CN108524395A - One group of moisturizing whitening mask liquid and preparation method thereof - Google Patents
One group of moisturizing whitening mask liquid and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61K8/9728—Fungi, e.g. yeasts
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention discloses one group of moisturizing whitening mask liquid and preparation method thereof, which includes the component of following quality proportioning：2~6 parts of glycerine, 0.1~0.5 part of SANGELOSE 60L, 0.1~0.5 part of PEG 14M, 0.05~0.2 part of Sodium Hyaluronate, 0.5~2 part of AA2G, 0.5~3 part of Isin glue collagen, 0.2~0.5 part of 17/6 copolymers of PEG/PPG, 1,3 3~8 parts of butanediols, 0.1~0.5 part of Phenoxyethanol, 0.1~0.5 part of 40 rilanit specials of PEG, 0.1~0.5 part of methyl hydroxybenzoate, 0.1~0.5 part of dipotassium glycyrrhizinate, 5~10 parts of sodium citrate buffer solution, 0~1 part of plant extraction liquid add deionized water to 100 parts of full dose.Using SANGELOSE 60L as efficient thickeners, thickening effect is not influenced the present invention by pH value and ionic strength substantially.The protective film of soft comfortable can be formed after use on the skin, there is good moistening effect, nourishes rough skin.Quality of the present invention is salubrious, the effect of easily absorbing, can smoothing microgroove, realize deep moisturizing, and the present invention prevents skin obscure by inhibiting the formation of melanin, reduction to have melanin, and whitening effect is more stable, lasting.
Description
Technical field
The invention belongs to technical field of skin care, and in particular to one group high moisturizing whitening mask liquid and preparation method thereof.
Background technology
It is continuously improved as people realize the maintenance of skin, various skin care brands are come into being with category.In recent years, face
Film is even more greatly to be pursued by female consumer.The most basic and most important purpose of facial mask is in daily face cleaning and basis
Skin is maintained and is repaired between skin care, realizes its specific function, for example, replenishing water and preserving moisture, Whitening, spot, antiallergic of releiving,
Smoothing wrinkle anti-aging, balance skin grease etc..The principle of facial mask is to utilize the of short duration time for resting on face, and face skin is temporary
When be isolated with extraneous pollution, promote the pore of skin expand, promote sweat gland secretion and metabolic, be conducive to skin exclusion table
The oil substances of the product and accumulation of chrotoplast metabolism, nutritional ingredient penetrates into the cuticula of epidermis in facial mask, makes skin
Become soft, bright, flexible.
Nowadays facial mask on the market mostly (is paid by thickener of carbomer and adjusts female, Li Jihua, Wei Xiaoyi, Chang Gang, Xia Wen, Cui
A kind of beautiful tea tree hydrosol anti-acne jelly facial masks of rainbow and preparation method thereof [P] Chinese patents： CN105434290A,
2016.03.30；WANG XIAOYAN anti-acne plant extract facial mask [P] Chinese patents：CN106580805A, 2017.04.26), but block
The thickening effect of wave nurse is affected by pH value, it usually needs adds the alkaline matters such as triethanolamine, sodium hydroxide to improve
Consistency, prepares relatively complicated, easily causes irritation to skin, increases skin burden.To overcome the said goods disadvantage, we use
Some new materials prepare moisturizing whitening mask, and product can form comfortable protective film and lock moisture, improve moistening effect,
And there is good whitening function.
Invention content
The purpose of the present invention is to provide one group of moisturizing whitening mask liquid and preparation method thereof, the facial mask liquid deep moisturizing,
Moisturizing whitening effect is apparent, and preparation method is simple, easy to use.
