CN111991275A - Refreshing type face cleansing oil and preparation method thereof - Google Patents

Refreshing type face cleansing oil and preparation method thereof Download PDF

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Publication number
CN111991275A
CN111991275A CN202011075949.XA CN202011075949A CN111991275A CN 111991275 A CN111991275 A CN 111991275A CN 202011075949 A CN202011075949 A CN 202011075949A CN 111991275 A CN111991275 A CN 111991275A
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oil
refreshing
emulsifier
skin
parts
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CN111991275B (en
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陆锦平
罗嵘
陈晓朋
李雪竹
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Aussia Australia Ltd
Guangzhou Ousia Industrial Co ltd
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Aussia Australia Ltd
Guangzhou Ousia Industrial Co ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/31Hydrocarbons
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34Alcohols
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • A61K8/375Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/49Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
    • A61K8/4993Derivatives containing from 2 to 10 oxyalkylene groups
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/67Vitamins
    • A61K8/678Tocopherol, i.e. vitamin E
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/81Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
    • A61K8/8105Compositions of homopolymers or copolymers of unsaturated aliphatic hydrocarbons having only one carbon-to-carbon double bond; Compositions of derivatives of such polymers
    • A61K8/8111Homopolymers or copolymers of aliphatic olefines, e.g. polyethylene, polyisobutene; Compositions of derivatives of such polymers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/72Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
    • A61K8/84Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
    • A61K8/86Polyethers
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q17/00Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
    • A61Q17/005Antimicrobial preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/10Washing or bathing preparations
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/59Mixtures
    • A61K2800/592Mixtures of compounds complementing their respective functions
    • A61K2800/5922At least two compounds being classified in the same subclass of A61K8/18

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Abstract

The invention relates to a cosmetic, in particular to refreshing facial cleanser and a preparation method thereof. The refreshing facial cleansing oil comprises, by weight, 70-90 parts of grease and 8-25 parts of emulsifier; 0.1-2 parts of skin conditioner and 0.1-2 parts of essence or essential oil. The facial cleanser is characterized in that a facial cleanser cream is prepared by combining special grease and an emulsifier and matching proper essential oil and a skin conditioner system, wherein the facial cleanser cream is fresh and has good skin-friendly moistening effect and excellent cleaning effect.

Description

Refreshing type face cleansing oil and preparation method thereof
Technical Field
The invention relates to a cosmetic, in particular to refreshing facial cleanser and a preparation method thereof.
Background
In daily life, people often need to remove makeup and clean faces after makeup, but researches propose that the people also need to remove makeup after makeup is not carried out, people contact certain dust, computer radiation, kitchen oil smoke and the like every day in daily life to cause that a lot of dirt exists in pores and skin of people can secrete a lot of grease, the dirt is removed cleanly by only depending on facial cleanser, and therefore the people also need to remove makeup and clean faces without makeup.
Various makeup removing cleansing products are available on the market at present, most of the makeup removing cleansing products are grease added with an emulsifier, among the products, some products with strong cleansing capability can easily cause tight feeling on the skin after use and can possibly damage the horny layer of the skin, and some products with general cleansing capability can only clean dirt on the surface layer of the skin and can not deeply clean the skin, so that pore blockage can be caused.
Disclosure of Invention
In order to solve the technical problems, the invention provides a refreshing facial cleanser in a first aspect, which comprises the components of grease, an emulsifier and a skin conditioner.
As a preferable technical scheme of the invention, the refreshing facial cleansing oil comprises, by weight, 70-90 parts of grease, 8-25 parts of emulsifier and 0.1-2 parts of skin conditioner.
As a preferable technical scheme of the invention, the refreshing facial cleansing oil further comprises 0.1-2 parts by weight of essence or essential oil.
As a preferable technical scheme of the invention, the grease is selected from one or more of hydrocarbons, fatty alcohol, fatty acid ester, glyceride, silicone oil and silicon wax.
In a preferred embodiment of the present invention, the fat or oil is selected from one or more of hydrogenated polyisobutene, C13-14 isoparaffin, liquid paraffin, soybean oil, peach kernel oil, jojoba seed oil, isopropyl palmitate, isocetyl stearoyloxy stearate, caprylic/capric triglyceride, isopropyl myristate, pentaerythritol tetra (ethyl hexanoate) and isostearyl isostearate.
