CN112675079A - Quick-emulsifying cleansing oil - Google Patents
Quick-emulsifying cleansing oil Download PDFInfo
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- CN112675079A CN112675079A CN202110045321.3A CN202110045321A CN112675079A CN 112675079 A CN112675079 A CN 112675079A CN 202110045321 A CN202110045321 A CN 202110045321A CN 112675079 A CN112675079 A CN 112675079A
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Abstract
The invention discloses a quick-emulsifying cleansing oil, and belongs to the technical field of cosmetics. In the components of the quick emulsifying cleansing oil, PEG-20 glyceryl triisostearate, PEG-3 glyceryl isostearate, polysorbate-80 and sorbitan polyether-30 tetraoleate with specific contents are used as emulsifying agents and added into an oil phase system, and the oily matrix and lipophilic ingredients in the components can well dissolve color cosmetics on skin; the hydrophilic components such as emulsifier in the components can increase the washability of the product, reduce the greasy feeling of the skin during use, have soft touch and do not remain on the skin after cleaning. The product has the advantages of high refreshing degree, strong emulsifying ability, high emulsifying speed and strong makeup removing ability. The invention also provides a preparation method of the rapid emulsification cleansing oil, which is simple in operation steps and can realize industrial large-scale production.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to quick-emulsifying cleansing oil.
Background
With the improvement of living standard of people, people pay more attention to self image, and cosmetics become necessities of daily life. On the other hand, the market demand for cleansing oils has increased, but the cleansing oils on the market have the following problems: (1) most cleansing oils only pay attention to cleansing ability and are not clear and moist; (2) the cleansing oil product has not strong enough emulsifying power and not fast enough emulsifying speed; (3) some cleansing oils have unsatisfactory cleansing ability, and particularly have poor cleansing effect on heavy makeup.
Disclosure of Invention
Based on the defects of the prior art, the invention aims to provide the quick-emulsifying cleansing oil which is used as the oil-based cleansing oil and has the characteristics of high freshness, strong emulsifying capacity, high emulsifying speed and strong cleansing capacity.
In order to achieve the purpose, the invention adopts the technical scheme that:
the quick-emulsifying cleansing oil comprises the following components in percentage by mass: 48-86% of oil base material, 12-50% of emulsifier, 0.5-1% of antioxidant and the balance of vegetable oil; the emulsifier comprises PEG-20 glyceryl triisostearate, PEG-3 glyceryl isostearate, polysorbate-80 and sorbitan polyether-30 tetraoleate.
The quick-emulsifying cleansing oil takes PEG-20 glyceryl triisostearate, PEG-3 glyceryl isostearate, polysorbate-80 and sorbitan polyether-30 tetraoleate with specific contents as emulsifying agents to be added into an oil phase system, has the effects of dissolving when meeting oil and self-emulsifying when meeting water, realizes oil-water integration of the components through microemulsion, and meets the requirement of special oil-water balance in the microemulsion. The oily matrix and the lipophilic component in the product components can well dissolve the color cosmetics on the skin; the hydrophilic components such as emulsifier in the components can increase the washability of the product, reduce the greasy feeling of the skin during use, have soft touch and do not remain on the skin after cleaning.
Preferably, the quick-emulsifying cleansing oil comprises the following components in percentage by mass: 49.85-85.35% of oil base material, 12-47% of emulsifier, 0.5-1% of antioxidant and the balance of vegetable oil.
Preferably, the emulsifier comprises PEG-20 glyceryl triisostearate accounting for 3-15% of the mass of the quick-emulsifying cleansing oil, PEG-3 glyceryl isostearate accounting for 2-12%, polysorbate-80 accounting for 2-10% and sorbitol polyether-30 tetraoleate accounting for 5-15%.
The emulsifier obtained by mixing the components in a specific ratio can obviously improve the emulsifying capacity of the product, increase the washability of the product, provide better skin use touch feeling for the cleansing oil product and improve the use experience.
Preferably, the oil-based substrate comprises caprylic/capric triglyceride, olive oil, C12～15Alcohol benzoates and glycerol tri (ethyl hexanoate);
more preferably, the oil base comprises 19.85-70.35% of caprylic/capric triglyceride, 5-10% of olive oil and 5-20% of C by mass of the quick-emulsifying cleansing oil12～15Alcohol benzoate and 5-15% of glycerol tri (ethyl hexanoate).
The oil-based matrix obtained by combining the grease according to the proportion can obviously improve the makeup removing capability of the product; all the components are common cosmetic additives and basically have no stimulation to human skin.
