CN110831948B - 使用烯酮添加剂制备铂有机硅氧烷络合物的方法 - Google Patents

使用烯酮添加剂制备铂有机硅氧烷络合物的方法 Download PDF

Info

Publication number
CN110831948B
CN110831948B CN201880044882.8A CN201880044882A CN110831948B CN 110831948 B CN110831948 B CN 110831948B CN 201880044882 A CN201880044882 A CN 201880044882A CN 110831948 B CN110831948 B CN 110831948B
Authority
CN
China
Prior art keywords
penten
methyl
carbon atoms
ketone
additive
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201880044882.8A
Other languages
English (en)
Chinese (zh)
Other versions
CN110831948A (zh
Inventor
Z·李
A·米尔沃德
M-S·邹
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Dow Silicones Corp
Original Assignee
Dow Corning Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Corning Corp filed Critical Dow Corning Corp
Publication of CN110831948A publication Critical patent/CN110831948A/zh
Application granted granted Critical
Publication of CN110831948B publication Critical patent/CN110831948B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/38—Polysiloxanes modified by chemical after-treatment
    • C08G77/382—Polysiloxanes modified by chemical after-treatment containing atoms other than carbon, hydrogen, oxygen or silicon
    • C08G77/398—Polysiloxanes modified by chemical after-treatment containing atoms other than carbon, hydrogen, oxygen or silicon containing boron or metal atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/12—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing organo-metallic compounds or metal hydrides
    • B01J31/123—Organometallic polymers, e.g. comprising C-Si bonds in the main chain or in subunits grafted to the main chain
    • B01J31/124—Silicones or siloxanes or comprising such units
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B47/00—Formation or introduction of functional groups not provided for in groups C07B39/00 - C07B45/00
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F15/00—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table
    • C07F15/0006—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic Table compounds of the platinum group
    • C07F15/0086—Platinum compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
    • C07F7/02—Silicon compounds
    • C07F7/08—Compounds having one or more C—Si linkages
    • C07F7/0803—Compounds with Si-C or Si-Si linkages
    • C07F7/0825—Preparations of compounds not comprising Si-Si or Si-cyano linkages
    • C07F7/0827—Syntheses with formation of a Si-C bond
    • C07F7/0829—Hydrosilylation reactions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/30—Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
    • B01J2231/32—Addition reactions to C=C or C-C triple bonds
    • B01J2231/323—Hydrometalation, e.g. bor-, alumin-, silyl-, zirconation or analoguous reactions like carbometalation, hydrocarbation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/80—Complexes comprising metals of Group VIII as the central metal
    • B01J2531/82—Metals of the platinum group
    • B01J2531/828—Platinum
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/06—Preparatory processes
    • C08G77/08—Preparatory processes characterised by the catalysts used

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
CN201880044882.8A 2017-07-20 2018-07-18 使用烯酮添加剂制备铂有机硅氧烷络合物的方法 Active CN110831948B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201762534952P 2017-07-20 2017-07-20
US62/534952 2017-07-20
PCT/US2018/042583 WO2019018461A1 (en) 2017-07-20 2018-07-18 PROCESS FOR THE PREPARATION OF PLATINUM-ORGANOSILOXANE COMPLEXES WITH AN ENONDE ADDITIVE

Publications (2)

Publication Number Publication Date
CN110831948A CN110831948A (zh) 2020-02-21
CN110831948B true CN110831948B (zh) 2022-08-23

Family

ID=63104092

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201880044882.8A Active CN110831948B (zh) 2017-07-20 2018-07-18 使用烯酮添加剂制备铂有机硅氧烷络合物的方法

Country Status (6)

Country Link
US (1) US10723843B2 (enExample)
EP (1) EP3655415B1 (enExample)
JP (1) JP6929457B2 (enExample)
KR (1) KR102354560B1 (enExample)
CN (1) CN110831948B (enExample)
WO (1) WO2019018461A1 (enExample)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10787474B2 (en) * 2017-07-20 2020-09-29 Dow Silicones Corporation Process for preparing platinum organosiloxane complexes

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3474123A (en) * 1964-08-05 1969-10-21 Ici Ltd Production of organosilicon compounds
US5175325A (en) * 1991-02-14 1992-12-29 Dow Corning Limited Platinum complexes and use thereof
US5312937A (en) * 1993-10-07 1994-05-17 Dow Corning Corporation Method for the preparation of platinum complexes
CN106573942A (zh) * 2014-06-13 2017-04-19 莫门蒂夫性能材料股份有限公司 使用环二烯添加剂的铂催化的氢化硅烷化反应

