CN115475129A - Preparation and application of cosmetic active component - Google Patents
Preparation and application of cosmetic active component Download PDFInfo
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- CN115475129A CN115475129A CN202211257778.1A CN202211257778A CN115475129A CN 115475129 A CN115475129 A CN 115475129A CN 202211257778 A CN202211257778 A CN 202211257778A CN 115475129 A CN115475129 A CN 115475129A
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 43
- 238000002360 preparation method Methods 0.000 title claims abstract description 24
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 43
- 241000208680 Hamamelis mollis Species 0.000 claims abstract description 43
- 241001261506 Undaria pinnatifida Species 0.000 claims abstract description 43
- 229940118846 witch hazel Drugs 0.000 claims abstract description 43
- 239000004480 active ingredient Substances 0.000 claims abstract description 38
- 238000005406 washing Methods 0.000 claims abstract description 25
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 24
- 229940105902 mint extract Drugs 0.000 claims abstract description 14
- HDTRYLNUVZCQOY-UHFFFAOYSA-N α-D-glucopyranosyl-α-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OC1C(O)C(O)C(O)C(CO)O1 HDTRYLNUVZCQOY-UHFFFAOYSA-N 0.000 claims abstract description 12
- HDTRYLNUVZCQOY-WSWWMNSNSA-N Trehalose Natural products O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-WSWWMNSNSA-N 0.000 claims abstract description 12
- HDTRYLNUVZCQOY-LIZSDCNHSA-N alpha,alpha-trehalose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 HDTRYLNUVZCQOY-LIZSDCNHSA-N 0.000 claims abstract description 12
- 239000012535 impurity Substances 0.000 claims abstract description 12
- 238000000034 method Methods 0.000 claims abstract description 7
- 230000003020 moisturizing effect Effects 0.000 claims abstract description 7
- 238000002791 soaking Methods 0.000 claims abstract description 6
- 239000007788 liquid Substances 0.000 claims description 29
- 235000011399 aloe vera Nutrition 0.000 claims description 28
- 241001116389 Aloe Species 0.000 claims description 27
- 238000001035 drying Methods 0.000 claims description 27
- 239000000463 material Substances 0.000 claims description 27
- 238000002156 mixing Methods 0.000 claims description 26
- 239000000243 solution Substances 0.000 claims description 25
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 23
- 238000001704 evaporation Methods 0.000 claims description 17
- 235000007866 Chamaemelum nobile Nutrition 0.000 claims description 16
- 244000042664 Matricaria chamomilla Species 0.000 claims description 16
- 235000007232 Matricaria chamomilla Nutrition 0.000 claims description 16
- 230000008020 evaporation Effects 0.000 claims description 15
- 241000220317 Rosa Species 0.000 claims description 14
- 238000010438 heat treatment Methods 0.000 claims description 14
- 239000002994 raw material Substances 0.000 claims description 14
- 241001506047 Tremella Species 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 13
- 238000005119 centrifugation Methods 0.000 claims description 12
- 102000008186 Collagen Human genes 0.000 claims description 11
- 108010035532 Collagen Proteins 0.000 claims description 11
- 238000004140 cleaning Methods 0.000 claims description 11
- 229920001436 collagen Polymers 0.000 claims description 11
- 241000241413 Propolis Species 0.000 claims description 10
- 238000007664 blowing Methods 0.000 claims description 10
- 229940069949 propolis Drugs 0.000 claims description 10
- 238000012216 screening Methods 0.000 claims description 10
- 229940069521 aloe extract Drugs 0.000 claims description 8
- 108010059892 Cellulase Proteins 0.000 claims description 7
- 229940106157 cellulase Drugs 0.000 claims description 7
- 239000007864 aqueous solution Substances 0.000 claims description 6
- 239000006228 supernatant Substances 0.000 claims description 6
- 238000010009 beating Methods 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 5
- 238000001816 cooling Methods 0.000 claims description 5
- 230000001105 regulatory effect Effects 0.000 claims description 5
- 241001474374 Blennius Species 0.000 claims description 3
- 230000002087 whitening effect Effects 0.000 claims description 3
- 230000008569 process Effects 0.000 claims description 2
- 244000144927 Aloe barbadensis Species 0.000 claims 1
- 235000002961 Aloe barbadensis Nutrition 0.000 claims 1
- 239000008267 milk Substances 0.000 claims 1