As a preferable technical scheme of the invention, the emulsifier is selected from one or more of polysorbate-60, polysorbate-85, polysorbate-80, polyglycerol-6 myristate, polyglycerol-10 myristate, polyglycerol-6 dicaprate, polyglycerol-10 dimyristate, polyglycerol-6 caprylate, laureth-4 and laureth-23.
As a preferable technical scheme, the emulsifier is a mixture of polysorbate-85 and laureth-4.
In a preferred embodiment of the present invention, the skin conditioner is tocopherol acetate and/or bisabolol.
As a preferred technical solution of the present invention, the essential oil is selected from one or more of melaleuca alternifolia leaf oil, rose essential oil, sweet orange peel oil, sea buckthorn essential oil, chamomile oil, mint essential oil, lavender oil, peony essential oil, and peony seed essential oil.
The second aspect of the invention provides a preparation method of refreshing facial cleansing oil, which comprises the following steps:
(1) dissolving oil at 62-68 deg.C, adding emulsifier when the oil is uniform and transparent, stirring to dissolve until the sample is clear, and stirring at 250-300 rpm/min;
(2) and (2) the temperature in the step (1) is lower than 50 ℃, a skin conditioner and essence or essential oil are added, and the mixture is uniformly stirred, wherein the stirring speed is 250-300 rpm/min.
The invention has the following beneficial effects:
1. the facial cleanser oil disclosed by the invention can be used for well cleaning residual cosmetics on the face and cleaning facial grease and dirt in pores;
2. the cleansing oil disclosed by the invention has good stability;
3. the cleansing oil disclosed by the invention has the effects of resisting bacteria and diminishing inflammation, repairing skin and shrinking pores, is safe and has no side effect;
4. the cleansing oil disclosed by the invention can soften and dry the epidermis, can enhance the water retention capacity and provide moderate moisture, and has good moisturizing performance;
5. the viscosity of the cleansing oil is very low, and after the cleansing oil is used, the phenomenon of greasiness cannot occur;
6. the natural plant jojoba seed oil and various mild and non-irritant grease are added into the system, so that the property is mild, the skin care effect is obvious, the system is suitable for long-term use, and the emulsifier with specific content can easily realize the face cleaning effect under the mutual synergistic action with the grease, the skin conditioner and the emulsifier, and skin allergy and irritation can not be caused;
7. the essence or the essential oil is added in the system, so that the facial cleansing oil has good smell;
8. the cleansing oil with refreshing and excellent cleaning effects is prepared by the synergistic effect of the combination of the special oil and the special emulsifier, the skin conditioning agent and the essential oil.
Detailed Description
The first aspect of the invention provides refreshing type cleansing oil which comprises the components of grease, an emulsifier and a skin conditioner.
Preferably, the refreshing facial cleansing oil comprises, by weight, 70-90 parts of grease, 8-25 parts of emulsifier and 0.1-2 parts of skin conditioner.
The refreshing facial cleansing oil also comprises 0.1-2 parts by weight of essence or essential oil.
The oil is selected from one or more of hydrocarbons, fatty alcohol, fatty acid ester, glyceride, silicone oil and silicon wax.
Preferably, the oil is selected from one or more of hydrogenated polyisobutene, C13-14 isoparaffin, liquid paraffin, soybean oil, peach kernel oil, jojoba seed oil, isopropyl palmitate, isocetyl stearoyl oxystearate, caprylic/capric triglyceride, isopropyl myristate, pentaerythritol tetra (ethyl hexanoate), and isostearyl isostearate.
More preferably, the oil is a mixture of hydrogenated polyisobutene, C13-14 isoparaffin, jojoba seed oil, isocetyl stearoyloxystearate, caprylic/capric triglyceride, pentaerythritol tetra (ethylhexanoate), isostearyl isostearate.
Most preferably, the oil is hydrogenated polyisobutene, C13-14 isoparaffin, jojoba seed oil, isocetyl stearoyl stearate, caprylic/capric triglyceride, pentaerythritol tetra (ethylhexanoic) ester, a mixture of isostearyl isostearate, hydrogenated polyisobutene, C13-14 isoparaffin, jojoba seed oil, isocetyl stearoyl stearate, caprylic/capric triglyceride, pentaerythritol tetra (ethylhexanoic) ester, isostearyl isostearate, in weight amounts of: (20-28): (18-25): (0.08-0.12): (2.5-3.3): (30.5-33.28): (1.02-1.23): (0.8-1.2).
