CN111377770A - Foliar fertilizer for preparing chrysalidocarpus lutescens by using traditional Chinese medicine residues and manufacturing method thereof - Google Patents
Foliar fertilizer for preparing chrysalidocarpus lutescens by using traditional Chinese medicine residues and manufacturing method thereof Download PDFInfo
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- CN111377770A CN111377770A CN202010207189.7A CN202010207189A CN111377770A CN 111377770 A CN111377770 A CN 111377770A CN 202010207189 A CN202010207189 A CN 202010207189A CN 111377770 A CN111377770 A CN 111377770A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05F—ORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C, e.g. FERTILISERS FROM WASTE OR REFUSE
- C05F5/00—Fertilisers from distillery wastes, molasses, vinasses, sugar plant or similar wastes or residues, e.g. from waste originating from industrial processing of raw material of agricultural origin or derived products thereof
- C05F5/006—Waste from chemical processing of material, e.g. diestillation, roasting, cooking
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- Fertilizers (AREA)
Abstract
The invention belongs to the field of fertilizers, and mainly relates to a foliar fertilizer for preparing chrysalidocarpus lutescens by using traditional Chinese medicine residues and a preparation method thereof, which mainly comprises the steps of drying the traditional Chinese medicine residues in the step (1), putting the dried traditional Chinese medicine residues into a container, crushing the traditional Chinese medicine residues, and sieving the crushed traditional Chinese medicine residues with a 200-mesh and 300-mesh sieve to obtain 100g of traditional Chinese medicine residue powder, wherein the mass ratio of ionic liquid to the traditional Chinese medicine residue powder is 7-: 1; (2) adding ionic liquid into the step (1); (3) adding 30g of brown algae powder into the mixed system in the step (2), and performing auxiliary extraction for 40-60min under the power of 100W by using a microwave extraction instrument to obtain a filtrate A; (5) adding sugar alcohol and the like. The foliar fertilizer disclosed by the invention can promote the content and stability of trace elements in leaves, can effectively prevent the occurrence of leaf blight of the setaria seguinii after being sprayed with the foliar fertilizer, reduces the transpiration effect of the leaves, keeps the moisture of the leaves, can obviously improve the content of chlorophyll in the leaves, and prevents the setaria seguinii from yellowing.
Description
Technical Field
The invention belongs to the field of fertilizers, and particularly relates to a method for preparing a foliage fertilizer for chrysalidocarpus lutescens by using traditional Chinese medicine residues.
Background
The Semiaquilegia adoxoides is tropical and prefers warm, humid and half-shady environment. The cold resistance is not strong, leaves yellow below the temperature of 20 ℃, the lowest overwintering temperature needs to be above 10 ℃, and the leaves can be frozen to death at about 5 ℃. Therefore, the south China can be cultivated in open field, and the Yangtze river basin and the areas in the north of the Yangtze river should be maintained in a greenhouse. The growth is slow in the seedling stage and rapid later. Is suitable for loose, well-drained and fertile soil. Dense branches and leaves, evergreen all the year round and strong shade resistance.
When the malva neglecta is planted, the phenomena of yellow and dry leaves and the like are easy to occur, and the production and the appearance of the malva neglecta plant are influenced. In addition, leaf blight is a common disease of the solanum lycopodium, the morbidity is high, diseased spots of the leaves of a diseased plant are accumulated, even the leaves die in severe cases, even the tree crown dies, and the growth of the solanum lycopodium is seriously threatened. The leaf blight is caused by strawberry anthrax, and the anthrax fungi are a kind of plant pathogenic bacteria distributed globally, especially in tropical zone, subtropical zone, etc., resulting in great economic loss. The existing prevention and treatment method is to strengthen nursing, trim the diseased leaves in time, and spray 600 times and 800 times of zineb, chlorothalonil, carbendazim, thiophanate and the like during disease attack. At present, no special foliar fertilizer for the mallow is available in the market, and most of the foliar fertilizer is used for treating and treating after the disease is caused, but no prevention and treatment measures are taken.
