CN111377771A - Flower fertilizer prepared from traditional Chinese medicine residues for preparing abelmoschus manihot and preparation method thereof - Google Patents
Flower fertilizer prepared from traditional Chinese medicine residues for preparing abelmoschus manihot and preparation method thereof Download PDFInfo
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- CN111377771A CN111377771A CN202010207681.4A CN202010207681A CN111377771A CN 111377771 A CN111377771 A CN 111377771A CN 202010207681 A CN202010207681 A CN 202010207681A CN 111377771 A CN111377771 A CN 111377771A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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Abstract
The invention belongs to the field of fertilizers, and mainly relates to a flower fertilizer for preparing abelmoschus manihot by using traditional Chinese medicine residues and a preparation method thereof, which mainly comprises the following steps of (1) drying the residues; (2) dissolving tetrabutylammonium chloride 0.3g in 100ml of water, heating the solution at 35-45 deg.C, and dropwise adding KH with pH of 6.1-7.82PO4/K2H2PO4The dropping time of the buffer solution is 60min until the system turns turbid from clear; (3) extracting; (4) then extracting; (5) adding sugar alcohol, peat and other components. The fertilizer disclosed by the invention can promote the content and stability of trace elements in the fertilizer, promote the absorption of the fertilizer by the abelmoschus manihot to nutrient substances, and effectively promote the growth of the abelmoschus manihot, promote the absorption of the fertilizer by the abelmoschus manihot to the nutrient substances, and obviously improve the content of chlorophyll in leaves.
Description
Technical Field
The invention belongs to the field of fertilizers, and particularly relates to a method for preparing a sunflower fertilizer by using traditional Chinese medicine residues.
Background
The Semiaquilegia adoxoides is tropical and prefers warm, humid and half-shady environment. The cold resistance is not strong, leaves yellow below the temperature of 20 ℃, the lowest overwintering temperature needs to be above 10 ℃, and the leaves can be frozen to death at about 5 ℃. Therefore, the south China can be cultivated in open field, and the Yangtze river basin and the areas in the north of the Yangtze river should be maintained in a greenhouse. The growth is slow in the seedling stage and rapid later. Is suitable for loose, well-drained and fertile soil. Dense branches and leaves, evergreen all the year round and strong shade resistance.
The leaf blight is a common disease of the solanum lycopodium, the morbidity is high, diseased leaf spots of diseased plants are accumulated, even leaves die in severe cases, even tree crowns die, and the growth of the solanum lycopodium is seriously threatened. The leaf blight is caused by strawberry anthrax, and the anthrax fungi are a kind of plant pathogenic bacteria distributed globally, especially in tropical zone, subtropical zone, etc., resulting in great economic loss. The existing prevention and treatment method is to strengthen nursing, trim the diseased leaves in time, and spray 600 times and 800 times of zineb, chlorothalonil, carbendazim, thiophanate and the like during disease attack.
At present, no special fertilizer for the mallow is available in the market, decomposed liquid fertilizer or compound fertilizer is mostly adopted to promote vigorous growth of plants, and most of the measures are treatment measures after the onset of leaf blight and no prevention measures are taken.
Disclosure of Invention
In order to solve the technical problems, the invention mainly provides a flower fertilizer for preparing the loose-tail anemone by using traditional Chinese medicine residues and a manufacturing method thereof, the traditional Chinese medicine is mainly from natural medicines and processed products thereof, comprises botanical medicines, animal medicines, mineral medicines and partial chemical and biological products, contains rich organic matters and elements beneficial to plants, and the flower fertilizer can lead the loose-tail anemone to grow fast and better in plant growth by using the traditional Chinese medicine residues as the flower fertilizer base material of the loose-tail anemone, can improve the permeability of soil and has the function of preventing leaf blight.