Hydrogenated polyisobutenesThe facial cleanser is a lipid closest to sebum of a human body, has good affinity to the skin, can be integrated with the skin lipid membrane of the human body, forms a natural barrier on the surface of the skin, has extremely high chemical stability, and can effectively maintain the stability and the skin affinity of the facial cleanser when being added into the facial cleanser.
C13-14 isoparaffinIs a mixture of branched aliphatic hydrocarbons having 13 or 14 carbons in the chain, which increases the hydration of the skin by forming a protective layer on the skin surface, a thin film preventing skin evaporation, and by accumulating water in the uppermost layer of the skin, and which can also act as a solvent, thickener and gel to formAnd (4) dividing.
Jojoba seed oilThe chemical molecular arrangement of the compound is very similar to that of human sebum, is very easy to be classified and absorbed by skin, has good fine moistening and moisturizing performances, has excellent hydrophilicity, and can effectively regulate and maintain the moisture of human skin, prevent wrinkles and soften the skin.
Pentaerythritol tetra (ethylhexanoate)The hindered fatty acid ester belongs to hindered ester, has four ester bonds to form a three-dimensional structure, has very high stability, and has good stability for additives such as an emulsifier.
Isocetyl stearyl acyloxy stearateThe product has good dispersibility, can uniformly disperse other components, makes the prepared product more exquisite and rich in texture, and can bring fresh and smooth touch to the skin, so that the skin becomes moist and full.
Caprylic/capric triglycerideThe oil is a high-definition odorless oil, belongs to derivatives of palm oil or coconut oil, has compatible characteristics with human skin, is suitable for people with various skin types, does not have greasy feeling after being used, and has stable storage performance.
Isostearyl alcohol isostearateThe long carbon chain ester can endow the skin with excellent adhesion and skin moistening performance, has luxurious skin feeling, is soft and not greasy, can be cooperated with the horny layer to obviously improve the hydration and the protection function, and enables the skin to naturally keep the optimal level of the hydration, but when the long carbon chain ester is used alone, the long carbon chain ester may have certain irritation on the skin and is not friendly to the sensitive people of the skin.
The cleansing oil disclosed by the invention not only can well clean residual cosmetics on the face, but also can clean grease on the face and dirty objects in pores. The possible reason is that the hydrogenated polyisobutene in the oil is close to the sebum of a human body, the chemical molecular arrangement of jojoba seed oil is very similar to that of the sebum of the human body, other facial oil and dirt in pores can be dissolved and taken out more according to the similar compatibility principle, and then the hydrogenated polyisobutene is emulsified with water under the action of an emulsifier so as to be separated from the skin; it is also possible that the main chemical component of the sweet orange peel oil in the essential oil is limonene which has a good cleaning effect and can help to remove excess sebum, and the synergistic effect of the essential oil and the grease ensures that the cleansing oil has a good cleaning effect.
The compounding of the specific grease in the invention ensures that the prepared cleansing oil has low viscosity and does not have greasy phenomenon after the interface oil is used.
The emulsifier is one or more selected from polysorbate-60, polysorbate-85, polysorbate-80, polyglycerol-6 myristate, polyglycerol-10 myristate, polyglycerol-6 dicaprate, polyglycerol-10 dimyristate, polyglycerol-6 caprylate, laureth-4, and laureth-23.
Preferably, the emulsifier is a mixture of polysorbate-85 and laureth-4.
More preferably, the emulsifier is a mixture of polysorbate-85 and laureth-4, and the weight ratio of polysorbate-85 to laureth-4 is (6.2-10): (4.2-6.2).
Polysorbate-85Can be dispersed in water, and can emulsify oil when meeting water.
Laureth-4Easily dissolved in oil and polar solvent, is in a diffusion shape in water, has good emulsifying property, but can cause skin allergy and sensitivity phenomena to some people sensitive to skin when being used alone.
The compound emulsifier used in the invention has excellent emulsifying effect on grease, the synergistic effect of the compound emulsifier with specific content with grease, skin conditioner and emulsifier can easily realize the face cleaning effect, and skin allergy and irritation caused by the use of laureth-4 can not be caused, but the face cleaning oil of the invention has fresh texture after use. The possible reasons are that the bisabolol in the skin conditioner can be used as an active ingredient to reduce the irritation of the laureth-4 type irritant component, the natural plant jojoba seed oil and a plurality of mild and non-irritant oils are added in the system, the nature is mild, and the cleansing oil disclosed by the invention is enabled to be warm and non-irritant under the synergistic action of the oils and the skin conditioner in the oil system, so that the cleansing oil has a fresh texture after being used.
The cleansing oil of the present invention has good stability performance, on one hand, due to the stability of hydrogenated polyisobutene, pentaerythritol tetra (ethyl hexanoate) ester per se, and on the other hand, probably because the C13-14 isoparaffin, together with polysorbate-85 and laureth-4 in the emulsifier, may form a stable milky substance which, in turn, cooperates with other components in the system to increase the stability of the resulting cleansing oil.
The skin conditioning agent is tocopherol acetate and/or bisabolol.
Preferably, the skin conditioning agent is a mixture of tocopherol acetate and bisabolol.
More preferably, the skin conditioner is a mixture of tocopherol acetate and bisabolol, and the weight ratio of the tocopherol acetate to the bisabolol is (4.6-5.2): (0.8:1.3).
Tocopherol acetateBelongs to vitamin E derivatives, can be dissolved in grease, is insoluble in water, has extremely strong reducibility, and can be used as an antioxidant.
BisabololIs an active ingredient, can protect and care allergic skin, has good stability and good compatibility with skin, and also has antibacterial and anti-inflammatory effects.
In the invention, the compound use of the tocopherol acetate and the bisabolol as the skin conditioning agents can prevent the oxidative rancidity of the grease from influencing the appearance and the smell of the product, and the product has the effects of resisting bacteria and diminishing inflammation, repairing the skin and shrinking pores, and is safe and free of side effects.
The essential oil is selected from one or more of melaleuca alternifolia leaf oil, rose essential oil, sweet orange peel oil, sea buckthorn essential oil, chrysanthemum morifolium oil, mint essential oil, mixed lavender oil, peony essential oil and peony seed essential oil.
Preferably, the essential oil is a mixture of melaleuca alternifolia leaf oil, sweet orange peel oil, chamomile oil and mixed lavender oil.
More preferably, the essential oil is a mixture of melaleuca alternifolia leaf oil, sweet orange peel oil, chrysanthemum morifolium ramat oil and miscellaneous lavender oil, and the weight ratio of the melaleuca alternifolia leaf oil, the sweet orange peel oil, the chrysanthemum morifolium ramat oil and the miscellaneous lavender oil is (6-10): (8-12): (3-7): (4.5-8).
Oil of Melaleuca alternifoliaHas antibacterial effect, has strong transdermal penetration promoting effect, can help absorption of other effective components, and is suitable for various skin types.
Sweet orange peel oilIs obtained by squeezing orange peel, not only has the faint scent of orange, but also has good cleaning function, and more importantly, has the efficacy of oxidation resistance.
White flower spring yellow chrysanthemum oilCan separate 20 kinds of triterpenes with anti-inflammatory effect, has anti-inflammatory effect, can eliminate free radicals, and has good antioxidant effect.
Mixed lavender oilHas fragrance of lavender-like flower fragrance, contains linalyl acetate, lavender alcohol, lavender acetate, etc., and has antibacterial, disinfectant, refreshing, tranquilizing, and fatigue relieving effects.
In the invention, the essential oil not only ensures that the product has good smell, but also has antioxidant performance, and can be used for effectively preventing the oxidative rancidity of the oil by being cooperated with the skin conditioner to act on the oil.
The essence can be added with different types of essences according to different odor requirements.
The addition of the essence or the essential oil makes the invention have good smell.
In the invention, jojoba seed oil in the system has skin-friendly property and has the function of regulating moisture of skin, isostearyl isostearate belongs to long carbon chain ester and has the function of regulating moisture of skin, a skin regulator can inhibit oxidation of intercellular lipid and soften dry epidermis, and essential oil can promote metabolism, enhance water retention capacity and provide moderate moisture.
The second aspect of the invention provides a preparation method of refreshing facial cleansing oil, which comprises the following steps:
(1) dissolving oil at 62-68 deg.C, adding emulsifier when the oil is uniform and transparent, stirring to dissolve until the sample is clear, and stirring at 250-300 rpm/min;
(2) and (2) the temperature in the step (1) is lower than 50 ℃, a skin conditioner and essence or essential oil are added, and the mixture is uniformly stirred, wherein the stirring speed is 250-300 rpm/min.
The cleansing oil with refreshing and excellent cleaning effects is prepared by the synergistic effect of the combination of the special oil and the special emulsifier, the skin conditioner and the essential oil.
Several specific examples of the present invention are given below, but the present invention is not limited by the examples.
The raw materials used in the examples of the present invention are shown in Table 1, but are not limited to these raw materials.
TABLE 1
Figure BDA0002716596960000071
Examples
Example 1
A refreshing facial cleanser comprises, by weight, 85.51 parts of grease and 13.6 parts of emulsifier; 0.6 part of skin conditioner.
The refreshing facial cleansing oil also comprises 0.29 part by weight of essential oil.
The oil is a mixture of hydrogenated polyisobutene, C13-14 isoparaffin, jojoba seed oil, isocetyl stearoyl stearate, caprylic/capric triglyceride, pentaerythritol tetra (ethyl hexanoate) and isostearyl isostearate.
The weight of the hydrogenated polyisobutene, the C13-14 isoparaffin, the jojoba seed oil, the isocetyl stearoyl oxystearate, the caprylic/capric triglyceride, the pentaerythritol tetra (ethyl hexanoate) and the isostearyl isostearate is 25: 23: 0.1: 3: 32.24: 1.17: 1.
the emulsifier is a mixture of polysorbate-85 and laureth-4.
The weight ratio of the polysorbate-85 to the laureth-4 is 8: 5.6.
the skin conditioner is a mixture of tocopherol acetate and bisabolol.
The weight ratio of the tocopherol acetate to the bisabolol is 5: 1.
the essential oil is a mixture of melaleuca alternifolia leaf oil, sweet orange peel oil, chamomile oil and mixed lavender oil.
The weight ratio of the melaleuca alternifolia leaf oil, the sweet orange peel oil, the chrysanthemum morifolium oil and the mixed lavender oil is 8: 10: 5: 6.
the preparation method of the refreshing facial cleanser comprises the following steps:
(1) dissolving oil at 65 deg.C, adding emulsifier when the oil is uniform and transparent, stirring to dissolve until the sample is clear, and stirring at 280 rpm/min;
(2) and (2) heating the temperature in the step (1) to 40 ℃, adding a skin conditioner and essential oil, and uniformly stirring to obtain the refreshing facial cleanser, wherein the stirring speed is 280 rpm/min.
Example 2
A refreshing facial cleanser comprises, by weight, 85.51 parts of grease and 13.6 parts of emulsifier; 0.6 part of skin conditioner.
The refreshing facial cleanser also comprises 0.19 part by weight of essence.
The oil, emulsifier, and skin conditioner were the same as in example 1.
The preparation method of the refreshing facial cleanser comprises the following steps:
(1) dissolving oil at 65 deg.C, adding emulsifier, stirring to dissolve until the sample is clear, and stirring at 280 rpm/min;
(2) and (2) heating the temperature in the step (1) to 40 ℃, adding a skin conditioner and essence, and uniformly stirring to obtain the refreshing facial cleanser, wherein the stirring speed is 280 rpm/min.
Example 3
A refreshing cleansing oil comprises, by weight, 87.63 parts of oil and 12 parts of emulsifier; 0.15 part of skin conditioner.
The refreshing facial cleansing oil also comprises 0.22 weight part of essential oil.
The oil is a mixture of hydrogenated polyisobutene, C13-14 isoparaffin, jojoba seed oil, isocetyl stearoyl stearate, caprylic/capric triglyceride, pentaerythritol tetra (ethyl hexanoate) and isostearyl isostearate.
The weight of the hydrogenated polyisobutene, the C13-14 isoparaffin, the jojoba seed oil, the isocetyl stearoyl oxystearate, the caprylic/capric triglyceride, the pentaerythritol tetra (ethyl hexanoate) and the isostearyl isostearate is 24.5: 27: 0.1: 3.3: 30.4: 1.23: 1.1.
the emulsifiers, skin conditioners, essential oils were as in example 1.
The preparation method of the refreshing facial cleanser is the same as that of example 1.
Example 4
A refreshing facial cleanser comprises, by weight, 85.51 parts of grease and 13.6 parts of emulsifier; 0.6 part of skin conditioner.
The refreshing facial cleansing oil also comprises 0.29 part by weight of essential oil.
The oil is a mixture of hydrogenated polyisobutene, C13-14 isoparaffin, isocetyl stearoyl oxystearate, caprylic/capric triglyceride, pentaerythritol tetra (ethyl hexanoate) and isostearyl isostearate.
