CN112494404A - Dendrobium officinale skin-tendering repairing and moisturizing mask and preparation method thereof - Google Patents
Dendrobium officinale skin-tendering repairing and moisturizing mask and preparation method thereof Download PDFInfo
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- CN112494404A CN112494404A CN202011560120.9A CN202011560120A CN112494404A CN 112494404 A CN112494404 A CN 112494404A CN 202011560120 A CN202011560120 A CN 202011560120A CN 112494404 A CN112494404 A CN 112494404A
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- extract
- parts
- sodium
- mixture
- skin
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Classifications
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- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A61K8/35—Ketones, e.g. benzophenone
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/42—Amides
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
- A61K8/494—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom
- A61K8/4953—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds with more than one nitrogen as the only hetero atom containing pyrimidine ring derivatives, e.g. minoxidil
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
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Abstract
The invention relates to a dendrobium officinale skin-tendering, repairing and moisturizing mask and a preparation method thereof, wherein the dendrobium officinale skin-tendering, repairing and moisturizing mask consists of a skin conditioner, a humectant, an antioxidant, an emollient, a thickener, an emulsifier, a chelating agent, a solubilizer and a solvent; in the technical scheme, the composition comprises components beneficial to skin conditioning, such as DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, oat (AVENA SATIVA) extract, fructus cnidii (CNIDIUM MONNIERI) extract, SCUTELLARIA BAICALENSIS (scutelaria BAICALENSIS) root extract, belvedere fruit (KOCHIA SCOPARIA) extract, SOPHORA flavescens (SOPHORA ANGUSTIFOLIA) root extract, grape (VITIS VINIFERA) seed extract, prickly pear (Opuntia Streptacantha) stem extract and the like; the product of the invention is beneficial to improving the skin temperature, expanding pores of the skin, promoting secretion and metabolism of sweat glands, increasing the oxygen content of the skin, being beneficial to removing products of metabolism of epidermal cells and accumulated grease substances from the skin, and leading the moisture in the mask to permeate into the cuticle of the epidermis, so that the skin becomes soft, and the skin is naturally bright and elastic.
Description
Technical Field
The invention relates to the technical field of cosmetics, and particularly relates to a dendrobium officinale skin-tendering, repairing and moisturizing mask and a preparation method thereof.
Background
The facial mask temporarily isolates outside air and pollution by using a short time of covering the facial mask, the skin temperature is increased, pores of the skin are expanded, the secretion and metabolism of sweat glands are promoted, the oxygen content of the skin is increased, the skin is favorable for removing products of metabolism of epidermal cells and accumulated grease substances, moisture in the facial mask permeates into the horny layer of the epidermis, the skin becomes soft, and the skin is naturally bright and elastic.
In order to increase the functions of the facial mask and meet the requirements of different consumer groups, in the technical field, the efficacy and the quality of the facial mask are improved by changing raw materials, improving the formula and changing the preparation process.
The facial mask mainly has four types, namely a paste type, a tearing type, a jelly type and a wet tissue type. The mud paste type facial mask is commonly an alga facial mask, a mud facial mask and the like, the tear type facial mask is the nasal paste special for blackheads, the jelly type is the best known as a sleep facial mask, and the wet tissue type is generally a facial mask paper which is packaged by a single sheet and is soaked with beauty treatment liquid. With the development of beauty science, a facial mask made of silk has appeared, and strictly speaking, it should be included in a wet tissue type facial mask.
In the prior art, the invention patent application with the patent publication number of CN109381345A discloses a skin-care beauty mask set and a mask using method, and discloses a skin-care beauty mask set, which comprises a mask sheet, a packaging bag and essence; the packaging bag comprises a mask sheet bag cavity, a first essence bag cavity and a second essence bag cavity; the first essence bag cavity and the second essence bag cavity are physically isolated and independently arranged; the facial mask bag cavity is separated from the first essence bag cavity and the second essence bag cavity through heat-sealing separation lines respectively; the essence of first composition is equipped with in first essence bag intracavity, the essence of second composition is equipped with in the second essence bag intracavity, contain facial mask inertia composition in the essence of first composition, including facial mask active ingredient in the essence of second composition.
The publication number CN104352371A discloses a whitening, anti-aging and freckle-removing mask solution and a preparation method thereof, and discloses a mask, wherein the mask solution comprises 3-5% of a whitening and anti-oxidation component B, a solubilizer component C, an anti-oxidation component D and a mask base solution component A in percentage by weight; the component B comprises a glycyrrhiza glabra extract and a hamamelis virginiana extract according to the weight ratio of 2-3: 1-2. The whitening, anti-aging and freckle-removing mask liquid can deeply nourish the skin and keep the moisture of the skin. The liquorice extract and the witch hazel extract are added, and the golden ratio is adopted, so that the whitening acne-removing cream has good whitening and acne-removing functions, and can obviously improve the skin state.
The existing makeup industry designs skin care products with different types and different effects aiming at people with different skin states, and it is very necessary to design a mild skin tendering, repairing and moisturizing mask suitable for most people. Therefore, it is an objective need to provide a skin rejuvenation and repairing hydrating mask with a fixed formula, which is convenient for consumers to use and provides an ideal cosmetic effect.
Disclosure of Invention
In order to overcome the defects of the existing skin care products, the invention aims to provide the dendrobium officinale skin-tendering repairing and moisturizing mask; the invention also aims to provide the dendrobium officinale skin-tendering repairing and moisturizing mask and the preparation method thereof.
The dendrobium officinale skin tendering and repairing hydrating mask is realized by the following technical scheme.
The dendrobium officinale skin tendering and repairing hydrating mask provided by the invention consists of a skin conditioner, a humectant, an antioxidant, an emollient, a thickener, an emulsifier, a chelating agent, a solubilizer and a solvent.