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2676182A (en) 1950-09-13 1954-04-20 Dow Corning Copolymeric siloxanes and methods of preparing them
US4288345A (en) * 1980-02-06 1981-09-08 General Electric Company Platinum complex
US4394317A (en) * 1981-02-02 1983-07-19 Sws Silicones Corporation Platinum-styrene complexes which promote hydrosilation reactions
US5424470A (en) * 1994-10-27 1995-06-13 Dow Corning Corporation Unsaturated ketones as accelerators for hydrosilation
FR2856402B1 (fr) * 2003-06-17 2005-08-26 Rhodia Chimie Sa Procede de preparation d'halogenoalkylchlorosilane
US20090171058A1 (en) 2007-12-31 2009-07-02 John Kilgour Low temperature platinum-vinylpolysiloxane hydrosilylation catalyst

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3474123A (en) * 1964-08-05 1969-10-21 Ici Ltd Production of organosilicon compounds
US5175325A (en) * 1991-02-14 1992-12-29 Dow Corning Limited Platinum complexes and use thereof
US5312937A (en) * 1993-10-07 1994-05-17 Dow Corning Corporation Method for the preparation of platinum complexes
CN106573942A (zh) * 2014-06-13 2017-04-19 莫门蒂夫性能材料股份有限公司 使用环二烯添加剂的铂催化的氢化硅烷化反应

Also Published As

Publication number Publication date
KR102354560B1 (ko) 2022-02-08
JP2020525543A (ja) 2020-08-27
KR20200026289A (ko) 2020-03-10
CN110831948A (zh) 2020-02-21
JP6929457B2 (ja) 2021-09-01
US20200148833A1 (en) 2020-05-14
EP3655415A1 (en) 2020-05-27
US10723843B2 (en) 2020-07-28
WO2019018461A1 (en) 2019-01-24
EP3655415B1 (en) 2021-06-16

Similar Documents

Publication Publication Date Title
CN105669966B (zh) 聚醚硅氧烷的生产
CN103588804B (zh) 使用钴催化剂的脱氢硅烷化以及交联
EP3135679B1 (en) Use of bis (alkoxysilyl-vinylene) group-containing silicon compounds as a curing agent for room temperature curable organopolysiloxane compositions
JP3651572B2 (ja) 部分付加環状オルガノハイドロジェンシロキサンの製造方法
JP6621226B2 (ja) シロキサン及びその製造方法
JPWO2017126562A1 (ja) 新規イソシアニド化合物及びヒドロシリル化反応触媒
CN1893910A (zh) 用于活性成分释放的环硅氧烷合成物
KR102354560B1 (ko) 엔온 첨가제를 사용하여 백금 유기실록산 착물을 제조하는 방법
CA1273351A (en) Method for making silylaroylhalides and reaction products
CN1854144A (zh) 具有硅烷醇基有机聚硅氧烷的制造方法
JP7181277B2 (ja) 白金オルガノシロキサン錯体の調製プロセス
CN102633829B (zh) 一种制备氨基硅氧烷的方法
TWI707861B (zh) 矽化合物之製造方法以及矽化合物
JP5913208B2 (ja) 新規フルオレン化合物及びその製造方法
JP4470886B2 (ja) 環状有機ケイ素化合物の製造方法
CN108912332B (zh) 一种用碳酸铯催化硅烷氧化制备笼型倍半硅氧烷的方法
JP5311091B2 (ja) ポリカルボシラン及びその製造方法
JP4172342B2 (ja) 環状有機ケイ素化合物及びその製造方法
JP2026001941A (ja) 有機ケイ素化合物
WO2007007597A1 (ja) 新規な有機ケイ素化合物及びその製造方法
DE102007013608A1 (de) Si-substituierte Chinone als Co-Katalysatoren in der Übergangsmetall-katalysierten Hydrosilylierung
JP2006160887A (ja) 経時による臭気の発生が極めて少ないポリオキシアルキレン変性オルガノポリシロキサンの製造方法
TW202100534A (zh) 矽烷化合物之製造方法
JPS58143844A (ja) 付加反応用白金触媒組成物

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant