CN110433091A - A kind of eye make-up remover and preparation method thereof - Google Patents
A kind of eye make-up remover and preparation method thereof Download PDFInfo
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- CN110433091A CN110433091A CN201910847831.5A CN201910847831A CN110433091A CN 110433091 A CN110433091 A CN 110433091A CN 201910847831 A CN201910847831 A CN 201910847831A CN 110433091 A CN110433091 A CN 110433091A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The present invention relates to a kind of eye make-up removers and preparation method thereof.The make-up remover component includes: caprylic/capric triglyceride 25~35%, four oleate 10~15% of PEG-30 anhydrous sorbitol, ethylhexyl palmitate 10~15%, Permethyl 99A 10~15%, isohexadecane 10~15%, microwax 5~12%, stereth -21 3~8%, silica 2~5%, camellia flower extract 3~6%, essence 0.01~0.02%.The make-up remover is mild, has good makeup removing effect, while having anti-wrinkle effect to eye circumference wrinkle, crow's feet.
Description
Technical field
The invention belongs to make-up remover and its preparation field, in particular to a kind of eye make-up remover and preparation method thereof.
Background technique
Makeup removing is the basis of skin care, and residual adornment is oily dirt, and meeting blocked pore breathes cell from smooth, interferes skin
Skin is normally metabolic, so that skin becomes coarse gradually, pore is coarse, colour of skin yellowing, also breeds dark grain, acne.At present
Cleansing product in the market has: makeup remover, makeup removing breast, makeup remover, make-up remover.
Wherein, the ingredient that uses of makeup remover and make-up remover is emulsifier and grease, can be merged with color make-up greasy dirt on the face,
Again thoroughly dissolving color make-up in a manner of water emulsification.And the water content of makeup removing breast is more compared to makeup remover and make-up remover, it is same
Sample is that the more difficult color make-up pigmentolysis removed with water is washed with water product and is removed grease using grease.Present many human eyes
Portion all uses the cosmetics such as eye shadow, mascara, informer that eye portion is made to have romantic charm, however the makeup removing of these cosmetics is one
The troubling thing of part.Cleansing product currently on the market such as makeup remover and make-up remover etc. have certain makeup removing effect, such as
Chinese patent CN104825344A discloses a kind of oil-free make up remover for being exclusively used in eyeliner, and the make up remover is by following weight percent
Raw material than meter forms: 1~15% glycerol, 1~10% butanediol, 1~10% propylene glycol, 1~10%PEG-7 glycerol coconut oil
Ester, 2~8%PEG-80 anhydrous sorbitol laurate, 2~6%PEG-30 anhydrous sorbitol, four oleate, 1~5%PEG-6
Caprylic/capric glyceride type, 1~3%1,2 isoprenes, 1~3% Jojoba wax PEG-120 esters；Surplus is water.But it should
Make up remover makeup removing effect is bad.
Summary of the invention
Technical problem to be solved by the invention is to provide a kind of eye make-up removers and preparation method thereof, to overcome existing skill
The defects of eye makeup removal products makeup removing effect is general in art.
The present invention provides a kind of eye make-up remover, and the make-up remover component includes: that caprylic/capric is sweet according to weight percent
Oily three esters 25~35%, four oleate 10~15% of PEG-30 anhydrous sorbitol, ethylhexyl palmitate 10~15%, different 12
Alkane 10~15%, isohexadecane 10~15%, microwax 5~12%, stereth -21 3~8%, silica 2~5%, mountain
Flos Camelliae Japonicae extract 3~6%, (daily) essence 0.01~0.02%.
The make-up remover component includes: caprylic/capric triglyceride 25%, PEG-30 Sorbitan according to weight percent
Four oleate 11.99% of alcohol, ethylhexyl palmitate 12%, Permethyl 99A 15%, isohexadecane 15%, microwax 5% are stearic
Alcohol polyethers -21 8%, silica 5%, camellia flower extract 3%, (daily) essence 0.01%.