Wherein the skin conditioning agent is selected from the group consisting of Dendrobium officinale (Dendrobium CANDIDUM) extract, Tetrahydrophylpyrimidinecarboxylic acid, a mixture consisting of water, glycerin, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM MONNIERI) extract, Scutellaria BAICALENSIS (Scutellaria BAICALENSIS) root extract, Kochia SCOPARIA (Kochia SCOPARIA) extract, Sophora flavescens (Sophora ANGUSTIFOLIA) root extract, Vitis vinifera (VITIS VINIFERA) seed extract, Opuntia streptacanthantha stem extract, caprylyl hydroxamic acid, ethylhexyl glycerin and propylene glycol, erythritol, Helianthus ANNUUS (Helianthus ANNUUS) seed oil, a mixture consisting of sodium hyaluronate cross-linked polymer, sodium hyaluronate, acetylated sodium hyaluronate, hydrolyzed sodium hyaluronate, 1, 2-pentanediol, ethylhexyl glycerin, water, sodium hyaluronate, one or more of p-hydroxyacetophenone and geranium (PELARGONIUM GRAVEOLENS) oil;
the humectant is selected from one or more of the group consisting of glycerin, butylene glycol, panthenol, hydroxyethyl urea, and 1, 2-hexanediol;
the antioxidant is 3-o-ethyl ascorbic acid or tocopherol (vitamin E);
the emollient is isononyl isononanoate;
the thickening agent is selected from one or more of the group consisting of acrylic acid (acrylate)/C10-30 alkanol acrylate cross-linked polymer, sodium polyacrylate grafted starch and hydroxyethyl cellulose;
the emulsifier is a mixture consisting of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
the chelating agent is EDTA disodium;
the solubilizer is PEG-40 hydrogenated castor oil;
the solvent is water.
In the technical scheme of the invention, the other extracts except the DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract can be obtained from the market.
Further, in the technical scheme of the invention, the dendrobium officinale skin-tendering repairing and moisturizing mask comprises the following raw materials in parts by weight:
wherein the skin conditioner is selected from the group consisting of Dendrobium officinale (Dendrobium CANDIDUM) extract 0.3-0.8 parts, Tetrahydrophylpyrimidinecarboxylic acid 0.06-0.12 parts, a mixture consisting of water, glycerin, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM) extract, Scutellaria BAICALENSIS (Scutellaria BAICALENSIS) root extract, Kochia SCOPARIA (KOCHIA SCOPARIA) extract, Sophora flavescens (Sophora ANGUSTIFOLIA) root extract, grape (VITIS VINIFERA) seed extract, Opuntia Streptacantha stem extract, caprylyl hydroxamic acid, ethylhexyl glycerin, propylene glycol 1-5 parts, erythritol 0.3-0.8 part, sunflower (Helianthus ANNUUS) seed oil 0.05-0.12 part, a mixture consisting of sodium hyaluronate cross-linked polymer, sodium hyaluronate, sodium acetylate, hydrolyzed sodium hyaluronate, 1, 2-pentylene glycol, ethylhexylene glycol 0.28-0.12 part of water, 0.02-0.08 part of sodium hyaluronate, 0.2-0.8 part of p-hydroxyacetophenone, and 0.0001-0.0005 part of geranium vanilloides (PELARGONIUM GRAVEOLENS) oil;
the composition comprises, by weight, 0.5-5 parts of sodium hyaluronate cross-linked polymer, 0.5-5 parts of sodium hyaluronate, 0.5-5 parts of acetylated sodium hyaluronate, 0.5-5 parts of 1, 2-pentanediol, 0.5-5 parts of ethylhexylglycerin and 70-97 parts of water;
the humectant is selected from 3-9 parts of glycerin, 1-8 parts of butanediol, 0.1-0.8 part of panthenol, 0.6-1.4 parts of hydroxyethyl urea and 0.2-0.8 part of 1, 2-hexanediol;
the antioxidant is 0.1-0.6 part of 3-o-ethyl ascorbic acid and 0.02-0.08 part of tocopherol (vitamin E);
the emollient is isononyl isononanoate 0.06-0.14 parts;
the thickening agent is selected from 0.06-0.12 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.06-0.12 part of sodium polyacrylate grafted starch and 0.16-0.28 part of hydroxyethyl cellulose;
the emulsifier is selected from 0.06-0.12 part of a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7; the mixture of the sodium acrylate/sodium acryloyldimethyl taurate copolymer, the isohexadecane and the laureth-7 comprises 63-68 parts by weight of the sodium acrylate/sodium acryloyldimethyl taurate copolymer, 10-30 parts by weight of the isohexadecane and 3-15 parts by weight of the laureth-7;
the chelating agent is 0.02-0.08 part of EDTA disodium;
the solubilizer is 0.0002 to 0.001 part of PEG-40 hydrogenated castor oil;
70-88 parts of solvent water.
Wherein, the mixture comprises water, glycerol, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM MONNIERI) extract, SCUTELLARIA BAICALENSIS (scutellarria BAICALENSIS) root extract, KOCHIA SCOPARIA (KOCHIA SCOPARIA) extract, SOPHORA flavescens (SOPHORA ANGUSTIFOLIA) root extract, grape (VITIS VINIFERA) seed extract, prickly pear (Opuntia Streptacantha) stem extract, caprylyl hydroximic acid, ethylhexyl glycerol and propylene glycol, and each component is 70-90 parts by weight, preferably 75-85 parts by weight, more preferably 80 parts by weight; 1-5 parts of glycerol, preferably 2-4 parts, more preferably 3 parts; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of oat (AVENA SATIVA) extract; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of fructus Cnidii (CNIDIUM MONNIERI) extract; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of SCUTELLARIA BAICALENSIS (scutelaria BAICALENSIS) root extract; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of Kochia SCOPARIA (KOCHIA SCOPARIA) extract; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of radix Sophorae Flavescentis (Sophora ANGUSTIFOLIA) root extract; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of grape (VITIS VINIFERA) seed extract; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of stem extract of prickly pear (Opuntia Streptacantha); 0.05-0.2 part of caprylyl hydroximic acid, preferably 0.1-0.8 part, more preferably 0.6 part; 0.05-0.2 parts of ethylhexyl glycerol, preferably 0.1-0.8 parts, more preferably 0.6 parts; 0.1 to 0.5 part of propylene glycol, preferably 0.2 to 0.4 part, and more preferably 0.3 part.