- 210000004080 milk Anatomy 0.000 claims 1
- 235000013336 milk Nutrition 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 7
- 208000003351 Melanosis Diseases 0.000 abstract description 4
- 230000037303 wrinkles Effects 0.000 abstract description 4
- 206010008570 Chloasma Diseases 0.000 abstract description 2
- 230000003796 beauty Effects 0.000 abstract description 2
- 230000009286 beneficial effect Effects 0.000 abstract description 2
- 230000005855 radiation Effects 0.000 abstract description 2
- 241000908178 Tremella fuciformis Species 0.000 abstract 3
- 230000032683 aging Effects 0.000 abstract 1
- 238000012360 testing method Methods 0.000 description 15
- 235000011187 glycerol Nutrition 0.000 description 11
- 208000002874 Acne Vulgaris Diseases 0.000 description 5
- 206010000496 acne Diseases 0.000 description 5
- 241000109329 Rosa xanthina Species 0.000 description 3
- 235000004789 Rosa xanthina Nutrition 0.000 description 3
- 230000008439 repair process Effects 0.000 description 3
- 201000010251 cutis laxa Diseases 0.000 description 2
- 230000002255 enzymatic effect Effects 0.000 description 2
- 230000001815 facial effect Effects 0.000 description 2
- 238000007602 hot air drying Methods 0.000 description 2
- 239000000413 hydrolysate Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 206010013786 Dry skin Diseases 0.000 description 1
- 235000006679 Mentha X verticillata Nutrition 0.000 description 1
- 235000002899 Mentha suaveolens Nutrition 0.000 description 1
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 1
- 244000269722 Thea sinensis Species 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000037336 dry skin Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000012847 fine chemical Substances 0.000 description 1
- 238000000703 high-speed centrifugation Methods 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000005507 spraying Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- 230000001225 therapeutic effect Effects 0.000 description 1
- 238000012795 verification Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9711—Phaeophycota or Phaeophyta [brown algae], e.g. Fucus
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Animal Behavior & Ethology (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Botany (AREA)
- Dermatology (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a preparation method and application of a cosmetic active component, which comprises the following steps: s1, putting wakame and witch hazel into a washing machine for washing, and washing impurities; s2, soaking the undaria pinnatifida and the witch hazel for 1-2 hours by using ethanol, draining and taking out, wherein the method has the beneficial effects that: the active ingredients of the undaria pinnatifida and the witch hazel are extracted by adding the undaria pinnatifida and the witch hazel, the beauty and the face are maintained, the skin condition is improved, the treatment efficiency is improved, the trehalose is added to achieve the effects of moisturizing, preventing radiation, resisting skin wrinkles and improving the skin adaptability, the tremella fuciformis extract, the glycerol and the mint extract are added, the tremella fuciformis extract has the effects of moisturizing, resisting aging, removing wrinkles and tightening the skin, freckle and chloasma can be removed by applying the tremella fuciformis extract, the glycerol and the mint extract have an auxiliary effect on the active ingredients of the cosmetics, and the working efficiency is improved.
Description
Technical Field
The invention relates to the technical field of cosmetics, in particular to preparation and application of an active ingredient of a cosmetic.
Background
The cosmetic is a chemical industrial product or a fine chemical product which is applied to any part of the surface of a human body, such as skin, hair, nails, lips and teeth, by smearing, spraying or the like, so as to achieve the purposes of cleaning, maintaining, beautifying, modifying and changing the appearance, or correcting the smell of the human body and keeping a good state.
Disclosure of Invention
The invention aims to provide preparation and application of a cosmetic active ingredient, and aims to solve the problems of low efficiency, impure extraction of the active ingredient and poor skin protection in the preparation of the existing cosmetic active ingredient in the background technology.