To reach said effect, the present invention adopts the following technical scheme that but not limited to this：
One group of whitening moisturizing face masque liquid, includes the component of following mass fraction：2~6 parts of glycerine, hypromellose are hard
0.1~0.5 part of fat oxygen ether (SANGELOSE-60L), 0.1~0.5 part of PEG-14M, 0.05~0.2 part of Sodium Hyaluronate, L- are anti-
Bad 0.5~2 part of hematic acid 2- glucosides (AA2G), 0.5~3 part of Isin glue collagen, PEG/PPG-17/6 copolymers 0.2~0.5
Part, 3~8 parts of 1,3 butylene glycol, 0.1~0.5 part of Phenoxyethanol, 0.1~0.5 part of Cremophor RH40, methyl hydroxybenzoate
0.1~0.5 part, 0.1~0.5 part of dipotassium glycyrrhizinate, 5~10 parts of sodium citrate buffer solution, 0~1 part of plant extracts, add from
Sub- water is to 100 parts of full dose.
Further, the plant extracts that can be added is 0.01~1 part, and the plant extracts can include as next
Kind or multiple combinations ingredient：Grape seed extract, Fructus Cucumidis sativi extract, tea tree extract, rose extract, green-tea extract, water
Fly Ji guest, ginseng extract, pine tree root extract, gadol extract, hamamelis extract, extractive of perilla, apple extraction
Object, Baical Skullcap root P.E, Turmeric P.E, Ganodenna Lucidum P.E.
The present invention using hypromellose tristearin oxygen ether (SANGELOSE-60L), PEG-14M combination as thickening
Agent, AA2G as whitening composition, the combination of PEG/PPG-17/6 copolymers, Cremophor RH40 as surfactant,
The facial mask performance of keeping humidity and whitening performance of preparation reach best, and the pH value of facial mask liquid is 5.5~6.8,
Mildly do not stimulate skin.
PEG/PPG-17/6 copolymers wherein in surfactant, Cremophor RH40 portion rate be 1：0.2~
2.5。
The present invention is using hypromellose tristearin oxygen ether (SANGELOSE-60L) as thickener, and thickening effect is not
It is influenced by pH value.And when using conventional carbomer as thickener, it needs to adjust pH, and the facial mask pair prepared by sodium hydroxide
The stimulation of skin is big.
The present invention provides a kind of preparation method of moisturizing whitening mask liquid, and described method includes following steps：
(1) sterilization after agitated kettle is cleaned；
(2) by glycerine, 1,3 butylene glycol, dipotassium glycyrrhizinate, methyl hydroxybenzoate, PEG-14M, Phenoxyethanol, PEG-40 hydrogen
Change in castor oil, PEG/PPG-17/6 copolymers addition agitated kettle, is heated to 75~80 DEG C；
(3) after the component dissolving completely in step (2), stirring is cooled to 55 DEG C, is added in obtained mixture transparent
Matter acid sodium；
(4) AA2G is dissolved in sodium citrate buffer solution, AA2G storing solutions is made, it is spare；
(5) after the component dissolving completely in step (3), stirring is cooled to 40 DEG C, is added in obtained mixture
SANGELOSE-60L, Isin glue collagen, AA2G storing solutions, plant extracts, are uniformly mixed；
(6) be added deionized water be uniformly mixed, sterilizing to get.
Compared with prior art, the method have the advantages that：
1. the present invention is using SANGELOSE-60L as efficient thickeners, thickening effect is not strong by pH value and solion
Spend the influence of (sweat).The protective film of soft comfortable can be formed after use on the skin, nourishes rough skin has good moisturizing effect
Fruit.
2. Sodium Hyaluronate deep moisturizing of the present invention forms layer of transparent hydration shell in skin surface, increases skin keratin
The moisture of layer, penetrates into skin corium, makes the tender moistening of skin, has fabulous water conservation and water lock effect.
3. AA2G of the present invention is one of vitamin C derivatives, it is present in the enzyme in skin-α glucosidases using latter
It acts on AA2G to be allowed to slowly release free vitamin C, to realize white-skinned face function.
4. whitening moisturizing face masque liquid quality provided by the invention is salubrious, easily absorbs, there is deep moisturizing, significant whitening effect
Fruit, and preparation method is simple, it is easy to use.