In the technical scheme of the invention, in an optimal scheme, the dendrobium officinale skin-tendering and repairing hydrating mask comprises the following raw materials in parts by weight:
wherein the skin conditioner is selected from the group consisting of Dendrobium officinale (Dendrobium CANDIDUM) 0.4-0.6 parts by weight, tetrahydro methyl pyrimidinecarboxylic acid 0.08-0.11 parts by weight, water, glycerin, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM MONNIERI) extract, Scutellaria BAICALENSIS (SCUTELLARIA BAICALENSIS) root extract, Kochia SCOPARIA (KOCHIA SCOPARIA) extract, Sophora flavescens (SOPHORA GUSTIFOLIA) root extract, grape (VITIS VINIFERA) seed extract, Opuntia Streptacantha stem extract, caprylyl hydroxamic acid, ethylhexyl glycerin, propylene glycol mixture 1.5-3 parts by weight, erythritol 0.4-0.6 part by weight, sunflower (Helianthus ANNUUS) seed oil 0.08-0.11 part by weight, sodium hyaluronate cross-linked polymer, sodium hyaluronate, hydrolyzed hyaluronic acid, sodium hyaluronate, 2-0.24 parts by weight, 2-24 parts by weight, and 0.18 parts by weight of ethyl hexylglycerin mixture, 0.04-0.06 part of sodium hyaluronate, 0.4-0.6 part of p-hydroxyacetophenone, and 00015-0.0003 part of geranium vanilloides (PELARGONIUM GRAVEOLENS) oil;
the humectant is selected from 4-8 parts of glycerin, 3-6 parts of butanediol, 0.2-0.6 part of panthenol, 0.8-1.2 parts of hydroxyethyl urea and 0.4-0.6 part of 1, 2-hexanediol;
the antioxidant is 0.12-0.26 part of 3-o-ethyl ascorbic acid and 0.04-0.06 part of tocopherol (vitamin E);
the emollient is isononyl isononanoate 0.08-0.12 parts;
the thickening agent is selected from 0.08-0.11 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.08-0.11 part of sodium polyacrylate grafted starch and 0.18-0.22 part of hydroxyethyl cellulose;
the emulsifier is selected from 0.08 to 0.11 part of a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
the chelating agent is 0.04-0.06 part of EDTA disodium;
the solubilizer is 0.0006 to 0.0009 part of PEG-40 hydrogenated castor oil;
78-86 parts of solvent water.
In the technical solution of the present invention, most preferably, wherein the skin conditioner is selected from the group consisting of 0.5 parts by weight of DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, 0.1 parts by weight of tetrahydro methylpyrimidine carboxylic acid, a mixture consisting of water, glycerin, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM MONNIERI) extract, SCUTELLARIA BAICALENSIS (scutelaria BAICALENSIS) root extract, KOCHIA SCOPARIA (KOCHIA) extract, SOPHORA flavescens (SOPHORA gustifolia) root extract, grape (VITIS VINIFERA) seed extract, Opuntia ficus indica (Opuntia streptacanthata) stem extract, octanoyl hydroxamic acid, ethylhexylglycerin, propylene glycol, 2 parts by weight of erythritol, 0.1 part by weight of sunflower (heliothus ANNUUS) seed oil, a mixture consisting of sodium hyaluronate cross-linked polymer, sodium hyaluronate, sodium hydrolyzed, hyaluronic acid, 1, 2-pentanediol, ethylhexylglycerin, and water, 0.05 parts by weight of sodium hyaluronate, p-hydroxyacetophenone 0.5 parts and geranium savonii (PELARGONIUM GRAVEOLENS) oil 0.0002 parts;
the mixture consists of 1 part of sodium hyaluronate cross-linked polymer, 1 part of sodium hyaluronate, 1 part of acetylated sodium hyaluronate, 1 part of hydrolyzed sodium hyaluronate, 1 part of 1, 2-pentanediol, 1 part of ethylhexyl glycerin and 94 parts of water in parts by weight;
the humectant is selected from 6 parts of glycerol, 4 parts of butanediol, 0.3 part of panthenol, 1 part of hydroxyethyl urea and 0.5 part of 1, 2-hexanediol;
the antioxidant is 0.2 part of 3-o-ethyl ascorbic acid and 0.05 part of tocopherol (vitamin E);
the emollient is isononyl isononanoate 0.1 part;
the thickening agent is selected from 0.1 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1 part of sodium polyacrylate grafted starch and 0.2 part of hydroxyethyl cellulose;
the emulsifier is selected from 0.1 part of a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
the chelating agent is 0.05 part of EDTA disodium;
the solubilizer is 0.0008 part of PEG-40 hydrogenated castor oil;
83.349 parts of solvent water.
In the invention, the extraction method of the dendrobium extract comprises the following steps:
(1) cleaning fresh dendrobium officinale stem leaves, airing or drying and dehydrating to be dry, and then grinding the dendrobium officinale into fine powder by using a wall breaking machine;
(2) adding the dendrobium officinale powder into a container, adding an extraction solvent, wherein the weight ratio of feed liquid is 1: 9 to 2: 8, extracting with water and glycerol (the ratio of the solvent to the water to the alcohol is 1: 1);
(3) homogenizing and stirring during leaching to make the powder material fully contact with solvent, leaching at 75-85 deg.C, preferably 80 deg.C for 1.5-3.5 hr, preferably 2 hr, and cooling;
(4) cooling to below 45 deg.C, adding antiseptic, and filtering with 100-220 mesh, preferably 200 mesh filter cloth;
(5) standing for 48 hr, collecting supernatant, and vacuum filtering with 0.8-1.2 μm, preferably 1 μm microporous folding filter core to obtain herba Dendrobii extract.
Further, the preparation method of the dendrobium officinale skin-tendering repairing and moisturizing mask in the technical scheme of the invention comprises the following steps:
mixing raw materials of butanediol, p-hydroxyacetophenone, 1, 2-hexanediol and a proper amount of solvent, heating to 45-55 ℃, and pre-dissolving to form a phase B;
mixing raw materials of glycerol, panthenol, erythritol, hydroxyethyl urea, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, sodium polyacrylate grafted starch, sodium hyaluronate, hydroxyethyl cellulose and a proper amount of solvent, heating to 85-90 ℃, homogenizing, stirring, dispersing uniformly, and cooling to about 50 ℃ to form a phase A;
step three, adding phase C into phase A, homogenizing and dispersing uniformly; the phase C comprises sunflower (Helianthus ANNUUS) seed oil, isononyl isononanoate, tocopherol (vitamin E), and emulsifier composed of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
step four, adding the dispersed phase B into the mixture formed in the step three, uniformly stirring, and cooling to below 45 ℃;
step five, adding the phase D and the solubilized phase E into the mixture formed in the step four, and uniformly stirring; the D phase comprises herba Dendrobii (Dendrobium CANDIDUM) extract, 3-o-ethyl ascorbic acid, tetrahydro-methyl pyrimidinecarboxylic acid, a mixture of water, glycerol, oat (AVENA SATIVA) extract, fructus Cnidii (CNIDIUM MONNIERI) extract, radix Scutellariae (SCUTELLARIA BAICALENSIS) root extract, fructus Kochiae (KOCHIA SCOPARIA) extract, radix Sophorae Flavescentis (SOPHORA ANTIFOLIA) root extract, fructus Vitis Viniferae (VITIS VINIFERA) seed extract, radix et caulis Opuntiae Dillenii (Opuntia Streptacantha) stem extract, caprylyl hydroximic acid, ethylhexyl glycerol, propylene glycol, a mixture of sodium hyaluronate cross-linked polymer, sodium hyaluronate, sodium acetylated hyaluronate, hydrolyzed sodium hyaluronate, 1, 2-pentanediol, ethylhexyl glycerol, a mixture of water, and a mixture of EDTA and disodium; said E phase comprises PEG-40 hydrogenated castor oil and geranium oil (Pelargonium GRAVEOLENS);
and F, filtering and discharging after the product formed in the fifth step is qualified in inspection.