In order to achieve the above object, the present invention provides a method for preparing a cosmetic active ingredient, comprising the steps of:
s1, putting wakame and witch hazel into a washing machine for washing, and washing impurities;
s2, soaking the undaria pinnatifida and the witch hazel for 1-2 hours by using ethanol, draining and taking out;
s3, drying the wakame and the witch hazel after cleaning, and drying for later use;
s4, washing rose, naturally airing, crushing the rose, undaria pinnatifida and witch hazel, and sorting the crushed rose to obtain an active raw material;
s5, decocting the active raw materials by using boiling water for 15-30min, draining and taking out to obtain a treated material, and collecting and utilizing drained water;
s6, crushing chamomile to 20-30 meshes, mixing the crushed chamomile with a treatment material, and adding enzymolysis liquid to perform wall breaking treatment to obtain a solid-liquid mixture;
s7, adding trehalose, a propolis extracting solution and an aloe extracting solution into the solid-liquid mixture, heating and mixing, heating to 40-55 ℃, stirring for 30-55min, cooling to 30-35 ℃, adding hydrolyzed collagen, and stirring for 1-3h to obtain an active solution;
s8, mixing the active liquid in the S7 with the water drained in the S5, and performing centrifugal treatment after mixing;
s9, after centrifugal treatment, adding a tremella extract, glycerol and a mint extract, uniformly mixing, and then carrying out negative pressure evaporation concentration to obtain the active ingredients of the cosmetics.
Preferably, the Undaria pinnatifida, the witch hazel, the ethanol, the rose, the chamomile, the enzymolysis liquid, the trehalose, the propolis extracting solution, the aloe extracting solution, the hydrolyzed collagen, the tremella extracting solution, the glycerol and the mint extracting solution comprise the following components in parts by mass: undaria pinnatifida: 10-50 parts of witch hazel, 10-30 parts of ethanol: 5-20 parts of rose: 2-20 parts of chamomile: 1-10 parts of enzymolysis liquid: 2-10 parts of trehalose: 1-5 parts of propolis extract: 1-4 parts of aloe extract: 1-5 parts of hydrolyzed collagen: 5-9 parts of tremella extract: 1-2 parts of glycerol: 10-25 parts of mint extract: 5-15 parts.
Preferably, the drying process in S3 specifically includes the following steps:
s21, putting the undaria pinnatifida and the witch hazel into a dryer, and drying by blowing hot air at 35-50 ℃ for 5-10min;
s22, heating to 55-65 ℃, continuously blowing hot air, drying for 10-20min, and taking out.
Preferably, the sorting process in S4 specifically includes the steps of:
s31, screening the crushed materials through a screen of 10-40 meshes;
and S32, crushing the unsuccessfully screened materials again, and screening the materials for the second time through a screen with 30-60 meshes.
Preferably, the enzymatic hydrolysate is a cellulase aqueous solution.
Preferably, the preparation method of the aloe extract in S7 specifically includes the following steps:
s71, cleaning fresh aloe leaves, drying the cleaned fresh aloe leaves, and beating aloe mesophyll to form viscous liquid;
and S72, adding pure water according to the proportion of 1-1.4, and stirring to obtain the aloe extracting solution.
Preferably, the centrifugation in S8 includes the following specific steps:
s81, mixing, pouring into a centrifuge for centrifugation at the speed of 1000-1800rpm/m for 10-50min;
and S82, taking the supernatant.
Preferably, the negative pressure evaporation and concentration in S9 specifically includes the following steps:
s91, evaporating and concentrating for 10-30min under the negative pressure of 700-800kPa, and then regulating the pressure to 1000-1400kPa for secondary evaporation and concentration;
s92, removing the separated impurities to obtain the cosmetic active component.
Preferably, the undaria pinnatifida and witch hazel are used for preparing the active ingredients of the moisturizing and whitening cosmetics.
