CN110693806A - Skin care composition, skin care essence and preparation method thereof - Google Patents
Skin care composition, skin care essence and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/98—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin
- A61K8/987—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution of animal origin of species other than mammals or birds
- A61K8/988—Honey; Royal jelly, Propolis
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/99—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from microorganisms other than algae or fungi, e.g. protozoa or bacteria
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- A—HUMAN NECESSITIES
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- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/10—General cosmetic use
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention is suitable for the technical field of skin care, and provides a skin care composition, skin care essence and a preparation method thereof; the skin care composition comprises the following raw materials in parts by weight: 1-10 parts of aloe vera leaf extract; 1-10 parts of beneficial fungi; 1-20 parts of fermented product of beneficial fungi; 1-10 parts of hyaluronic acids; 1-20 parts of biological sugar gum. Through mutual matching, synergistic effect and synergistic interaction of all the components, the anti-aging function can be achieved; on one hand, the skin care composition also realizes the effects of efficiently moisturizing, repairing skin barriers and promoting the skin to form beneficial bacterium colonies, has definite and safe effect and no adverse reaction, and thoroughly makes up for the obvious defect of insufficient functions of products sold on the market; on the other hand, the composition is a water-soluble substance, so that the composition can be added into cosmetics in different formulations such as water aqua, emulsion, cream, essence and the like, and has wide application.
Description
Technical Field
The invention belongs to the technical field of skin care, and particularly relates to a skin care composition, skin care essence and a preparation method thereof.
Background
The epidermis layer of human body is divided into basal layer, spinous layer, granular layer, transparent layer and cuticle, and the healthy and dense cuticle can prevent the pollution and the invasion of substances such as live bacteria, dust, pollutants, pore secretion and the like to the epidermal cells at the outermost layer. Damage to the stratum corneum can cause the stratum lucidum, stratum granulosum, stratum spinosum, stratum basale cells to lose protection and sink layer by layer or even seriously damage the dermis layer. The skin is characterized in that a microbial layer is arranged outside the epidermis of the skin and consists of beneficial bacteria and harmful bacteria, when the beneficial bacteria are in a state that the dominant harmful bacteria are in a disadvantage, the microbial layer has no harm to the skin, when the harmful bacteria are in a state that the dominant beneficial bacteria are in a disadvantage, the microbial layer can cause skin problems such as skin itch, if the skin is damaged by mechanical movement such as scratching or the skin is in a damaged state, the harmful bacteria can invade and damage deeper cell and cell environments, because many microorganisms exist in the living environment, the beneficial bacteria and the harmful bacteria on the epidermis can not be cleaned and sterilized, and the beneficial bacteria and the harmful bacteria are maintained to inhibit the harmful bacteria so that bacterial colonies on the skin are in good balance. However, it is not enough to balance the micro-ecology alone, so skin care should increase the function of repair in addition to the necessary moisture retention, repair is needed to repair the cellular environment, promote the skin's ability to resist the invasion, promote cell proliferation so that the stratum corneum is dense to form a good complete epidermal skin barrier, and repair the balance of the microbial layer to form a good beneficial microbial layer barrier.
Skin care products on the market at present are uneven, the effect of repairing skin barriers is not ideal, and the problems of unclear effect purpose and certain adverse reaction are generally existed.
Disclosure of Invention
The embodiment of the invention provides a skin care composition, and aims to solve the problems that the existing skin care product is not ideal in effect of repairing skin barriers, and has unclear effect purpose and certain adverse reaction.
The embodiment of the invention is realized in such a way that the skin care composition comprises the following raw materials in parts by weight:
the embodiment of the invention also provides a skin care essence which comprises the skin care composition, a composition A and a composition B;
wherein the composition A comprises the following components in parts by weight:
10-80 parts of dipropylene glycol; 10-80 parts of isononyl isononanoate; 10-80 parts of glycerol; 0-40 parts of glyceryl polyether-261; 10-40 parts of trehalose; 1-5 parts of PEG-7 olive oleate; 1-5 parts of spirulina maxima extract; (ii) acrylic/vinyl isodecanoate crosspolymers;
the composition B comprises the following components in parts by weight:
polysorbate-601-5 parts; 1-5 parts of propolis extract; 1-5 parts of ubiquinone; 1-5 parts of triethanolamine; 1-3 parts of glycerol caprylate.
The embodiment of the invention also provides a preparation method of the skin care essence, which comprises the following steps:
weighing Aloe barbadensis leaf extract, beneficial bacteria, fermented product of the beneficial bacteria, hyaluronic acids, and biological sugar gum, and mixing to obtain skin care composition;
weighing dipropylene glycol, isononyl isononanoate, glycerol, glyceryl polyether-26, trehalose, PEG-7 olive oleate, a spirulina maxima extract and an acrylic acid (ester)/isodecyl vinyl ester cross-linked polymer according to the weight, and mixing to obtain a composition A;
weighing polysorbate-60, propolis extract, ubiquinone, triethanolamine, and glyceryl caprylate, and mixing to obtain composition B;
adding water and the composition A into a water phase pot, stirring, heating to 85-95 ℃, and preserving heat for 20-30 minutes to obtain a first mixed solution;
cooling the first mixed solution to 38-50 ℃, sequentially adding the skin care composition and the composition B, and uniformly stirring to obtain a second mixed solution;
and cooling the second mixed solution to 32-37 ℃, filtering and standing to obtain the product.