Disclosure of Invention
Aiming at the technical problems, the invention mainly provides a leaf fertilizer for preparing the chrysalidocarpus lutescens by using traditional Chinese medicine residues and a manufacturing method thereof, wherein the traditional Chinese medicines are mainly derived from natural medicines and processed products thereof, comprise botanical medicines, animal medicines, mineral medicines and partial chemical and biological products, contain rich organic matters and elements beneficial to plants, and the leaf fertilizer for the chrysalidocarpus lutescens uses the traditional Chinese medicine residues as the bottom material of the leaf fertilizer for the chrysalidocarpus lutescens, can enable the plants of the chrysalidocarpus lutescens to grow better, plays a role in preventing leaf blight, can promote photosynthesis of leaves, keeps balance of photosynthesis and transpiration, effectively increases the chlorophyll content in the leaves, and prevents the leaves from yellowing.
The invention is realized by the following technical scheme:
(1) drying the traditional Chinese medicine residues, putting the dried traditional Chinese medicine residues into a container, crushing the traditional Chinese medicine residues, and sieving the crushed traditional Chinese medicine residues with a sieve of 200 meshes and 300 meshes to obtain 100g of traditional Chinese medicine residue powder, wherein the mass ratio of the ionic liquid to the traditional Chinese medicine residue powder is 7-8: 1;
(2) adding ionic liquid into the step (1);
(3) adding 30g of brown algae powder into the mixed system in the step (2), and performing auxiliary extraction for 40-60min under the power of 100W by using a microwave extraction instrument to obtain a filtrate A;
(4) extracting the filtrate A for 5-10min under the conditions that the microwave power is 600W and the temperature is 75 ℃ to obtain filtrate B;
(5) extracting the filtrate B for 5-10min under the conditions that the microwave power is 600W and the temperature is 95 ℃ to obtain filtrate C;
(6) and adding sugar alcohol into the filtrate C to prepare the foliage fertilizer for the chrysalidocarpus lutescens.
The ionic liquid in the step (2) is one of octyl tributyl phosphonium bromide, octyl tributyl phosphonium chloride, 1-butyl-3-methylimidazole bromine salt and 1-butyl-3-methylimidazole chlorine salt ionic liquid.
The sugar alcohol is one or more of sorbitol, maltitol and mannitol, the concentration of the sugar alcohol is 75-120g/L, and the added amount is 0.1 time of the filtrate C.
When in use, the foliar fertilizer is diluted by 15 to 20 times and then uniformly sprayed on the surface of the sunflower seeds.
Has the advantages that:
the foliar fertilizer disclosed by the invention can promote the content and stability of trace elements in leaves, can effectively prevent the occurrence of leaf blight of the setaria sinica diels after being uniformly sprayed, can promote photosynthesis of the leaves, keep balance of photosynthesis and transpiration, keep moisture of the leaves, and simultaneously can improve the content of chlorophyll in the leaves and prevent the setaria sinica diels from yellowing.
Detailed Description
Example 1:
a method for preparing foliar fertilizer for the sunflower by using traditional Chinese medicine residues comprises the following steps:
(1) drying the traditional Chinese medicine residues, putting the dried traditional Chinese medicine residues into a container, crushing the traditional Chinese medicine residues, and sieving the crushed traditional Chinese medicine residues with a sieve of 200 meshes and 300 meshes to obtain 100g of traditional Chinese medicine residue powder, wherein the mass ratio of the ionic liquid to the traditional Chinese medicine residue powder is 7-8: 1;
(2) adding ionic liquid into the step (1);
(3) adding 30g of brown algae powder into the mixed system in the step (2), and performing auxiliary extraction for 40-60min under the power of 100W by using a microwave extraction instrument to obtain a filtrate A;
(4) extracting the filtrate A for 5-10min under the conditions that the microwave power is 600W and the temperature is 75 ℃ to obtain filtrate B;
(5) extracting the filtrate B for 5-10min under the conditions that the microwave power is 600W and the temperature is 95 ℃ to obtain filtrate C;
(6) and adding sugar alcohol into the filtrate C to prepare the foliage fertilizer for the chrysalidocarpus lutescens.
The sugar alcohol is one or more of sorbitol, maltitol and mannitol, the concentration of the sugar alcohol is 75-120g/L, and the added amount is 0.1 time of the filtrate C.
The ionic liquid in the step (2) is one of octyl tributyl phosphonium bromide, octyl tributyl phosphonium chloride, 1-butyl-3-methylimidazole bromine salt and 1-butyl-3-methylimidazole chlorine salt ionic liquid.
When in use, the foliar fertilizer is diluted by 20 times and then uniformly sprayed on the surface of the sunflower seeds.
Example 2:
a method for preparing foliar fertilizer for the sunflower by using traditional Chinese medicine residues comprises the following steps:
(1) drying the traditional Chinese medicine residues, putting the dried traditional Chinese medicine residues into a container, crushing the traditional Chinese medicine residues, and sieving the crushed traditional Chinese medicine residues with a sieve of 200 meshes and 300 meshes to obtain 100g of traditional Chinese medicine residue powder, wherein the mass ratio of the ionic liquid to the traditional Chinese medicine residue powder is 7-8: 1;
(2) adding ionic liquid into the step (1);
(3) adding 30g of brown algae powder into the mixed system in the step (2), and performing auxiliary extraction for 40-60min under the power of 100W by using a microwave extraction instrument to obtain a filtrate A;
(4) extracting the filtrate A for 5-10min under the conditions that the microwave power is 600W and the temperature is 75 ℃ to obtain filtrate B;
(5) extracting the filtrate B for 5-10min under the conditions that the microwave power is 600W and the temperature is 95 ℃ to obtain filtrate C;
(6) and adding sugar alcohol into the filtrate C to prepare the foliage fertilizer for the chrysalidocarpus lutescens.
The sugar alcohol is one or more of sorbitol, maltitol and mannitol, the concentration of the sugar alcohol is 75-120g/L, and the added amount is 0.1 time of the filtrate C.
The ionic liquid in the step (2) is one of octyl tributyl phosphonium bromide, octyl tributyl phosphonium chloride, 1-butyl-3-methylimidazole bromine salt and 1-butyl-3-methylimidazole chlorine salt ionic liquid.
When in use, the foliar fertilizer is diluted by 20 times and then uniformly sprayed on the surface of the sunflower seeds.
Example 3:
a method for preparing foliar fertilizer for the sunflower by using traditional Chinese medicine residues comprises the following steps:
(1) drying the traditional Chinese medicine residues, putting the dried traditional Chinese medicine residues into a container, crushing the traditional Chinese medicine residues, and sieving the crushed traditional Chinese medicine residues with a sieve of 200 meshes and 300 meshes to obtain 100g of traditional Chinese medicine residue powder, wherein the mass ratio of the ionic liquid to the traditional Chinese medicine residue powder is 7-8: 1;
(2) adding ionic liquid into the step (1);
(3) adding 30g of brown algae powder into the mixed system in the step (2), and performing auxiliary extraction for 40-60min under the power of 100W by using a microwave extraction instrument to obtain a filtrate A;
(4) extracting the filtrate A for 5-10min under the conditions that the microwave power is 600W and the temperature is 75 ℃ to obtain filtrate B;
(5) extracting the filtrate B for 5-10min under the conditions that the microwave power is 600W and the temperature is 95 ℃ to obtain filtrate C;
(6) and adding sugar alcohol into the filtrate C to prepare the foliage fertilizer for the chrysalidocarpus lutescens.
The sugar alcohol is one or more of sorbitol, maltitol and mannitol, the concentration of the sugar alcohol is 75-120g/L, and the added amount is 0.1 time of the filtrate C.
The ionic liquid in the step (2) is one of octyl tributyl phosphonium bromide, octyl tributyl phosphonium chloride, 1-butyl-3-methylimidazole bromine salt and 1-butyl-3-methylimidazole chlorine salt ionic liquid.
When in use, the foliar fertilizer is diluted by 20 times and then uniformly sprayed on the surface of the sunflower seeds.
The leaves of the malva sylvestris of examples 1 to 3 were washed with clear water, cut into small pieces of the same size, and placed in a culture, 5 to 10 wounds were pricked with an inoculating needle on one side of the veins, and the leaf blight germs were inoculated on the wounds, and simultaneously, woundless inoculation was performed on the other side of the veins. The control group is plant leaves which are not cultivated by the foliar fertilizer used in the application, the same inoculation method is carried out, and after 5 days of cultivation, the disease incidence condition of each plant is observed. In examples 1-3, the wound-inoculated side was successfully stained and the color turned brown, while the non-wound-inoculated side remained healthy green. Both sides of the control leaf were stained brown.
The chlorophyll content in the leaves of the plant of the malva sylvestris is measured by adopting a portable nondestructive testing instrument for the chlorophyll content of the plant leaves of the malva sylvestris, then the leaf fertilizer of the embodiment 1-3 is adopted to uniformly spray the leaves of the malva sylvestris, the control group sprays water, and the chlorophyll content in the same leaves of the malva sylvestris of the embodiment 1-3 and the control group is measured after 6 hours, as shown in the following table:
table 1 shows the chlorophyll content (mg/g) in the leaves of examples 1 to 3 and comparative example
| Chlorophyll content (mg/g) | Before treatment | After treatment |
| Example 1 | 0.021 | 0.026 |
| Example 2 | 0.032 | 0.037 |
| Example 3 | 0.027 | 0.032 |
| Comparative example | 0.028 | 0.029 |
TABLE 1
The conventional operations in the operation steps of the present invention are well known to those skilled in the art and will not be described herein.
The embodiments described above are intended to explain the technical solutions of the present invention in detail, and the description of the embodiments disclosed in the present invention is not intended to limit the scope of the present invention, but to describe the present invention. Accordingly, the scope of the present invention is not limited by the above embodiments, but is defined by the claims or their equivalents. Any modification, addition or substitution of the similar means within the scope of the principle of the present invention should be included in the scope of the present invention.
Claims (7)
1. A method for preparing foliar fertilizer for chrysalidocarpus lutescens by utilizing traditional Chinese medicine residues is characterized by comprising the following steps:
(1) drying the traditional Chinese medicine residues, putting the dried traditional Chinese medicine residues into a container, crushing the traditional Chinese medicine residues and sieving the crushed traditional Chinese medicine residues with a sieve of 200 meshes and 300 meshes to obtain 100g of traditional Chinese medicine residue powder;
(2) adding ionic liquid into the step (1), wherein the mass ratio of the ionic liquid to the traditional Chinese medicine slag powder is 7-8: 1;
(3) adding 30g of brown algae powder into the mixed system in the step (2), and performing auxiliary extraction for 40-60min under the power of 100W by using a microwave extraction instrument to obtain a filtrate A;
(4) adding the crushed medicine residues in the step (1) into the mixed system in the step (2), adding 30g of brown algae powder, and extracting by using a microwave extractor to obtain a filtrate A;
(5) extracting the filtrate A to obtain filtrate B;
(6) extracting the filtrate B to obtain filtrate C;
(7) and adding sugar alcohol into the filtrate C to prepare the foliage fertilizer for the chrysalidocarpus lutescens.
2. The manufacturing method of the foliar fertilizer for preparing the setaria sinica with the traditional Chinese medicine residue as claimed in claim 1, is characterized in that: the sugar alcohol is one or more of sorbitol, maltitol and mannitol, the concentration of the sugar alcohol is 75-120g/L, and the added amount is 0.1 time of the filtrate C.