Description of the drawings
Fig. 1 difference facial masks use rear skin moisture value variation diagram
Specific implementation mode
Below in conjunction with specific embodiment, the technical solution that the present invention is further explained, these embodiments are merely to illustrate
The present invention and do not limit the scope of the invention, after reading the present invention, those skilled in the art carry out the present invention
Various forms of modifications, equivalent replacement or improvement etc., fall within the application range as defined in the appended claims.
Embodiment 1
According to following preparation method and type PEG/PPG-17/6 copolymers, the PEG-40 hydrogen of one Surfactant of table
Change castor oil, PEG-60 rilanit specials are screened.
(1) sterilization after agitated kettle is cleaned；
(2) according to glycerine, 1,3 butylene glycol, dipotassium glycyrrhizinate, methyl hydroxybenzoate, the PEG- described in claim 1
14M, the number of Phenoxyethanol and surfactant are added in agitated kettle, are heated to 75~80 DEG C；
(3) after the component dissolving completely in step (2), stirring is cooled to 55 DEG C, and right is added in obtained mixture
It is required that the number of Sodium Hyaluronate described in 1；
(4) AA2G is dissolved in sodium citrate buffer solution, AA2G storing solutions is made, it is spare；
(5) after the component dissolving completely in step (3), stirring is cooled to 40 DEG C, and right is added in obtained mixture
It is required that the number of SANGELOSE-60L described in 1, Isin glue collagen, AA2G storing solutions, plant extracts, are uniformly mixed；
(6) be added deionized water be uniformly mixed, sterilizing to get.
The type of one surfactant of table is screened
The experimental results showed that apparent muddiness occurs in prescription three, therefore surfactant is set in moisturizing whitening mask liquid
PEG/PPG-17/6 copolymers and Cremophor RH40, when the two combines, solubilizing effect is best.
Embodiment 2
The dosage of Surfactant PEG/PPG-17/6 copolymers and Cremophor RH40 is screened, and the two is used
Amount design is as follows：
The dosage of two surfactant of table is screened
The experimental results showed that slight haziness occurs in prescription four, prescription five and prescription six are in clear state；Place is taken respectively
The facial mask liquid of side five and prescription six is applied to skin, and slight stimulation occurs in prescription six, and prescription five is mild non-stimulated.Therefore, really
Determine the dosage portion rate of Surfactant PEG/PPG-17/6 copolymers and PEG-40 rilanit specials in moisturizing whitening mask liquid
It is 1：0.2~2.5.
Embodiment 3
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：2 parts of glycerine, 0.1 part of SANGELOSE-60L, 0.1 part of PEG-14M, 0.05 part of Sodium Hyaluronate, 0.5 part of AA2G,
0.5 part of Isin glue collagen, 0.2 part of PEG/PPG-17/6 copolymers, 3 parts of 1,3- butanediols, 0.1 part of Phenoxyethanol, PEG-40 hydrogen
Change 0.1 part of castor oil, 0.1 part of methyl hydroxybenzoate, 0.1 part of dipotassium glycyrrhizinate, 5 parts of sodium citrate buffer solution, adds deionized water extremely
100 parts of full dose.
The preparation method of moisturizing whitening mask liquid of the present invention is included the following steps by the mass fraction of above-mentioned each ingredient：
(1) sterilization after agitated kettle is cleaned；
(2) by glycerine, 1,3 butylene glycol, dipotassium glycyrrhizinate, methyl hydroxybenzoate, PEG-14M, Phenoxyethanol, PEG-40 hydrogen
Change in castor oil, PEG/PPG-17/6 copolymers addition agitated kettle, is heated to 75~80 DEG C；
(3) after the component dissolving completely in step (2), stirring is cooled to 55 DEG C, is added in obtained mixture transparent
Matter acid sodium；
(4) AA2G is dissolved in sodium citrate buffer solution, AA2G storing solutions is made, it is spare；
(5) after the component dissolving completely in step (3), stirring is cooled to 40 DEG C, is added in obtained mixture
SANGELOSE-60L, Isin glue collagen, AA2G storing solutions, plant extracts, are uniformly mixed；
(6) be added deionized water be uniformly mixed, sterilizing to get.