According to the skin care composition provided by the embodiment of the invention, the aloe vera leaf extract, the beneficial bacteria, the fermented product of the beneficial bacteria, the hyaluronic acids and the biological glycosaminoglycans are matched with each other, have a synergistic effect and achieve an anti-aging function; on one hand, the skin care composition also realizes the effects of efficiently moisturizing, repairing skin barriers and promoting the skin to form beneficial bacterium colonies, has definite and safe effect and no adverse reaction, and thoroughly makes up for the obvious defect of insufficient functions of products sold on the market; on the other hand, the composition is a water-soluble substance, so that the composition can be added into cosmetics in different formulations such as water aqua, emulsion, cream, essence and the like, and has wide application.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
According to the embodiment of the invention, the aloe vera leaf extract, the beneficial bacteria, the fermented product of the beneficial bacteria, the hyaluronic acid and the biological carbohydrate gum are mutually matched, have synergistic effect and are synergistic together, so that the obtained skin care composition can achieve the anti-aging function; on one hand, the skin care composition also realizes the effects of efficiently moisturizing, repairing skin barriers and promoting the skin to form beneficial bacterium colonies, has definite and safe effect and no adverse reaction, and thoroughly makes up for the obvious defect of insufficient functions of products sold on the market; on the other hand, the composition is a water-soluble substance, so that the composition can be added into cosmetics in different formulations such as water aqua, emulsion, cream, essence and the like, and has wide application.
The aloe vera leaf extract is prepared by selecting aloe vera leaves in Yuanjiang province as a raw material, extracting the extract with high efficiency and high activity through microbial fermentation and metabolism, and due to the fermentation of microorganisms, the component retains the biological active substances of the aloe vera leaves to a great extent, and the biological active substances of the component form smaller molecular active substances through fermentation, so that the aloe vera leaf extract is more easily compatible with skin to play corresponding functions.
The beneficial bacteria are selected from beneficial bacteria such as saccharomyces cerevisiae (such as picked strains on the surfaces of plants such as blueberries, grapes and red rice) or coated saccharomycetes, lactobacillus plantarum and bifidobacteria, the beneficial bacteria are inactivated beneficial bacteria cells, and the substance can promote the skin to form a good beneficial bacteria layer, reduce and inhibit the propagation of harmful bacteria on the skin and protect the skin.
The fermented product of beneficial bacteria is prepared by culturing selected bacteria such as Saccharomyces cerevisiae (such as bacteria picked on the surface of plants such as blueberry, grape, red rice, etc.) or coated yeast, Lactobacillus plantarum, Bifidobacterium, etc. with Aloe barbadensis leaf of Yunan Yuanjiang, and obtaining fermented product such as mucopolysaccharide, aloin, flavone, vitamins, mineral elements and essence extracted from cells by biological extraction, such as peptide, amino acid, nucleic acid, etc., and performing nanofiltration, resin treatment, membrane sterilization, etc. to obtain fermented product of selected bacteria and intracellular essence substance of bacteria.
The hyaluronic acids refer to hyaluronic acid, sodium hyaluronate, hydrolyzed hyaluronic acid, cross-linked sodium hyaluronate, acetylated hyaluronic acid and the like, namely a large amount of hyaluronic acid-hyaluronic acid bacteria mixture is obtained by fermenting and culturing hyaluronic acid production bacteria, then pure hyaluronic acid is obtained by the processes of sterilization, decoloration, sterilization filtration, alcohol extraction, drying, screening and the like, a part of hyaluronic acid is selected to be neutralized by sodium hydroxide to obtain sodium hyaluronate, a part of neutralized hyaluronic acid is selected to be inoculated to acetyl through a combination reaction to obtain acetylated sodium hyaluronate, and a part of hyaluronic acid is selected to be subjected to an enzymatic cleavage method to obtain hydrolyzed hyaluronic acid with a smaller molecular weight. The hyaluronic acid obtained by fermentation belongs to acidic components of larger molecules, can form a moisturizing film on the skin when used for skin care, helps the skin to moisturize, the sodium hyaluronate belongs to a neutral component of larger molecules, has excellent compatibility with other components in the formula, does not influence the stability of the formula, and forms a layer of moisturizing film in skin care. The sodium hyaluronate is a cationic component, has excellent skin conditioning effect, such as skin moisturizing effect, and can reduce the generation of static electricity on hair covered on skin. The hydrolyzed hyaluronic acid belongs to small molecular hyaluronic acid, has strong activity, and can easily enter into the epidermal layer of skin to exert effects, such as increasing the content of hyaluronic acid in the skin, promoting the production of hyaluronic acid by the skin, and improving the barrier function of the skin.
The biological carbohydrate gum is prepared by taking non-transgenic plants (soybeans and corns) as raw materials, adding polysaccharide production bacteria, culturing and fermenting to obtain polysaccharide, sterilizing, filtering, extracting with alcohol, and extracting pure biological carbohydrate gum.
In the embodiment of the invention, the aloe barbadensis leaf extract, the fermented product of the beneficial bacteria and the beneficial bacteria can improve the anti-invasion capability of the skin, for example, the proliferation and the thickening of horny layer of skin cells are promoted to form a good microbial layer environment, the combination of hyaluronic acid and bioglycan gum can play a moisturizing capability of 1+1>2, the synergy of all components in the skin care composition can balance the microbial layer outside, the combination of internal factors and large molecules can promote the moisturizing and repairing functions to be carried out, the high-efficiency moisturizing and balanced repairing can be realized, good beneficial microbial layer barrier and physiological barrier can be formed, and the skin care effect of all components can be greatly improved.