The make-up remover component includes: caprylic/capric triglyceride 30%, PEG-30 Sorbitan according to weight percent
Four oleate 10% of alcohol, ethylhexyl palmitate 10%, Permethyl 99A 10%, isohexadecane 15%, microwax 9%, stearyl alcohol
Polyethers -21 5%, silica 5%, camellia flower extract 5.99%, (daily) essence 0.01%.
The make-up remover component includes: caprylic/capric triglyceride 35%, PEG-30 Sorbitan according to weight percent
Four oleate 14% of alcohol, ethylhexyl palmitate 15%, Permethyl 99A 10%, isohexadecane 10%, microwax 8%, stearyl alcohol
Polyethers -21 3%, silica 2%, camellia flower extract 2.98%, (daily) essence 0.02%.
The present invention also provides a kind of preparation methods of eye make-up remover, comprising the following steps:
(1) by caprylic/capric triglyceride 25~35%, four oleate 10~15% of PEG-30 anhydrous sorbitol, palm
Sour ethylhexyl 10~15%, Permethyl 99A 10~15%, isohexadecane 10~15%, microwax 5~12% and stearyl alcohol are poly-
Ether -21 3~8% mixes, and is heated to 85 ° -90 °；
(2) 2~5%, 85 ° of -90 ° of stirrings of silica and homogeneous is added in the solution into step (1) after heating, then cools down；
(3) 40 ° -45 ° are cooled in step (2), sequentially add camellia flower extract 3~6%, (daily) essence 0.01~
0.02%, it discharges after stirring；
Material content is weight percentage in step (1)~(3).
Mixing time is 20~40min in the step (2)；Homogenizing time is 2~5min.
Mixing time is 20~30min in the step (3).
Beneficial effect
In the present invention caprylic/capric triglyceride and four oleate of PEG-30 anhydrous sorbitol be makeup removing main component, two
Person is combined together, mild non-stimulated, can quickly remove ornaments and formal dress to eye cosmetics such as eye shadow, mascara, informers, not need after makeup removing
It is cleaned again, and camellia (CAMELLIA JAPONICA) flower extract etc. can reduce eye wrinkle-removing, play anti-wrinkle effect.
Specific embodiment
Present invention will be further explained below with reference to specific examples.It should be understood that these embodiments are merely to illustrate the present invention
Rather than it limits the scope of the invention.In addition, it should also be understood that, after reading the content taught by the present invention, those skilled in the art
Member can make various changes or modifications the present invention, and such equivalent forms equally fall within the application the appended claims and limited
Range.
Embodiment 1
A kind of eye make-up remover is present embodiments provided, which includes: caprylic/capric according to weight percent
Triglycerides 25%, four oleate 11.99% of PEG-30 anhydrous sorbitol, ethylhexyl palmitate 12%, Permethyl 99A 15%,
Isohexadecane 15%, microwax 5%, stereth -21 8%, silica 5%, camellia flower extract 3%, (daily) essence
0.01%.
The present embodiment also provides a kind of preparation method of eye make-up remover, specifically:
(1) by caprylic/capric triglyceride 25%, four oleate 11.99% of PEG-30 anhydrous sorbitol, palm acid ethyl
Own ester 12%, Permethyl 99A 15%, isohexadecane 15%, microwax 5% and stereth -21 8% put into main cooker mixing,
It is heated to 85 °；
(2) solution into step (1) after heating is slowly added to silica 5%, and opens 15 turns/min of stirring, when silica is complete
The control of homogenizer revolving speed is opened in 1500 turns/min by portion after adding, homogeneous is closed after opening 2 minutes, and 85 ° are persistently stirred 20min,
Then cool down；
(3) 40 ° are cooled in step (2), sequentially adds camellia flower extract 3%, (daily) essence 0.01%, stirred
It discharges after 20min；
Material content is weight percentage in step (1)~(3).
Embodiment 2
A kind of eye make-up remover is present embodiments provided, which includes: caprylic/capric according to weight percent
Triglycerides 30%, four oleate 10% of PEG-30 anhydrous sorbitol, ethylhexyl palmitate 10%, Permethyl 99A 10% are different
Hexadecane 15%, microwax 9%, stereth -21 5%, silica 5%, camellia flower extract 5.99%, (daily) essence
0.01%.
