CN113893215B - Eye tightening and repairing composition, application and eye cream and preparation method thereof - Google Patents

Eye tightening and repairing composition, application and eye cream and preparation method thereof Download PDF

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Publication number
CN113893215B
CN113893215B CN202111178048.8A CN202111178048A CN113893215B CN 113893215 B CN113893215 B CN 113893215B CN 202111178048 A CN202111178048 A CN 202111178048A CN 113893215 B CN113893215 B CN 113893215B
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eye
tightening
agent
repairing
parts
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CN113893215A (en
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董明生
周鑫
戴志慧
岑茵
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Guangzhou Hanmay Cosmetics Co ltd
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Guangzhou Hanmay Cosmetics Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/99Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/494Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
    • A61K8/4953Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom containing pyrimidine ring derivatives, e.g. minoxidil
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/55Phosphorus compounds
    • A61K8/553Phospholipids, e.g. lecithin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/64Proteins; Peptides; Derivatives or degradation products thereof
    • A61K8/65Collagen; Gelatin; Keratin; Derivatives or degradation products thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/676Ascorbic acid, i.e. vitamin C
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9789Magnoliopsida [dicotyledons]
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A61K8/9783Angiosperms [Magnoliophyta]
    • A61K8/9794Liliopsida [monocotyledons]
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/005Preparations for sensitive skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations
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    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
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    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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    • A61K2800/85Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
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    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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Abstract

The invention discloses an eye tightening and repairing composition, application and eye cream and a preparation method thereof, and relates to the field of cosmetics. The composition comprises lactobacillus fermentation lysate, tea extract, pomegranate peel extract, small fruit coffee seed extract, caffeine and small fruit coffee seed extract, collagen, acetyl tetrapeptide-5, turmeric root extract and peach resin extract, and is applied to the field of cosmetics. The formula of the application contains various active substances with antioxidant and repairing functions, caffeine can promote permeation and absorption of other active substances, and meanwhile, the eye bags are eliminated, lecithin can promote the active substances to be accepted by skin more easily, and can be absorbed more easily, so that the anti-wrinkle, tightening and repairing effects on the skin of eyes are improved.

Description

Eye tightening and repairing composition, application and eye cream and preparation method thereof
Technical Field
The invention relates to the field of cosmetics, in particular to an eye tightening and repairing composition, application and eye cream and a preparation method thereof.
Background
Eyes are called as heart windows, eye skin is affected by factors such as illumination, environmental pressure, blink, smile and the like in the fast-paced living environment, various problems such as slackening, dry streak, fish tail streak, black eye, eye bags and the like occur, and the skin around the eyes is 10 times thinner than the skin at other parts of the face, so that the aging speed is higher, and various eye skin problems can be encountered at any age.
At present, the existing cosmetics aiming at the functions of repairing and anti-wrinkle of the eye skin are generally weak in effect, the functions of tightening, anti-wrinkle, repairing and the like are not obvious enough, the eye skin is sensitive and fragile, and a large amount of chemical substance raw materials contained in the cosmetics are easy to cause allergy or discomfort. Products which are mild and insensitive and have obvious functions of resisting wrinkles, repairing and the like on the skin of eyes are urgently needed to be developed.
Disclosure of Invention
The invention provides an eye tightening and repairing composition, application and eye cream and a preparation method thereof, which are used for providing a product with mild, crease-resistant, repairing and better tightening functions.
In order to solve the technical problems, one of the purposes of the invention is to provide an eye tightening and repairing composition which comprises the following raw materials in parts by weight:
eye protection agent: 0.5-2 parts;
black eye removing factor: 0.2-0.6 parts;
skin tightening agent: 0.3-1.5 parts;
repairing agent: 0.1-0.8 parts;
anti-wrinkle agent: 0.5-2 parts;
wherein the eye protection agent comprises lactobacillus fermented lysate, tea (CAMELLIASINENSIS) leaf extract, PUNICA GRANATUM (PUNICA GRANATUM) pericarp extract and coffee cherries (coffearabica) seed extract a, the black eye removing factor comprises caffeine and coffee cherries (COFFEA araica) seed extract B, the skin tightening agent comprises collagen and acetyl tetrapeptide-5, the repairing agent comprises turmeric (CURCUMA LONGA) root extract, and the anti-wrinkle agent comprises peach (prunes PERSICA) resin extract.
