CN114712270B - Mild cleansing oil and preparation method thereof - Google Patents
Mild cleansing oil and preparation method thereof Download PDFInfo
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- CN114712270B CN114712270B CN202210307245.3A CN202210307245A CN114712270B CN 114712270 B CN114712270 B CN 114712270B CN 202210307245 A CN202210307245 A CN 202210307245A CN 114712270 B CN114712270 B CN 114712270B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
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Abstract
The invention discloses mild cleansing oil and a preparation method thereof, wherein the cleansing oil comprises the following components in percentage by weight: 18.00 to 25.00 percent of sunflower seed oil, 14.00 to 21.00 percent of grape seed oil, 16.00 to 20.00 percent of low freezing point grease, 13.00 to 19.50 percent of emulsifying agent, 2.00 to 5.00 percent of jojoba seed oil, 0.80 to 1.00 percent of rice chaff oil, 0.30 to 0.60 percent of antioxidant, 0.10 to 0.60 percent of Butyrospermum parkii fruit fat extract and the balance of caprylic acid/capric acid triglyceride. According to the invention, a large amount of vegetable oil is used as a main oil component, and components such as low freezing point oil, antioxidants and the like are matched, so that the phenomenon that the vegetable oil is separated out of the prepared cleansing oil at the freezing point of-5 ℃ can be prevented, and the convenience of use of consumers in winter is improved. Meanwhile, the composition and the proportion of the emulsifier are optimized, so that the cosmetic removing force is ensured, the cosmetic removing agent is mild, and the cosmetic removing agent is also suitable for sensitive muscles and does not damage sebum membranes for a long time.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to mild cleansing oil and a preparation method thereof, in particular to mild cleansing oil mainly comprising vegetable oil and a preparation method thereof.
Background
The cleansing oil is a cosmetic for cleansing and cleaning residues of makeup cosmetics and skin pore secretions, which are specially used for cleansing, thereby keeping skin clean. The cleansing oil is an oily preparation mainly composed of transparent liquid oily components, and is easier to spread and remove makeup compared with cleansing cream; it is more moist than make-up remover. With the improvement of life quality of people, the requirements on the cleansing oil are not only limited to rapid cleansing and cleaning, but also environment-friendly, low-irritation and natural green components are pursued from raw materials. The common grease used for removing the makeup oil comprises mineral oil, isohexadecane, dioctyl carbonate and the like, and is mainly synthetic grease. The vegetable oil has natural green environmental protection property and is moist, so that the vegetable oil replaces part of the synthetic oil and is more and more favored by consumers. The main purpose of the cleansing oil is to remove the makeup, and when the dosage of the emulsifier in the cleansing oil is large, the cleansing oil can achieve the effects of good cleansing power and strong degreasing power, but skin dryness can be caused by frequent use; when the amount of the emulsifier is small, the cleansing power of the emulsifier can not meet the requirement, and balance is required in experiments.
The prior patent document CN102198061A describes a mild cleansing oil with skin care effect, which comprises 79 to 89.9 percent of vegetable oil, 10 to 20 percent of emulsifier, 0.1 to 1 percent of essential oil and 0 to 5 percent of humectant. Although it has a good makeup removing effect, there are two disadvantages to be overcome due to the addition of a large amount of vegetable oil: firstly, easy rancidity; secondly, vegetable oil is easy to separate out near the low-temperature freezing point, which causes inconvenient use.
Disclosure of Invention
Aiming at the defects of the prior art, the invention aims to provide mild cleansing oil and a preparation method thereof.
In order to overcome the defects of plant cleansing oil in the market, not only the effect during cleansing oil is emphasized, but also the phenomena of degreasing of skin, drying of skin in the later period, acne and the like possibly caused by long-term use of the cleansing oil are emphasized from the characteristic of the cleansing oil. By studying these problems, we have conducted sufficient experiments on both cleansing power and sensitive muscle tests, and thus finally prepared a mild cleansing oil of the present invention.
The invention aims at realizing the following technical scheme:
in a first aspect, the invention provides a mild cleansing oil, which comprises the following components in percentage by weight:
preferably, the low freezing point oil is coco-caprylate/caprate.
Preferably, the emulsifier comprises sorbitol polyether-30 tetraoleate and polyglycerol-2 sesquioleate; the weight percentage of the sorbitol polyether-30 tetraoleate and the polyglycerol-2 sesquioleate in the mild cleansing oil is 12.00-17.00% and 1.00-2.50% respectively.
