parts by weight: 0.05-0.7 part of glucosyl hesperidin, 0.005-0.1 part of carboxymethyl chitosan, 0.001-0.1 part of glabridin, 0.0001-0.05 part of palmitoyl tripeptide-5 and 0.0001-0.06 part of passion fruit extract.
2. The composition for removing dark circles according to claim 1, which is characterized by comprising the following components in parts by weight: 0.3 part of glucosyl hesperidin, 0.05 part of carboxymethyl chitosan, 0.07 part of glabridin, 0.015 part of palmitoyl tripeptide-5 and 0.04 part of passion fruit extract.
3. A black eye removal cosmetic which is characterized by comprising the black eye removal composition of claim 1 or 2 and an auxiliary agent.
4. The cosmetic for removing dark circles in accordance with claim 3, wherein the adjuvant is disodium EDTA, propylene glycol, 1, 2-hexanediol, p-hydroxyacetophenone, and water.
5. The preparation method of the black eye removing cosmetic as claimed in claim 4, wherein the preparation method comprises the following steps:
(1) accurately weighing the components in proportion:
component 1: EDTA disodium, propylene glycol, 1, 2-hexanediol and p-hydroxyacetophenone;
and (2) component: glucosyl hesperidin, carboxymethyl chitosan, glabridin, palmitoyl tripeptide-5, and fructus Plumeriae Acutifoliae extract;
(2) adding the components of the component 1 and water into a pot, heating, homogenizing, stirring, defoaming, and then continuously stirring and cooling;
(3) maintaining the temperature of the material in the pot; dissolving and dispersing the component 2 uniformly, adding into a pot, homogenizing, stirring, cooling, and discharging.
6. The method according to claim 5, wherein the heating temperature in the step (2) is 80 to 85 ℃.
7. The method as claimed in claim 5, wherein the homogenization speed in step (2) is 2000-3000rpm for 2-5 min; the homogenization speed in the step (3) is 2000-3000rpm, and the time is 2-4 min.
8. The method according to claim 5, wherein the stirring speed before the foaming in the step (2) is 10 to 25rpm for 3 to 5 min.
9. The method of claim 5, wherein the defoaming in step (2) is performed by vacuum defoaming.
10. The method according to claim 5, wherein the subsequent stirring and cooling in step (2) is carried out by: stirring at 10-25rpm, and cooling to 45 deg.C; in the step (3), the stirring speed is 10-25rpm, and the temperature is reduced to 30 ℃.
Priority Applications (1)
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115363986A (en) * | 2022-09-29 | 2022-11-22 | 广东丸美生物技术股份有限公司 | Skin care composition with black eye improving effect, preparation method thereof and cosmetic |
| CN115531266A (en) * | 2022-09-30 | 2022-12-30 | 泉后(广州)生物科技研究院有限公司 | Composition for removing eye bags and application thereof |
| CN115778862A (en) * | 2022-12-03 | 2023-03-14 | 周嘉奇 | Make-up base and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108403526A (en) * | 2018-05-12 | 2018-08-17 | 佛山云裳化妆品有限公司 | A kind of plant composition for skin care removing pouch and application |
| CN110227053A (en) * | 2019-07-12 | 2019-09-13 | 惠州市好好爱日化用品有限公司 | Compact maintenance eye-care compositions and its preparation and application |
| CN111973506A (en) * | 2020-07-23 | 2020-11-24 | 广州市科能化妆品科研有限公司 | Composition for resisting wrinkles, removing dark circles and removing pouches and application thereof |
-
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- 2022-04-22 CN CN202210426269.0A patent/CN114652631B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108403526A (en) * | 2018-05-12 | 2018-08-17 | 佛山云裳化妆品有限公司 | A kind of plant composition for skin care removing pouch and application |
| CN110227053A (en) * | 2019-07-12 | 2019-09-13 | 惠州市好好爱日化用品有限公司 | Compact maintenance eye-care compositions and its preparation and application |
| CN111973506A (en) * | 2020-07-23 | 2020-11-24 | 广州市科能化妆品科研有限公司 | Composition for resisting wrinkles, removing dark circles and removing pouches and application thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115363986A (en) * | 2022-09-29 | 2022-11-22 | 广东丸美生物技术股份有限公司 | Skin care composition with black eye improving effect, preparation method thereof and cosmetic |
| CN115531266A (en) * | 2022-09-30 | 2022-12-30 | 泉后(广州)生物科技研究院有限公司 | Composition for removing eye bags and application thereof |
| CN115531266B (en) * | 2022-09-30 | 2024-03-12 | 泉后(广州)生物科技研究院有限公司 | Composition for removing pouch and application thereof |
| CN115778862A (en) * | 2022-12-03 | 2023-03-14 | 周嘉奇 | Make-up base and preparation method thereof |
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| CN114652631B (en) | 2023-10-13 |
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