By adopting the scheme, the caffeine can promote permeation and absorption of other active substances by external use, is also an effective lipolysis-promoting substance, is used for eliminating the eye bags, achieves the effect of tightening the skin around the eyes, has the vasoconstriction characteristic, can reduce eye edema and increase blood circulation, and can be accepted by the skin more easily according to a similar mutual dissolution principle, and the interaction of the three substances can be exerted to the maximum; the lactobacillus fermentation lysate has higher active substance content, has strong anti-aging effect, the tea extract contains extremely rich procyanidine, the oxidation resistance of the procyanidine is 20 times stronger than that of vitamin C and 50 times stronger than that of vitamin E, the procyanidine plays a key role in the stability of collagen and the maintenance of elastin, so that the skin firmness is improved, the pomegranate peel extract has strong oxidation resistance, and a layer of film can be formed on the skin surface by high molecular weight carbohydrate, so that the effects of instant firmness and lifting are provided for the skin, and the appearance of fine lines and wrinkles is reduced; the collagen has good affinity with surrounding tissues, so that the collagen has the function of repairing tissues, elastic fibers and collagen fibers in the skin can be repaired to enable the skin to recover and tighten, and the acetyl tetrapeptide-5 can eliminate edema and improve the elasticity and smoothness of the skin; the turmeric root extract has strong activation effect on luciferase, so the turmeric root extract has strong anti-allergic and anti-inflammatory capabilities; the peach resin is beneficial to wound self-healing and has remarkable repairing effect. The application utilizes the synergistic effect of the components, reduces the irritation of raw materials to the skin, and has the effects of tightening, resisting wrinkles and removing dark circles on the eye skin.
Preferably, the composition further comprises 0.01 to 0.1 parts of tetrahydropyrimidine carboxylic acid and 0.1 to 0.5 parts of 3-o-ethyl ascorbic acid.
Preferably, the eye protection agent comprises 10wt% of lactobacillus fermented lysate, 10wt% of tea (CAMELLIASINENSIS) leaf extract, 10wt% of pomegranate (PUNICA GRANATUM) pericarp extract and 2wt% of small fruit coffee (coffearabica) seed extract, the de-black eye factor comprises 63.5wt% of caffeine and 28.5wt% of small fruit coffee (COFFEA araica) seed extract, the tightening agent comprises 4wt% of collagen and 0.16wt% of acetyl tetrapeptide-5, the repairing agent comprises 2wt% of turmeric (curcumca LONGA) root extract, and the anti-wrinkle agent comprises 10wt% of peach (prunes persona) resin extract.
The preparation method comprises the following raw material components:
tetrahydropyrimidine carboxylic acid: 0.05 parts;
3-o-ethyl ascorbic acid: 0.3 parts;
eye protection agent: 1 part;
black eye removing factor: 0.6 parts;
skin tightening agent: 0.8 parts;
repairing agent: 0.5 parts;
anti-wrinkle agent: 1 part.
Preferably, the eye protector comprises lactobacillus fermented lysate, folium Camelliae sinensis (CAMELLIASINENSIS) leaf extract, pericarpium Granati (PUNICA GRANATUM) extract, leuconostoc mesenteroides/radix Raphani (RAPHANUS SATIVUS) root fermented product filtrate, coffee cherokee (coffeaaarabica) seed extract and water; the black eye removing factors include caffeine, coffee cherries (COFFEA araica) seed extract and lecithin; the skin tightening agent comprises collagen, acetyl tetrapeptide-5, 1, 2-hexanediol, hyaluronic acid, glycerol and water; the repairing agent comprises Curcuma LONGA (Curcuma LONGA) root extract, sodium benzoate, potassium sorbate, glycerol and water; the anti-wrinkle agent comprises peach (PRUNUS PERICA) resin extract, 1, 2-hexanediol, ethylhexyl glycerol and water.