Present invention immersion face paper is affixed on face when use or is applied directly to face, standing 15~after twenty minutes,
Being cleaned or being massaged with clear water makes the present invention absorb completely.
Embodiment 4
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：6 parts of glycerine, 0.5 part of SANGELOSE-60L, 0.5 part of PEG-14M, 0.2 part of Sodium Hyaluronate, 2 parts of AA2G, fish glue
1 part of former albumen, 0.3 part of PEG/PPG-17/6 copolymers, 8 parts of 1,3 butylene glycol, 0.3 part of Phenoxyethanol, PEG-40 hydrogenated castors
0.5 part of oil, 0.5 part of methyl hydroxybenzoate, 0.5 part of dipotassium glycyrrhizinate, 10 parts of sodium citrate buffer solution, 0.5 part of grape seed extract,
Add deionized water to 100 parts of full dose.
Preparation method is the same as embodiment 3.
Embodiment 5
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：3 parts of glycerine, 0.3 part of SANGELOSE-60L, 0.3 part of PEG-14M, 0.1 part of Sodium Hyaluronate, 1 part of AA2G, fish glue
0.8 part of former albumen, 0.3 part of PEG/PPG-17/6 copolymers, 5 parts of 1,3 butylene glycol, 0.3 part of Phenoxyethanol, PEG-40 hydrogenate castor
0.3 part of sesame oil, 0.3 part of methyl hydroxybenzoate, 0.5 part of dipotassium glycyrrhizinate, 8 parts of sodium citrate buffer solution, 1 part of tea tree extract, add
Deionized water is to 100 parts of full dose.
Preparation method is the same as embodiment 3.
Embodiment 6
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：3 parts of glycerine, 0.3 part of SANGELOSE-60L, 0.3 part of PEG-14M, 0.1 part of Sodium Hyaluronate, 1 part of AA2G, fish glue
0.5 part of former albumen, 0.3 part of PEG/PPG-17/6 copolymers, 5 parts of 1,3 butylene glycol, 0.3 part of Phenoxyethanol, PEG-40 hydrogenate castor
0.3 part of sesame oil, 0.3 part of methyl hydroxybenzoate, 0.5 part of dipotassium glycyrrhizinate, 8 parts of sodium citrate buffer solution, 1 part of Fructus Cucumidis sativi extract, add
Deionized water is to 100 parts of full dose.
Preparation method is the same as embodiment 3.
Embodiment 7
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：2 parts of glycerine, 0.4 part of SANGELOSE-60L, 0.1 part of PEG-14M, 0.05 part of Sodium Hyaluronate, 0.5 part of AA2G,
0.5 part of Isin glue collagen, 0.2 part of PEG/PPG-17/6 copolymers, 3 parts of 1,3- butanediols, 0.1 part of Phenoxyethanol, PEG-40 hydrogen
Change 0.1 part of castor oil, 0.1 part of methyl hydroxybenzoate, 0.1 part of dipotassium glycyrrhizinate, 6 parts of sodium citrate buffer solution, green-tea extract
0.8 part, add deionized water to 100 parts of full dose.
Preparation method is the same as embodiment 3.
Embodiment 8
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：2 parts of glycerine, 0.5 part of SANGELOSE-60L, 0.1 part of PEG-14M, 0.05 part of Sodium Hyaluronate, 0.5 part of AA2G,
3 parts of Isin glue collagen, 0.2 part of PEG/PPG-17/6 copolymers, 3 parts of 1,3 butylene glycol, 0.1 part of Phenoxyethanol, PEG-40 hydrogenations
0.1 part of castor oil, 0.1 part of methyl hydroxybenzoate, 0.1 part of dipotassium glycyrrhizinate, 9 parts of sodium citrate buffer solution, 0.02 part of silibinin,
Add deionized water to 100 parts of full dose.