Compared with the prior art, the invention has the beneficial effects that:
by adding the undaria pinnatifida and the witch hazel, active ingredients of the undaria pinnatifida and the witch hazel are extracted, the beauty and the face are maintained, the skin condition is improved, the treatment efficiency is improved, trehalose is added to achieve the effects of moisturizing, radiation protection, skin wrinkle resistance and skin adaptability improvement, tremella extract, glycerin and mint extract are added, the tremella extract has the effects of moisturizing, anti-aging, wrinkle removal and skin tightening, freckle and chloasma can be removed through frequent application, the glycerin and mint extract can assist active ingredients of cosmetics, and the working efficiency is improved.
Detailed Description
The invention provides a technical scheme that: a method for preparing cosmetic active ingredients comprises the following steps:
s1, taking the undaria pinnatifida and the witch hazel, putting the undaria pinnatifida and the witch hazel into a washing machine for washing, washing impurities, and washing the undaria pinnatifida and the witch hazel through the washing machine, so that the treatment efficiency of materials and the preparation stability are improved;
s2, soaking the undaria pinnatifida and the witch hazel for 1-2 hours by using ethanol, draining and taking out;
s3, drying the wakame and the witch hazel after cleaning, and drying for later use;
s4, washing the roses, naturally airing, crushing the roses, the undaria pinnatifida and the witch hazel, sorting the crushed roses to obtain active raw materials, crushing the active raw materials, sorting the crushed raw materials, and taking out the crushed materials with proper sizes from the undaria pinnatifida and the witch hazel, so that the preparation efficiency is improved;
s5, decocting the active raw materials by using boiling water for 15-30min, draining and taking out to obtain a treated material, and collecting and utilizing drained water;
s6, smashing chamomile to 20-30 meshes, mixing the smashed chamomile with a treatment material, and adding the mixture into enzymatic hydrolysate for wall breaking treatment to obtain a solid-liquid mixture;
s7, adding trehalose, a propolis extracting solution and an aloe extracting solution into the solid-liquid mixture, heating and mixing, heating to 40-55 ℃, stirring for 30-55min, then cooling to 30-35 ℃, adding hydrolyzed collagen, stirring for 1-3h to obtain an active solution, heating and stirring to fully extract the internal therapeutic solution, cooling and stirring to prevent damage to the hydrolyzed collagen, and improving the stability;
s8, mixing the active liquid in the S7 with the water drained in the S5, and performing centrifugal treatment after mixing;
s9, after centrifugal treatment, adding a tremella extract, glycerol and a mint extract, uniformly mixing, and performing negative pressure evaporation concentration to obtain the active ingredients of the cosmetics.
The health-care tea comprises the following components in parts by mass: wakame seaweed: 10-50 parts of witch hazel, 10-30 parts of ethanol: 5-20 parts of rose: 2-20 parts of chamomile: 1-10 parts of enzymolysis liquid: 2-10 parts of trehalose: 1-5 parts of propolis extract: 1-4 parts of aloe extract: 1-5 parts of hydrolyzed collagen: 5-9 parts of tremella extract: 1-2 parts of glycerol: 10-25 parts of mint extract: 5-15 parts.
The drying process in the step S3 specifically includes the following steps:
s21, putting the undaria pinnatifida and the witch hazel into a dryer, and drying by blowing hot air at the temperature of 35-50 ℃ for 5-10min;
s22, heating to 55-65 ℃, continuously blowing hot air for drying for 10-20min, taking out, and drying the undaria pinnatifida and the witch hazel, so that the treatment efficiency is improved.
The sorting processing in S4 specifically includes the following steps:
s31, screening the crushed materials through a screen with 10-40 meshes;
and S32, crushing the unsuccessfully screened materials again, and performing secondary screening treatment on the unsuccessfully screened materials through a 30-60-mesh screen after secondary crushing.
Wherein the enzymolysis solution is cellulase water solution.
The preparation method of the aloe extract in S7 specifically comprises the following steps:
s71, cleaning fresh aloe leaves, drying the cleaned fresh aloe leaves, and beating aloe mesophyll to form viscous liquid;
s72, adding pure water in a proportion of 1-1.4 and stirring the mixture after adding the pure water in a proportion of 1.5-3 to obtain an aloe extracting solution, extracting aloe, and mixing the aloe extracting solution with water to obtain the aloe extracting solution, so that the treatment efficiency is improved.