The present embodiment also provides a kind of preparation method of eye make-up remover, specifically:
(1) by caprylic/capric triglyceride 30%, four oleate 10% of PEG-30 anhydrous sorbitol, palm acid ethyl oneself
Ester 10%, Permethyl 99A 10%, isohexadecane 15%, microwax 9% and stereth -21 5% put into main cooker mixing, add
Heat is to 85 °；
(2) solution into step (1) after heating is slowly added to silica 5%, and opens 20 turns/min of stirring, when silica is complete
The control of homogenizer revolving speed is opened in 1500 turns/min by portion after adding, homogeneous is closed after opening 3 minutes, and 85 ° are persistently stirred 30min,
Then cool down；
(3) 42 ° are cooled in step (2), sequentially adds camellia flower extract 5.99%, (daily) essence 0.01%, stirs
It discharges after mixing 30min；
Material content is weight percentage in step (1)~(3).
Embodiment 3
A kind of eye make-up remover is present embodiments provided, which includes: caprylic/capric according to weight percent
Triglycerides 35%, four oleate 14% of PEG-30 anhydrous sorbitol, ethylhexyl palmitate 15%, Permethyl 99A 10% are different
Hexadecane 10%, microwax 8%, stereth -21 3%, silica 2%, camellia flower extract 2.98%, (daily) essence
0.02%.
The present embodiment also provides a kind of preparation method of eye make-up remover, specifically:
(1) by caprylic/capric triglyceride 35%, four oleate 14% of PEG-30 anhydrous sorbitol, palm acid ethyl oneself
Ester 15%, Permethyl 99A 10%, isohexadecane 10%, microwax 8% and stereth -21 3% put into main cooker mixing, add
Heat is to 90 °；
(2) solution into step (1) after heating is slowly added to silica 2%, and opens 20 turns/min of stirring, when silica is complete
The control of homogenizer revolving speed is opened in 1500 turns/min by portion after adding, homogeneous unlatching is closed after five minutes, and 90 ° are persistently stirred 40min,
Then cool down；
(3) 45 ° are cooled in step (2), sequentially adds camellia flower extract 2.98%, (daily) essence 0.02%, stirs
It discharges after mixing 30min；
Material content is weight percentage in step (1)~(3).
Comparative example 1
According to embodiment 1, make-up remover component does not add caprylic/capric triglyceride, and Permethyl 99A weight percent is changed to
40%, remaining is same as Example 1.
The preparation method of make-up remover is removed and does not add caprylic/capric triglyceride, Permethyl 99A weight percent is changed to 40%
Outside, remaining is same as Example 1.
Comparative example 2
According to embodiment 1, caprylic/capric triglyceride weight percent is changed to 20%, PEG-30 mistake in make-up remover component
Four oleate weight percent of water sorbierite is changed to 16.99%, remaining is same as Example 1.
The preparation method of make-up remover is changed to 20%, PEG-30 Sorbitan except caprylic/capric triglyceride weight percent
Four oleate weight percent of alcohol is changed to outside 16.99%, remaining is same as Example 1.
Comparative example 3
According to embodiment 1, make-up remover component does not add four oleate of PEG-30 anhydrous sorbitol, Permethyl 99A weight percent
Than being changed to 26.99%, remaining is same as Example 1.
Except four oleate of PEG-30 anhydrous sorbitol is not added, Permethyl 99A weight percent changes the preparation method of make-up remover
Outside 26.99%, remaining is same as Example 1.
Comparative example 4
According to embodiment 1, four oleate weight percent of PEG-30 anhydrous sorbitol is changed to 8% in make-up remover component, pungent
Acid/Triglyceride DDD weight percent is changed to 28.99%, remaining is same as Example 1.
The preparation method of make-up remover is changed to 8% except four oleate weight percent of PEG-30 anhydrous sorbitol, caprylic/capric
Triglycerides weight percent is changed to outside 28.99%, remaining is same as Example 1.
Comparative example 5
According to embodiment 1, make-up remover component does not add camellia flower extract, and Permethyl 99A weight percent is changed to 18%,
Remaining is same as Example 1.