Preparation method is the same as embodiment 3.
Embodiment 9
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：2 parts of glycerine, 0.2 part of SANGELOSE-60L, 0.1 part of PEG-14M, 0.05 part of Sodium Hyaluronate, 0.6 part of AA2G,
2 parts of Isin glue collagen, 0.2 part of PEG/PPG-17/6 copolymers, 3 parts of 1,3 butylene glycol, 0.3 part of Phenoxyethanol, PEG-40 hydrogenations
0.1 part of castor oil, 0.1 part of methyl hydroxybenzoate, 0.1 part of dipotassium glycyrrhizinate, 10 parts of sodium citrate buffer solution, apple extract 0.7
Part, add deionized water to 100 parts of full dose.
Preparation method is the same as embodiment 3.
Embodiment 10
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：3 parts of glycerine, 0.3 part of SANGELOSE-60L, 0.1 part of PEG-14M, 0.05 part of Sodium Hyaluronate, 1 part of AA2G, fish
2 parts of collagen, 0.2 part of PEG/PPG-17/6 copolymers, 3 parts of 1,3 butylene glycol, 0.2 part of Phenoxyethanol, PEG-40 hydrogenate castor
0.1 part of sesame oil, 0.2 part of methyl hydroxybenzoate, 0.1 part of dipotassium glycyrrhizinate, 5 parts of sodium citrate buffer solution, 0.3 part of extractive of perilla,
0.05 part of Baical Skullcap root P.E adds deionized water to 100 parts of full dose.
Preparation method is the same as embodiment 3.
Embodiment 11
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：4 parts of glycerine, 0.3 part of SANGELOSE-60L, 0.5 part of PEG-14M, 0.2 part of Sodium Hyaluronate, 0.5 part of AA2G, fish
3 parts of collagen, 0.2 part of PEG/PPG-17/6 copolymers, 2 parts of 1,3 butylene glycol, 0.1 part of Phenoxyethanol, PEG-40 hydrogenate castor
0.1 part of sesame oil, 0.3 part of methyl hydroxybenzoate, 0.1 part of dipotassium glycyrrhizinate, 6 parts of sodium citrate buffer solution, 0.1 part of Turmeric P.E,
Add deionized water to 100 parts of full dose.
Preparation method is the same as embodiment 3.
Embodiment 12
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：5 parts of glycerine, 0.4 part of SANGELOSE-60L, 0.1 part of PEG-14M, 0.1 part of Sodium Hyaluronate, 0.5 part of AA2G, fish
1 part of collagen, 0.2 part of PEG/PPG-17/6 copolymers, 2 parts of 1,3 butylene glycol, 0.2 part of Phenoxyethanol, PEG-40 hydrogenate castor
0.1 part of sesame oil, 0.1 part of methyl hydroxybenzoate, 0.1 part of dipotassium glycyrrhizinate, 5 parts of sodium citrate buffer solution, 0.2 part of rhodiola root add
Ionized water is to 100 parts of full dose.
Preparation method is the same as embodiment 3.
Embodiment 13
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：5 parts of glycerine, 0.2 part of SANGELOSE-60L, 0.2 part of PEG-14M, 0.15 part of Sodium Hyaluronate, 0.5 part of AA2G,
1 part of Isin glue collagen, 0.2 part of PEG/PPG-17/6 copolymers, 5 parts of 1,3 butylene glycol, 0.1 part of Phenoxyethanol, PEG-40 hydrogenations
0.1 part of castor oil, 0.5 part of methyl hydroxybenzoate, 0.1 part of dipotassium glycyrrhizinate, 5 parts of sodium citrate buffer solution, pine tree root extract 0.1
Part, add deionized water to 100 parts of full dose.
Preparation method is the same as embodiment 3.
Embodiment 14
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：3 parts of glycerine, 0.1 part of SANGELOSE-60L, 0.5 part of PEG-14M, 0.1 part of Sodium Hyaluronate, 0.5 part of AA2G, fish
2 parts of collagen, 0.3 part of PEG/PPG-17/6 copolymers, 3 parts of 1,3 butylene glycol, 0.5 part of Phenoxyethanol, PEG-40 hydrogenate castor
0.2 part of sesame oil, 0.2 part of methyl hydroxybenzoate, 0.1 part of dipotassium glycyrrhizinate, 5 parts of sodium citrate buffer solution, 0.3 part of ginseng extract,
Add deionized water to 100 parts of full dose.
Preparation method is the same as embodiment 3.
Embodiment 15
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：4 parts of glycerine, 0.5 part of SANGELOSE-60L, 0.1 part of PEG-14M, 0.05 part of Sodium Hyaluronate, 0.5 part of AA2G,
3 parts of Isin glue collagen, 0.2 part of PEG/PPG-17/6 copolymers, 5 parts of 1,3 butylene glycol, 0.3 part of Phenoxyethanol, PEG-40 hydrogenations
0.4 part of castor oil, 0.1 part of methyl hydroxybenzoate, 0.1 part of dipotassium glycyrrhizinate, 5 parts of sodium citrate buffer solution, camomile extract 0.2
Part, 0.5 part of hamamelis extract, add deionized water to 100 parts of full dose.
Preparation method is the same as embodiment 3.
Embodiment 16
The present embodiment provides a kind of moisturizing whitening mask liquid and preparation method thereof, which includes following mass fraction
Component：6 parts of glycerine, 0.5 part of SANGELOSE-60L, 0.5 part of PEG-14M, 0.07 part of Sodium Hyaluronate, 2 parts of AA2G, fish
3 parts of collagen, 0.5 part of PEG/PPG-17/6 copolymers, 8 parts of 1,3 butylene glycol, 0.2 part of Phenoxyethanol, PEG-40 hydrogenate castor
0.1 part of sesame oil, 0.5 part of methyl hydroxybenzoate, 0.1 part of dipotassium glycyrrhizinate, 5 parts of sodium citrate buffer solution, 0.1 part of Ganodenna Lucidum P.E,
0.2 part of ginseng extract adds deionized water to 100 parts of full dose.
Preparation method is the same as embodiment 3.
Embodiment 17
Moisturizing whitening mask liquid prepared by Example 3 carries out white-skinned face function inspection, and the method for inspection and result are as follows：
1. the preparation of solution
(1) phosphate buffer (PBS) of pH=6.8 is prepared
(2) preparation of l-tyrosine solution：Weigh l-tyrosine 22.65mg, with the phosphate buffer constant volume after precooling in
To get the l-tyrosine solution of a concentration of 200U/mL in 50mL volumetric flasks, 4 DEG C of refrigerations are spare.
(3) preparation of tyrosinase extracting solution：The potato that 4 DEG C are pre-chilled is cleaned, is removed the peel, chopping weighs in right amount in mortar
In.By 1：5(w：V) PBS is added in ratio, firmly squeezes.Extracting solution is filtered out with 2 layers of gauze, immediately in the rotating speed of 3000r/min
5min is centrifuged, takes supernatant spare in 4 DEG C of refrigerations.
(4) it is prepared by test solution：The facial mask liquid 10g for taking best prescription, adds deionized water constant volume in 100mL volumetric flasks,
Up to a concentration of 1mg/mL by test solution.
(5) preparation of AA2G comparison liquids：AA2G powder 0.01g are taken, deionized water constant volume is added in 10mL volumetric flasks,
Up to the AA2G comparison liquids of a concentration of 1mg/mL.
2. experimental implementation
Shown in table three, reagent is sequentially added into test tube, and 10min is kept the temperature in 30 DEG C of water-baths.It is then respectively adding junket ammonia
Sour zyme extract 1.0mL, mixing are transferred quickly to after reacting 1min at 30 DEG C in cuvette, and absorbance is measured at 475nm
Value, every group of parallel test three times, are denoted as T001, T002, T003.
