CN110538095A - Peony seed oil cleansing oil and preparation method thereof - Google Patents

Peony seed oil cleansing oil and preparation method thereof Download PDF

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Publication number
CN110538095A
CN110538095A CN201810521328.6A CN201810521328A CN110538095A CN 110538095 A CN110538095 A CN 110538095A CN 201810521328 A CN201810521328 A CN 201810521328A CN 110538095 A CN110538095 A CN 110538095A
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CN
China
Prior art keywords
oil
peony seed
cleansing
seed oil
cleansing oil
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201810521328.6A
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Chinese (zh)
Inventor
苑军浩
刘明富
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Guangzhou Yonghe Biotechnology Co ltd
Original Assignee
Guangzhou Yonghe Biotechnology Co ltd
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Publication date
Application filed by Guangzhou Yonghe Biotechnology Co ltd filed Critical Guangzhou Yonghe Biotechnology Co ltd
Priority to CN201810521328.6A priority Critical patent/CN110538095A/en
Publication of CN110538095A publication Critical patent/CN110538095A/en
Pending legal-status Critical Current

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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q1/00Make-up preparations; Body powders; Preparations for removing make-up
    • A61Q1/14Preparations for removing make-up
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations

Abstract

the invention discloses peony seed oil cleansing oil and a preparation method thereof. The peony seed oil cleansing oil comprises the following components in percentage by mass: 42-50% of peony seed oil, 30-40% of olive oil, 8-10% of ethylhexyl palmitate, 8-10% of PEG-20 glycerol triisostearate and 1-1.5% of tocopheryl acetate. According to the invention, through the blending of the variety and the content of the vegetable oil, the problems that the cost is high when the peony seed oil is used alone, and the skin is easily burdened when the olive oil is used alone are solved; by optimizing the emulsifier and other auxiliary agents, the prepared cleansing oil has high dissolving capacity for color cosmetics, the emulsion has small particle size and is easy to wash when the cleansing oil is added with clear water for massage and emulsification after makeup removal, an oil film is not left on the skin after washing, pores can be deeply cleaned without excessive cleaning, and the skin is not tight after washing.