The weight of the hydrogenated polyisobutene, the C13-14 isoparaffin, the isocetyl stearoyl oxystearate, the caprylic/capric triglyceride, the pentaerythritol tetra (ethyl hexanoate) and the isostearyl isostearate is 25: 23: 3: 32.24: 1.17: 1.
the emulsifiers, skin conditioners, essential oils were as in example 1.
The preparation of the refreshing facial cleanser is the same as that of example 1.
Example 5
A refreshing facial cleanser comprises, by weight, 85.51 parts of grease and 13.6 parts of emulsifier; 0.6 part of skin conditioner.
The oil, emulsifier, and skin conditioner were the same as in example 1.
The preparation method of the refreshing facial cleanser comprises the following steps:
(1) dissolving oil at 65 ℃, adding an emulsifier when the oil is uniform and transparent, stirring and dissolving until a sample is in a clear state, wherein the stirring speed is 280 rpm/min;
(2) and (2) heating the temperature in the step (1) to 40 ℃, adding a skin conditioner, and uniformly stirring to obtain the refreshing facial cleanser, wherein the stirring speed is 280 rpm/min.
Example 6
A refreshing facial cleanser comprises, by weight, 85.51 parts of grease and 13.6 parts of emulsifier; 0.6 part of skin conditioner.
The refreshing facial cleansing oil also comprises 0.29 part by weight of essential oil.
The oil, emulsifier and essential oil were as in example 1.
The skin conditioner is bisabolol.
The preparation method of the refreshing facial cleanser is the same as that of example 1.
Example 7
A refreshing facial cleanser comprises, by weight, 85.51 parts of grease and 13.6 parts of emulsifier; 0.6 part of skin conditioner.
The oil and fat and the emulsifier were the same as in example 1.
The skin conditioner is tocopherol acetate.
The preparation method of the refreshing facial cleanser comprises the following steps:
(1) dissolving oil at 65 deg.C, adding emulsifier when the oil is uniform and transparent, stirring to dissolve until the sample is clear, and stirring at 280 rpm/min;
(2) and (2) heating the temperature in the step (1) to 40 ℃, adding a skin conditioner, and uniformly stirring to obtain the refreshing facial cleanser, wherein the stirring speed is 280 rpm/min.
Example 8
A refreshing facial cleanser comprises, by weight, 85.51 parts of grease and 13.6 parts of emulsifier; 0.6 part of skin conditioner.
The refreshing facial cleansing oil also comprises 0.29 part by weight of essential oil.
The oil, emulsifier and essential oil were as in example 1.
The skin conditioner is tocopherol acetate.
The weight ratio of the tocopherol acetate to the bisabolol is 5: 1.
the preparation method of the refreshing facial cleanser is the same as that of example 1.
Example 9
A refreshing facial cleanser comprises, by weight, 85.51 parts of grease and 13.6 parts of emulsifier; 0.6 part of skin conditioner.
The refreshing facial cleansing oil also comprises 0.29 part by weight of essential oil.
The oil, skin conditioner, and essential oil were the same as in example 1.
The emulsifier is polysorbate-85.
The preparation method of the refreshing facial cleanser is the same as that of example 1.
Example 10
A refreshing facial cleanser comprises, by weight, 85.51 parts of grease and 13.6 parts of emulsifier; 0.6 part of skin conditioner.
The refreshing facial cleansing oil also comprises 0.29 part by weight of essential oil.
The oil, skin conditioner, and essential oil were the same as in example 1.
The emulsifier is laureth-4.
The preparation method of the refreshing facial cleanser is the same as that of example 1.
Example 11
A refreshing facial cleanser comprises, by weight, 85.51 parts of grease and 13.6 parts of emulsifier; 0.6 part of skin conditioner.
The refreshing facial cleansing oil also comprises 0.29 part by weight of essential oil.
The oil, skin conditioner, and essential oil were the same as in example 1.
The emulsifier is a mixture of polysorbate-85 and laureth-4.
The weight ratio of the polysorbate-85 to the laureth-4 is 6: 6.5.
the preparation method of the refreshing facial cleanser is the same as that of example 1.
Example 12
A refreshing facial cleanser comprises, by weight, 85.51 parts of grease and 13.6 parts of emulsifier; 0.6 part of skin conditioner.
The refreshing facial cleansing oil also comprises 0.29 part by weight of essential oil.