The invention is realized by the following technical scheme:
(1) drying the traditional Chinese medicine residues, putting the dried traditional Chinese medicine residues into a container, crushing the traditional Chinese medicine residues, sieving the crushed traditional Chinese medicine residues with a 60-80-mesh sieve, and averagely dividing the traditional Chinese medicine residues into two parts, namely 100g of each of the traditional Chinese medicine residues A and B;
(2) dissolving tetrabutylammonium chloride 0.3g in 100ml of water, heating the solution at 35-45 deg.C, and dropwise adding KH with pH of 6.1-7.82PO4/K2H2PO4The dropping time of the buffer solution is 60min until the system turns turbid from clear;
(3) adding one part of the dregs crushed in the step (1) into the mixed system in the step (2), and performing auxiliary extraction for 40-60min under the power of 100W by adopting a microwave extractor to obtain a filtrate A;
(4) extracting the filtrate A for 5-10min under the conditions that the microwave power is 600W and the temperature is 95 ℃ to obtain filtrate B;
(5) and (3) mixing the filtrate B with the other part of the traditional Chinese medicine residues in the step (1), and then adding a mixture of sugar alcohol, peat, charcoal ash and peanut shells to obtain the sunflower fertilizer.
The sugar alcohol is one or more of sorbitol, maltitol and mannitol, the concentration of the sugar alcohol is 75-120g/L, and the added amount is 0.2 times of that of the filtrate B;
the addition ratio of the peat, the charcoal ash and the peanut shells is 2-3:2-3:1-2, and the addition amount of the three components accounts for 10-15% of the mass of the Chinese medicine residues;
when the fertilizer is used, the obtained fertilizer can be buried in a pot culture at a depth of 5-6cm, the upper layer is covered with nutrient soil, and the fertilizer is watered thoroughly until the water seeps to the bottom of the pot.
Has the advantages that:
the fertilizer disclosed by the invention can promote the content and stability of trace elements in the fertilizer, promote the absorption of the malva lutescens on nutrient substances in the fertilizer, and effectively promote the growth of the malva lutescens, promote the absorption of the malva lutescens on the nutrient substances in the fertilizer, and meanwhile, can obviously improve the content of chlorophyll in leaves and prevent the leaves of the malva lutescens from yellowing; promoting the vigorous growth of plants and preventing the occurrence of the alternaria leaf blight of the setaria segetum; the adoption of the continuous extraction mode can effectively extract the nutrient components in the herb residues, and simultaneously, can accelerate the degradation of the herb residues in the soil and improve the effective utilization rate of lignin.
Detailed Description
Example 1:
(1) drying the traditional Chinese medicine residues, putting the traditional Chinese medicine residues into a container, crushing the traditional Chinese medicine residues, sieving the traditional Chinese medicine residues by a 60-mesh sieve, and averagely dividing the traditional Chinese medicine residues into two parts, namely 100g of each of the medicine residue A and the medicine residue B;
(2) 0.3g of tetrabutylammonium chloride was added to 100ml of water to dissolve it, the resulting solution was heated at a constant temperature of 37 ℃ and then added dropwise to the solutionDripping KH with pH of 6.12PO4/K2H2PO4The dropping time of the buffer solution is 60min until the system turns turbid from clear;
(3) adding the crushed residue A in the step (1) into the mixed system in the step (2), and performing auxiliary extraction for 45min under the power of 100W by using a microwave extractor to obtain a filtrate A;
(4) extracting the filtrate A for 5-10min under the conditions that the microwave power is 600W and the temperature is 95 ℃ to obtain filtrate B;
(5) and (3) mixing the filtrate B with the dregs B in the step (1), and then adding a mixture of sugar alcohol, peat, charcoal ash and peanut shells to obtain the sunflower fertilizer.
The sugar alcohol is one or more of sorbitol, maltitol and mannitol, the concentration of the sugar alcohol is 95g/L, and the added amount is 0.2 times of that of the filtrate B;
the addition ratio of the peat, the charcoal ash and the peanut shells is 2-3:2-3:1-2, and the addition amount of the three components accounts for 10-15% of the mass of the Chinese medicine residues;
when the fertilizer is used, the obtained fertilizer can be buried in a pot culture at a depth of 5-6cm, the upper layer is covered with nutrient soil, and the fertilizer is watered thoroughly until the water seeps to the bottom of the pot.