Preferably, the antioxidant comprises tocopherol acetate.
The tocopherol acetate is a common additive of personal care and sanitary products, and can improve the protection of the products on skin injury when being used for removing the makeup oil products, thereby further enriching the functions of the products.
Preferably, the vegetable oil comprises seabuckthorn fruit oil, jojoba oil, sweet orange essential oil and meadowfoam seed oil.
More preferably, the vegetable oil and fat comprises 0.05% of seabuckthorn fruit oil, 1% of jojoba oil, 0.1% of sweet orange essential oil and 1% of meadowfoam seed oil by mass of the quick-emulsifying cleansing oil.
In the vegetable oil, the seabuckthorn fruit oil is rich in various beneficial fatty acids such as palmitic acid and the like and nutrient substances such as vitamins and carotene and the like, and can be compatible with facial oil and deep into skin when being applied to makeup removing oil, so that the skin problems of multiple parts have the effect of alleviating; the chemical molecular arrangement of the jojoba oil is similar to that of sebum of human beings, so that the jojoba oil is very easy to be classified and absorbed by skin, is a common skin-care functional component, can help skin to be moistened and moisturized to a certain extent, improves elasticity, can improve symptoms such as skin inflammation and sensitivity and the like, and unblocks pores; the meadowfoam seed oil contains more than 98 percent of long-chain fatty acid with antioxidant function, can prolong the shelf life of products when being used in products in the field of cosmetics, and has certain skin moistening function.
The invention also aims to provide a preparation method of the quick-emulsifying cleansing oil.
The preparation method of the quick emulsifying cleansing oil comprises the following steps: and (3) stirring and mixing the oil base materials uniformly, heating, adding the emulsifier, mixing and stirring uniformly, preserving heat, cooling to normal temperature, adding the antioxidant and the vegetable oil, and mixing uniformly to obtain the quick-emulsifying cleansing oil.
The preparation method of the product has simple operation steps and can realize industrialized large-scale production.
Preferably, the heating temperature is 68-72 ℃, and the heat preservation time is 25-30 min.
The invention has the beneficial effects that: the invention provides a quick-emulsifying cleansing oil, wherein components of the product are added into an oil phase system by taking PEG-20 glyceryl triisostearate, PEG-3 glyceryl isostearate, polysorbate-80 and sorbitan polyether-30 tetraoleate with specific contents as emulsifying agents, and an oily matrix and lipophilic ingredients in the components can well dissolve color cosmetics on skin; the hydrophilic components such as emulsifier in the components can increase the washability of the product, reduce the greasy feeling of the skin during use, have soft touch and do not remain on the skin after cleaning. The product has the advantages of high refreshing degree, strong emulsifying ability, high emulsifying speed and strong makeup removing ability. The invention also provides a preparation method of the rapid emulsification cleansing oil, which is simple in operation steps and can realize industrial large-scale production.
Drawings
FIG. 1 is a comparison of results of simulated makeup removal tests of the rapid-emulsifying makeup remover oil of the present invention (right) and a commercial benchmark cleansing product (left);
FIG. 2 is a comparison graph of the results of the simulated skin irritation test of the quick emulsifying cleansing oil of the present invention and other common surfactants.
Detailed Description
For better illustrating the objects, technical solutions and advantages of the present invention, the present invention will be further described with reference to specific examples, which are intended to be understood in detail, but not intended to limit the present invention.
Examples 1 to 10
The formula of the quick-emulsifying cleansing oil in each embodiment of the invention is shown in tables 1-2.
The preparation method of the quick-emulsifying cleansing oil in each embodiment comprises the following steps: and (3) uniformly mixing the oil base, the emulsifier, the antioxidant and the vegetable oil to obtain the orange transparent liquid quick-emulsifying cleansing oil.
TABLE 1
TABLE 2
The products obtained in the embodiments 1-10 are subjected to property test according to GB/T29990, and meanwhile, the improvement standard of the heat-resistant and cold-resistant indexes is tested: respectively standing in an aseptic incubator at 48 ℃ and 15 ℃ below zero for 1 month, and then, returning to room temperature and observing, and setting a temperature cycle test: and standing the products in an aseptic incubator for 1 month under the cyclic change of 48-15 ℃, and then, restoring the products to the room temperature and observing the products. Tests show that the products obtained in examples 1-10 have no obvious difference in appearance before and after the experiment, the products have no layering phenomenon, the tested acid value is less than or equal to 5(mg/g), the peroxide value is less than or equal to 10(mmol/kg), and the total number of all bacterial colonies also meets the sanitary standard, which indicates that the products obtained by the invention have environmental stability.