The skin care composition provided by the embodiment of the invention is a water-soluble substance, and can be added into cosmetics in different dosage forms such as water aqua, emulsion, cream, essence and the like, for example, the embodiment of the invention provides skin care essence added with the skin care composition, and the skin care essence comprises the following components:
the skin care essence comprises the skin care composition, a composition A and a composition B;
wherein the composition A comprises the following components in parts by weight:
10-80 parts of dipropylene glycol; 10-80 parts of isononyl isononanoate; 10-80 parts of glycerol; 0-40 parts of glyceryl polyether-261; 10-40 parts of trehalose; 1-5 parts of PEG-7 olive oleate; 1-5 parts of spirulina maxima extract; 1-5 parts of acrylic acid (ester)/isodecyl vinyl ester cross-linked polymer;
the composition B comprises the following components in parts by weight:
polysorbate-601-5 parts; 1-5 parts of propolis extract; 1-5 parts of ubiquinone; 1-5 parts of triethanolamine; 1-3 parts of glycerol caprylate.
Wherein the giant spirulina belongs to the cyanophyta and the Oscillatoriaceae, is grayish green, has the cell width of 7-9 μm, the length less than the width, the spiral spacing of 70-80 μm, a microtip top, no constriction on a transverse wall and particles on two sides of the transverse wall.
Wherein, the glycerol polyether-26 is glycerol addition product of 26 mol of epoxy ethylene, is used as humectant and lubricant, is stable in wide pH value range applied in cosmetics and washing products, and has good compatibility with cation, nonionic and anionic surfactants.
In a preferred embodiment of the present invention, the composition a further comprises the following components in parts by weight:
1-5 parts of sodium polyacrylate; 1-3 parts of p-hydroxyacetophenone; 1-3 parts of gold.
The sodium polyacrylate plays roles in thickening, dispersing, suspending, stabilizing and the like in the skin care essence, and is beneficial to the performance of thickening, foaming, stabilizing, emulsifying, dispersing, bonding, film forming, water retention and the like of the skin care essence.
The p-hydroxyacetophenone is mild, free of additive and free of irritant preservative, has the functions of resisting oxidation, tranquilizing and relieving in the skin care essence, and has a synergistic effect when being compounded with other preservatives.
Wherein, the gold fine particles (or active gold) are added into the skin care essence, so that the gold fine particles can permeate into the skin, a good introduction environment is created, the skin can better absorb nutrition, and the skin is shinier and fuller; meanwhile, the gold particles subjected to the micro treatment can penetrate into the skin, so that the immune system of skin cells is strengthened, and the effect of tensioning aged skin is achieved.
The sodium polyacrylate, p-hydroxyacetophenone and gold components play a certain auxiliary role in the skin care essence, and can be optionally added.
In a preferred embodiment of the present invention, the composition B further comprises the following components in parts by weight:
1-3 parts of caprylyl hydroximic acid; 1-3 parts of propylene glycol, 1-5 parts of phenoxyethanol, 1-3 parts of essence, 1-3 parts of caramel color and 3-3 parts of CI 130151.
Wherein, the caprylyl hydroximic acid is an organic acid with antiseptic effect, and plays a role in moisturizing and antisepsis in skin care essence.
The above components of caprylyl hydroximic acid, propylene glycol, phenoxyethanol, essence, caramel color and CI13015 respectively play a certain auxiliary role in antisepsis, moisture preservation, coloring and the like in the skin care essence, and can be selectively added.
In the embodiment of the invention, the preparation method of the skin care essence comprises the following steps:
weighing Aloe barbadensis leaf extract, beneficial bacteria, fermented product of the beneficial bacteria, hyaluronic acid and biogel according to the amount, mixing, and stirring to obtain skin care composition;
weighing dipropylene glycol, isononyl isononanoate, glycerol, glyceryl polyether-26, trehalose, PEG-7 olive oleate, a spirulina maxima extract and an acrylic acid (ester)/isodecyl vinyl ester cross-linked polymer according to the weight, mixing and uniformly stirring to obtain a composition A;
weighing polysorbate-60, propolis extract, ubiquinone, triethanolamine and glyceryl caprylate, mixing, and stirring to obtain composition B;
adding 900-1500 parts of water and the composition A into a water phase pot, stirring, heating to 85-95 ℃, and preserving heat for 20-30 minutes to obtain a first mixed solution;
cooling the first mixed solution to 38-50 ℃, sequentially adding the skin care composition and the composition B, and uniformly stirring to obtain a second mixed solution;
and cooling the second mixed solution to 32-37 ℃, filtering and standing to obtain the product.
In a preferred embodiment of the present invention, the step of weighing dipropylene glycol, isononyl isononanoate, glycerin, glyceryl polyether-26, trehalose, PEG-7 olive oleate, spirulina maxima extract, and acrylic acid/vinyl isodecanoate crosspolymer according to the amount and mixing to obtain composition a specifically comprises:
weighing dipropylene glycol, isononyl isononanoate, glycerol, glyceryl polyether-26, trehalose, PEG-7 olive oleate, a spirulina maxima extract, an acrylic acid (ester)/vinyl isodecanoate cross-linked polymer, sodium polyacrylate, p-hydroxyacetophenone and gold according to the weight, and mixing to obtain the composition A.
In a preferred embodiment of the present invention, the step of weighing polysorbate-60, propolis extract, ubiquinone, triethanolamine, and glyceryl caprylate according to the amount, and mixing to obtain composition B specifically comprises:
weighing polysorbate-60, propolis extract, ubiquinone, triethanolamine, glyceryl caprylate, caprylyl hydroxamic acid, propylene glycol, phenoxyethanol, essence, caramel color and CI13015, and mixing to obtain composition B.
In a preferred embodiment of the present invention, the step of adding water and the composition a into a water phase pot, stirring, heating to 85-95 ℃, and keeping the temperature for 20-30 minutes to obtain a first mixed solution specifically includes:
adding water and the composition A into a water phase pot, stirring, heating to 85 ℃, and keeping the temperature for 25 minutes to obtain a first mixed solution.