The product of the invention is beneficial to improving the skin temperature, expanding pores of the skin, promoting secretion and metabolism of sweat glands, increasing the oxygen content of the skin, being beneficial to removing products of metabolism of epidermal cells and accumulated grease substances from the skin, and leading the moisture in the mask to permeate into the cuticle of the epidermis, so that the skin becomes soft, and the skin is naturally bright and elastic.
In order to make the purpose and technical solution of the embodiments of the present invention clearer, the technical solution of the embodiments of the present invention will be clearly and completely described below with reference to the implementation examples of the embodiments of the present invention. It is to be understood that the embodiments described are only a few embodiments of the present invention, and not all embodiments. All other embodiments, which can be made by a person skilled in the art without inventive effort based on the described embodiments of the invention, fall within the scope of protection of the invention.
Detailed Description
The technical solution of the present invention is further illustrated by the following specific examples. In the following specific examples, extracts other than the DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract are commercially available.
The raw materials are all commercial products purchased from related production enterprises or commercial departments.
In the following examples, the extraction method of the dendrobium extract is as follows:
(1) cleaning fresh dendrobium officinale stem leaves, airing or drying and dehydrating to be dry, and then grinding the dendrobium officinale into fine powder by using a wall breaking machine;
(2) adding the dendrobium officinale powder into a container, adding an extraction solvent, wherein the weight ratio of feed liquid is 1: 9, extracting with water and glycerol (the ratio of the solvent to the water to the alcohol is 1: 1);
(3) homogenizing and stirring during leaching to ensure that the powder is fully contacted with the solvent, wherein the leaching temperature is 80 ℃, the leaching time is 2 hours, and the temperature is reduced;
(4) cooling to below 45 deg.C, adding antiseptic, and filtering with 200 mesh filter cloth;
(5) standing for 48 hr, collecting supernatant, and vacuum filtering with 1 μm microporous folding filter core to obtain herba Dendrobii extract.
Example 1
In this example 1, the raw materials are sequentially weighed, and the skin conditioner comprises, by weight: DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract 0.5 kg, tetrahydro-methyl pyrimidinecarboxylic acid 0.1 kg, mixture consisting of water, glycerol, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM MONNIERI) extract, SCUTELLARIA BAICALENSIS (scutelaria BAICALENSIS) root extract, KOCHIA SCOPARIA (KOCHIA SCOPARIA) extract, SOPHORA flavescens (sophera ANGUSTIFOLIA) root extract, grape (VITIS VINIFERA) seed extract, Opuntia ficus indica (Opuntia Streptacantha) stem extract, caprylyl hydroximic acid, ethylhexyl glycerol, propylene glycol 2 kg, erythritol 0.5 kg, sunflower (helioanthus ANNUUS) seed oil 0.1 kg, mixture consisting of sodium hyaluronate cross-linked polymer, sodium hyaluronate hydrolysate, 1, 2-pentanediol, ethylhexyl glycerol, water 0.2 kg, sodium hyaluronate 0.05 kg, p-hydroxyacetophenone 0.5 kg and geranium savoury (PELARGONIUM GRAVEOLENS) oil 0.0002 kg; the humectant comprises 6 kg of glycerin, 4 kg of butanediol, 0.3 kg of panthenol, 1 kg of hydroxyethyl urea and 0.5 kg of 1, 2-hexanediol; antioxidant 0.2 kg of 3-o-ethyl ascorbic acid and 0.05 kg of tocopherol (vitamin E); the emollient is isononyl isononanoate 0.1 kg; the thickening agent comprises 0.1 kg of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1 kg of sodium polyacrylate grafted starch and 0.2 kg of hydroxyethyl cellulose; the oxidant is selected from 0.1 kg of a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7; chelating agent EDTA disodium 0.05 kg; solubilizer PEG-40 hydrogenated castor oil 0.0008 kg; 83.349 kg of solvent water.
Preparing the dendrobium officinale skin-tendering repairing water-replenishing mask by the weighed raw materials according to the following steps;
mixing raw materials of butanediol, p-hydroxyacetophenone, 1, 2-hexanediol and a proper amount of solvent, heating to 52 ℃, and pre-dissolving to form a phase B;
mixing raw materials of glycerol, panthenol, erythritol, hydroxyethyl urea, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, sodium polyacrylate grafted starch, sodium hyaluronate, hydroxyethyl cellulose and a proper amount of solvent, heating to 88 ℃, homogenizing, stirring, dispersing uniformly, and cooling to about 50 ℃ to form a phase A;
step three, adding phase C into phase A, homogenizing and dispersing uniformly; the phase C comprises sunflower (Helianthus ANNUUS) seed oil, isononyl isononanoate, tocopherol (vitamin E), and emulsifier composed of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
step four, adding the dispersed phase B into the mixture formed in the step three, uniformly stirring, and cooling to below 45 ℃;
step five, adding the phase D and the solubilized phase E into the mixture formed in the step four, and uniformly stirring; the D phase comprises herba Dendrobii (Dendrobium CANDIDUM) extract, 3-o-ethyl ascorbic acid, tetrahydro-methyl pyrimidinecarboxylic acid, a mixture of water, glycerol, oat (AVENA SATIVA) extract, fructus Cnidii (CNIDIUM MONNIERI) extract, radix Scutellariae (SCUTELLARIA BAICALENSIS) root extract, fructus Kochiae (KOCHIA SCOPARIA) extract, radix Sophorae Flavescentis (SOPHORA ANTIFOLIA) root extract, fructus Vitis Viniferae (VITIS VINIFERA) seed extract, radix et caulis Opuntiae Dillenii (Opuntia Streptacantha) stem extract, caprylyl hydroximic acid, ethylhexyl glycerol, propylene glycol, a mixture of sodium hyaluronate cross-linked polymer, sodium hyaluronate, sodium acetylated hyaluronate, hydrolyzed sodium hyaluronate, 1, 2-pentanediol, ethylhexyl glycerol, a mixture of water, and a mixture of EDTA and disodium; said E phase comprises PEG-40 hydrogenated castor oil and geranium oil (Pelargonium GRAVEOLENS);
and F, filtering and discharging after the product formed in the fifth step is qualified through inspection to obtain the product.