Comparative examples 1 to 10
The products of comparative examples 1-10 differ from the products of examples 1-10 only in formulation, and the cleansing oil formulations of the comparative examples are shown in tables 3-4.
TABLE 3
TABLE 4
Effect example 1
In order to verify the makeup removing capability of the product disclosed by the invention, the products obtained in examples 1-10 and comparative examples 1-10 are subjected to a simulated makeup removing test. Uniformly coating 20 silicon rubber sheets with a commercially available foundation liquid with wear resistance and high long-acting performance according to the average amount so as to simulate the condition of the human skin when being coated with color cosmetics; respectively smearing 10mL of products obtained in examples 1-10 and comparative examples 1-10 on wet sponge, installing the products on a wiping tester capable of wiping circularly, using the products to wipe the makeup simulation silica gel film for 30 times respectively, simulating the mechanical process of makeup removal, and respectively evaluating the test results, wherein the evaluation grades are as follows: good (complete makeup removal), good (only minor/small amount of makeup residue), normal (partial makeup residue), poor (more makeup residue), and poor (almost no makeup removal effect). The test results are shown in table 5.
TABLE 5
| Product(s) | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 |
| Evaluation of | Is preferably used | Is preferably used | Is preferably used | Is preferably used | Is preferably used |
| Product(s) | Example 6 | Example 7 | Example 8 | Example 9 | Example 10 |
| Evaluation of | Good taste | Is preferably used | Is preferably used | Is preferably used | Is preferably used |
| Product(s) | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | Comparative example 5 |
| Evaluation of | Is poor | Is poor | In general | In general | In general |
| Product(s) | Comparative example 6 | Comparative example 7 | Comparative example 8 | Comparative example 9 | Comparative example 10 |
| Evaluation of | In general | In general | In general | In general | Is preferably used |
As can be seen from the table, the quick emulsified cleansing oil product obtained in the embodiment of the invention is matched with the oil-based matrix and the emulsifier in a specific ratio, and has excellent cleansing capability; wherein the product resulting from the formulation of example 6 has the most preferred makeup removal capability. The samples tested in example 6 and a common commercial cleanser were subjected to a rub-off test under the same conditions as described above using a wear scrub tester (Sheen Instruments, CA, USA), and the results are shown in fig. 1, which shows that the quick-emulsifying cleansing oil of the present invention has a better cleansing power and can completely replace the existing commercial cleanser.
Effect example 2
In order to verify the rapid emulsification capability of the product disclosed by the invention, the products obtained in examples 1-10 and comparative examples 1-10 are subjected to a simulated emulsification test. And (3) dripping 2mL of the products of the groups into 98mL of deionized water, and calculating the time required for complete emulsification of the products and whitening (turbidity) of the clear water by taking a blank clear water group as a control. The test results are shown in table 6.
TABLE 6
| Product(s) | Example 1 | Example 2 | Example 3 | Example 4 | Example 5 |
| Time of emulsification | 14s | 12s | 11s | 10s | 9s |
| Product(s) | Example 6 | Example 7 | Example 8 | Example 9 | Example 10 |
| Time of emulsification | 8s | 6s | 5s | 3s | 2s |
| Product(s) | Comparative example 1 | Comparative example 2 | Comparative example 3 | Comparative example 4 | Comparative example 5 |
| Time of emulsification | 16s | 15s | 16s | 25s | 18s |
| Product(s) | Comparative example 6 | Comparative example 7 | Comparative example 8 | Comparative example 9 | Comparative example 10 |
| Time of emulsification | 35s | 32s | 30s | 34s | 15s |
As can be seen from the table, the quick emulsifying cleansing oil product obtained in the embodiment of the invention is matched with four specific emulsifiers, and has excellent quick emulsifying capacity compared with the product obtained in the comparative example.