In a preferred embodiment of the present invention, after cooling the first mixed solution to 38 ℃ to 50 ℃, sequentially adding the skin care composition and the composition B, and uniformly stirring to obtain a second mixed solution, specifically includes:
and cooling the first mixed solution to 39 ℃, sequentially adding the skin care composition and the composition B, and uniformly stirring to obtain a second mixed solution.
In a preferred embodiment of the present invention, the step of cooling the second mixed solution to 32 to 37 ℃, filtering, and standing to obtain the second mixed solution specifically includes:
and cooling the second mixed solution to 36 ℃, filtering and standing to obtain the product.
The skin care composition and the skin care essence of the present invention are further described below with reference to specific embodiments, and it should be noted that, in the case of no conflict, any combination between the embodiments or technical features described below may form a new embodiment. The equipment and raw materials used are all available on the market or commonly used in the field. The methods in the following examples are conventional in the art unless otherwise specified.
The aloe vera leaf extract is prepared by selecting aloe vera leaves of Yunan Yuanjiang as a raw material, fermenting the aloe vera leaves which are beaten into juice for 35-60 hours at normal temperature and normal pressure by using microorganisms (S.Cerevisiae, Lactobacillus plantarum and Bifidobacterium) to obtain substances with high efficiency and high activity, namely mannan, galactose, arabinose, pectin, aldehyde polysaccharide, barbaloin, flavone, vitals, mineral elements, anthraquinone and aloesin. The effects of the present invention can be achieved by adding the components in the amounts of the present invention in the following examples.
The beneficial bacteria are selected from beneficial bacteria such as saccharomyces cerevisiae (such as picked strains on the surfaces of plants such as blueberries, grapes, red rice and the like) or coated saccharomycetes, lactobacillus plantarum, bifidobacteria and the like, the beneficial bacteria are selected from beneficial bacteria such as lactobacillus plantarum, bifidobacteria and the like, the beneficial bacteria are inactivated beneficial bacteria cells, and the substance can promote the skin to form a good beneficial bacteria layer, reduce and inhibit the propagation of harmful bacteria on the skin and protect the skin. In other words, in the following examples, inactivated saccharomyces cerevisiae, saccharomyces tectori, lactobacillus plantarum, and bifidobacterium were used in any ratio, and the effects of the present invention were achieved by adding the inactivated saccharomyces cerevisiae, saccharomyces tectori, lactobacillus plantarum, and bifidobacterium in the amounts added in the present invention.
The fermented product of beneficial bacteria is obtained by selecting beneficial bacteria such as Saccharomyces cerevisiae (such as picked bacteria on the surface of plants such as blueberry, grape, red rice and the like) or coated yeast, lactobacillus plantarum, bifidobacterium and the like, fermenting and culturing the beneficial bacteria for 13-18 hours at normal temperature and pressure by taking aloe vera leaf juice in Yunan Yuanjiang as a culture medium to obtain fermented products such as mucopolysaccharide, aloin, flavone, vitamins, mineral elements and essence (peptide, amino acid, nucleic acid and the like) extracted from the biological extract, and then performing nanofiltration, resin treatment, membrane sterilization and other processes to obtain the fermented product of the selected bacteria and the intracellular essence substances of the bacteria. In the following examples, the filtrate of the saccharomyces cerevisiae fermentation product, the filtrate of the tectorial membrane yeast fermentation product, the filtrate of the lactobacillus plantarum fermentation product, and the filtrate of the bifidobacterium fermentation product, which are added according to the amount of the present invention, are all used to achieve the effect of the present invention.
Hyaluronic acids, namely hyaluronic acid, sodium hyaluronate, hydrolyzed hyaluronic acid, cross-linked sodium hyaluronate, acetylated hyaluronic acid and the like, are prepared by fermenting and culturing hyaluronic acid producing bacteria to obtain a large amount of hyaluronic acid-hyaluronic acid bacteria mixture, and then performing sterilization, decoloration, sterilization filtration, alcohol extraction, drying, screening and other processes to obtain pure hyaluronic acid, wherein sodium hyaluronate is obtained by neutralizing sodium hydroxide on the basis of hyaluronic acid, sodium hyaluronate is obtained by inoculating acetyl on the basis of sodium hyaluronate through chemical combination reaction to obtain sodium acetylated hyaluronate, and hydrolyzed hyaluronic acid is obtained by performing enzymatic cleavage on the basis of hyaluronic acid to obtain hydrolyzed hyaluronic acid with a smaller molecular weight. The hyaluronic acid obtained by fermentation belongs to acidic components of larger molecules, can form a moisturizing film on the skin when used for skin care, helps the skin to moisturize, the sodium hyaluronate belongs to a neutral component of larger molecules, has excellent compatibility with other components in the formula, does not influence the stability of the formula, and forms a layer of moisturizing film in skin care. The sodium hyaluronate is a cationic component, has excellent skin conditioning effect, such as skin moisturizing effect, and can reduce the generation of static electricity on hair covered on skin. The hydrolyzed hyaluronic acid belongs to small molecular hyaluronic acid, has strong activity, and can easily enter into the epidermal layer of skin to exert effects, such as increasing the content of hyaluronic acid in the skin, promoting the production of hyaluronic acid by the skin, and improving the barrier function of the skin. In the following examples, the effect of the present invention can be achieved by adding different hyaluronic acid products either individually or in combination, that is, the effect of the present invention can be achieved by using sodium acetylated hyaluronate, hydrolyzed hyaluronic acid, sodium hyaluronate and the like in any ratio and adding the hyaluronic acid, hydrolyzed hyaluronic acid, sodium hyaluronate and the like in the amount of the present invention.