Preferably, the antioxidant is tocopherol (vitamin E).
Preferably, the cleansing oil further comprises 0.01 to 0.50 weight percent of other components.
Preferably, the other ingredients include one or more of bergamot (CITRUS AURANTIUM BERGMIA) oil, geranium (PELARGONIUM GRAVEOLENS) oil, calendula (CALENDULA OFFICINALIS) flower extract, white pool flower (LIMNANTHES ALBA) seed oil, rosemary (ROSMARINUS OFFICINALIS) leaf extract, lime (CITRUS AURANTIUM DULCIS) peel oil.
As a preferred scheme, the mild cleansing oil comprises the following components in percentage by weight:
as a preferred scheme, the mild cleansing oil comprises the following components in percentage by weight:
as a preferred scheme, the mild cleansing oil comprises the following components in percentage by weight:
as a preferred scheme, the mild cleansing oil comprises the following components in percentage by weight:
as a preferred scheme, the mild cleansing oil comprises the following components in percentage by weight:
as a preferred scheme, the mild cleansing oil comprises the following components in percentage by weight:
in a second aspect, the invention also provides a preparation method of the mild cleansing oil, which comprises the following steps:
s1, taking a butter extract of a Butyrospermum parkii and caprylic/capric triglyceride as phase A, weighing according to weight percentage, mixing in an emulsifying pot, heating to 45-50 ℃, uniformly stirring and dissolving, and then cooling to 30 ℃;
s2, taking sunflower seed oil, grape seed oil, low-freezing point grease, jojoba seed oil, rice bran oil, an emulsifier and an antioxidant as a phase B, sequentially adding the phases into an emulsifying pot after weighing according to weight percentage, and stirring and dissolving uniformly;
s3, taking other components as a phase C, sequentially adding the components into an emulsifying pot after weighing according to weight percentage, stirring and dissolving uniformly, and obtaining the mild cleansing oil after inspection is qualified.
Compared with the prior art, the invention has the following beneficial effects:
1) According to the invention, a large amount of vegetable oil is used as a main oil component, and components such as low freezing point oil, antioxidants and the like are matched, so that the phenomenon that the vegetable oil is separated out of the prepared cleansing oil at the freezing point of-5 ℃ can be prevented, and the convenience of use of consumers in winter is improved. Meanwhile, the composition and the proportion of the emulsifier are optimized, so that the cosmetic removing force is ensured, the cosmetic removing agent is mild, sensitive muscles are also suitable, and the sebum membrane is not damaged for a long time.
2) In the production process for preparing the cleansing oil, vegetable wax with higher melting point is firstly dissolved and then is produced at low temperature, so that secondary heating of most vegetable oil is avoided, and long-term stability of the vegetable oil is protected.
Drawings
Other features, objects and advantages of the present invention will become more apparent upon reading of the detailed description of non-limiting embodiments, given with reference to the accompanying drawings in which:
FIG. 1 is a schematic view of a production process for preparing the mild cleansing oil of the invention;
FIG. 2 shows the cleansing effect of each cleansing oil prepared; wherein, fig. 2A is a photograph before cleaning; FIG. 2B is a photograph of cleansing oil prepared in example 2; fig. 2C is a photograph of cleansing oil prepared in comparative example 4.
Detailed Description
The present invention will be described in detail with reference to specific examples. The following examples will assist those skilled in the art in further understanding the present invention, but are not intended to limit the invention in any way. It should be noted that variations and modifications could be made by those skilled in the art without departing from the inventive concept. These are all within the scope of the present invention.
Example 1
The present example provides a mild cleansing oil and a preparation method thereof, wherein the weight percentage (unit:%) of each component of the cleansing oil is shown in table 1. The preparation method specifically comprises the following steps (the production flow diagram is shown in figure 1):
1. mixing Butyrospermum parkii fruit lipid extract and caprylic/capric triglyceride as phase A, heating to 45-50deg.C, stirring at 100rpm for 15min, and cooling to 30deg.C at 100 rpm;
2. the sunflower seed oil, the grape seed oil, the low-freezing point oil, the jojoba seed oil, the rice bran oil, the emulsifier and the antioxidant are taken as phase B, and are sequentially added into an emulsifying pot after being weighed according to weight percentage, and are stirred for 10min at the stirring speed of 100rpm to be uniformly dissolved;
3. and (3) taking other components as a phase C, sequentially adding the components into an emulsifying pot after weighing according to the weight percentage, stirring at 30 ℃ and a stirring speed of 100rpm for 10min to dissolve uniformly, and obtaining the mild cleansing oil after inspection.