Effect example 3
To verify the skin suitability of the product according to the invention, the product obtained in example 1 was subjected to a simulated skin irritation test. The test method comprises the following steps: adding 1mL of the product aqueous solution (named as Cithrol 10GTIS) obtained in example 1 with the mass concentration of 30% into accurately weighed 70mg of zein, placing the zein in a rotary instrument, mixing the liquid for 20min at the speed of 40r/min, centrifuging the liquid for 4min at the speed of 10000r/min to separate the liquid from the mass, removing solid residues, and heating the residual zein solution at 50 ℃ overnight; after all the water had disappeared, the mass of the remaining undissolved zein was weighed and the mass percentage of dissolved zein (dissolution rate)%, was finally calculated. The above procedure was repeated 6 times, and the resulting data were averaged to obtain final average values while setting a control group which replaced the aqueous product solution of example 1 with 8% SLS (sodium lauryl sulfate) aqueous solution, 8% SLES (sodium lauryl ether sulfate) aqueous solution, 6% SLES aqueous solution and 3% cabba 30 (cocamidopropyl betaine) aqueous solution, 2% SLES aqueous solution and 7% cabba 30 aqueous solution by mass and equivalent water. The test results are shown in fig. 2.
Since zein is a corn-derived water-insoluble protein that is widely used to test potential skin irritation and the degree of protein denaturation that results from skin care products, it is generally believed that the higher the zein dissolution rate in a simulated skin test, the more irritating the skin the product tested. As can be seen from the figure, compared with other common skin care product surface active additives, the zein dissolution rate of the product obtained by the invention (5.9%) is only equivalent to that of water (5.69%), which indicates that the quick-emulsifying cleansing oil disclosed by the invention has extremely small irritation to the skin.
Finally, it should be noted that the above embodiments are only used for illustrating the technical solutions of the present invention and not for limiting the protection scope of the present invention, and although the present invention is described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions can be made on the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention.
Claims (10)
1. The quick-emulsifying cleansing oil is characterized by comprising the following components in percentage by mass: 48-86% of oil base material, 12-50% of emulsifier, 0.5-1% of antioxidant and the balance of vegetable oil; the emulsifier comprises PEG-20 glyceryl triisostearate, PEG-3 glyceryl isostearate, polysorbate-80 and sorbitan polyether-30 tetraoleate.
2. The quick-emulsifying cleansing oil according to claim 1, comprising the following components in percentage by mass: 49.85-85.35% of oil base material, 12-47% of emulsifier, 0.5-1% of antioxidant and the balance of vegetable oil.
3. The quick-emulsifying cleansing oil according to claim 1, wherein the emulsifier comprises 3 to 15% of PEG-20 glyceryl triisostearate, 2 to 12% of PEG-3 glyceryl isostearate, 2 to 10% of polysorbate-80 and 5 to 15% of sorbitan polyether-30 tetraoleate by mass of the quick-emulsifying cleansing oil.
4. The fast emulsifying cleansing oil according to claim 1 wherein said oil-based base comprises caprylic/capric triglyceride, olive oil, C12～15Alcohol benzoates and glycerol tri (ethyl hexanoate).
5. The quick-emulsifying cleansing oil according to claim 4, wherein the oil-based base comprises 19.85 to 70.35% by mass of caprylic/capric triglyceride, 5 to 10% by mass of olive oil, and 5 to 20% by mass of C12～15Alcohol benzoate and 5-15% of glycerol tri (ethyl hexanoate).
6. The fast emulsifying cleansing oil according to claim 1 wherein said antioxidant comprises tocopheryl acetate.
7. The quick emulsifying cleansing oil according to claim 1, wherein said vegetable oil comprises seabuckthorn fruit oil, jojoba oil, sweet orange essential oil and meadowfoam seed oil.
8. The quick-emulsifying cleansing oil according to claim 7, wherein the vegetable oil comprises 0.05% of seabuckthorn fruit oil, 1% of jojoba oil, 0.1% of orange essential oil and 1% of meadowfoam seed oil by mass.
9. The method for preparing the quick emulsifying cleansing oil according to any one of claims 1 to 8, wherein the quick emulsifying cleansing oil is obtained by uniformly mixing the oil-based base material, heating, adding the emulsifier, uniformly mixing, uniformly stirring, keeping the temperature, cooling to normal temperature, and finally adding the antioxidant and the vegetable oil and uniformly mixing.
10. The method for preparing the rapid emulsifying cleansing oil according to claim 9, wherein the heating temperature is 68-72 ℃, and the heat preservation time is 25-30 min.
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| CN114146022A (en) * | 2021-11-08 | 2022-03-08 | 上海麦吉丽日用品有限公司 | Prebiotics cleansing oil gel for cosmetics and preparation method thereof |
| CN114712270A (en) * | 2022-03-25 | 2022-07-08 | 仁和全域(上海)大健康研究院有限公司 | Mild cleansing oil and preparation method thereof |
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