The oil, skin conditioner, and essential oil were the same as in example 1.
The emulsifier is a mixture of polysorbate-85 and laureth-4.
The weight ratio of the polysorbate-85 to the laureth-4 is 10.5: 4.
the preparation method of the refreshing facial cleanser is the same as that of example 1.
Example 13
A refreshing facial cleanser comprises, by weight, 85.51 parts of grease and 25 parts of emulsifier; 0.6 part of skin conditioner.
The refreshing facial cleansing oil also comprises 0.29 part by weight of essential oil.
The oil, emulsifier, skin conditioner, essential oil were the same as in example 1.
The preparation method of the refreshing facial cleanser is the same as that of example 1.
Example 14
A refreshing facial cleanser comprises, by weight, 85.51 parts of grease and 8 parts of emulsifier; 0.6 part of skin conditioner.
The refreshing facial cleansing oil also comprises 0.29 part by weight of essential oil.
The oil, emulsifier, skin conditioner, essential oil were the same as in example 1.
The preparation method of the refreshing facial cleanser is the same as that of example 1.
Firstly, the using effect of the cleansing oil of 1 to 14 in the embodiment of the invention is tested:
(1) the testing personnel are involved: make up 20-45 years old volunteers at least 4 times a week for 60 cases.
(2) The test method comprises the following steps: after the face of the volunteer is made up, the face cleansing oil with the size of a monobasic coin is smeared on the dry upper face and is massaged for about 1 minute in a circling way, then water is added to continue massaging for about half minute in a circling way, the face cleansing oil is washed clean by warm water, and the days for trying the face cleansing oil is 14 days.
(3) And (3) testing results: table 2 is the volunteer's evaluation of makeup removal effect; table 3 is the evaluation of the refreshing feeling of the volunteers for the evaluation of the makeup removing effect.
TABLE 2
Figure BDA0002716596960000121
Figure BDA0002716596960000131
TABLE 3
Figure BDA0002716596960000132
Secondly, the sanitation indexes of the cleansing oil in the embodiment 1 of the invention are tested:
safety tests were carried out on the samples submitted for inspection according to the standards of the cosmetic hygiene code (2007 edition)
1. For microbiological testing
The items of colony total, mold and yeast total, faecal coliform group, staphylococcus aureus and pseudomonas aeruginosa of the cleansing oil in the example 1 all meet the requirements.
2. Sanitary chemistry detection
The results of mercury, arsenic and lead detection of the facial cleanser in example 1 all meet the requirements.
Thirdly, the cleansing oil of the invention in the embodiment 1-9 is subjected to a skin closed patch test:
1. the testing personnel are involved: 30 tested persons have healthy skin and no skin disease allergy and accord with the test volunteer selection standard.
2. The spot pasting method comprises the following steps: the selected area is not more than 50mm2And qualified spot test equipment with the depth of about 1 mm. The method comprises the steps of putting a test object into a small chamber of a spot tester, wherein the dosage is about 0.020 mL-0.025 mL, sticking the spot tester added with the test object to the back or the curved side of the forearm of a subject by using a low-sensitization adhesive tape, slightly pressing the spot tester by using a palm to uniformly stick the spot tester to the skin for 24 hours, observing skin reactions according to the standard of table 1 after 0.5 hour (after an indentation disappears), 24 hours and 48 hours after the spot tester of the test object is removed, and recording the observation results according to the skin reactions in 2015 edition of technical Specification for cosmetic safety.
3. The experimental results are as follows: the result of the human body skin patch experiment shows that: 30 subjects observed skin reactions at 0.5, 24, and 48 hours by the spot test using the cleansing oil (examples 1 to 9) according to the present invention, wherein 0 skin reaction using the cleansing oil of examples 1 to 9 was a positive reaction.
Fourthly, stability test experiments are carried out on the cleansing oils 1 to 14 in the examples of the present invention:
the cleansing oils of examples 1 to 14 were stored at room temperature, 50 ℃, 5 ℃ for 1 week, 2 weeks, and 1 month, respectively, and the appearance was visually compared with the freshly prepared samples, and the stability was evaluated according to the following criteria, a: no significant change in the sample was observed under this condition; b: the smell is changed; c: the color is changed: d: there is a delamination phenomenon.