3. The ionic liquid in the step (2) is one of octyl tributyl phosphonium bromide, octyl tributyl phosphonium chloride, 1-butyl-3-methylimidazole bromine salt and 1-butyl-3-methylimidazole chlorine salt ionic liquid.
4. The manufacturing method of the foliar fertilizer for preparing the setaria sinica with the traditional Chinese medicine residue as claimed in claim 1, is characterized in that: and (3) performing auxiliary extraction for 40-60min by adopting a microwave extractor under the power of 100W to obtain a filtrate A.
5. The manufacturing method of the foliar fertilizer for preparing the setaria sinica with the traditional Chinese medicine residue as claimed in claim 1, is characterized in that: and (4) extracting the filtrate A for 5-10min under the conditions that the microwave power is 600W and the temperature is 75 ℃ to obtain filtrate B.
6. The manufacturing method of the foliar fertilizer for preparing the setaria sinica with the traditional Chinese medicine residue as claimed in claim 1, is characterized in that: and (5) extracting the filtrate B for 5-10min under the conditions that the microwave power is 600W and the temperature is 95 ℃ to obtain filtrate C.
7. A foliar fertilizer for preparing a sunflower seed by using traditional Chinese medicine dregs, which is characterized by being prepared by the method of any one of claims 1 to 5.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010207189.7A CN111377770A (en) | 2020-03-23 | 2020-03-23 | Foliar fertilizer for preparing chrysalidocarpus lutescens by using traditional Chinese medicine residues and manufacturing method thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202010207189.7A CN111377770A (en) | 2020-03-23 | 2020-03-23 | Foliar fertilizer for preparing chrysalidocarpus lutescens by using traditional Chinese medicine residues and manufacturing method thereof |
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| CN111377770A true CN111377770A (en) | 2020-07-07 |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104774087A (en) * | 2015-03-27 | 2015-07-15 | 深圳柏施泰环境科技有限公司 | Biological preparation, its preparation method, and its application in soil improvement and fertilizers |
| CN105801252A (en) * | 2016-03-08 | 2016-07-27 | 梅州市枫景园林有限公司 | Garden landscape plant cultivation fertilizer |
| CN106220364A (en) * | 2016-08-02 | 2016-12-14 | 北京雷力海洋生物新产业股份有限公司 | A kind of composite foliage fertilizer and its preparation method and application |
| CN108752115A (en) * | 2018-08-06 | 2018-11-06 | 天长市天兴园林绿化工程有限公司 | A kind of anti-Chinese Rose foliar fertilizer |
| CN109867560A (en) * | 2017-12-04 | 2019-06-11 | 山东庞大生物集团有限公司 | Complex microorganism foliage bacterial fertilizer and preparation method thereof |
-
2020
- 2020-03-23 CN CN202010207189.7A patent/CN111377770A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104774087A (en) * | 2015-03-27 | 2015-07-15 | 深圳柏施泰环境科技有限公司 | Biological preparation, its preparation method, and its application in soil improvement and fertilizers |
| CN105801252A (en) * | 2016-03-08 | 2016-07-27 | 梅州市枫景园林有限公司 | Garden landscape plant cultivation fertilizer |
| CN106220364A (en) * | 2016-08-02 | 2016-12-14 | 北京雷力海洋生物新产业股份有限公司 | A kind of composite foliage fertilizer and its preparation method and application |
| CN109867560A (en) * | 2017-12-04 | 2019-06-11 | 山东庞大生物集团有限公司 | Complex microorganism foliage bacterial fertilizer and preparation method thereof |
| CN108752115A (en) * | 2018-08-06 | 2018-11-06 | 天长市天兴园林绿化工程有限公司 | A kind of anti-Chinese Rose foliar fertilizer |
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Application publication date: 20200707 |