CN111607987A - 一种棉用活性染料羊毛低温浅色染色工艺 - Google Patents

一种棉用活性染料羊毛低温浅色染色工艺 Download PDF

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CN111607987A
CN111607987A CN202010432672.5A CN202010432672A CN111607987A CN 111607987 A CN111607987 A CN 111607987A CN 202010432672 A CN202010432672 A CN 202010432672A CN 111607987 A CN111607987 A CN 111607987A
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penetration enhancer
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季正英
王锦鹏
宋仁华
钱东浩
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Zhangjiagang Yangzi Dyeing And Finishing Co ltd
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Abstract

本发明公开了一种棉用活性染料羊毛低温浅色染色工艺，包含以下步骤，步骤一：高温前处理。在室温下加入渗透促进剂，去油剂，纯碱，运行10min，再升温到70℃并保温20min，溢流水洗15min，排水。其中所述渗透促进剂为ALBAFLOW FFW，且其用量为0.5mL/L；所述去油剂为TISSOCYL RC9‑C，且其用量为1mL/L；所述纯碱用量为0.3‑0.5g/L。本发明通过使用棉用活性染料在60℃左右对羊毛进行染色，减少羊毛在98℃高温染色条件下的强力损伤和黄变程度，减少羊毛纤维本身的色泽对染色后纤维颜色的影响，确保染色后颜色鲜艳亮丽，染色后各项染色牢度良好，同时能够提高颜色的可重现性，提高生产效率。