The centrifugation treatment in S8 comprises the following specific steps:
s81, mixing, pouring into a centrifuge for centrifugation at the speed of 1000-1800rpm/m for 10-50min;
s82, taking the supernatant, performing high-speed centrifugation on the mixed liquid through a centrifuge, and taking out the supernatant to improve the purity.
The negative pressure evaporation and concentration in the S9 specifically comprises the following steps:
s91, after evaporation concentration is carried out for 10-30min under the negative pressure of 700-800kPa, the pressure is regulated to 1000-1400kPa for secondary evaporation concentration, and the stability and the efficiency of preparation are improved through negative pressure evaporation concentration;
s92, removing the separated impurities, and removing residual impurities in the cosmetic, so that the preparation stability is improved, and the cosmetic active ingredient is obtained.
Wherein, the undaria pinnatifida and the witch hazel are applied to the preparation of active ingredients of moisturizing and whitening cosmetics.
Example 1 preparation of a cosmetic active ingredient, the components in parts by mass are: undaria pinnatifida: 10 parts of witch hazel, 10 parts of ethanol: 5 parts of rose: 2 parts and chamomile: 1 part of cellulase aqueous solution: 2 parts of trehalose: 1 part, propolis extract: 1 part of aloe extract: 1 part of hydrolyzed collagen: 5 parts of tremella extract: 1 part of glycerol: 10 parts of mint extract: 5 parts of the raw materials.
A method for preparing cosmetic active ingredients comprises the following steps:
s1, putting wakame and witch hazel into a washing machine for washing, and washing impurities;
s2, soaking the undaria pinnatifida and the witch hazel for 1 hour by using ethanol, draining and taking out;
s3, after cleaning, putting the undaria pinnatifida and the witch hazel into a dryer, drying the undaria pinnatifida and the witch hazel by blowing hot air, wherein the hot air temperature is 35 ℃, the hot air drying time is 5min, heating to 55 ℃, continuously blowing hot air for drying for 10min, taking out, and drying for later use;
s4, washing rose, naturally airing, crushing the rose, the undaria pinnatifida and the witch hazel, screening the crushed materials through a screen with 10 meshes, crushing the unsuccessfully screened materials again, and screening the secondarily crushed materials through a screen with 30 meshes to obtain active raw materials;
s5, decocting the active raw materials by using boiling water, draining and taking out after decocting for 15min to obtain a treated material, and collecting and utilizing drained water;
s6, smashing chamomile to 20 meshes, mixing the smashed chamomile with a treatment material, and adding a cellulase aqueous solution for wall breaking treatment to obtain a solid-liquid mixture;
s7, cleaning fresh aloe leaves, drying the cleaned fresh aloe leaves, beating the aloe leaf flesh to form viscous liquid, adding pure water according to the proportion of 1.5, stirring to obtain an aloe extracting solution, adding trehalose, a propolis extracting solution and the aloe extracting solution into a solid-liquid mixture, heating, mixing for 30min after heating to 40 ℃, then cooling to 30 ℃, adding hydrolyzed collagen, and stirring for 1h to obtain an active solution;
s8, mixing the active liquid in the S7 with the water drained in the S5, pouring the mixture into a centrifuge for centrifugation, wherein the centrifugation speed is 1000rpm/m, the centrifugation time is 10min, and taking supernatant to obtain the active liquid;
s9, adding a tremella extract, glycerol and a mint extract after centrifugal treatment, uniformly mixing, carrying out evaporation concentration for 10min under the negative pressure of 700kPa, regulating the pressure to 1000kPa for secondary evaporation concentration, and removing separated impurities to obtain a cosmetic active ingredient.
Example 2 preparation of a cosmetic active ingredient, the components in parts by mass are: wakame seaweed: 50 parts of witch hazel, 30 parts of ethanol: 20 parts of rose: 20 parts of chamomile: 10 parts of cellulase aqueous solution: 10 parts of trehalose: 5 parts of propolis extract: 4 parts of aloe extract: 5 parts of hydrolyzed collagen: 9 parts of tremella extract: 2 parts of glycerol: 25 parts of mint extract: 15 parts.
