CN112169811A - 一种硫酸钯溶液的制备方法 - Google Patents
一种硫酸钯溶液的制备方法 Download PDFInfo
- Publication number
- CN112169811A CN112169811A CN202011164815.5A CN202011164815A CN112169811A CN 112169811 A CN112169811 A CN 112169811A CN 202011164815 A CN202011164815 A CN 202011164815A CN 112169811 A CN112169811 A CN 112169811A
- Authority
- CN
- China
- Prior art keywords
- palladium
- solution
- sulfate solution
- reaction vessel
- stirring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 title claims abstract description 87
- 229910052763 palladium Inorganic materials 0.000 title claims abstract description 41
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 title claims abstract description 23
- 238000002360 preparation method Methods 0.000 title abstract description 10
- 239000000243 solution Substances 0.000 claims abstract description 32
- 238000006243 chemical reaction Methods 0.000 claims abstract description 19
- 238000003756 stirring Methods 0.000 claims abstract description 17
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 13
- 239000000654 additive Substances 0.000 claims abstract description 11
- 230000000996 additive effect Effects 0.000 claims abstract description 11
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000706 filtrate Substances 0.000 claims abstract description 10
- 229910017604 nitric acid Inorganic materials 0.000 claims abstract description 10
- 238000010992 reflux Methods 0.000 claims abstract description 10
- 239000011259 mixed solution Substances 0.000 claims abstract description 8
- 238000001816 cooling Methods 0.000 claims abstract description 6
- 239000013078 crystal Substances 0.000 claims abstract description 6
- 239000008367 deionised water Substances 0.000 claims abstract description 6
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 6
- 238000007865 diluting Methods 0.000 claims abstract description 6
- 238000001914 filtration Methods 0.000 claims abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000000034 method Methods 0.000 claims description 10
- DLFVBJFMPXGRIB-UHFFFAOYSA-N Acetamide Chemical compound CC(N)=O DLFVBJFMPXGRIB-UHFFFAOYSA-N 0.000 claims description 6
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 claims description 3
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims description 3
- 239000000047 product Substances 0.000 abstract description 10
- 239000007788 liquid Substances 0.000 abstract description 5
- 239000000779 smoke Substances 0.000 abstract description 4
- 239000003153 chemical reaction reagent Substances 0.000 abstract description 3
- 239000002244 precipitate Substances 0.000 abstract description 3
- 238000010438 heat treatment Methods 0.000 description 4
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 2
- 229910052801 chlorine Inorganic materials 0.000 description 2
- 239000000460 chlorine Substances 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 239000002253 acid Substances 0.000 description 1
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 1
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 1
- 235000011130 ammonium sulphate Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000011978 dissolution method Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 150000002941 palladium compounds Chemical class 0.000 description 1
- NXJCBFBQEVOTOW-UHFFFAOYSA-L palladium(2+);dihydroxide Chemical compound O[Pd]O NXJCBFBQEVOTOW-UHFFFAOYSA-L 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/02—Sulfur, selenium or tellurium; Compounds thereof
- B01J27/053—Sulfates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G55/00—Compounds of ruthenium, rhodium, palladium, osmium, iridium, or platinum
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
Description
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202011164815.5A CN112169811B (zh) | 2020-10-27 | 2020-10-27 | 一种硫酸钯溶液的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN202011164815.5A CN112169811B (zh) | 2020-10-27 | 2020-10-27 | 一种硫酸钯溶液的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN112169811A true CN112169811A (zh) | 2021-01-05 |
CN112169811B CN112169811B (zh) | 2023-03-24 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN202011164815.5A Active CN112169811B (zh) | 2020-10-27 | 2020-10-27 | 一种硫酸钯溶液的制备方法 |
Country Status (1)
Country | Link |
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CN (1) | CN112169811B (zh) |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1057902A2 (en) * | 1999-06-01 | 2000-12-06 | Lucent Technologies Inc. | Improved process for synthesizing a palladium replenisher for electroplating baths |
CN1430579A (zh) * | 2000-04-06 | 2003-07-16 | 法国梅塔勒科技公司 | 钯络合物盐及其在调整沉积钯或其合金之一的电解液的钯浓度中的应用 |
CN103395847A (zh) * | 2013-07-24 | 2013-11-20 | 励福实业(江门)贵金属有限公司 | 硫酸四氨合钯的合成方法 |
CN108823554A (zh) * | 2018-07-12 | 2018-11-16 | 深圳市化讯半导体材料有限公司 | 一种化学镀钯液、其制备方法和其使用方法以及应用 |
CN109295482A (zh) * | 2018-09-14 | 2019-02-01 | 金川集团股份有限公司 | 一种氨钯络合物及其制备方法 |
CN111732133A (zh) * | 2020-06-17 | 2020-10-02 | 中船重工黄冈贵金属有限公司 | 一种硫酸四氨钯的制备方法 |
-
2020
- 2020-10-27 CN CN202011164815.5A patent/CN112169811B/zh active Active
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1057902A2 (en) * | 1999-06-01 | 2000-12-06 | Lucent Technologies Inc. | Improved process for synthesizing a palladium replenisher for electroplating baths |
CN1430579A (zh) * | 2000-04-06 | 2003-07-16 | 法国梅塔勒科技公司 | 钯络合物盐及其在调整沉积钯或其合金之一的电解液的钯浓度中的应用 |
CN103395847A (zh) * | 2013-07-24 | 2013-11-20 | 励福实业(江门)贵金属有限公司 | 硫酸四氨合钯的合成方法 |
CN108823554A (zh) * | 2018-07-12 | 2018-11-16 | 深圳市化讯半导体材料有限公司 | 一种化学镀钯液、其制备方法和其使用方法以及应用 |
CN109295482A (zh) * | 2018-09-14 | 2019-02-01 | 金川集团股份有限公司 | 一种氨钯络合物及其制备方法 |
CN111732133A (zh) * | 2020-06-17 | 2020-10-02 | 中船重工黄冈贵金属有限公司 | 一种硫酸四氨钯的制备方法 |
Non-Patent Citations (1)
Title |
---|
李凡华等: "《贵金属及其合金》", 31 January 2015, 合肥:中国科技大学出版社 * |
Also Published As
Publication number | Publication date |
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CN112169811B (zh) | 2023-03-24 |
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TR01 | Transfer of patent right |
Effective date of registration: 20240219 Address after: 737100 No. 2 Lanzhou Road, Beijing Road Street, Jinchuan District, Jinchang City, Gansu Province Patentee after: Jinchuan Group Nickel Cobalt Co.,Ltd. Country or region after: China Patentee after: LANZHOU JINCHUAN ADVANGCED MATERIALS TECHNOLOGY Co.,Ltd. Address before: 737103 No. 98, Jinchuan Road, Jinchang, Gansu Patentee before: JINCHUAN GROUP Co.,Ltd. Country or region before: China Patentee before: LANZHOU JINCHUAN ADVANGCED MATERIALS TECHNOLOGY Co.,Ltd. |
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