Example 2
The embodiment provides a mild cleansing oil and a preparation method thereof, wherein the cleansing oil comprises the following components in percentage by weight as shown in table 1. The preparation method is the same as in example 1.
Example 3
The embodiment provides a mild cleansing oil and a preparation method thereof, wherein the cleansing oil comprises the following components in percentage by weight as shown in table 1. The preparation method is the same as in example 1.
Example 4
The embodiment provides a mild cleansing oil and a preparation method thereof, wherein the cleansing oil comprises the following components in percentage by weight as shown in table 1. The preparation method is the same as in example 1.
Example 5
The embodiment provides a mild cleansing oil and a preparation method thereof, wherein the cleansing oil comprises the following components in percentage by weight as shown in table 1. The preparation method is the same as in example 1.
Example 6
The embodiment provides a mild cleansing oil and a preparation method thereof, wherein the cleansing oil comprises the following components in percentage by weight as shown in table 1. The preparation method is the same as in example 1.
TABLE 1
Comparative example 1
The comparative example provides a cleansing oil and a preparation method thereof, wherein the cleansing oil comprises the components with the weight percentage shown in table 2, and the addition amount of coco-caprylate/caprate is reduced and the addition amount of sunflower seed oil is increased compared with the components of the cleansing oil in example 1. The preparation method is the same as in example 1.
Comparative example 2
The comparative example provides a cleansing oil and a preparation method thereof, wherein the weight percentage of each component of the cleansing oil is shown in table 2, and the addition amount of coco-caprylate/caprate is increased and the addition amount of sunflower seed oil is reduced compared with the components of the cleansing oil in example 5. The preparation method is the same as in example 1.
Comparative example 3
The comparative example provides a cleansing oil and a preparation method thereof, wherein the cleansing oil comprises the components with the weight percentage shown in table 2, and the addition amount of the sorbitol polyether-30 tetraoleate is correspondingly increased compared with the cleansing oil of example 1 without adding polyglycerol-2 sesquioleate. The preparation method is the same as in example 1.
Comparative example 4
The comparative example provides a cleansing oil and a preparation method thereof, wherein the cleansing oil comprises the components with the weight percentage shown in table 2, and the addition amount of polyglycerol-2-sesquioleate is increased and the addition amount of sorbitol polyether-30 tetraoleate is reduced compared with the components of the cleansing oil in example 2. The preparation method is the same as in example 1.
Comparative example 5
The comparative example provides a cleansing oil and a preparation method thereof, wherein the cleansing oil comprises the components with the weight percentages shown in table 2, and no tocopherol is added compared with the cleansing oil of example 1. The preparation method is the same as in example 1.
Comparative example 6
The comparative example provides a cleansing oil and a preparation method thereof, wherein the weight percentage of each component of the cleansing oil is shown in table 2, and the addition amount of tocopherol is reduced compared with the components of the cleansing oil of example 6. The preparation method is the same as in example 1.
TABLE 2
Performance testing
Test experiment 1: low temperature freezing experiments
The cleansing oil products prepared in the above examples and comparative examples were kept at constant temperatures of-5 ℃ and-15 ℃ for 24H, respectively, and the oil precipitation phenomenon was observed, and then the products were returned to room temperature to see whether they were all returned to normal. The results are shown in Table 3.
TABLE 3 Table 3
As can be seen from the results of Table 3, the cleansing oils prepared in the examples of the present invention showed no oil precipitation at 0℃and-5℃and had oil precipitation at-15℃and recovered to normal state after leaving to room temperature. In comparative example 1, however, the amount of the oil added at the freezing point was decreased, which resulted in precipitation at-5℃but recovered to normal state after leaving at room temperature.
Test experiment 2: high temperature antioxidant experiment
The cleansing oil products prepared in each example and comparative example were respectively kept at 0 ℃,25 ℃ and 45 ℃ for 8 weeks, and the cleansing oil products were recovered to room temperature, and the change of the odor of the products was tested by comparison, so as to determine the oxidation resistance of the products.
TABLE 4 Table 4
As can be seen from the results in table 4, the cleansing oil product prepared in the example of the present invention is stable at the test temperature for 8 weeks, and has no obvious rancid smell; in comparative example 5, however, the addition of no antioxidant and too little antioxidant in comparative example 6 resulted in a slight change in odor at 25℃and a significant change in odor at 45 ℃. That is, it is stated that no antioxidant is added or that too little antioxidant is added, the prepared cleansing oil has a remarkable rancid smell.