In order to solve the above technical problems, a second object of the present invention is to provide an application of an eye tightening and repairing composition in cosmetics.
In order to solve the technical problems, the invention provides an eye tightening and repairing eye cream, which is prepared by mixing an eye tightening and repairing composition and auxiliary materials, wherein the addition amount of the eye tightening and repairing composition is 1.71-7.5 wt%.
The preparation method comprises the following raw material components:
an eye tightening and repair composition: 1.71wt% to 7.5wt%;
humectant: 2.81wt% to 7.65wt%;
chelating agent: 0.01wt% to 0.05wt%;
and (3) a thickening agent: 0.3wt% to 1wt%;
antioxidant: 0.11wt% to 0.5wt%;
emulsifying agent: 0.8wt% to 2.5wt%;
an emollient: 2.5wt% to 8wt%;
preservative: 0.1wt% to 0.5wt%;
functional auxiliary agent: 0.5wt% to 1.5wt%;
water: the balance.
Preferably, the humectant comprises butylene glycol, polyglycerol-10, sodium hyaluronate and 1, 2-hexanediol, the chelating agent is disodium EDTA, the thickener comprises an ammonium acryloyldimethyl taurate/VP copolymer, sodium acrylic acid (ester) copolymer and lecithin, the antioxidant comprises p-hydroxyacetophenone and tocopherol, the emulsifier comprises cetostearyl alcohol a, cetostearyl glucoside, cetostearyl alcohol olivate and sorbitan olivate, the emollient comprises isononyl isononanoate, canola oil, polydimethylsiloxane, cyclomethicone and PEG-10 dimethicone cross-linked polymer, the preservative comprises phenoxyethanol and ethylhexyl glycerol, and the functional auxiliary agent is cetostearyl alcohol B.
In order to solve the above technical problems, a fourth object of the present invention is to provide a method for preparing an eye tightening and repairing eye cream, comprising the steps of:
(1) Mixing ammonium acryloyldimethyl taurate/VP copolymer, sodium acrylate copolymer, lecithin, p-hydroxyacetophenone, sodium hyaluronate, EDTA disodium, polyglycerin-10, butanediol and water, adding into a container, heating to 82-85deg.C, and stirring to obtain mixture A;
(2) Mixing cetostearyl alcohol A, cetostearyl glucoside, cetostearyl alcohol B, cetostearyl olive oleate, sorbitan olive oleate, tocopherol, isononyl isononanoate and canola oil, adding the mixture into a container, heating the mixture to 80-82 ℃, and uniformly stirring the mixture to obtain a mixture B;
(3) Mixing polydimethylsiloxane, cyclomethicone and PEG-10 polydimethylsiloxane cross-linked polymer, adding into a container, and stirring uniformly to obtain the C mixture.
(4) Cooling the mixture C to 42-45 ℃, adding the eye tightening and repairing composition into a container, and uniformly stirring to obtain a mixture D;
(5) Mixing 1, 2-hexanediol, phenoxyethanol and ethylhexyl glycerol, and stirring to obtain eye cream.
Compared with the prior art, the embodiment of the invention has the following beneficial effects:
the caffeine can promote permeation and absorption of other active substances, meanwhile, the pouch is eliminated, the small fruit coffee seed extract increases blood circulation, the lactobacillus fermentation lysate, the pomegranate rind extract and the tea extract have strong anti-aging effects, the collagen, the peach resin and the turmeric root extract have the function of repairing tissues, the lecithin promotes the active substances to be accepted by the skin more easily, the active substances are absorbed more easily, and the anti-wrinkle, tightening and repairing effects on the skin of eyes are improved.