Biological carbohydrate gums are prepared by taking non-transgenic plants (soybeans and corns) as raw materials, adding polysaccharide production bacteria, culturing and fermenting to obtain polysaccharide, sterilizing, filtering, extracting with alcohol, and extracting pure biological carbohydrate gums. The effect of the invention can be achieved by adding the components according to the addition amount of the invention in the embodiment. The biopolysaccharide gums used in the examples below were FUCOGEL, purchased from solabia group, inc.
Example 1
A skin care composition comprises the following raw materials in parts by weight: 10 parts of aloe vera leaf extract; 6 parts of beneficial bacteria (saccharomyces cerevisiae, tectorial membrane saccharomycete, lactobacillus plantarum and bifidobacterium in a weight ratio of 1: 1: 1: 1); 15 parts of fermented products of the beneficial bacteria (saccharomyces cerevisiae fermentation product filtrate, tectorial membrane yeast fermentation product filtrate, lactobacillus plantarum fermentation product filtrate and bifidobacterium fermentation product filtrate in a volume ratio of 1: 1: 1: 1); 6 parts of hyaluronic acids (acetylated sodium hyaluronate and sodium hyaluronate in a weight ratio of 1: 1); 20 parts of biological sugar gum (FUCOGEL).
A skin care essence comprising the skin care composition, the composition A and the composition B; wherein the composition A comprises the following components in parts by weight:
80 parts of dipropylene glycol, 60 parts of isononyl isononanoate, 60 parts of glycerol, 2640 parts of glycerol polyether, 20 parts of trehalose, 5 parts of PEG-7 olive oleate, 5 parts of spirulina maxima extract, 3 parts of acrylic acid (ester)/vinyl isodecanoate cross-linked polymer, 3 parts of sodium polyacrylate, 3 parts of p-hydroxyacetophenone and 1 part of gold;
the composition B comprises the following components in parts by weight:
polysorbate-605, propolis extract 5 parts, ubiquinone 3 parts, triethanolamine 3 parts, glyceryl caprylate 1 part, caprylyl hydroximic acid 1 part, propylene glycol 3 parts, phenoxyethanol 3 parts, essence 1 part, caramel color 1 part, and CI 130151 parts.
The preparation method of the skin care essence comprises the following steps:
the preparation method comprises the following steps: weighing raw materials according to the formula amount; placing the mixture in a clean and sterilized vessel;
and (3) heating: adding water and the composition A into a water phase pot, stirring, heating to 85 ℃, and keeping the temperature for 25 minutes;
cooling: cooling to 39 deg.C, sequentially adding skin care composition and composition B, and stirring;
and (5) cooling again: cooling to 36 deg.C, filtering, and standing;
filling: and after the inspection is qualified, filling, packaging and spraying codes to obtain a finished product.
Warehousing: and warehousing after the inspection is qualified.
Example 2
A skin care composition comprises the following raw materials in parts by weight: 5 parts of aloe vera leaf extract; 3 parts of beneficial bacteria (lactobacillus plantarum and bifidobacterium in a weight ratio of 1: 1); 10 parts of fermented products of beneficial bacteria (lactobacillus plantarum fermented product filtrate and bifidobacterium fermented product filtrate with the volume ratio of 1: 1); 3 parts of hyaluronic acids (acetylated sodium hyaluronate and hydrolyzed hyaluronic acid in a weight ratio of 1: 1); 15 parts of biological sugar gum (FUCOGEL).
A skin care essence comprising the skin care composition, the composition A and the composition B; wherein the composition A comprises the following components in parts by weight:
80 parts of dipropylene glycol, 60 parts of isononyl isononanoate, 60 parts of glycerol, 2640 parts of glycerol polyether, 20 parts of trehalose, 5 parts of PEG-7 olive oleate, 5 parts of spirulina maxima extract, 3 parts of acrylic acid (ester)/vinyl isodecanoate cross-linked polymer, 3 parts of sodium polyacrylate, 3 parts of p-hydroxyacetophenone and 1 part of gold;
the composition B comprises the following components in parts by weight:
polysorbate-605, propolis extract 5 parts, ubiquinone 3 parts, triethanolamine 3 parts, glyceryl caprylate 1 part, caprylyl hydroximic acid 1 part, propylene glycol 3 parts, phenoxyethanol 3 parts, essence 1 part, caramel color 1 part, and CI 130151 parts.
The preparation method of the skin care essence comprises the following steps:
the preparation method comprises the following steps: weighing raw materials according to the formula amount; placing the mixture in a clean and sterilized vessel;
and (3) heating: adding water and the composition A into a water phase pot, stirring, heating to 90 ℃, and keeping the temperature for 25 minutes;
cooling: cooling to 40 deg.C, sequentially adding skin care composition and composition B, and stirring;
and (5) cooling again: cooling to 32 ℃, filtering and standing;
filling: and after the inspection is qualified, filling, packaging and spraying codes to obtain a finished product.
Warehousing: and warehousing after the inspection is qualified.
Example 3
A skin care composition comprises the following raw materials in parts by weight: 1 part of aloe vera leaf extract; 1 part of beneficial bacteria (saccharomyces cerevisiae, lactobacillus plantarum and bifidobacterium in a weight ratio of 1: 1: 1); 5 parts of fermented products of the beneficial bacteria (saccharomyces cerevisiae fermentation product filtrate, lactobacillus plantarum fermentation product filtrate and bifidobacterium fermentation product filtrate in a volume ratio of 1: 1: 1); 1 part of hyaluronic acids (hyaluronic acid); 5 parts of biological glucide (FUCOGEL).
