CN1140561C - 处理含二羟基化合物残留物的方法 - Google Patents

处理含二羟基化合物残留物的方法 Download PDF

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Publication number
CN1140561C
CN1140561C CNB971928096A CN97192809A CN1140561C CN 1140561 C CN1140561 C CN 1140561C CN B971928096 A CNB971928096 A CN B971928096A CN 97192809 A CN97192809 A CN 97192809A CN 1140561 C CN1140561 C CN 1140561C
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CN
China
Prior art keywords
steam
tower
dihydroxy compound
compound
reaction
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Expired - Fee Related
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CNB971928096A
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English (en)
Chinese (zh)
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CN1212712A (zh
Inventor
P・布劳内
P·布劳内
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BASF SE
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BASF SE
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Publication of CN1212712A publication Critical patent/CN1212712A/zh
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Publication of CN1140561C publication Critical patent/CN1140561C/zh
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/78—Preparation processes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/88—Separation; Purification; Use of additives, e.g. for stabilisation by treatment giving rise to a chemical modification of at least one compound
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/20—Dihydroxylic alcohols
    • C07C31/207—1,4-Butanediol; 1,3-Butanediol; 1,2-Butanediol; 2,3-Butanediol
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
    • C08G63/88—Post-polymerisation treatment
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J11/00—Recovery or working-up of waste materials
    • C08J11/02—Recovery or working-up of waste materials of solvents, plasticisers or unreacted monomers

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Sustainable Development (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CNB971928096A 1996-03-06 1997-03-04 处理含二羟基化合物残留物的方法 Expired - Fee Related CN1140561C (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE19608614A DE19608614A1 (de) 1996-03-06 1996-03-06 Verfahren zur Aufarbeitung von Dihydroxyverbindungen enthaltenden Rückständen
DE19608614.0 1996-03-06

Publications (2)

Publication Number Publication Date
CN1212712A CN1212712A (zh) 1999-03-31
CN1140561C true CN1140561C (zh) 2004-03-03

Family

ID=7787365

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB971928096A Expired - Fee Related CN1140561C (zh) 1996-03-06 1997-03-04 处理含二羟基化合物残留物的方法

Country Status (8)

Country Link
US (1) US6174970B1 (https=)
EP (1) EP0885252A2 (https=)
JP (1) JP2000506203A (https=)
KR (1) KR19990087569A (https=)
CN (1) CN1140561C (https=)
AU (1) AU2095197A (https=)
DE (1) DE19608614A1 (https=)
WO (1) WO1997032915A2 (https=)

Families Citing this family (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6245879B1 (en) * 1999-01-29 2001-06-12 Shell Oil Company Purification of 1,3-propanediol in carbonyl-containing stream
DE19929791A1 (de) * 1999-06-29 2001-02-01 Basf Ag Verfahren zur kontinuierlichen Herstellung von Polybutylenterephthalat aus Terephthalsäure und Butandiol
US6576774B2 (en) * 2000-07-20 2003-06-10 Shell Oil Company Process for recycling polytrimethylene terephthalate cyclic dimer
US6906164B2 (en) * 2000-12-07 2005-06-14 Eastman Chemical Company Polyester process using a pipe reactor
ES2540542T3 (es) * 2000-12-07 2015-07-10 Grupo Petrotemex, S.A. De C.V. Procedimiento de poliéster de bajo coste que usa un reactor tubular
DE10125677B4 (de) * 2001-05-25 2013-05-16 Lurgi Zimmer Gmbh Verfahren und Vorrichtung zur Herstellung von Polytrimethylenterephthalat
DE10125678B4 (de) * 2001-05-25 2011-04-14 Lurgi Zimmer Gmbh Verfahren und Vorrichtung zur Herstellung von Polyethylenterephthalat
US7264847B2 (en) * 2003-02-19 2007-09-04 Robert P. Bentley, Sr. Lower alkyl carboxylic acid moieties for preventing oxidative corrosion of metals and organoleptic stabilizer for food and beverages
US7135541B2 (en) 2003-06-06 2006-11-14 Eastman Chemical Company Polyester process using a pipe reactor
US7074879B2 (en) * 2003-06-06 2006-07-11 Eastman Chemical Company Polyester process using a pipe reactor
US7332548B2 (en) * 2004-03-04 2008-02-19 Eastman Chemical Company Process for production of a polyester product from alkylene oxide and carboxylic acid
US7649109B2 (en) * 2006-12-07 2010-01-19 Eastman Chemical Company Polyester production system employing recirculation of hot alcohol to esterification zone
US7943094B2 (en) 2006-12-07 2011-05-17 Grupo Petrotemex, S.A. De C.V. Polyester production system employing horizontally elongated esterification vessel
US20080139780A1 (en) * 2006-12-07 2008-06-12 Debruin Bruce Roger Polyester production system employing short residence time esterification
US7863477B2 (en) * 2007-03-08 2011-01-04 Eastman Chemical Company Polyester production system employing hot paste to esterification zone
US7847053B2 (en) * 2007-07-12 2010-12-07 Eastman Chemical Company Multi-level tubular reactor with oppositely extending segments
US7868129B2 (en) * 2007-07-12 2011-01-11 Eastman Chemical Company Sloped tubular reactor with spaced sequential trays
US7842777B2 (en) * 2007-07-12 2010-11-30 Eastman Chemical Company Sloped tubular reactor with divided flow
US7872090B2 (en) * 2007-07-12 2011-01-18 Eastman Chemical Company Reactor system with optimized heating and phase separation
US7868130B2 (en) * 2007-07-12 2011-01-11 Eastman Chemical Company Multi-level tubular reactor with vertically spaced segments
US7872089B2 (en) 2007-07-12 2011-01-18 Eastman Chemical Company Multi-level tubular reactor with internal tray
US7829653B2 (en) * 2007-07-12 2010-11-09 Eastman Chemical Company Horizontal trayed reactor
US7858730B2 (en) 2007-07-12 2010-12-28 Eastman Chemical Company Multi-level tubular reactor with dual headers
KR102306544B1 (ko) * 2017-09-07 2021-09-30 주식회사 엘지화학 에스터화 반응에서의 1가 알코올의 제거 방법 및 이를 포함하는 에스터 조성물의 제조 방법
KR102138788B1 (ko) * 2017-09-07 2020-07-28 주식회사 엘지화학 에스터 조성물의 제조 시스템 및 이를 이용한 에스터 조성물의 제조 방법

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3852164A (en) 1973-03-30 1974-12-03 S Chow Purification of 1,4-butanediol by vacuum distillation with side stream recovery
DE2514116C3 (de) * 1975-03-29 1983-03-17 Basf Ag, 6700 Ludwigshafen Verfahren zur kontinuierlichen Herstellung von linearen, hochmolekularen Polybutylenterephthalaten
DE2728407A1 (de) * 1977-06-24 1979-01-04 Basf Ag Verfahren zur behandlung von butandiol, das als kondensat bei der herstellung von polybutylenterephthalaten erhalten wurde
US5561218A (en) * 1993-10-05 1996-10-01 Basf Aktiengesellschaft Working up residues containing dihydroxy compounds
DE4333929A1 (de) * 1993-10-05 1995-04-06 Basf Ag Verfahren zur Aufarbeitung von Dihydroxyverbindungen enthaltenden Rückständen
DE19509957A1 (de) * 1995-03-18 1996-09-19 Basf Ag Verfahren zur Aufarbeitung von Dihydroxyverbindungen enthaltenden Rückständen

Also Published As

Publication number Publication date
DE19608614A1 (de) 1997-09-11
KR19990087569A (ko) 1999-12-27
EP0885252A2 (de) 1998-12-23
US6174970B1 (en) 2001-01-16
AU2095197A (en) 1997-09-22
WO1997032915A3 (de) 1997-10-30
JP2000506203A (ja) 2000-05-23
CN1212712A (zh) 1999-03-31
WO1997032915A2 (de) 1997-09-12

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