Except camellia flower extract is not added, Permethyl 99A weight percent is changed to outside 18% the preparation method of make-up remover,
Yu Jun is same as Example 1.
Comparative example 6
According to embodiment 1, make-up remover component camellia extract weight percentage is changed to 1%, Permethyl 99A weight percent
Than being changed to 17%, remaining is same as Example 1.
The preparation method of make-up remover is changed to 1% except camellia extract weight percentage, and Permethyl 99A weight percent changes
Outside 17%, remaining is same as Example 1.
Comparative example 7
According to embodiment 1, make-up remover component camellia extract weight percentage is changed to 8%, Permethyl 99A weight percent
Than being changed to 10%, remaining is same as Example 1.
The preparation method of make-up remover is changed to 8% except camellia extract weight percentage, and Permethyl 99A weight percent changes
Outside 10%, remaining is same as Example 1.
Comparative example 8
According to Chinese patent CN104825344A, this comparative example provides a kind of oil-free make up remover for being exclusively used in eyeliner,
The make up remover is made of the raw material of following weight percent meter: 3% glycerol, 10% butanediol, 10% propylene glycol, 3%PEG-7 are sweet
Oil palm oleate, 8%PEG-80 anhydrous sorbitol laurate, four oleate of 11.99%PEG-30 anhydrous sorbitol, 5%
PEG-6 caprylic/capric glyceride type, 3%1,2 isoprenes, 3% Jojoba wax PEG-120 esters, surplus is water.
To make up remover in make-up remover in embodiment 1-3 and comparative example 1-7, comparative example 8 carries out makeup removing effect, anti-wrinkle effect is commented
Estimate.
1. makeup removing effect is assessed
Using make up remover in make-up remover in embodiment 1-3 and comparative example 1-7, comparative example 8, respectively to 20 of health
Women tester carries out test assessment, and using ten point system, 10 points best for makeup removing effect, 9 gradation, and 1 point of makeup removing effect is worst.
It is averaged, as a result as shown in table 1 below.
Table 1
As shown in Table 1, make-up remover respectively removes ornaments and formal dress to eye shadow, mascara, informer in embodiment 1-3, has makeup removing well
Effect.When make-up remover does not add caprylic/capric triglyceride, four oleate of PEG-30 anhydrous sorbitol or changes both objects
The dosage of matter, it is poor to the makeup removing effect of eye shadow, mascara, informer, illustrate caprylic/capric triglyceride and PEG-30 dehydration
Four oleate of sorbierite is the main component of makeup removing, and only works as caprylic/capric triglyceride and PEG-30 anhydrous sorbitol four
Oleate could have preferable makeup removing effect to eye shadow, mascara, informer etc. in amount ranges of the invention.Comparative example 8
Although PEG-30 anhydrous sorbitol four oleate of the middle make up remover containing equivalent, due to other compositions difference, to eye shadow,
Mascara, the makeup removing effect of informer are poor.
2. wrinkling resistance is assessed
Using make up remover in make-up remover in embodiment 1-3 and comparative example 1-7, comparative example 8, respectively to 20 of health
Women tester carries out test assessment, and using ten point system, 10 points best for anti-wrinkle effect, 9 gradation, and 1 point of anti-wrinkle effect is worst.
Daily using twice, it is used continuously 4 weeks, is averaged, as a result as shown in table 2 below.
Table 2
As shown in Table 2, make-up remover has apparent anti-wrinkle effect to crow's feet, eye circumference wrinkle in embodiment 1-3.Work as makeup removing
Cream does not add camellia flower extract or changes the dosage of camellia flower extract, to the anti-wrinkle effect of crow's feet, eye circumference wrinkle
It is substantially reduced, illustrates that camellia flower extract plays main influence to the anti-wrinkle effect of make-up remover.Make up remover is to fish tail in comparative example 8
Line, the anti-wrinkle effect of eye circumference wrinkle are bad.