Example 2
In this example 2, the following raw materials were weighed in sequence: skin conditioner DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract 0.4 kg, tetrahydro methyl pyrimidinecarboxylic acid 0.08 kg, mixture of water, glycerin, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM MONNIERI) extract, SCUTELLARIA BAICALENSIS (scutelaria BAICALENSIS) root extract, KOCHIA SCOPARIA (KOCHIA SCOPARIA) extract, SOPHORA flavescens (sophera ANGUSTIFOLIA) root extract, grape (VITIS VINIFERA) seed extract, Opuntia Streptacantha stem extract, caprylyl hydroximic acid, ethylhexyl glycerin, propylene glycol 1.5 kg, erythritol 0.4 kg, sunflower (helioanthes hunnus) seed oil 0.08 kg, mixture of sodium hyaluronate cross-linked polymer, sodium hyaluronate hydrolysate, 1, 2-pentanediol, ethylhexyl glycerin, water 0.18 kg, sodium hyaluronate 0.04 kg, p-hydroxyacetophenone 0.4 kg and geranium savonii (PELARGONIUM GRAVEOLENS) oil 00015 kg;
the humectant is selected from the group consisting of 4 kg of glycerin, 3 kg of butylene glycol, 0.2 kg of panthenol, 0.8 kg of hydroxyethyl urea, and 0.4 kg of 1, 2-hexanediol;
antioxidant 0.12 kg of 3-o-ethyl ascorbic acid and 0.04 kg of tocopherol (vitamin E);
the emollient is isononyl isononanoate 0.08 kg;
the thickening agent is selected from 0.08 kg of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.08 kg of sodium polyacrylate grafted starch and 0.18 kg of hydroxyethyl cellulose;
the emulsifier is selected from 0.08 kg of a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
the chelating agent is 0.04 kg of EDTA disodium;
the solubilizer is 0.0006 kg of PEG-40 hydrogenated castor oil;
78 kg of solvent water.
Preparing the dendrobium officinale skin-tendering repairing water-replenishing mask by the weighed raw materials according to the following steps;
mixing raw materials of butanediol, p-hydroxyacetophenone, 1, 2-hexanediol and a proper amount of solvent, heating to 55 ℃, and pre-dissolving to form a phase B;
mixing raw materials of glycerol, panthenol, erythritol, hydroxyethyl urea, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, sodium polyacrylate grafted starch, sodium hyaluronate, hydroxyethyl cellulose and a proper amount of solvent, heating to 86 ℃, homogenizing, stirring, dispersing uniformly, and cooling to about 50 ℃ to form a phase A;
step three, adding phase C into phase A, homogenizing and dispersing uniformly; the phase C comprises sunflower (Helianthus ANNUUS) seed oil, isononyl isononanoate, tocopherol (vitamin E), and emulsifier composed of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
step four, adding the dispersed phase B into the mixture formed in the step three, uniformly stirring, and cooling to below 45 ℃;
step five, adding the phase D and the solubilized phase E into the mixture formed in the step four, and uniformly stirring; the D phase comprises herba Dendrobii (Dendrobium CANDIDUM) extract, 3-o-ethyl ascorbic acid, tetrahydro-methyl pyrimidinecarboxylic acid, a mixture of water, glycerol, oat (AVENA SATIVA) extract, fructus Cnidii (CNIDIUM MONNIERI) extract, radix Scutellariae (SCUTELLARIA BAICALENSIS) root extract, fructus Kochiae (KOCHIA SCOPARIA) extract, radix Sophorae Flavescentis (SOPHORA ANTIFOLIA) root extract, fructus Vitis Viniferae (VITIS VINIFERA) seed extract, radix et caulis Opuntiae Dillenii (Opuntia Streptacantha) stem extract, caprylyl hydroximic acid, ethylhexyl glycerol, propylene glycol, a mixture of sodium hyaluronate cross-linked polymer, sodium hyaluronate, sodium acetylated hyaluronate, hydrolyzed sodium hyaluronate, 1, 2-pentanediol, ethylhexyl glycerol, a mixture of water, and a mixture of EDTA and disodium; said E phase comprises PEG-40 hydrogenated castor oil and geranium oil (Pelargonium GRAVEOLENS);
and F, filtering and discharging after the product formed in the fifth step is qualified in inspection.
Example 3
In this example 3, the following raw materials were weighed in sequence: DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract 0.6 kg, tetrahydro-methyl pyrimidinecarboxylic acid 0.11 kg, mixture consisting of water, glycerol, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM MONNIERI) extract, SCUTELLARIA BAICALENSIS (scutelaria BAICALENSIS) root extract, KOCHIA SCOPARIA (KOCHIA SCOPARIA) extract, SOPHORA flavescens (sophera ANGUSTIFOLIA) root extract, grape (VITIS VINIFERA) seed extract, Opuntia ficus indica (Opuntia Streptacantha) stem extract, caprylyl hydroximic acid, ethylhexyl glycerol, propylene glycol 3 kg, erythritol 0.6 kg, sunflower (helioanthus ANNUUS) seed oil 0.11 kg, mixture consisting of sodium hyaluronate cross-linked polymer, sodium hyaluronate hydrolysate, sodium hyaluronate, 1, 2-pentanediol, ethylhexyl glycerol, water 0.24 kg, sodium hyaluronate 0.06 kg, p-hydroxyacetophenone 0.6 kg and geranium savoury (PELARGONIUM GRAVEOLENS) oil 0.0003 kg;
the humectant is selected from the group consisting of 8 kg of glycerin, 6 kg of butylene glycol, 0.6 kg of panthenol, 1.2 kg of hydroxyethyl urea, and 0.6 kg of 1, 2-hexanediol;
antioxidant 0.26 kg of 3-o-ethyl ascorbic acid and 0.06 kg of tocopherol (vitamin E);
the emollient is isononyl isononanoate 0.12 kg;
the thickening agent is selected from 0.11 kg of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.11 kg of sodium polyacrylate grafted starch and 0.22 kg of hydroxyethyl cellulose;
the emulsifier is selected from 0.11 kg of a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
the chelating agent is 0.06 kg of EDTA disodium;
the solubilizer is 0.0009 kg of PEG-40 hydrogenated castor oil;
86 kg of solvent water.