A method for preparing cosmetic active ingredients comprises the following steps:
s1, putting wakame and witch hazel into a washing machine for washing, and washing impurities;
s2, soaking the undaria pinnatifida and the witch hazel for 2 hours by using ethanol, draining and taking out;
s3, after cleaning, putting the undaria pinnatifida and the witch hazel into a dryer, blowing hot air for drying treatment, wherein the hot air temperature is 50 ℃, the hot air drying time is 10min, then heating to 65 ℃, continuing blowing hot air for drying for 20min, taking out, and drying for later use;
s4, washing rose, naturally airing, crushing the rose, the undaria pinnatifida and the witch hazel, screening the crushed materials through a 40-mesh screen, crushing the unsuccessfully screened materials again, and screening the secondarily crushed materials through a 60-mesh screen to obtain active raw materials;
s5, decocting the active raw materials by using boiling water, draining and taking out the active raw materials after decocting for 30min to obtain a treated material, and collecting and utilizing drained water;
s6, smashing chamomile to 30 meshes, mixing the smashed chamomile with a treatment material, and adding cellulase aqueous solution for wall breaking treatment to obtain a solid-liquid mixture;
s7, cleaning fresh aloe leaves, drying the cleaned fresh aloe leaves, beating the aloe leaf flesh to form viscous liquid, adding pure water according to the proportion of 1.4;
s8, mixing the active liquid in the S7 with the water drained in the S5, pouring the mixture into a centrifuge for centrifugation, wherein the centrifugation speed is 1800rpm/m, the centrifugation time is 50min, and taking supernatant to obtain the active liquid;
s9, adding a tremella extract, glycerol and a mint extract after centrifugal treatment, uniformly mixing, carrying out evaporation concentration for 30min under the negative pressure of 800kPa, regulating the pressure to 1400kPa for secondary evaporation concentration, and removing separated impurities to obtain a cosmetic active ingredient.
Performance testing
Effect verification experiment of cosmetic active ingredients in examples 1 to 2:
1. test grouping
Test groups 1-2: cosmetic active ingredients prepared in examples 1 to 2;
control group: cosmetic active ingredients on the general market.
2. Test method
Samples of test group 1, test group 2 and control group were taken, 12 men and women with dry skin, loose skin and acne were sampled, 12 men and women were divided into three groups, one group was coated with the sample of test group 1, the other group was coated with the sample of test group 2, the last group was coated with the sample of control group, 3g of the corresponding sample was coated at one time, the affected area was evenly coated, cosmetic active ingredients were observed every 5h from the start of coating, and the states of different cosmetic active ingredients were recorded.
3. Test results
The results are shown in the following table:
test results of test group 1, test group 2 and control group in examples 1 to 2 shown below
| Grouping | Observation time | Facial repair condition | Completion of facial repair |
| Test group 1 | 30h | Moistening skin, tightening skin, reducing acne, and eliminating acne mark | 35h |
| Test group 2 | 30h | Moist skin, compact skin, reduced acne and obvious acne mark | 40h |
| Control group | 30h | Skin moisture, skin laxity, and no decrease of pox and pox | 60h |
As can be seen from the data of the test results in the above table, the skin repair effect of the cosmetic active ingredients in the test groups 1 and 2 is far better than that of the cosmetic active ingredients on the common market.