Drawings
Fig. 1: results of tightening, pouch removal and wrinkle test (5 min) before the eye tightening and repairing eye cream of example 3 of the present invention was not used;
fig. 2: results of tightening, pouch removal and wrinkle test (5 min) after use of an eye tightening and repairing eye cream in embodiment 3 of the invention;
fig. 3: results of tightening, pouch removal and black eye testing (15 days) before the eye tightening and repair cream of example 3 of the present invention was not used;
fig. 4: results of tightening, pouch removal and black eye test (15 days) after use of an eye tightening and repair eye cream in accordance with embodiment 3 of the present invention.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Table 1 below is the source of the raw materials used in the present application:
TABLE 1 Source of raw materials
Preparation example 1
An eye tightening and repairing composition comprises the following raw material components: tetrahydropyrimidine carboxylic acid: 0.01g; 3-o-ethyl ascorbic acid: 0.1g; eye protection agent: 0.5g; black eye removing factor: 0.2g; skin tightening agent: 0.3g; repairing agent: 0.1g; anti-wrinkle agent: 0.5g.
Preparation example 2
An eye tightening and repairing composition comprises the following raw material components: tetrahydropyrimidine carboxylic acid: 0.05g; 3-o-ethyl ascorbic acid: 0.3g; eye protection agent: 1g; black eye removing factor: 0.6g; skin tightening agent: 0.8g; repairing agent: 0.5g; anti-wrinkle agent: 1g.
Preparation example 3
An eye tightening and repairing composition comprises the following raw material components: tetrahydropyrimidine carboxylic acid: 0.1g; 3-o-ethyl ascorbic acid: 0.5g; eye protection agent: 2g; black eye removing factor: 1g; skin tightening agent: 1.5g; repairing agent: 0.8g; anti-wrinkle agent: 2g.
The specific components of each of the above preparation examples 1 to 3 are as follows:
the eye protection agent comprises 2wt% of coffee cherries (coffearabica) seed extract, 1wt% of Leuconostoc mesenteroides/radish (RAPHANUS SATIVUS) root fermentation product filtrate, 10wt% of pomegranate (PUNICA GRANATUM) pericarp extract, 10wt% of tea (CAMELLIASINENSIS) leaf extract, 10wt% of lactobacillus fermentation lysate and 67wt% of water, specifically 16671LL-Revital-Eyes (probiotic composite eye protection agent) available from Guangzhou nori biotechnology limited company;
the de-black eye factor comprises 63.5wt% caffeine, 28.5 small fruit coffee (COFFEA araica) seed extract and 8wt% lecithin, specifically ecoselim, available from Shenzhen city, and cosmetic limited;
the skin tightening agent comprises 0.16wt% of acetyl tetrapeptide-5, 4wt% of collagen, 0.84wt% of 1, 2-hexanediol, 4wt% of hyaluronic acid, 55wt% of glycerol and 36wt% of water, specifically-AT5, purchased from guangzhou Ai Meige biotechnology limited;
the repairing agent comprises 2wt% of turmeric (CURCUMA LONGA) root extract, 0.2wt% of sodium benzoate, 0.2wt% of potassium sorbate, 50wt% of glycerin and 47.6wt% of water, specifically Turmericextract turmeric repairing agent, available from Guangzhou North Biotech Co., ltd;
the anti-wrinkle agent comprises 10wt% of peach (PRUNUS PERSIA) resin extract, 2wt% of 1, 2-hexanediol, 0.1wt% of ethylhexyl glycerol and 87.9wt% of water, specifically Yinmedeline PG, available from Shanghai Jia leaf Biotechnology Co.
Examples 1 to 3
The eye tightening and repairing eye cream is prepared by the following steps that the components, the contents and the technological parameters are shown in table 2:
(1) The materials of all components in the formula are accurately weighed, and meanwhile, the production equipment is cleaned.