Preparing the dendrobium officinale skin-tendering repairing water-replenishing mask by the weighed raw materials according to the following steps;
mixing raw materials of butanediol, p-hydroxyacetophenone, 1, 2-hexanediol and a proper amount of solvent, heating to 55 ℃, and pre-dissolving to form a phase B;
mixing raw materials of glycerol, panthenol, erythritol, hydroxyethyl urea, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, sodium polyacrylate grafted starch, sodium hyaluronate, hydroxyethyl cellulose and a proper amount of solvent, heating to 86 ℃, homogenizing, stirring, dispersing uniformly, and cooling to about 50 ℃ to form a phase A;
step three, adding phase C into phase A, homogenizing and dispersing uniformly; the phase C comprises sunflower (Helianthus ANNUUS) seed oil, isononyl isononanoate, tocopherol (vitamin E), and emulsifier composed of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
step four, adding the dispersed phase B into the mixture formed in the step three, uniformly stirring, and cooling to below 45 ℃;
step five, adding the phase D and the solubilized phase E into the mixture formed in the step four, and uniformly stirring; the D phase comprises herba Dendrobii (Dendrobium CANDIDUM) extract, 3-o-ethyl ascorbic acid, tetrahydro-methyl pyrimidinecarboxylic acid, a mixture of water, glycerol, oat (AVENA SATIVA) extract, fructus Cnidii (CNIDIUM MONNIERI) extract, radix Scutellariae (SCUTELLARIA BAICALENSIS) root extract, fructus Kochiae (KOCHIA SCOPARIA) extract, radix Sophorae Flavescentis (SOPHORA ANTIFOLIA) root extract, fructus Vitis Viniferae (VITIS VINIFERA) seed extract, radix et caulis Opuntiae Dillenii (Opuntia Streptacantha) stem extract, caprylyl hydroximic acid, ethylhexyl glycerol, propylene glycol, a mixture of sodium hyaluronate cross-linked polymer, sodium hyaluronate, sodium acetylated hyaluronate, hydrolyzed sodium hyaluronate, 1, 2-pentanediol, ethylhexyl glycerol, a mixture of water, and a mixture of EDTA and disodium; said E phase comprises PEG-40 hydrogenated castor oil and geranium oil (Pelargonium GRAVEOLENS);
and F, filtering and discharging after the product formed in the fifth step is qualified through inspection to obtain the product.
Example 4
In this example 4, the following raw materials were weighed: DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract 0.3 kg, tetrahydro-methyl pyrimidinecarboxylic acid 0.06 kg, mixture consisting of water, glycerol, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM MONNIERI) extract, SCUTELLARIA BAICALENSIS (scutelaria BAICALENSIS) root extract, KOCHIA SCOPARIA (KOCHIA SCOPARIA) extract, SOPHORA flavescens (sophera ANGUSTIFOLIA) root extract, grape (VITIS VINIFERA) seed extract, Opuntia ficus indica (Opuntia Streptacantha) stem extract, caprylyl hydroximic acid, ethylhexyl glycerol, propylene glycol 1 kg, erythritol 0.3 kg, sunflower (helioanthus ANNUUS) seed oil 0.05 kg, mixture consisting of sodium hyaluronate cross-linked polymer, sodium hyaluronate hydrolysate, 1, 2-pentanediol, ethylhexyl glycerol, water 0.12 kg, sodium hyaluronate 0.02 kg, p-hydroxyacetophenone 0.2 kg and geranium savoury (PELARGONIUM GRAVEOLENS) oil 0.0001 kg;
the humectant is selected from the group consisting of 3 kg of glycerin, 1 kg of butylene glycol, 0.1 kg of panthenol, 0.6 kg of hydroxyethyl urea, and 0.2 kg of 1, 2-hexanediol;
antioxidant 0.1 kg of 3-o-ethyl ascorbic acid and 0.02 kg of tocopherol (vitamin E);
the emollient is isononyl isononanoate 0.06 kg;
the thickening agent is selected from 0.06 kg of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.06 kg of sodium polyacrylate grafted starch and 0.16 kg of hydroxyethyl cellulose;
the emulsifier is selected from 0.06 kg of a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
the chelating agent is 0.02 kg of EDTA disodium;
the solubilizer is 0.0002 kg of PEG-40 hydrogenated castor oil;
70 kg of solvent water.
Preparing the dendrobium officinale skin-tendering repairing water-replenishing mask by the weighed raw materials according to the following steps;
mixing raw materials of butanediol, p-hydroxyacetophenone, 1, 2-hexanediol and a proper amount of solvent, heating to 52 ℃, and pre-dissolving to form a phase B;
mixing raw materials of glycerol, panthenol, erythritol, hydroxyethyl urea, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, sodium polyacrylate grafted starch, sodium hyaluronate, hydroxyethyl cellulose and a proper amount of solvent, heating to 88 ℃, homogenizing, stirring, dispersing uniformly, and cooling to about 50 ℃ to form a phase A;
step three, adding phase C into phase A, homogenizing and dispersing uniformly; the phase C comprises sunflower (Helianthus ANNUUS) seed oil, isononyl isononanoate, tocopherol (vitamin E), and emulsifier composed of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
step four, adding the dispersed phase B into the mixture formed in the step three, uniformly stirring, and cooling to below 45 ℃;
step five, adding the phase D and the solubilized phase E into the mixture formed in the step four, and uniformly stirring; the D phase comprises herba Dendrobii (Dendrobium CANDIDUM) extract, 3-o-ethyl ascorbic acid, tetrahydro-methyl pyrimidinecarboxylic acid, a mixture of water, glycerol, oat (AVENA SATIVA) extract, fructus Cnidii (CNIDIUM MONNIERI) extract, radix Scutellariae (SCUTELLARIA BAICALENSIS) root extract, fructus Kochiae (KOCHIA SCOPARIA) extract, radix Sophorae Flavescentis (SOPHORA ANTIFOLIA) root extract, fructus Vitis Viniferae (VITIS VINIFERA) seed extract, radix et caulis Opuntiae Dillenii (Opuntia Streptacantha) stem extract, caprylyl hydroximic acid, ethylhexyl glycerol, propylene glycol, a mixture of sodium hyaluronate cross-linked polymer, sodium hyaluronate, sodium acetylated hyaluronate, hydrolyzed sodium hyaluronate, 1, 2-pentanediol, ethylhexyl glycerol, a mixture of water, and a mixture of EDTA and disodium; said E phase comprises PEG-40 hydrogenated castor oil and geranium oil (Pelargonium GRAVEOLENS);
and F, after the product formed in the fifth step is qualified, filtering and discharging to obtain the product of the embodiment.