Example 2:
(1) drying the traditional Chinese medicine residues, putting the dried traditional Chinese medicine residues into a container, crushing the traditional Chinese medicine residues, sieving the crushed traditional Chinese medicine residues with a 80-mesh sieve, and averagely dividing the traditional Chinese medicine residues into two parts, namely 100g of each of the medicine residue A and the medicine residue B;
(2) dissolving tetrabutylammonium chloride 0.3g in 100ml of water, heating the solution at 45 deg.C, and dropwise adding KH of pH 7.8 into the solution2PO4/K2H2PO4The dropping time of the buffer solution is 60min until the system turns turbid from clear;
(3) adding one part of the dregs crushed in the step (1) into the mixed system in the step (2), and performing auxiliary extraction for 60min under the power of 100W by using a microwave extractor to obtain a filtrate A;
(4) extracting the filtrate A for 5-10min under the conditions that the microwave power is 600W and the temperature is 95 ℃ to obtain filtrate B;
(5) and (3) mixing the filtrate B with the other part of the traditional Chinese medicine residues in the step (1), and then adding a mixture of sugar alcohol, peat, charcoal ash and peanut shells to obtain the sunflower fertilizer.
The sugar alcohol is one or more of sorbitol, maltitol and mannitol, the concentration of the sugar alcohol is 75g/L, and the added amount of the sugar alcohol is 0.2 times of that of the filtrate B;
the addition ratio of the peat, the charcoal ash and the peanut shells is 2-3:2-3:1-2, and the addition amount of the three components accounts for 10-15% of the mass of the Chinese medicine residues;
when the fertilizer is used, the obtained fertilizer can be buried in a pot culture at a depth of 5-6cm, the upper layer is covered with nutrient soil, and the fertilizer is watered thoroughly until the water seeps to the bottom of the pot.
Example 3:
(1) drying the traditional Chinese medicine residues, putting the dried traditional Chinese medicine residues into a container, crushing the traditional Chinese medicine residues, sieving the crushed traditional Chinese medicine residues by a 70-mesh sieve, and averagely dividing the traditional Chinese medicine residues into two parts, namely 100g of each of the medicine residue A and the medicine residue B;
(2) dissolving tetrabutylammonium chloride 0.3g in 100ml of water, heating the solution at 35 deg.C, and dropwise adding KH of pH 6.7 into the solution2PO4/K2H2PO4The dropping time of the buffer solution is 60min until the system turns turbid from clear;
(3) adding one part of the dregs crushed in the step (1) into the mixed system in the step (2), and performing auxiliary extraction for 40-60min under the power of 100W by adopting a microwave extractor to obtain a filtrate A;
(4) extracting the filtrate A for 5-10min under the conditions that the microwave power is 600W and the temperature is 95 ℃ to obtain filtrate B;
(5) and (3) mixing the filtrate B with the other part of the traditional Chinese medicine residues in the step (1), and then adding a mixture of sugar alcohol, peat, charcoal ash and peanut shells to obtain the sunflower fertilizer.
The sugar alcohol is one or more of sorbitol, maltitol and mannitol, the concentration of the sugar alcohol is 120g/L, and the added amount of the sugar alcohol is 0.2 times of that of the filtrate B;
the addition ratio of the peat, the charcoal ash and the peanut shells is 2-3:2-3:1-2, and the addition amount of the three components accounts for 10-15% of the mass of the Chinese medicine residues;
when the fertilizer is used, the obtained fertilizer can be buried in a pot culture at a depth of 5-6cm, the upper layer is covered with nutrient soil, and the fertilizer is watered thoroughly until the water seeps to the bottom of the pot.
Comparative example 1:
and (3) culturing the loose-tail sunflower pot culture by adopting a common flower fertilizer sold in the market.
The measurement was performed for each of the okra of examples 1 to 3 and comparative example 1, and the measurement was performed after 3 months of growth.
The chlorophyll is measured by extracting fresh leaf chlorophyll with acetone direct extraction method, measuring absorbance at 645 nm and 663nm, and calculating the total chlorophyll content of each treated leaf.