A skin care essence comprising the skin care composition, the composition A and the composition B; wherein the composition A comprises the following components in parts by weight:
80 parts of dipropylene glycol, 60 parts of isononyl isononanoate, 60 parts of glycerol, 2640 parts of glycerol polyether, 20 parts of trehalose, 5 parts of PEG-7 olive oleate, 5 parts of spirulina maxima extract, 3 parts of acrylic acid (ester)/vinyl isodecanoate cross-linked polymer, 3 parts of sodium polyacrylate, 3 parts of p-hydroxyacetophenone and 1 part of gold;
the composition B comprises the following components in parts by weight:
polysorbate-605, propolis extract 5 parts, ubiquinone 3 parts, triethanolamine 3 parts, glyceryl caprylate 1 part, caprylyl hydroximic acid 1 part, propylene glycol 3 parts, phenoxyethanol 3 parts, essence 1 part, caramel color 1 part, and CI 130151 parts.
The preparation method of the skin care essence comprises the following steps:
the preparation method comprises the following steps: weighing raw materials according to the formula amount; placing the mixture in a clean and sterilized vessel;
and (3) heating: adding water and the composition A into a water phase pot, stirring, heating to 90 ℃, and keeping the temperature for 25 minutes;
cooling: cooling to 45 deg.C, sequentially adding skin care composition and composition B, and stirring;
and (5) cooling again: cooling to 35 deg.C, filtering, and standing;
filling: and after the inspection is qualified, filling, packaging and spraying codes to obtain a finished product.
Warehousing: and warehousing after the inspection is qualified.
Further, based on the above example 1, the present invention is based on the improvement of the formulation of the skin care composition, and the following comparative examples 1 to 8 are also performed, specifically as follows:
comparative example 1
Only the raw materials in parts by weight of the skin care composition are replaced by: 10 parts of aloe vera leaf extract; 15 parts of fermented products of the beneficial bacteria (saccharomyces cerevisiae fermentation product filtrate, tectorial membrane yeast fermentation product filtrate, lactobacillus plantarum fermentation product filtrate and bifidobacterium fermentation product filtrate in a volume ratio of 1: 1: 1: 1); 6 parts of hyaluronic acids (acetylated sodium hyaluronate and sodium hyaluronate in a weight ratio of 1: 1); 20 parts of biological sugar gum (FUCOGEL). The other components and the preparation process are the same as example 1.
Comparative example 2
Only the raw materials in parts by weight of the skin care composition are replaced by: 10 parts of aloe vera leaf extract; 30 parts of fermented product of the beneficial bacteria ((saccharomyces cerevisiae fermentation product filtrate, tectorial membrane yeast fermentation product filtrate, lactobacillus plantarum fermentation product filtrate and bifidobacterium fermentation product filtrate in a volume ratio of 1: 1: 1), 3 parts of hyaluronic acids (sodium hyaluronate and sodium hyaluronate in a weight ratio of 1: 1), 20 parts of sodium laureth sulfate, 80 parts of sodium lauroyl sarcosinate, 10 parts of cocamidopropyl betaine, 3930 parts of polyquaternium-3930 parts, polysorbate-2030 parts, 5 parts of xanthan gum, 5 parts of methylparaben, 5 parts of phenoxyethanol, 5 parts of essence and 5 parts of lactic acid, wherein the rest components and the preparation process are the same as in example 1.
Comparative example 3
Only the raw materials in parts by weight of the skin care composition are replaced by: 10 parts of aloe vera leaf extract; 6 parts of hyaluronic acids (acetylated sodium hyaluronate and sodium hyaluronate in a weight ratio of 1: 1); 20 parts of biological sugar gum (FUCOGEL). The other components and the preparation process are the same as example 1.
Comparative example 4
Only the raw materials in parts by weight of the skin care composition are replaced by: 10 parts of aloe vera leaf extract; 30 parts of hyaluronic acids (acetylated sodium hyaluronate and sodium hyaluronate in a weight ratio of 1: 1); 5 parts of scutellaria root extract; 30 parts of rose extract; 3 parts of a sophora flavescens extract; 5 parts of licorice extract; 10 parts of Hamamelis virginiana extract; 10 parts of collagen; 8 parts of butanediol. The other components and the preparation process are the same as example 1.
Comparative example 5
Only the raw materials in parts by weight of the skin care composition are replaced by: 10 parts of aloe vera leaf extract; 6 parts of beneficial bacteria (saccharomyces cerevisiae, tectorial membrane saccharomycete, lactobacillus plantarum and bifidobacterium in a weight ratio of 1: 1: 1: 1); 6 parts of hyaluronic acids (acetylated sodium hyaluronate and sodium hyaluronate in a weight ratio of 1: 1); 20 parts of biological sugar gum (FUCOGEL). The other components and the preparation process are the same as example 1.
Comparative example 6
Only the raw materials in parts by weight of the skin care composition are replaced by: 10 parts of aloe vera leaf extract; 6 parts of beneficial bacteria (saccharomyces cerevisiae, tectorial membrane saccharomycete, lactobacillus plantarum and bifidobacterium in a weight ratio of 1: 1: 1: 1); 5 parts of methyl hydroxybenzoate; 5 parts of essence; 10 parts of ethanol; 10 parts of PEG-60 hydrogenated castor oil; 3 parts of citric acid; 3 parts of trisodium citrate; and 3 parts of disodium EDTA. The other components and the preparation process are the same as example 1.