(2) Mixing ammonium acryloyldimethyl taurate/VP copolymer, a composite thickener, p-hydroxyacetophenone, sodium hyaluronate, EDTA disodium, polyglycerol-10, butanediol and water, adding into an emulsifying pot, heating to 82-85 ℃, and uniformly stirring to obtain a mixture A, wherein the mass ratio of the sodium acrylate copolymer to lecithin is 3:1, specifically Lecigel;
(3) Mixing a composite emulsifier A, cetostearyl alcohol, a composite emulsifier B, tocopherol, isononyl isononanoate and canola oil, adding into an emulsifying pot, heating to 80-82 ℃, and uniformly stirring to obtain a mixture B, wherein the composite emulsifier A comprises the following components in percentage by mass: 1, in particular to MONTANOV 68, wherein the composite emulsifier B is prepared from cetostearyl alcohol olive oleate and sorbitan olive oleate according to the mass ratio of 1:1, specifically oliem 1000;
(4) Adding the composite emollient into an emulsifying pot, homogenizing at high speed (2800 r/min) for 8 min, and preserving heat for 20 min to obtain a C mixture, wherein the composite emollient comprises polydimethylsiloxane, cyclomethicone and PEG-10 dimethicone cross-linked polymer according to the mass ratio of 6:3:1, and specifically CBSIL-1020.
(5) Cooling the mixture C to 42-45 ℃, adding the pre-mixed eye tightening and repairing composition into an emulsifying pot, and uniformly stirring to obtain a mixture D;
(6) Mixing 1, 2-hexanediol and a preservative, stirring for 20-30 minutes, sampling, detecting, discharging after passing, and preparing the eye cream, wherein the preservative comprises phenoxyethanol and ethylhexyl glycerol according to the mass ratio of 9:1, and specifically PE9010.
TABLE 2 Components, contents and process parameters in examples 1-3
Comparative preparation example 1
An eye tightening composition, the reagents and process parameters used in each step are the same as those of preparation example 3, except that the addition amount of the tightening agent is 0.
Comparative preparation example 2
An eye tightening composition, the reagents and process parameters used in each step were the same as those of preparation example 3, except that the addition amount of the eye protection agent was 0.
Comparative preparation example 3
An eye tightening composition, the reagents and process parameters used in each step were the same as those of preparation example 3, except that the addition amount of the black eye removing factor was 0.
Comparative preparation example 4
An eye tightening and repairing composition, the reagents and process parameters used in each step are the same as those in preparation example 3, except that the addition amount of the repairing agent is 0.
Comparative preparation example 5
An eye tightening composition, the reagents and process parameters used in each step were the same as those of preparation example 3, except that the addition amount of the anti-wrinkle agent was 0.
Comparative example 1
The procedure and the reagents and process parameters used in each procedure were the same as in example 3, except that the eye tightening and repairing composition of preparation 3 was replaced with the eye tightening and repairing composition of comparative preparation 1.
Comparative example 2
The procedure and the reagents and process parameters used in each procedure were the same as in example 3, except that the eye tightening and repairing composition of preparation 3 was replaced with the eye tightening and repairing composition of comparative preparation 2.
Comparative example 3
The procedure and the reagents and process parameters used in each procedure were the same as in example 3, except that the eye tightening and repairing composition of preparation 3 was replaced with the eye tightening and repairing composition of comparative preparation 3.
Comparative example 4
The procedure and the reagents and process parameters used in each procedure were the same as in example 3, except that the eye tightening and repairing composition of preparation 3 was replaced with the eye tightening and repairing composition of comparative preparation 4.
Comparative example 5
The procedure and the reagents and process parameters used in each procedure were the same as in example 3, except that the eye tightening and repairing composition of preparation 3 was replaced with the eye tightening and repairing composition of comparative preparation 5.
Performance test
1. Tightening, pouch and wrinkle removal test (5 min)
Test requirements: selecting male and female volunteers 18-45 years old meeting the test requirements as a test subject;
sample to be tested: examples 1-3 and comparative examples 1-5;
the test method comprises the following steps: selecting male and female volunteers (25-45 years old), dividing into 20 people/group, photographing and recording the eye skin condition of the volunteers, smearing eye cream on the eye skin, observing skin change after 5min, and photographing for comparison;
test results: scoring was performed between 0-10 scores according to the use effect, 9-10 scores were good, 7-8 scores were good, 5-6 scores were general, 3-4 scores were poor, 1-2 scores were poor, and the average was taken, and the scoring results are shown in table 3, and the detection results of example 3 were shown in fig. 1-2.