The results of the experiment are shown in table 4:
TABLE 4
Figure BDA0002716596960000141
Figure BDA0002716596960000151
As a result of the above-described performance test, example 1 was the most preferable example of examples 1 to 14. And the color of the facial oils in examples 1-8 was observed to be pale yellow; the facial oils of examples 10, 11, 14 were lighter in color than the facial oils of examples 1-8; the cleansing oils of examples 9, 12, and 13 were darker than the cleansing oils of examples 1 to 8. This is probably because the high or low level of polysorbate-85 in the facial oil affects the color of the facial oil.

Claims (10)

1. The refreshing facial cleanser is characterized by comprising the components of oil, an emulsifier and a skin conditioner.
2. The refreshing facial cleansing oil according to claim 1, wherein the components of the refreshing facial cleansing oil comprise, by weight, 70-90 parts of oil and fat, 8-25 parts of emulsifier and 0.1-2 parts of skin conditioner.
3. The refreshing facial cleansing oil according to claim 2, wherein the components of the refreshing facial cleansing oil further comprise 0.1-2 parts by weight of essence or essential oil.
4. The refreshing facial cleansing oil according to claim 1 or 2, wherein the oil is selected from one or more of hydrocarbons, fatty alcohols, fatty acids, fatty acid esters, glycerides, silicone oils and silicone waxes.
5. The refreshing facial cleansing oil according to claim 4, wherein the oil is selected from one or more of hydrogenated polyisobutene, C13-14 isoparaffin, liquid paraffin, soybean oil, peach kernel oil, jojoba oil, isopropyl palmitate, isocetyl stearoyloxy stearate, caprylic/capric triglyceride, isopropyl myristate, pentaerythritol tetra (ethyl hexanoate) and isostearyl isostearate.
6. The refreshing facial cleansing oil according to claim 1 or 2, wherein the emulsifier is one or more selected from polysorbate-60, polysorbate-85, polysorbate-80, polyglyceryl-6 myristate, polyglyceryl-10 myristate, polyglyceryl-6 dicaprate, polyglyceryl-10 dimyristate, polyglyceryl-6 caprylate, laureth-4, laureth-23.
7. The refreshing facial cleansing oil according to claim 6, wherein the emulsifier is a mixture of polysorbate-85 and laureth-4.
8. The refreshing facial oil according to claim 1 or 2, wherein the skin conditioning agent is tocopherol acetate and/or bisabolol.
9. The refreshing facial cleansing oil according to claim 3, wherein the essential oil is selected from one or more of melaleuca alternifolia leaf oil, rose essential oil, sweet orange peel oil, sea buckthorn essential oil, chamomile oil, mint essential oil, lavender oil, peony essential oil and peony seed essential oil.
10. A method for preparing a refreshing facial cleanser according to claim 3 or 9, wherein the preparation process comprises:
(1) dissolving oil at 62-68 deg.C, adding emulsifier when the oil is uniform and transparent, stirring to dissolve until the sample is clear, and stirring at 250-300 rpm/min;
(2) and (2) the temperature in the step (1) is lower than 50 ℃, a skin conditioner and essence or essential oil are added, and the mixture is uniformly stirred, wherein the stirring speed is 250-300 rpm/min.
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112675079A (en) * 2021-01-13 2021-04-20 铂臻(广州)生物科技有限公司 Quick-emulsifying cleansing oil

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102883707A (en) * 2010-05-14 2013-01-16 富士胶片株式会社 Cleansing cosmetic
CN109846760A (en) * 2019-04-23 2019-06-07 上海舒彩网络科技有限公司 Vegetable fat composite and application, clean face oil and preparation method in cosmetics

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102883707A (en) * 2010-05-14 2013-01-16 富士胶片株式会社 Cleansing cosmetic
CN109846760A (en) * 2019-04-23 2019-06-07 上海舒彩网络科技有限公司 Vegetable fat composite and application, clean face oil and preparation method in cosmetics

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
上海新高姿化妆品有限公司广州分公司: "高姿滢采透亮卸妆油", 《国产非特殊用途化妆品备案平台》 *
佚名: "HOLA赫拉茶树植物调理卸妆油 不堵塞毛孔 干净不紧绷", 《白荔枝网,HTTP://WWW.BAILIZHI.COM/15983/》 *
彭冠杰,郭清泉主编: "《美白化妆品科学与技术》", 30 June 2019, 中国轻工业出版社 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112675079A (en) * 2021-01-13 2021-04-20 铂臻(广州)生物科技有限公司 Quick-emulsifying cleansing oil

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