Comparative example 7
Only the raw materials in parts by weight of the skin care composition are replaced by: 10 parts of aloe vera leaf extract; 6 parts of beneficial bacteria (saccharomyces cerevisiae, tectorial membrane saccharomycete, lactobacillus plantarum and bifidobacterium in a weight ratio of 1: 1: 1: 1); 15 parts of fermented products of the beneficial bacteria (saccharomyces cerevisiae fermentation product filtrate, tectorial membrane yeast fermentation product filtrate, lactobacillus plantarum fermentation product filtrate and bifidobacterium fermentation product filtrate in a volume ratio of 1: 1: 1: 1); 6 parts of hyaluronic acids (acetylated sodium hyaluronate and sodium hyaluronate in a weight ratio of 1: 1); 20 parts of biological glucal (FUCOGEL); 10 parts of ethanol. The other components and the preparation process are the same as example 1.
Comparative example 8
The procedure for preparation of the other ingredients was the same as in example 1 except that no skin care composition was added.
The components of the skin care composition contained in the skin care essence prepared in examples 1 to 3 and comparative examples 1 to 8 and the contents thereof were summarized as shown in table 1:
TABLE 1
Test example 1
The skin care essences obtained in the above examples 1 to 3 and comparative examples 1 to 8 were subjected to a moisturizing performance test in the following specific test manner: finding 110 female volunteers with the age between 18 and 50, averagely dividing into 11 groups, respectively drawing a fixed area with the thickness of 2 square centimeters at the forehead in an indoor environment with the temperature of 20 ℃ and the relative humidity of 50 percent, testing the skin moisture content in the fixed area by using a Corneometer CM285 skin moisture detector, and comprehensively obtaining skin moisture change data, wherein the test results are as shown in the following table 2:
TABLE 2
In summary, as can be seen from the test results in table 2, examples 1 to 3 to which the skin care composition was completely added had more remarkable moisturizing and moisturizing effects than comparative example 8 to which the skin care composition was not added, comparative example 1, comparative example 3, and comparative example 5 to which the skin care composition was not completely added, and comparative examples 2, comparative example 4, and comparative examples 6 to 7 to which the surplus ingredients were added.
Test example 2
The skin care essences obtained in the above examples 1 to 3 and comparative examples 1 to 8 were subjected to a test for assisting recovery of damaged skin, in a specific test manner: finding 110 female volunteers with age of 18-50, equally dividing into 11 groups, respectively drawing a fixed area of 2 square centimeters at the forehead in an indoor environment with 20 ℃ and 50% relative humidity, soaking the fixed area for 2 hours by using 5% SDS lotion to destroy the skin, then using the skin care essence on the fixed area twice a day for fourteen days, measuring the hydration of the arm by using a cutin measurer, and comprehensively obtaining skin hydration change data (the higher the hydration value is, the better the destroyed skin is repaired), wherein the test results are shown in the following table 3:
TABLE 3
| Sample (I) | Before use | After use 3 | After 7 days of use | After 14 days of use |
| Example 1 | -13 | 7 | 11 | 13 |
| Example 2 | -13 | 5 | 8 | 10 |
| Example 3 | -13 | 2 | 5 | 8 |
| Comparative example 1 | -13 | -1 | 3 | 7 |
| Comparative example 2 | -13 | -2 | 2 | 6 |
| Comparative example 3 | -13 | -4 | -1 | 4 |
| Comparative example 4 | -13 | -5 | -2 | 3 |
| Comparative example 5 | -13 | -3 | 1 | 5 |
| Comparative example 6 | -13 | -7 | -4 | 1 |
| Comparative example 7 | -13 | -6 | -3 | 2 |
| Comparative example 8 | -13 | -8 | -5 | -1 |
In summary, as can be seen from the test results of table 3, examples 1 to 3 in which the skin care composition was completely added had a more significant skin barrier repair effect than comparative example 8 in which the skin care composition was not added, comparative example 1, comparative example 3, and comparative example 5 in which the skin care composition was not completely added, and comparative examples 2, comparative example 4, and comparative examples 6 to 7 in which the surplus component was added.
Test example 3
The skin care essences obtained in the above examples 1 to 3 and comparative examples 1 to 8 were subjected to in vitro test for competitive inhibition of harmful bacteria in the following specific test modes: in each culture medium which is cultured until the strain number reaches 106 probiotics (lactobacillus plantarum, bifidobacterium and pathogenic bacteria (staphylococcus aureus and dry corynebacterium)), 110 groups of culture media with the strain number of 106 are selected for each fungus (lactobacillus plantarum, bifidobacterium, staphylococcus aureus and dry corynebacterium), 440 culture media with the strain number of 106 are added, the skin care essence obtained in the above examples 1-3 and comparative examples 1-8 is added into the culture media with the strain number of 106, namely, each fungus has 11 experimental groups, each experimental group has 10 experimental groups, then the fungus is placed back into a culture box with proper growth conditions corresponding to each fungus for continuous culture for 24 hours, the fungus number is recorded by a microorganism counting method, the comprehensive fungus number data is obtained as shown in table 4, wherein the culture temperature of the lactobacillus plantarum is 30-37 ℃, the pH value is 4.5-7.5; the culture temperature of the bifidobacterium is 37-41 ℃, and the pH value is 5.0-5.5; the culture temperature of the staphylococcus aureus is 28-38 ℃, and the pH value is 7.0-7.4; the culture temperature of the dry corynebacteria is 34-37 ℃, and the pH value is 7.0-7.6.
TABLE 4
In summary, as can be seen from the test results in table 4, examples 1 to 3 in which the skin care composition was completely added had a more significant effect on the ability to promote the formation of colonies of beneficial bacteria and inhibit the formation of colonies of harmful bacteria than comparative example 8 in which the skin care composition was not added, comparative example 1, comparative example 3, and comparative example 5 in which the skin care composition was not completely added, and comparative example 2, comparative example 4, and comparative examples 6 to 7 in which an excess component was added.