Description

Peony seed oil cleansing oil and preparation method thereof
Technical Field
the invention belongs to the technical field of cosmetics, and particularly relates to peony seed oil cleansing oil and a preparation method thereof.
Background
most natural vegetable oil can easily dissolve oil-soluble dirt and can be directly used for makeup removal. When the natural vegetable oil is directly used for makeup removal, the natural vegetable oil has strong greasy feeling when being washed by clear water, and the natural vegetable oil does not contain an emulsifier, so the natural vegetable oil does not have an emulsifying effect. In the prior art, the emulsifier is mostly added into the vegetable oil formula for improvement, so that the makeup remover oil can achieve the emulsifying effect when being washed by water. The emulsifier is a surfactant, and the excessive use of the emulsifier can cause certain damage to skin, and the insufficient use of the emulsifier can not achieve ideal emulsification effect. And because different vegetable oils have different fatty acid components and contents, the selection of the type and the addition amount of the emulsifier and the type of the vegetable oil has great influence on the integral emulsifying capacity of the cleansing oil and the particle size of the emulsified emulsion. Therefore, how to select the emulsifier and the auxiliary agent to be compounded with the vegetable oil is the key for preparing the makeup remover oil which has strong dissolving capacity of the makeup, does not have oil film residue and has no harm to the skin.
The olive oil is prepared by directly cold-pressing fresh olive fruits, and is thick and heavy, so that pores are easily blocked by directly using the olive oil as makeup removing oil, and fat grains, blackheads or acnes grow on the skin.
the peony seed oil is woody nut vegetable oil extracted from peony seeds, and can be externally used for beautifying, nourishing skin, eliminating pigmentation, reducing wrinkles, and making skin fine, smooth and elastic. Because the oil yield of the current peony seed oil is relatively low, compared with olive oil, the peony seed oil is high in price. In the prior art, the peony seed oil is compounded with other vegetable oil, and essential oil and emulsifier carbomer, lecithin or Arabic gum are added to prepare the cleansing oil, wherein the content of the peony seed oil is up to 75-85%; in addition, the inventor finds that the makeup remover oil has high dissolving and color-making capacity in the concrete application process, but still has the problems of poor emulsifying effect after water is added and residual oil film on the skin after washing with makeup remover clear water, and cannot deeply clean the skin.
Disclosure of Invention
in order to solve the defects and shortcomings of the prior art, the invention aims to provide the peony seed oil cleansing oil, and the problems of poor emulsification effect and high cost in the peony seed oil cleansing oil are solved through optimal compounding of the vegetable oil and the emulsifier.
The invention also aims to provide a preparation method of the peony seed oil cleansing oil.
The purpose of the invention is realized by the following technical scheme:
The peony seed oil cleansing oil comprises the following components in percentage by mass:
The sum of the percentages of the components is 100 percent.
Preferably, the peony seed oil cleansing oil consists of the following components in percentage by mass:
ethylhexyl palmitate (2-EHP), namely isooctyl palmitate, octyl palmitate, 2-ethylhexyl palmitate and 2-ethylhexyl palmitate, is clear and transparent liquid, is tasteless, insoluble in water, is compatible with most solvents, is a high-purity high-grade fatty acid ester product, is mainly used as a cosmetic raw material, and is an excellent skin softening agent. It has stable property, and is not easy to oxidize or generate odor.
PEG-20 glyceryl triisostearate is a multifunctional emulsifying dispersant, and the appearance of the multifunctional emulsifying dispersant is light yellow liquid; acid value (less than or equal to 10.0mgKOH/g) and saponification value (80-100mgKOH/g) can be obtained from the market, such as United chemical industries, Inc. of Yueyanoke Luode, Hunan.
The preparation method of the peony seed oil cleansing oil comprises the following steps:
(1) stirring and uniformly mixing the peony seed oil, the olive oil and the ethylhexyl palmitate in the peony cleansing oil component to obtain a mixture A;
(2) Adding PEG-20 glycerol triisostearate into the mixture A prepared in the step (1), and uniformly stirring to obtain a mixture B;
(3) And (3) adding tocopherol acetate into the mixture B prepared in the step (2), and uniformly stirring to obtain the peony seed oil cleansing oil.
The peony seed oil cleansing oil prepared by the invention is a faint yellow uniform liquid.
the application method of the peony seed oil cleansing oil comprises the following steps: and (3) drying hands, taking a proper amount of makeup removing oil, uniformly coating the makeup removing oil on the face, massaging for 2 minutes, adding clear water, massaging for 1 minute, and cleaning with clear water.
Compared with the prior art, the invention has the following advantages and beneficial effects:
According to the invention, through the blending of the variety and the content of the vegetable oil, the problems that the cost is high when the peony seed oil is used alone, and the skin is easily burdened when the olive oil is used alone are solved; by optimizing the emulsifier and other auxiliary agents, the prepared cleansing oil has high dissolving capacity for color cosmetics, the emulsion has small particle size and is easy to wash when the cleansing oil is added with clear water for massage and emulsification after cleansing, an oil film is not left on the skin after washing, pores can be deeply cleaned without excessive cleaning, the skin is not tight after washing, and the added tocopheryl acetate also enables the cleansing oil to have an antioxidant effect on the whole.
In addition, the peony seed oil cleansing oil provided by the invention has the advantages of easily available raw materials, low cost and easy market acceptance.
Detailed Description
The present invention will be described in further detail with reference to examples, but the embodiments of the present invention are not limited thereto.
Example 1
The embodiment provides a peony seed oil cleansing oil formula and a preparation method thereof, wherein the peony seed oil cleansing oil formula comprises the following components:
the formula of the peony seed oil cleansing oil comprises the following components:
(II) the preparation steps of the peony seed oil cleansing oil are as follows:
(1) stirring and uniformly mixing the peony seed oil, the olive oil and the ethylhexyl palmitate in the peony cleansing oil component to obtain a mixture A;
(2) Adding PEG-20 glycerol triisostearate into the mixture A prepared in the step (1), and uniformly stirring to obtain a mixture B;
(3) And (3) adding tocopherol acetate into the mixture B prepared in the step (2), and uniformly stirring to obtain the peony seed oil cleansing oil which is marked as sample 1. The health index of the health product meets the regulation of technical specifications for cosmetic safety (2015 edition); the sensory and physical and chemical indexes were measured by the method described in GB/T35914-2018, and the results are shown in Table 1.
TABLE 1 organoleptic, physicochemical indices of sample 1
the standard sample is a standard sample confirmed in the process of developing the cleansing oil
Example 2
The embodiment provides a peony seed oil cleansing oil formula and a preparation method thereof, wherein the peony seed oil cleansing oil formula comprises the following components:
the formula of the peony seed oil cleansing oil comprises the following components:
(II) the preparation steps of the peony seed oil cleansing oil are as follows:
The procedure was the same as in example 1 and the make-up remover prepared was designated as sample 2. The health index of the health product meets the regulation of technical specifications for cosmetic safety (2015 edition); the sensory and physical and chemical indexes were measured by the method described in GB/T35914-2018, and the results are shown in Table 2.
TABLE 2 organoleptic, physicochemical indices of sample 2
The standard sample is a standard sample confirmed in the process of developing the cleansing oil
Example 3
The embodiment provides a peony seed oil cleansing oil formula and a preparation method thereof, wherein the peony seed oil cleansing oil formula comprises the following components:
the formula of the peony seed oil cleansing oil comprises the following components:
(II) the preparation steps of the peony seed oil cleansing oil are as follows:
The procedure was the same as in example 1 and the make-up remover prepared was designated as sample 3. The health index of the health product meets the regulation of technical specifications for cosmetic safety (2015 edition); the sensory and physical and chemical indexes were measured by the method described in GB/T35914-2018, and the results are shown in Table 3.
TABLE 3 organoleptic, physicochemical indices of sample 3
The standard sample is a standard sample confirmed in the process of developing the cleansing oil
Comparative example 1
The comparative example provides cleansing oil, and the formula specifically comprises:
the cleansing oil was prepared according to the preparation procedure of example 1 and the conventional technical means in the art, and the prepared cleansing oil was designated as sample 4, and the hygiene index thereof was in accordance with the regulations of technical specifications for cosmetic safety (2015).
Comparative example 2
The comparative example provides cleansing oil, and the formula specifically comprises:
The cleansing oil was prepared according to the preparation procedure of example 1 and the conventional technical means in the art, and the prepared cleansing oil was designated as sample 5, and the hygiene index thereof was in accordance with the regulations of technical specifications for cosmetic safety (2015).
Comparative example 3
the comparative example provides cleansing oil, and the formula specifically comprises:
The cleansing oil was prepared according to the preparation procedure of example 1 and the conventional technical means in the art, and the prepared cleansing oil was designated as sample 6, and the hygiene index thereof was in accordance with the regulations of technical specifications for cosmetic safety (2015).
Comparative example 4
The comparative example provides cleansing oil, and the formula specifically comprises:
the cleansing oil was prepared according to the preparation procedure of example 1 and the conventional technical means in the art, and the prepared cleansing oil was designated as sample 7, and the hygiene index thereof was in accordance with the regulations of technical specifications for cosmetic safety (2015).
Comparative example 5
The monoglyceride in comparative example 4 was replaced with modified soybean lecithin, which is commonly used in the art, and the obtained cleansing oil was designated as sample 8, and the hygiene index thereof was in accordance with the regulations of technical safety standards for cosmetics (2015).
the self-emulsifying property test and the sensory property evaluation after use of the cleansing oil samples 1 to 8 are as follows:
The self-emulsifying property test method comprises the following steps: the cleansing oil samples 1 to 8 and deionized water were mixed in a ratio of 1: 2000, adding cleansing oil drops into deionized water, standing for 24 hours, and slightly stirring to obtain the emulsion to be detected. And detecting the average particle size of the emulsion by a dynamic laser light scattering particle size analyzer.
the sensory performance evaluation method after use comprises the following steps: the cleansing oil with the size of a monobasic coin is taken out by drying hands, is evenly smeared on the face, is massaged for 2 minutes, is added with clear water for massage for 1 minute, and is cleaned with the clear water. The testing personnel are involved: make up for at least 4 times a week for 100 total of 20-40 year-old volunteers.
TABLE 4 results of the self-emulsifiability tests for cleansing oil samples 1-8
Numbering average particle size of emulsion (. mu.m)
Sample 1 0.357
Sample 2 0.369
sample 3 0.380
Sample No. 4 0.389
Sample No. 5 0.360
sample No. 6 0.550
Sample 7 0.450
Sample 8 0.475
TABLE 5 results of sensory evaluation of cleansing oil samples 1 to 8 after use
The comprehensive experiment results show that the cleansing oil prepared by the invention has high dissolving capacity on makeup, the emulsion has small particle size and is easy to wash when the cleansing oil is added with clear water for massage and emulsification after makeup removal, no oil film is left on the skin after washing, pores can be deeply cleaned without excessive cleaning, the skin is not tight after washing, and the added tocopheryl acetate enables the cleansing oil to have an antioxidant effect; the cleansing oil provided by the invention has the advantages of easily available raw materials, low cost and contribution to market popularization. In addition, it was found in the above sensory test that sample 1 was most easily rinsed after removal of makeup.
the above embodiments are preferred embodiments of the present invention, but the present invention is not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.