TABLE 3 results of 5min Performance test of eye creams of examples 1-3 and comparative examples 1-5
Test item Scoring of Test item Scoring of
Example 1 7 Example 2 9
Example 3 8 Comparative example 1 5
Comparative example 2 5 Comparative example 3 5
Comparative example 4 6 Comparative example 5 5
2. Tightening, pouch removal and black eye test (15 days)
Test requirements: selecting male and female volunteers 18-45 years old meeting the test requirements as a test subject;
sample to be tested: examples 1-3 and comparative examples 1-5;
the test method comprises the following steps: male and female volunteers (25-45 years old) were selected and divided into 20 persons/group, the condition of the eye skin of the volunteers was recorded by photographing, and after 15 days, the change of the skin was observed and photographed for comparison.
Test results: scoring was performed between 0-10 scores based on the use effect, 9-10 scores were good, 7-8 scores were good, 5-6 scores were general, 3-4 scores were poor, 1-2 scores were poor, the average was taken, the scoring results are shown in Table 4, and FIGS. 3-4 are the test results of example 3.
TABLE 4 results of 15 day Performance test of eye creams of examples 1-3 and comparative examples 1-5
Test item Scoring of Test item Scoring of
Example 1 6 Example 2 10
Example 3 8 Comparative example 1 5
Comparative example 2 5 Comparative example 3 4
Comparative example 4 5 Comparative example 5 4
The eye cream prepared by the method can effectively improve the eye wrinkles in a short time and has anti-wrinkle and tightening effects on the skin of eyes as shown in the test results of the embodiment 3 in the figures 1-2 and the table 3.
The detection results of example 3 in fig. 3-4 and table 4 show that after the eye cream is used for 15 days, the eye cream has obvious desalination function on dark circles of eyes, and the anti-wrinkle tightening effect is obvious.
The foregoing embodiments have been provided for the purpose of illustrating the general principles of the present invention, and are not to be construed as limiting the scope of the invention. It should be noted that any modifications, equivalent substitutions, improvements, etc. made by those skilled in the art without departing from the spirit and principles of the present invention are intended to be included in the scope of the present invention.

Claims (8)

1. An eye tightening and repairing composition is characterized by comprising the following raw materials in parts by weight:
eye protection agent: 0.5-2 parts;
black eye removing factor: 0.2-0.6 parts;
skin tightening agent: 0.3-1.5 parts;
repairing agent: 0.1-0.8 parts;
anti-wrinkle agent: 0.5-2 parts;
wherein the eye protector comprises 2wt% of coffee cherries (coffearabica) seed extract, 1wt% of Leuconostoc mesenteroides/radish (RAPHANUS SATIVUS) root fermentation product filtrate, 10wt% of pomegranate (PUNICA GRANATUM) pericarp extract, 10wt% of tea (CAMELLIASINENSIS) leaf extract, 10wt% of lactobacillus fermentation lysate and 67wt% of water; the de-black eye factor comprises 63.5wt% caffeine, 28.5wt% small fruit coffee (COFFEA araica) seed extract, and 8wt% lecithin; the skin tightening agent comprises 0.16wt% of acetyl tetrapeptide-5, 4wt% of collagen, 0.84wt% of 1, 2-hexanediol, 4wt% of hyaluronic acid, 55wt% of glycerol and 36wt% of water; the repairing agent comprises 2wt% of turmeric (Curcuma LONGA) root extract, 0.2wt% of sodium benzoate, 0.2wt% of potassium sorbate, 50wt% of glycerin and 47.6wt% of water; the anti-wrinkling agent comprises 10wt% peach (PRUNUS PERICA) resin extract, 2wt%1, 2-hexanediol, 0.1wt% ethylhexyl glycerol, and 87.9wt% water.
2. An eye tightening composition as claimed in claim 1, wherein said composition further comprises 0.01 parts to 0.1 parts of tetrahydropyrimidine carboxylic acid and 0.1 parts to 0.5 parts of 3-o-ethyl ascorbic acid.
3. An eye tightening and repairing composition according to claim 2, comprising the following raw material components:
tetrahydropyrimidine carboxylic acid: 0.05 parts;
3-o-ethyl ascorbic acid: 0.3 parts;
eye protection agent: 1 part;
black eye removing factor: 0.6 parts;
skin tightening agent: 0.8 parts;
repairing agent: 0.5 parts;
anti-wrinkle agent: 1 part.
4. Use of an eye tightening and repairing composition according to any one of claims 1-3 in the preparation of cosmetics.
5. An eye tightening and repairing eye cream, which is prepared by mixing the eye tightening and repairing composition according to any one of claims 1-3 with auxiliary materials, wherein the addition amount of the eye tightening and repairing composition is 1.71wt% to 7.5wt%.
6. An eye tightening and repair eye cream as claimed in claim 5, comprising the following raw material components:
an eye tightening and repair composition: 1.71wt% to 7.5wt%;
humectant: 2.81wt% to 7.65wt%;
chelating agent: 0.01wt% to 0.05wt%;
and (3) a thickening agent: 0.3wt% to 1wt%;
antioxidant: 0.11wt% to 0.5wt%;
emulsifying agent: 0.8wt% to 2.5wt%;
an emollient: 2.5wt% to 8wt%;
preservative: 0.1wt% to 0.5wt%;
functional auxiliary agent: 0.5wt% to 1.5wt%;
water: the balance.
7. An eye tightening and repair cream as claimed in claim 6 wherein the humectant comprises butylene glycol, polyglycerin-10, sodium hyaluronate and 1, 2-hexanediol, the chelating agent is disodium EDTA, the thickener comprises an ammonium acryloyldimethyl taurate/VP copolymer, sodium acrylic acid (ester) copolymer and lecithin, the antioxidant comprises p-hydroxyacetophenone, tocopherol, the emulsifier comprises cetostearyl alcohol a, cetostearyl glucoside, cetostearyl olivate and sorbitan olivate, the emollient comprises isononyl isononanoate, canola oil, dimethicone, cyclodimethicone and PEG-10 dimethicone cross-linked polymer, the preservative comprises phenoxyethanol and ethylhexyl glycerol, and the functional aid is cetostearyl alcohol B.
8. A method for preparing an eye tightening and repairing eye cream according to claim 7, comprising the steps of:
(1) Mixing ammonium acryloyldimethyl taurate/VP copolymer, sodium acrylate copolymer, lecithin, p-hydroxyacetophenone, sodium hyaluronate, EDTA disodium, polyglycerin-10, butanediol and water, adding into a container, heating to 82-85deg.C, and stirring to obtain mixture A;
(2) Mixing cetostearyl alcohol A, cetostearyl glucoside, cetostearyl alcohol B, cetostearyl olive oleate, sorbitan olive oleate, tocopherol, isononyl isononanoate and canola oil, adding the mixture into a container, heating the mixture to 80-82 ℃, and uniformly stirring the mixture to obtain a mixture B;
(3) Mixing polydimethylsiloxane, cyclomethicone and PEG-10 polydimethylsiloxane crosslinked polymer, adding into a container, and stirring uniformly to obtain a C mixture;
(4) Cooling the mixture C to 42-45 ℃, adding the eye tightening and repairing composition into a container, and uniformly stirring to obtain a mixture D;
(5) Mixing 1, 2-hexanediol, phenoxyethanol and ethylhexyl glycerol, and stirring to obtain eye cream.
CN202111178048.8A 2021-10-09 2021-10-09 Eye tightening and repairing composition, application and eye cream and preparation method thereof Active CN113893215B (en)

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