Test experiment 3: experiments on make-up removal Effect
The cleansing effect of the mild cleansing oil is evaluated from two indexes of cleansing force and skin feel after use, and the evaluation of each index adopts grading.
Specific grading criteria for makeup removal force are:
stage 1: the color cosmetics and dirt are clean and quick in the use process.
2 stages: the cleansing power of the color makeup and dirt is general in the use process.
3 stages: the cleansing power of the color makeup and dirt is poor in the use process.
The specific grading standards after use are as follows:
stage 1: the skin has no adverse reaction after use, does not dry, and is fresh and moisture-keeping.
2 stages: the skin has no adverse reaction after use, and is not very dry and not very moist.
3 stages: the skin has no adverse reaction after use, and is greasy or dry.
The results of the evaluation of the cleansing power population for the cleansing oils of examples 1 to 6 and comparative examples 3 to 4 of the present invention are shown in Table 5. Wherein the cleaning force effect of example 2 and comparative example 4 is shown in fig. 1.
TABLE 5
The results of the evaluation of the skin feel crowd of the cleansing oils of examples 1 to 6 and comparative examples 3 to 4 of the present invention are shown in Table 6.
TABLE 6
As can be seen from the results of tables 5 and 6, when only sorbitol polyether-30 tetraoleate was used as an emulsifier in the cleansing oil of comparative example 3, the cleansing power reached level 1, but the cleansing power was too strong, and the skin was dry and the skin feel level was lowered by long-term use. When the addition amount of polyglycerol-2 sesquioleate is increased and the addition amount of sorbitol polyether-30 tetraoleate is reduced in the cleansing oil of comparative example 4, cleansing power of the cleansing oil is lowered, and a greasy phenomenon is generated.
There are many ways in which the invention may be practiced, and what has been described above is merely a preferred embodiment of the invention. It should be noted that the above examples are only for illustrating the present invention and are not intended to limit the scope of the present invention. It will be apparent to those skilled in the art that modifications may be made without departing from the principles of the invention, and such modifications are intended to be within the scope of the invention.
Claims (3)
1. The mild cleansing oil is characterized by comprising the following components in percentage by weight:
sunflower seed oil 18.00-25.00%
Grape seed oil 14.00-21.00%
16.00-20.00% of low freezing point grease
13-19.50% of emulsifying agent
Jojoba seed oil 2.00-5.00%
0.80-1.00% of rice bran oil
0.30-0.60% of antioxidant
0.10-0.60% of butter extract of Butyrospermum parkii
Caprylic/capric triglyceride balance;
the low-freezing point grease is coco-caprylate/caprate;
the emulsifier comprises sorbitol polyether-30 tetraoleate and polyglycerol-2 sesquioleate; the weight percentage of the sorbitol polyether-30 tetraoleate and the polyglycerol-2 sesquioleate in the mild cleansing oil is 12.00-17.00% and 1.00-2.50% respectively;
the antioxidant is tocopherol.
2. The mild cleansing oil according to claim 1, further comprising 0.01 to 0.5% by weight of other components;
the other components include one or more of bergamot fruit oil, geranium oil, calendula extract, white pool seed oil, rosemary leaf extract, and lime peel oil.
3. A method for preparing a mild cleansing oil according to any one of claims 1 to 2, comprising the steps of:
s1, taking a butter extract of a Butyrospermum parkii and caprylic/capric triglyceride as A phases, weighing according to weight percentage, putting into an emulsifying pot for mixing, heating to 45-50 ℃, stirring and dissolving uniformly, and then cooling to 30 ℃;
s2, taking sunflower seed oil, grape seed oil, low-freezing point grease, jojoba seed oil, rice bran oil, an emulsifier and an antioxidant as a phase B, sequentially adding the phases into an emulsifying pot after weighing according to weight percentage, and stirring and dissolving uniformly;
s3, taking other components as a phase C, sequentially adding the components into an emulsifying pot after weighing according to weight percentage, stirring and dissolving uniformly, and obtaining the mild cleansing oil after inspection is qualified.
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| US20210052478A1 (en) * | 2018-01-05 | 2021-02-25 | Altus Labs, Llc | Personal care compositions |
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| JP6234533B1 (en) * | 2016-10-27 | 2017-11-22 | 株式会社ファンケル | Cleansing oil |
| CN106726786A (en) * | 2017-02-10 | 2017-05-31 | 云南白药集团股份有限公司 | Makeup remover with moisture-keeping function |
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