Claims (3)

1. the peony seed oil cleansing oil is characterized by comprising the following components in percentage by mass:
2. the peony seed oil cleansing oil according to claim 1, which is characterized by comprising the following components in percentage by mass:
3. the preparation method of the peony seed oil cleansing oil as claimed in claim 1 or 2, characterized by comprising the following steps:
(1) Stirring and uniformly mixing peony seed oil, olive oil and ethylhexyl palmitate to obtain a mixture A;
(2) adding PEG-20 glycerol triisostearate into the mixture A prepared in the step (1), and uniformly stirring to obtain a mixture B;
(3) And (3) adding tocopherol acetate into the mixture B prepared in the step (2), and uniformly stirring to obtain the peony seed oil cleansing oil.
CN201810521328.6A 2018-05-28 2018-05-28 Peony seed oil cleansing oil and preparation method thereof Pending CN110538095A (en)

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113101239A (en) * 2021-04-20 2021-07-13 山东花物堂生物科技有限公司 Multiphase coated micro-emulsified facial cleansing oil and preparation method thereof
CN114504538A (en) * 2021-12-29 2022-05-17 武汉轻工大学 Cleansing oil containing soapberry oil and preparation method thereof

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CN105997778A (en) * 2016-05-13 2016-10-12 广州丹奇日用化工厂有限公司 Washing-free cleansing oil and preparing method thereof
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CN107661244A (en) * 2017-11-20 2018-02-06 菏泽瑞璞牡丹产业科技发展有限公司 A kind of skin-protection type makeup remover and preparation method thereof

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CN104800133A (en) * 2015-05-18 2015-07-29 广州科玛生物科技有限公司 Cleansing oil, preparation method thereof and application thereof
CN105997778A (en) * 2016-05-13 2016-10-12 广州丹奇日用化工厂有限公司 Washing-free cleansing oil and preparing method thereof
CN106635531A (en) * 2016-12-20 2017-05-10 铜陵凤丹种植科技开发有限责任公司 Handmade peony seed oil soap and manufacturing method thereof
CN107661244A (en) * 2017-11-20 2018-02-06 菏泽瑞璞牡丹产业科技发展有限公司 A kind of skin-protection type makeup remover and preparation method thereof

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113101239A (en) * 2021-04-20 2021-07-13 山东花物堂生物科技有限公司 Multiphase coated micro-emulsified facial cleansing oil and preparation method thereof
CN114504538A (en) * 2021-12-29 2022-05-17 武汉轻工大学 Cleansing oil containing soapberry oil and preparation method thereof

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