Example 5
In this example 5, the following raw materials were weighed: DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract 0.8 kg, tetrahydro-methyl pyrimidinecarboxylic acid 0.12 kg, mixture consisting of water, glycerol, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM MONNIERI) extract, SCUTELLARIA BAICALENSIS (scutelaria BAICALENSIS) root extract, KOCHIA SCOPARIA (KOCHIA SCOPARIA) extract, SOPHORA flavescens (sophera ANGUSTIFOLIA) root extract, grape (VITIS VINIFERA) seed extract, Opuntia ficus indica (Opuntia Streptacantha) stem extract, caprylyl hydroximic acid, ethylhexyl glycerol, propylene glycol 5 kg, erythritol 0.8 kg, sunflower (helioanthes ANNUUS) seed oil 0.12 kg, mixture consisting of sodium hyaluronate cross-linked polymer, sodium hyaluronate hydrolysate, 1, 2-pentanediol, ethylhexyl glycerol, water 0.28 kg, sodium hyaluronate 0.08 kg, p-hydroxyacetophenone 0.8 kg and geranium savoury (PELARGONIUM GRAVEOLENS) oil 0.0005 kg;
the humectant is selected from the group consisting of 9 kg of glycerin, 8 kg of butylene glycol, 0.8 kg of panthenol, 1.4 kg of hydroxyethyl urea, and 0.8 kg of 1, 2-hexanediol;
antioxidant 0.6 kg of 3-o-ethyl ascorbic acid and 0.08 kg of tocopherol (vitamin E);
the emollient is isononyl isononanoate 0.14 kg;
the thickening agent is selected from 0.12 kg of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.12 kg of sodium polyacrylate grafted starch and 0.28 kg of hydroxyethyl cellulose;
the emulsifier is selected from 0.12 kg of a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
the chelating agent is 0.08 kg of EDTA disodium;
the solubilizer is 0.001 kg of PEG-40 hydrogenated castor oil;
88 kg of solvent water.
Preparing the dendrobium officinale skin-tendering repairing water-replenishing mask by the weighed raw materials according to the following steps;
mixing raw materials of butanediol, p-hydroxyacetophenone, 1, 2-hexanediol and a proper amount of solvent, heating to 55 ℃, and pre-dissolving to form a phase B;
mixing raw materials of glycerol, panthenol, erythritol, hydroxyethyl urea, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, sodium polyacrylate grafted starch, sodium hyaluronate, hydroxyethyl cellulose and a proper amount of solvent, heating to 90 ℃, homogenizing, stirring, dispersing uniformly, and cooling to about 50 ℃ to form a phase A;
step three, adding phase C into phase A, homogenizing and dispersing uniformly; the phase C comprises sunflower (Helianthus ANNUUS) seed oil, isononyl isononanoate, tocopherol (vitamin E), and emulsifier composed of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
step four, adding the dispersed phase B into the mixture formed in the step three, uniformly stirring, and cooling to below 45 ℃;
step five, adding the phase D and the solubilized phase E into the mixture formed in the step four, and uniformly stirring; the D phase comprises herba Dendrobii (Dendrobium CANDIDUM) extract, 3-o-ethyl ascorbic acid, tetrahydro-methyl pyrimidinecarboxylic acid, a mixture of water, glycerol, oat (AVENA SATIVA) extract, fructus Cnidii (CNIDIUM MONNIERI) extract, radix Scutellariae (SCUTELLARIA BAICALENSIS) root extract, fructus Kochiae (KOCHIA SCOPARIA) extract, radix Sophorae Flavescentis (SOPHORA ANTIFOLIA) root extract, fructus Vitis Viniferae (VITIS VINIFERA) seed extract, radix et caulis Opuntiae Dillenii (Opuntia Streptacantha) stem extract, caprylyl hydroximic acid, ethylhexyl glycerol, propylene glycol, a mixture of sodium hyaluronate cross-linked polymer, sodium hyaluronate, sodium acetylated hyaluronate, hydrolyzed sodium hyaluronate, 1, 2-pentanediol, ethylhexyl glycerol, a mixture of water, and a mixture of EDTA and disodium; said E phase comprises PEG-40 hydrogenated castor oil and geranium oil (Pelargonium GRAVEOLENS);
and F, after the product formed in the fifth step is qualified, filtering and discharging to obtain the product of the embodiment.
The above description further describes a specific embodiment of the present invention with reference to specific examples, which are intended for the detailed description of the present invention and are not intended to limit the present invention. The above-mentioned embodiments are merely descriptions of the preferred embodiments of the present invention, and do not limit the technical concept and the protection scope of the present invention, and various modifications and improvements made to the technical concept by those skilled in the art without departing from the design concept of the present invention shall fall within the protection scope of the present invention.
Claims (10)
1. The dendrobium officinale skin tendering, repairing and moisturizing mask is characterized by consisting of a skin conditioner, a humectant, an antioxidant, a moisturizer, a thickener, an emulsifier, a chelating agent, a solubilizer and a solvent.
2. The DENDROBIUM officinale skin rejuvenation moisturizing mask as claimed in claim 1, wherein the skin conditioning agent is selected from the group consisting of DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, tetrahydromethyl pyrimidinecarboxylic acid, a mixture of water, glycerin, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM monieri) extract, SCUTELLARIA BAICALENSIS (scutelaria BAICALENSIS) root extract, KOCHIA SCOPARIA (KOCHIA SCOPARIA) extract, SOPHORA flavescens (sophera) root extract, grape (VITIS VINIFERA) seed extract, Opuntia fica (Opuntia Streptacantha) stem extract, caprylhydroxamic acid, a mixture of ethylhexyl glycerin and propylene glycol, erythritol, sunflower (heliothis ANNUUS) seed oil, a mixture of sodium hyaluronate cross-linked polymer, sodium hyaluronate acetylated, hydrolyzed sodium hyaluronate, 1, 2-pentanediol, ethylhexyl glycerin, water, sodium hyaluronate, one or more of p-hydroxyacetophenone and geranium (PELARGONIUM GRAVEOLENS) oil;
the humectant is selected from one or more of the group consisting of glycerin, butylene glycol, panthenol, hydroxyethyl urea, and 1, 2-hexanediol;
the antioxidant is 3-o-ethyl ascorbic acid and tocopherol (vitamin E);
the emollient is isononyl isononanoate;
the thickening agent is selected from one or more of the group consisting of acrylic acid (acrylate)/C10-30 alkanol acrylate cross-linked polymer, sodium polyacrylate grafted starch and hydroxyethyl cellulose;
the emulsifier is a mixture consisting of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
the chelating agent is EDTA disodium;
the solubilizer is PEG-40 hydrogenated castor oil;
the solvent is water.