It is worth noting that, as can be seen from the above examples 1 and comparative examples 1 to 8, the skin care composition has a synergistic effect on the components in the skin care essence, and is directly influenced by the content of the components, so as to balance the microbial layer on the outside, promote the moisturizing and repairing functions by the combination of the large and small molecules on the inside, realize efficient moisturizing and balanced repairing, form a good beneficial microbial layer barrier and a good physiological barrier, and greatly improve the skin care effect of the components.
In summary, the skin care composition and the skin care essence provided by the embodiment of the invention have synergistic effects through the mutual cooperation and synergistic effects of the aloe barbadensis leaf extract, the beneficial bacteria, the fermented product of the beneficial bacteria, the hyaluronic acids and the biological glycosaminoglycans, and can achieve the anti-aging function; on one hand, the skin care composition also realizes the effects of efficiently moisturizing, repairing skin barriers and promoting the skin to form beneficial bacterium colonies, has definite and safe effect and no adverse reaction, and thoroughly makes up for the obvious defect of insufficient functions of products sold on the market; on the other hand, the composition is a water-soluble substance, so that the composition can be added into cosmetics in different formulations such as water aqua, emulsion, cream, essence and the like, and has wide application.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents and improvements made within the spirit and principle of the present invention are intended to be included within the scope of the present invention.
Claims (10)
1. The skin care composition is characterized by comprising the following raw materials in parts by weight:
1-10 parts of aloe vera leaf extract;
1-10 parts of beneficial fungi;
1-20 parts of fermented product of beneficial fungi;
1-10 parts of hyaluronic acids;
1-20 parts of biological sugar gum.
2. The skin care composition of claim 1, comprising the following raw materials in parts by weight:
5-10 parts of aloe vera leaf extract;
3-6 parts of beneficial fungi;
5-15 parts of fermented product of beneficial fungi;
3-6 parts of hyaluronic acids;
5-20 parts of biological sugar gum.
3. The skin care composition of claim 1, comprising the following raw materials in parts by weight:
10 parts of aloe vera leaf extract;
6 parts of beneficial fungi;
15 parts of fermented product of beneficial fungi;
6 parts of hyaluronic acids;
20 parts of biological sugar gum.
4. The skin care composition of claim 1, wherein the beneficial bacteria is one or more of saccharomyces cerevisiae, tectorial membrane yeast, lactobacillus plantarum, and bifidobacterium.
5. The skin care composition according to claim 1, wherein the hyaluronic acid is one or more of hyaluronic acid, sodium hyaluronate, hydrolyzed hyaluronic acid, cross-linked sodium hyaluronate, and acetylated hyaluronic acid, and is obtained by fermentation, chemical combination, and neutralization.
6. The skin care composition of claim 1, wherein the biosaccharide is a biosaccharide that is fermentatively extracted from a non-transgenic plant.
7. A skin care essence comprising the skin care composition of claim 1, composition a and composition B;
wherein the composition A comprises the following components in parts by weight:
10-80 parts of dipropylene glycol; 10-80 parts of isononyl isononanoate; 10-80 parts of glycerol; 0-40 parts of glyceryl polyether-261; 10-40 parts of trehalose; 1-5 parts of PEG-7 olive oleate; 1-5 parts of spirulina maxima extract; 1-5 parts of acrylic acid (ester)/isodecyl vinyl ester cross-linked polymer;
the composition B comprises the following components in parts by weight:
polysorbate-601-5 parts; 1-5 parts of propolis extract; 1-5 parts of ubiquinone; 1-5 parts of triethanolamine; 1-3 parts of glycerol caprylate.
8. The skin care essence according to claim 7, wherein the composition A further comprises the following components in parts by weight:
1-5 parts of sodium polyacrylate; 1-3 parts of p-hydroxyacetophenone; 1-3 parts of gold.
9. The skin care essence according to claim 7, wherein the composition B further comprises the following components in parts by weight:
1-3 parts of caprylyl hydroximic acid; 1-3 parts of propylene glycol; 1-5 parts of phenoxyethanol; 1-3 parts of essence; 1-3 parts of caramel color; and CI 130151-3 parts.
10. A method of preparing a skin care essence according to any one of claims 7 to 9, comprising:
weighing Aloe barbadensis leaf extract, beneficial bacteria, fermented product of the beneficial bacteria, hyaluronic acids, and biological sugar gum, and mixing to obtain skin care composition;
weighing dipropylene glycol, isononyl isononanoate, glycerol, glyceryl polyether-26, trehalose, PEG-7 olive oleate, a spirulina maxima extract and an acrylic acid (ester)/isodecyl vinyl ester cross-linked polymer according to the weight, and mixing to obtain a composition A;
weighing polysorbate-60, propolis extract, ubiquinone, triethanolamine and glyceryl caprylate according to the amount, and mixing to obtain composition B;
adding water and the composition A into a water phase pot, stirring, heating to 85 ℃ and ~ 95 ℃, and preserving heat for 20 ~ 30 minutes to obtain a first mixed solution;
cooling the first mixed solution to 38 ℃ of ~ 50 ℃, sequentially adding the skin care composition and the composition B, and uniformly stirring to obtain a second mixed solution;
cooling the second mixed solution to 32 ℃ of ~ 37 ℃, filtering and standing to obtain the product.
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| CN111544370A (en) * | 2020-05-27 | 2020-08-18 | 广州蜜妆生物科技有限公司 | Composition capable of regulating and maintaining skin microecological balance |
| CN114983906A (en) * | 2022-07-09 | 2022-09-02 | 维怡美生物科技(广州)有限公司 | Repairing composition, and repairing cream and repairing water containing same |
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| CN115844748A (en) * | 2022-12-16 | 2023-03-28 | 优颜皮肤科学研究(广州)有限公司 | Eye composition and preparation method and application thereof |
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