Description

一种棉用活性染料羊毛低温浅色染色工艺
技术领域
本发明涉及羊毛纤维的染色技术领域，具体为一种棉用活性染料羊毛低温浅色染色工艺。
背景技术
羊毛从结构上来看是天然蛋白质纤维，分子中含有氨基，羧基，羟基等极性基团，可用酸性，金属络合，活性染料染色。羊毛纤维是天然纤维中抵抗日光，气候能力最强的一种纤维，但是紫外线、高温湿热等外界因素会对羊毛纤维的色泽造成影响，紫外线会破坏羊毛中的二硫键，使胱氨酸被氧化，颜色发黄；羊毛在60℃干热处理，对羊毛无大的影响，随着温度升高，羊毛逐渐变黄，在高温下羊毛容易变黄，此时羊毛原料与纤维素纤维，化学纤维相比其色泽比较黄暗。由于羊毛鳞片层的存在，羊毛一般是在高温98℃下染色，染浅色时染料用量少，加上羊毛在高温下发生黄变的特性，导致羊毛本身色泽对染色后颜色造成很大的影响，生产上需要多次返修复工，重现性差，生产效率低。
发明内容
本发明的目的在于提供一种棉用活性染料羊毛低温浅色染色工艺，解决了背景技术中所提出的问题。
为实现上述目的，本发明提供如下技术方案：一种棉用活性染料羊毛低温浅色染色工艺，包含以下步骤，步骤一：高温前处理。在室温下加入渗透促进剂，去油剂，纯碱，运行10min，再升温到70℃并保温20min，溢流水洗15min，排水。其中所述渗透促进剂为ALBAFLOWFFW，且其用量为0.5mL/L；所述去油剂为TISSOCYL RC9-C，且其用量为1mL/L；所述纯碱用量为0.3-0.5g/L；
步骤二：氧化漂白。在室温下加入渗透促进剂，氧漂活化剂，氨水，运行10min,再加入双氧水，运行10min，升温到70℃并保温60min，溢流水洗15min，排水。所述渗透促进剂为ALBAFLOW FFW，且其用量为0.5mL/L；所述氧漂活化剂为REDUZIN WO，且其用量为3mL/L；所述氨水用量为0.7mL/L；所述双氧水用量为10-30mL/L；
步骤三：去除残余活性氧。在室温下加入醋酸，生物酶，运行10min，升温到60℃并保温15min，溢流水洗10min，排水。其中所述醋酸用量为0.3mL/L；所述生物酶为INVAZYMECAT LIQ,且其用量为1mL/L；
步骤四：纱线染色。在室温下加入渗透促进剂，运行10分钟，再加入匀染剂，荧光增白剂，运行10分钟，再30min定量加入染料，再以0.5-1℃/min的速率升到50-60℃，再以20％/20％/30％比例分三次加入无水硫酸钠，每次加完运行10min，再保温30-60min，排水。其中所述渗透促进剂为ALBAFLOW FFW,且其用量为0.5mL/L；所述匀染剂为ALBAGEL B-LV，且其用量为2％；所述荧光增白剂为UVITEX NFW LIQ,且其用量为0-0.5％；所述染料为EVERZOL/REMAZOL/LEVAFIX等棉用活性染料；所述无水硫酸钠用量为40g/L；
步骤五：酸洗。在室温下加入醋酸，升温到40℃并保温10min，排水。
所述醋酸用量为1ml/L；
步骤六：柔软后处理。加入醋酸，柔软剂，升温到40℃并保温20min，排水。所述醋酸用量为0.5ml/L；所述柔软剂为SAPAMINE FPG,且其用量为2％。
与现有技术相比，本发明的有益效果如下：
本发明通过使用棉用活性染料在60℃左右对羊毛进行染色，减少羊毛在98℃高温染色条件下的强力损伤和黄变程度，减少羊毛纤维本身的色泽对染色后纤维颜色的影响，确保染色后颜色鲜艳亮丽，染色后各项染色牢度良好，同时能够提高颜色的可重现性，提高生产效率。
附图说明
通过阅读参照以下附图对非限制性实施例所作的详细描述，本发明的其它特征、目的和优点将会变得更明显：
图1为本发明一种棉用活性染料羊毛低温浅色染色工艺流程图；
具体实施方式
为使本发明实现的技术手段、创作特征、达成目的与功效易于明白了解，下面结合具体实施方式，进一步阐述本发明。
请参阅图1，本发明提供一种技术方案：一种棉用活性染料羊毛低温浅色染色工艺，包含以下步骤，步骤一：高温前处理。在室温下加入渗透促进剂，去油剂，纯碱，运行10min，再升温到70℃并保温20min，溢流水洗15min，排水。其中所述渗透促进剂为ALBAFLOWFFW，且其用量为0.5mL/L；所述去油剂为TISSOCYL RC9-C，且其用量为1mL/L；所述纯碱用量为0.3-0.5g/L；
步骤二：氧化漂白。在室温下加入渗透促进剂，氧漂活化剂，氨水，运行10min,再加入双氧水，运行10min，升温到70℃并保温60min，溢流水洗15min，排水。所述渗透促进剂为ALBAFLOW FFW，且其用量为0.5mL/L；所述氧漂活化剂为REDUZIN WO，且其用量为3mL/L；所述氨水用量为0.7mL/L；所述双氧水用量为10-30mL/L；
步骤三：去除残余活性氧。在室温下加入醋酸，生物酶，运行10min，升温到60℃并保温15min，溢流水洗10min，排水。其中所述醋酸用量为0.3mL/L；所述生物酶为INVAZYMECAT LIQ,且其用量为1mL/L；
步骤四：纱线染色。在室温下加入渗透促进剂，运行10分钟，再加入匀染剂，荧光增白剂，运行10分钟，再30min定量加入染料，再以0.5-1℃/min的速率升到50-60℃，再以20％/20％/30％比例分三次加入无水硫酸钠，每次加完运行10min，再保温30-60min，排水。其中所述渗透促进剂为ALBAFLOW FFW,且其用量为0.5mL/L；所述匀染剂为ALBAGEL B-LV，且其用量为2％；所述荧光增白剂为UVITEX NFW LIQ,且其用量为0-0.5％；所述染料为EVERZOL/REMAZOL/LEVAFIX等棉用活性染料；所述无水硫酸钠用量为40g/L；
步骤五：酸洗。在室温下加入醋酸，升温到40℃并保温10min，排水。
所述醋酸用量为1ml/L；
步骤六：柔软后处理。加入醋酸，柔软剂，升温到40℃并保温20min，排水。所述醋酸用量为0.5ml/L；所述柔软剂为SAPAMINE FPG,且其用量为2％。
实施例一
本实施例棉用活性染料羊毛低温浅色染色工艺,包含以下步骤：
步骤一：高温前处理。在室温下加入渗透促进剂，去油剂，纯碱，运行10min，再升温到70℃并保温20min，溢流水洗15min，排水。其中所述渗透促进剂为ALBAFLOW FFW，且其用量为0.5mL/L；所述去油剂为TISSOCYL RC9-C，且其用量为1mL/L；所述纯碱用量为0.4g/L；
步骤二：纱线染色。在室温下加入渗透促进剂，运行10分钟，再加入匀染剂，运行10分钟，再30min定量加入染料，再以0.5℃/min的速率升到50℃，再以20％/20％/30％比例分三次加入无水硫酸钠，每次加完运行10min，再保温45min，排水。其中所述渗透促进剂为ALBAFLOW FFW,且其用量为0.5mL/L；所述匀染剂为ALBAGEL B-LV，且其用量为2％；所述染料为REMAZOL棉用活性染料，且其用量为0.013％；所述无水硫酸钠用量为40g/L；
步骤三：酸洗。在室温下加入醋酸，升温到40℃并保温10min，排水。
所述醋酸用量为1ml/L；
步骤四：柔软后处理。加入醋酸，柔软剂，升温到40℃并保温20min，排水。所述醋酸用量为0.5ml/L；所述柔软剂为SAPAMINE FPG,且其用量为2％。
实施例二
本实施例棉用活性染料羊毛低温浅色染色工艺,包含以下步骤：
步骤一：高温前处理。在室温下加入渗透促进剂，去油剂，纯碱，运行10min，再升温到70℃并保温20min，溢流水洗15min，排水。其中所述渗透促进剂为ALBAFLOW FFW，且其用量为0.5mL/L；所述去油剂为TISSOCYL RC9-C，且其用量为1mL/L；所述纯碱用量为0.3g/L；
步骤二：氧化漂白。在室温下加入渗透促进剂，氧漂活化剂，氨水，运行10min,再加入双氧水，运行10min，升温到70℃并保温60min，溢流水洗15min，排水。所述渗透促进剂为ALBAFLOW FFW，且其用量为0.5mL/L；所述氧漂活化剂为REDUZIN WO，且其用量为3mL/L；所述氨水用量为0.7mL/L；所述双氧水用量为10mL/L；
步骤三：去除残余活性氧。在室温下加入醋酸，生物酶，运行10min，升温到60℃并保温15min，溢流水洗10min，排水。其中所述醋酸用量为0.3mL/L；所述生物酶为INVAZYMECAT LIQ,且其用量为1mL/L；
步骤四：纱线染色。在室温下加入渗透促进剂，运行10分钟，再加入匀染剂，荧光增白剂，运行10分钟，再30min定量加入染料，再以0.7℃/min的速率升到60℃，再以20％/20％/30％比例分三次加入无水硫酸钠，每次加完运行10min，再保温45min，排水。其中所述渗透促进剂为ALBAFLOW FFW,且其用量为0.5mL/L；所述匀染剂为ALBAGEL B-LV，且其用量为2％；所述荧光增白剂为UVITEX NFW LIQ,且其用量为0.35％；所述染料为REMAZOL/LEVAFIX等棉用活性染料，且其用量为0.0121％；所述无水硫酸钠用量为40g/L；
步骤五：酸洗。在室温下加入醋酸，升温到40℃并保温10min，排水。
所述醋酸用量为1ml/L；
步骤六：柔软后处理。加入醋酸，柔软剂，升温到40℃并保温20min，排水。所述醋酸用量为0.5ml/L；所述柔软剂为SAPAMINE FPG,且其用量为2％。
本发明通过使用棉用活性染料在60℃左右对羊毛进行染色，减少羊毛在98℃高温染色条件下的强力损伤和黄变程度，减少羊毛纤维本身的色泽对染色后纤维颜色的影响，确保染色后颜色鲜艳亮丽，染色后各项染色牢度良好，同时能够提高颜色的可重现性，提高生产效率。
以上显示和描述了本发明的基本原理和主要特征和本发明的优点，对于本领域技术人员而言，显然本发明不限于上述示范性实施例的细节，而且在不背离本发明的精神或基本特征的情况下，能够以其他的具体形式实现本发明。因此，无论从哪一点来看，均应将实施例看作是示范性的，而且是非限制性的，本发明的范围由所附权利要求而不是上述说明限定，因此旨在将落在权利要求的等同要件的含义和范围内的所有变化囊括在本发明内。不应将权利要求中的任何附图标记视为限制所涉及的权利要求。
此外，应当理解，虽然本说明书按照实施方式加以描述，但并非每个实施方式仅包含一个独立的技术方案，说明书的这种叙述方式仅仅是为清楚起见，本领域技术人员应当将说明书作为一个整体，各实施例中的技术方案也可以经适当组合，形成本领域技术人员可以理解的其他实施方式。

Claims (1)

1.一种棉用活性染料羊毛低温浅色染色工艺，其特征在于：包含以下步骤，步骤一：高温前处理。在室温下加入渗透促进剂，去油剂，纯碱，运行10min，再升温到70℃并保温20min，溢流水洗15min，排水。其中所述渗透促进剂为ALBAFLOW FFW，且其用量为0.5mL/L；所述去油剂为TISSOCYL RC9-C，且其用量为1mL/L；所述纯碱用量为0.3-0.5g/L；
步骤二：氧化漂白。在室温下加入渗透促进剂，氧漂活化剂，氨水，运行10min,再加入双氧水，运行10min，升温到70℃并保温60min，溢流水洗15min，排水。所述渗透促进剂为ALBAFLOW FFW，且其用量为0.5mL/L；所述氧漂活化剂为REDUZIN WO，且其用量为3mL/L；所述氨水用量为0.7mL/L；所述双氧水用量为10-30mL/L；
步骤三：去除残余活性氧。在室温下加入醋酸，生物酶，运行10min，升温到60℃并保温15min，溢流水洗10min，排水。其中所述醋酸用量为0.3mL/L；所述生物酶为INVAZYME CATLIQ,且其用量为1mL/L；
步骤四：纱线染色。在室温下加入渗透促进剂，运行10分钟，再加入匀染剂，荧光增白剂，运行10分钟，再30min定量加入染料，再以0.5-1℃/min的速率升到50-60℃，再以20％/20％/30％比例分三次加入无水硫酸钠，每次加完运行10min，再保温30-60min，排水。其中所述渗透促进剂为ALBAFLOW FFW,且其用量为0.5mL/L；所述匀染剂为ALBAGEL B-LV，且其用量为2％；所述荧光增白剂为UVITEX NFW LIQ,且其用量为0-0.5％；所述染料为EVERZOL/REMAZOL/LEVAFIX等棉用活性染料；所述无水硫酸钠用量为40g/L；
步骤五：酸洗。在室温下加入醋酸，升温到40℃并保温10min，排水。所述醋酸用量为1ml/L；
步骤六：柔软后处理。加入醋酸，柔软剂，升温到40℃并保温20min，排水。所述醋酸用量为0.5ml/L；所述柔软剂为SAPAMINE FPG,且其用量为2％。
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