Table trityrosine enzymatic activity test operation
Sample sets blank control 1 shown in table three is returned to zero, and negative control group is returned to zero with blank control 2, and positive controls are used
Blank control 3 is returned to zero, and gained sample sets absorbance value is denoted as A1, and negative control group absorbance value is denoted as A2, and positive controls are inhaled
Shading value is denoted as A3, and the inhibiting rate to tyrosinase is calculated as follows：
3. experimental result
The absorbance value that three groups of parallel tests measure is as shown in Table 4.
Four absorbance result (n=3) of table
The result shows that facial mask liquid is 69.54% to the inhibiting rate of tyrosinase.Therefore, the facial mask liquid pair that prepared by the present invention
Tyrosinase has inhibiting effect, has white-skinned face function.
Embodiment 18
Moisturizing whitening mask liquid prepared by Example 3 carries out moisture-keeping efficacy inspection, and the method for inspection and result are as follows：
Moisturizing whitening mask liquid and each 15mL of commercially available facial mask prepared by Example 3, is put into compression facial mask, waits for that it has been absorbed
It entirely and is sufficiently spread out, after spreading on 15min on hand, throws off facial mask, after remaining liq fully absorbs on hand, tested with moisture of skin
Instrument measures the variation of 30min inner skin water content in the same position of hand, and one group is measured per 2min, and every group of measurement 3 times is made even
Mean value.The result is shown in Figure 1：
It being measured through experiment, the skin moisture value before non-smearing mask substantially remains in 18%, after facial mask, moisture of skin
Value steeply rises, then because the aerial evaporation of moisture and skin are to the absorption of nutritional ingredient in facial mask, moisture value by
Gradually decline, self-made face pack is finally stablized and stablized 20% or so in 30% or so, ALBION healthy water facial masks.The result shows that this
Moisturizing whitening mask liquid prepared by invention has significant moistening effect.
Embodiment 19
Moisturizing whitening mask liquid prepared by Example 3 carries out sensory evaluation, and evaluation method and result are as follows：
20 parts of questionnaire is provided in this experiment altogether, and evaluation index includes the adhesion of facial mask liquid, irritation, the uniformity, painting
7 malleability, salubrious sense, lubrication sense and smell aspects are felt to give a mark according to 7 aspects, using arithmetic mean Data-Statistics,
Comprehensive evaluation result.Analyses Methods for Sensory Evaluation Results is shown in Table three.
Three Analyses Methods for Sensory Evaluation Results of table
The result shows that the facial mask liquid for preparing of the present invention it is mild it is non-stimulated, moisten moisturizing without bad smell, homogeneous, water.
Claims (6)
1. a kind of moisturizing whitening mask liquid, which is characterized in that include the component of following mass fraction：2~6 parts of glycerine,
0.1~0.5 part of SANGELOSE-60L, 0.1~0.5 part of PEG-14M, 0.05~0.2 part of Sodium Hyaluronate, AA2G 0.5~2
Part, 0.5~3 part of Isin glue collagen, 0.2~0.5 part of PEG/PPG-17/6 copolymers, 3~8 parts of 1,3 butylene glycol, Phenoxyethanol
0.1~0.5 part, 0.1~0.5 part of Cremophor RH40,0.1~0.5 part of methyl hydroxybenzoate, dipotassium glycyrrhizinate 0.1~0.5
Part, 5~10 parts of sodium citrate buffer solution, 0~1 part of plant extracts add deionized water to 100 parts of full dose.
2. moisturizing whitening mask liquid as described in claim 1, which is characterized in that 0.01~1 part of plant extracts.
3. moisturizing whitening mask liquid as described in claim 1, which is characterized in that PEG/PPG-17/6 copolymers, PEG-40 hydrogen
The portion rate for changing castor oil is 1：0.2~2.5.