The content of the trace elements is measured by a microwave digestion method-flame atomic absorption spectrometry.
Table 1 shows the growth of various factors of Helianthus lutescens after 3 months.
| Factor(s) | Plant height (cm) | Chlorophyll content (mg/g) | Fe concentration (mg/kg) | Mg concentration (Mg/kg) | Ca concentration (mg/kg) |
| Example 1 | 3.4 | 0.003 | 14.51 | 68.03 | 3.62 |
| Example 2 | 2.8 | 0.004 | 13.92 | 63.14 | 3.14 |
| Example 3 | 2.5 | 0.005 | 13.96 | 62.09 | 3.33 |
| Comparative example 1 | 2.3 | 0.001 | 9.87 | 43.20 | 2.11 |
TABLE 1
The conventional operations in the operation steps of the present invention are well known to those skilled in the art and will not be described herein.
The embodiments described above are intended to explain the technical solutions of the present invention in detail, and the description of the embodiments disclosed in the present invention is not intended to limit the scope of the present invention, but to describe the present invention. Accordingly, the scope of the present invention is not limited by the above embodiments, but is defined by the claims or their equivalents. Any modification, addition or substitution of the similar means within the scope of the principle of the present invention should be included in the scope of the present invention.
Claims (6)
1. A method for preparing flower fertilizer of chrysalidocarpus lutescens by using traditional Chinese medicine residues is characterized by comprising the following steps:
(1) drying the traditional Chinese medicine residues, putting the dried traditional Chinese medicine residues into a container, crushing the traditional Chinese medicine residues, sieving the crushed traditional Chinese medicine residues with a 60-80-mesh sieve, and averagely dividing the traditional Chinese medicine residues into two parts, namely 100g of each of the traditional Chinese medicine residues A and B;
(2) dissolving tetrabutylammonium chloride 0.3g in 100ml of water, heating the solution at 35-45 deg.C, and dropwise adding KH with pH of 6.1-7.82PO4/K2H2PO4The dropping time of the buffer solution is 60min until the system turns turbid from clear;
(3) adding the crushed medicine residue A in the step (1) into the mixed system in the step (2), and extracting by adopting a microwave extractor to obtain filtrate A;
(4) extracting the filtrate A again to obtain filtrate B;
(5) and (3) mixing the filtrate B with the dregs B in the step (1), and then adding a mixture of sugar alcohol, peat, charcoal ash and peanut shells to obtain the sunflower fertilizer.
2. The method for preparing the flower fertilizer of the sunflower seeds by using the traditional Chinese medicine residues as claimed in claim 1, is characterized in that: the sugar alcohol is one or more of sorbitol, maltitol and mannitol, the concentration of the sugar alcohol is 75-120g/L, and the added amount is 0.2 times of that of the filtrate B.
3. The method for preparing the flower fertilizer of the sunflower seeds by using the traditional Chinese medicine residues as claimed in claim 1, is characterized in that: the addition ratio of the peat, the charcoal ash and the peanut shells is 2-3:2-3:1-2, and the addition amount of the three components accounts for 10-15% of the mass of the traditional Chinese medicine residues.
4. The method for preparing the flower fertilizer of the sunflower seeds by using the traditional Chinese medicine residues as claimed in claim 1, is characterized in that: and in the extraction step in the step (3), a microwave extractor is adopted to perform auxiliary extraction for 40-60min under the power of 100W.
5. The method for preparing the flower fertilizer of the sunflower seeds by using the traditional Chinese medicine residues as claimed in claim 1, is characterized in that: and in the extraction step in the step (4), the filtrate A is extracted for 5-10min under the conditions that the microwave power is 600W and the temperature is 95 ℃.
6. A flower fertilizer for preparing abelmoschus manihot by using traditional Chinese medicine dregs, which is prepared by the method of any one of claims 1 to 5.
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| CN202010207681.4A CN111377771A (en) | 2020-03-23 | 2020-03-23 | Flower fertilizer prepared from traditional Chinese medicine residues for preparing abelmoschus manihot and preparation method thereof |
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Application publication date: 20200707 |