Claims (7)
1. a kind of eye make-up remover, which is characterized in that the make-up remover component includes: that caprylic/capric is sweet according to weight percent
Oily three esters 25~35%, four oleate 10~15% of PEG-30 anhydrous sorbitol, ethylhexyl palmitate 10~15%, different 12
Alkane 10~15%, isohexadecane 10~15%, microwax 5~12%, stereth -21 3~8%, silica 2~5%, mountain
Flos Camelliae Japonicae extract 3~6%, essence 0.01~0.02%.
2. make-up remover according to claim 1, which is characterized in that the make-up remover component includes: pungent according to weight percent
Acid/Triglyceride DDD 25%, four oleate 11.99% of PEG-30 anhydrous sorbitol, ethylhexyl palmitate 12%, different 12
Alkane 15%, isohexadecane 15%, microwax 5%, stereth -21 8%, silica 5%, camellia flower extract 3%, essence
0.01%.
3. make-up remover according to claim 1, which is characterized in that the make-up remover component includes: pungent according to weight percent
Acid/Triglyceride DDD 30%, four oleate 10% of PEG-30 anhydrous sorbitol, ethylhexyl palmitate 10%, Permethyl 99A
10%, isohexadecane 15%, microwax 9%, stereth -21 5%, silica 5%, camellia flower extract 5.99%, essence
0.01%.
4. make-up remover according to claim 1, which is characterized in that the make-up remover component includes: pungent according to weight percent
Acid/Triglyceride DDD 35%, four oleate 14% of PEG-30 anhydrous sorbitol, ethylhexyl palmitate 15%, Permethyl 99A
10%, isohexadecane 10%, microwax 8%, stereth -21 3%, silica 2%, camellia flower extract 2.98%, essence
0.02%.
5. a kind of preparation method of eye make-up remover, comprising the following steps:
(1) by caprylic/capric triglyceride 25~35%, four oleate 10~15% of PEG-30 anhydrous sorbitol, palmitinic acid second
The own ester 10~15% of base, Permethyl 99A 10~15%, isohexadecane 10~15%, microwax 5~12% and stereth -21
3~8% mixing, are heated to 85 ° -90 °；
(2) 2~5%, 85 ° of -90 ° of stirrings of silica and homogeneous is added in the solution into step (1) after heating, then cools down；
(3) 40 ° -45 ° are cooled in step (2), sequentially adds camellia flower extract 3~6%, essence 0.01~0.02%, stirs
It discharges after mixing；
Material content is weight percentage in step (1)~(3).
6. method according to claim 5, which is characterized in that mixing time is 20~40min in the step (2)；Homogeneous
Time is 2~5min.
7. method according to claim 5, which is characterized in that mixing time is 20~30min in the step (3).
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| Application Number | Priority Date | Filing Date | Title |
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| CN201910847831.5A CN110433091A (en) | 2019-09-09 | 2019-09-09 | A kind of eye make-up remover and preparation method thereof |
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| CN201910847831.5A CN110433091A (en) | 2019-09-09 | 2019-09-09 | A kind of eye make-up remover and preparation method thereof |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112494364A (en) * | 2020-12-25 | 2021-03-16 | 泉后(广州)生物科技研究院有限公司 | Smoothie makeup removing cream capable of quickly melting makeup and preparation method thereof |
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| CN106852117A (en) * | 2014-10-17 | 2017-06-13 | 莱雅公司 | For the solid water-free composition removed ornaments and formal dress on skin |
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2019
- 2019-09-09 CN CN201910847831.5A patent/CN110433091A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106852117A (en) * | 2014-10-17 | 2017-06-13 | 莱雅公司 | For the solid water-free composition removed ornaments and formal dress on skin |
Non-Patent Citations (2)
| Title |
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| 杭州睿蓝生物科技有限公司: "《http://ftba.nmpa.gov.cn:8181/ftban/itownet/hzp_ba/fw/pz.jsp?processid=20160831102224i6kyj&nid=20160831102224i6kyj》", 21 September 2016, 国产非特殊用途化妆品备案平台 * |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112494364A (en) * | 2020-12-25 | 2021-03-16 | 泉后(广州)生物科技研究院有限公司 | Smoothie makeup removing cream capable of quickly melting makeup and preparation method thereof |
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Application publication date: 20191112 |
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| RJ01 | Rejection of invention patent application after publication |