4. moisturizing whitening mask liquid according to claim 2, which is characterized in that the plant extracts includes as next
Kind or multiple combinations ingredient：Grape seed extract, Fructus Cucumidis sativi extract, tea tree extract, rose extract, green-tea extract, water
Fly Ji guest, ginseng extract, pine tree root extract, gadol extract, hamamelis extract, extractive of perilla, apple extraction
Object, Baical Skullcap root P.E, Turmeric P.E, Ganodenna Lucidum P.E.
5. a kind of preparation method of one group of moisturizing whitening mask liquid as described in claim 1, which is characterized in that including following step
Suddenly：
(1) sterilization after agitated kettle is cleaned；
(2) glycerine, 1,3 butylene glycol, dipotassium glycyrrhizinate, methyl hydroxybenzoate, PEG-14M, Phenoxyethanol, PEG-40 are hydrogenated into castor
Sesame oil, PEG/PPG-17/6 copolymers are added in agitated kettle, are heated to 75~80 DEG C；
(3) after the component dissolving completely in step (2), stirring is cooled to 55 DEG C, and hyaluronic acid is added in obtained mixture
Sodium；
(4) AA2G is dissolved in sodium citrate buffer solution, AA2G storing solutions is made, it is spare；
(5) after the component dissolving completely in step (3), stirring is cooled to 40 DEG C, is added in obtained mixture
SANGELOSE-60L, Isin glue collagen, AA2G storing solutions, plant extracts, are uniformly mixed；
(6) be added deionized water be uniformly mixed, sterilizing to get.
6. the preparation method of moisturizing whitening mask according to claim 5, which is characterized in that the pH value of facial mask liquid is 5.5
~6.8.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109662902A (en) * | 2019-02-20 | 2019-04-23 | 广州娇美生物科技有限公司 | A kind of beautiful skin facial mask liquid and preparation method containing arbutin active matter |
| CN109771612A (en) * | 2019-03-13 | 2019-05-21 | 海安艾拉新材料有限公司 | A kind of preparation method of antibacterial face mask cream |
| CN110179690A (en) * | 2019-06-12 | 2019-08-30 | 杭州蓝朗生物技术有限公司 | A kind of collagen modified form facial mask and preparation method thereof |
| CN110585041A (en) * | 2019-09-27 | 2019-12-20 | 罗梅英 | Preparation method of blend liquid of Chinese herbal medicine mask powder |
| CN113171326A (en) * | 2021-06-01 | 2021-07-27 | 林标粧 | Whitening and moisturizing mask |
| CN114588074A (en) * | 2022-04-19 | 2022-06-07 | 孙廷胜 | Anti-aging whitening moisturizing mask and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109662902A (en) * | 2019-02-20 | 2019-04-23 | 广州娇美生物科技有限公司 | A kind of beautiful skin facial mask liquid and preparation method containing arbutin active matter |
| CN109771612A (en) * | 2019-03-13 | 2019-05-21 | 海安艾拉新材料有限公司 | A kind of preparation method of antibacterial face mask cream |
| CN110179690A (en) * | 2019-06-12 | 2019-08-30 | 杭州蓝朗生物技术有限公司 | A kind of collagen modified form facial mask and preparation method thereof |
| CN110585041A (en) * | 2019-09-27 | 2019-12-20 | 罗梅英 | Preparation method of blend liquid of Chinese herbal medicine mask powder |
| CN113171326A (en) * | 2021-06-01 | 2021-07-27 | 林标粧 | Whitening and moisturizing mask |
| CN114588074A (en) * | 2022-04-19 | 2022-06-07 | 孙廷胜 | Anti-aging whitening moisturizing mask and preparation method thereof |
| CN114588074B (en) * | 2022-04-19 | 2024-01-02 | 孙廷胜 | Anti-aging whitening moisturizing mask and preparation method thereof |
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Application publication date: 20180914 |