In the present invention, unless otherwise explicitly stated or limited, the terms "mounted," "disposed," "connected," "fixed," "screwed" and the like are to be understood broadly, for example, as being fixedly connected, detachably connected, or integrated; can be mechanically or electrically connected; the terms may be directly connected or indirectly connected through an intermediate agent, and may be used for communicating the inside of two elements or interacting relation of two elements, unless otherwise specifically defined, and the specific meaning of the terms in the present invention can be understood by those skilled in the art according to specific situations.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (9)
1. Preparation of a cosmetic active ingredient, characterized in that it comprises the following steps:
s1, putting wakame and witch hazel into a washing machine for washing, and washing impurities;
s2, soaking the undaria pinnatifida and the witch hazel for 1-2 hours by using ethanol, draining and taking out;
s3, drying the wakame and the witch hazel after cleaning, and drying for later use;
s4, washing the rose, naturally airing, crushing the rose, the undaria pinnatifida and the witch hazel, and sorting the crushed rose to obtain an active raw material;
s5, decocting the active raw materials by using boiling water for 15-30min, draining and taking out to obtain a treated material, and collecting and utilizing drained water;
s6, crushing chamomile to 20-30 meshes, mixing the crushed chamomile with a treatment material, and adding enzymolysis liquid to perform wall breaking treatment to obtain a solid-liquid mixture;
s7, adding trehalose, a propolis extracting solution and an aloe extracting solution into the solid-liquid mixture, heating and mixing, heating to 40-55 ℃, stirring for 30-55min, cooling to 30-35 ℃, adding hydrolyzed collagen, and stirring for 1-3h to obtain an active solution;
s8, mixing the active liquid in the S7 with the water drained in the S5, and performing centrifugal treatment after mixing;
s9, after centrifugal treatment, adding a tremella extract, glycerol and a mint extract, uniformly mixing, and then carrying out negative pressure evaporation concentration to obtain the active ingredients of the cosmetics.
2. The preparation of a cosmetic active ingredient according to claim 1, characterized in that: the seaweed-type aloe vera milk comprises the following components in parts by mass: wakame seaweed: 10-50 parts of witch hazel, 10-30 parts of ethanol: 5-20 parts of rose: 2-20 parts of chamomile: 1-10 parts of enzymolysis liquid: 2-10 parts of trehalose: 1-5 parts of propolis extract: 1-4 parts of aloe extract: 1-5 parts of hydrolyzed collagen: 5-9 parts of tremella extract: 1-2 parts of glycerol: 10-25 parts of mint extract: 5-15 parts.
3. The preparation of a cosmetic active ingredient according to claim 2, characterized in that: the drying process in the step S3 specifically includes the steps of:
s21, putting the undaria pinnatifida and the witch hazel into a dryer, and drying by blowing hot air at 35-50 ℃ for 5-10min;
s22, heating to 55-65 ℃, continuously blowing hot air for drying for 10-20min, and taking out.
4. The preparation of a cosmetic active ingredient according to claim 3, characterized in that: the sorting process in S4 specifically includes the steps of:
s31, screening the crushed materials through a screen with 10-40 meshes;
and S32, crushing the unsuccessfully screened materials again, and performing secondary screening treatment on the unsuccessfully screened materials through a 30-60-mesh screen after secondary crushing.
5. The preparation of a cosmetic active ingredient according to claim 4, characterized in that: the enzymolysis liquid is cellulase aqueous solution.
6. The preparation of a cosmetic active ingredient according to claim 5, characterized in that: the preparation method of the aloe extract in the S7 specifically comprises the following steps:
s71, cleaning fresh aloe leaves, drying the cleaned fresh aloe leaves, and beating aloe mesophyll to form viscous liquid;
and S72, adding pure water according to the proportion of 1-1.4, and stirring to obtain the aloe extracting solution.
7. The preparation of a cosmetic active ingredient according to claim 6, characterized in that: the centrifugation treatment in S8 specifically includes:
s81, mixing, pouring into a centrifuge for centrifugation at the speed of 1000-1800rpm/m for 10-50min;
and S82, taking the supernatant.
8. The preparation of a cosmetic active ingredient according to claim 7, characterized in that: the negative pressure evaporation and concentration in the step S9 specifically comprises the following steps:
s91, evaporating and concentrating for 10-30min under the negative pressure of 700-800kPa, and then regulating the pressure to 1000-1400kPa for secondary evaporation and concentration;
s92, removing the separated impurities to obtain the cosmetic active component.
9. Use of the undaria pinnatifida and witch hazel according to any one of claims 1 to 8 for preparing an active ingredient of a moisturizing and whitening cosmetic.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115919698A (en) * | 2023-01-09 | 2023-04-07 | 广州德芙化妆品有限公司 | Composition with effects of tightening and resisting wrinkles and application thereof |
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