3. The DENDROBIUM officinale skin rejuvenation and moisturizing mask as claimed in claim 2, wherein the skin conditioning agent is selected from the group consisting of 0.3-0.8 parts by weight of DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, 0.06-0.12 parts by weight of tetrahydro methyl pyrimidinecarboxylic acid, 1-5 parts by weight of a mixture consisting of water, glycerin, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM MONNIERI) extract, SCUTELLARIA BAICALENSIS (scutelaria BAICALENSIS) root extract, KOCHIA SCOPARIA (KOCHIA SCOPARIA) extract, SOPHORA flavescens (sophia ANGUSTIFOLIA) root extract, grape (VITIS VINIFERA) seed extract, Opuntia ficus indica (Opuntia Streptacantha) stem extract, caprylhydroxamic acid, ethylhexylglycerin, propylene glycol, 0.3-0.8 parts by weight of erythritol, 0.05-0.12 parts by weight of sunflower (hehelenos ANNUUS) seed oil, sodium hyaluronate, 0.12-0.28 part of a mixture consisting of 1, 2-pentanediol, ethylhexylglycerin and water, 0.02-0.08 part of sodium hyaluronate, 0.2-0.8 part of p-hydroxyacetophenone and 0.0001-0.0005 part of geranium savianum (PELARGONIUM GRAVEOLENS) oil; the composition comprises, by weight, 0.5-5 parts of sodium hyaluronate cross-linked polymer, 0.5-5 parts of sodium hyaluronate, 0.5-5 parts of acetylated sodium hyaluronate, 0.5-5 parts of hydrolyzed sodium hyaluronate, 0.5-5 parts of 0.5, 2-pentanediol, 0.5-5 parts of ethylhexylglycerin and 70-97 parts of water;
the humectant is selected from 3-9 parts of glycerin, 1-8 parts of butanediol, 0.1-0.8 part of panthenol, 0.6-1.4 parts of hydroxyethyl urea and 0.2-0.8 part of 1, 2-hexanediol;
the antioxidant is 0.1-0.6 part of 3-o-ethyl ascorbic acid and 0.02-0.08 part of tocopherol (vitamin E);
the emollient is isononyl isononanoate 0.06-0.14 parts;
the thickening agent is selected from 0.06-0.12 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.06-0.12 part of sodium polyacrylate grafted starch and 0.16-0.28 part of hydroxyethyl cellulose;
the emulsifier is selected from 0.06-0.12 part of a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7; the mixture of the sodium acrylate/sodium acryloyldimethyl taurate copolymer, the isohexadecane and the laureth-7 comprises 63-68 parts by weight of the sodium acrylate/sodium acryloyldimethyl taurate copolymer, 10-30 parts by weight of the isohexadecane and 3-15 parts by weight of the laureth-7;
the chelating agent is 0.02-0.08 part of EDTA disodium;
the solubilizer is 0.0002 to 0.001 part of PEG-40 hydrogenated castor oil;
70-88 parts of solvent water.
4. The DENDROBIUM officinale skin rejuvenation and moisturizing mask as claimed in claim 3, wherein the skin conditioning agent is selected from the group consisting of 0.4-0.6 parts by weight of DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, 0.08-0.11 parts by weight of tetrahydro methyl pyrimidinecarboxylic acid, 1.5-3 parts by weight of a mixture consisting of water, glycerin, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM MONNIERI) extract, SCUTELLARIA BAICALENSIS (scutelaria BAICALENSIS) root extract, KOCHIA SCOPARIA (KOCHIA SCOPARIA) extract, SOPHORA flavescens (sorhora nitifolia) root extract, grape (VITIS VINIFERA) seed extract, Opuntia ficus indica (Opuntia Streptacantha) stem extract, caprylhydroxamic acid, ethylhexylglycerin, propylene glycol, 0.4-0.6 parts by weight of erythritol, 0.08-0.11 parts by weight of sunflower (HELIANTHUS ANNUUS) seed oil, 0.08-0.11 parts by weight of acetylated polymer, sodium hyaluronate, 0.18 to 0.24 portion of mixture consisting of 1, 2-pentanediol, ethylhexylglycerin and water, 0.04 to 0.06 portion of sodium hyaluronate, 0.4 to 0.6 portion of p-hydroxyacetophenone and 00015 to 0.0003 portion of geranium savianum (PELARGONIUM GRAVEOLENS) oil;
the humectant is selected from 4-8 parts of glycerin, 3-6 parts of butanediol, 0.2-0.6 part of panthenol, 0.8-1.2 parts of hydroxyethyl urea and 0.4-0.6 part of 1, 2-hexanediol;
the antioxidant is 0.12-0.26 part of 3-o-ethyl ascorbic acid and 0.04-0.06 part of tocopherol (vitamin E);
the emollient is isononyl isononanoate 0.08-0.12 parts;
the thickening agent is selected from 0.08-0.11 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.08-0.11 part of sodium polyacrylate grafted starch and 0.18-0.22 part of hydroxyethyl cellulose;
the emulsifier is selected from 0.08 to 0.11 part of a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
the chelating agent is 0.04-0.06 part of EDTA disodium;
the solubilizer is 0.0006 to 0.0009 part of PEG-40 hydrogenated castor oil;
78-86 parts of solvent water.
5. The DENDROBIUM officinale skin rejuvenation and moisturizing mask as claimed in claim 4, wherein the skin conditioning agent is selected from the group consisting of 0.5 parts by weight of DENDROBIUM officinale (DENDROBIUM CANDIDUM) extract, 0.1 parts by weight of tetrahydro methyl pyrimidinecarboxylic acid, water, glycerin, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM monerii) extract, SCUTELLARIA BAICALENSIS (scutelaria baicaliensis) root extract, KOCHIA SCOPARIA (KOCHIA SCOPARIA) extract, SOPHORA flavescens (sophorea ANGUSTIFOLIA) root extract, grape (VITIS VINIFERA) seed extract, Opuntia japonica (Opuntia streptacanthacantha) stem extract, caprylyl hydroxamic acid, ethylhexyl glycerin, propylene glycol, 2 parts by weight of a mixture, erythritol 0.5 parts by weight, sunflower (heliothis ANNUUS) seed oil 0.1 parts by weight, sodium hyaluronate cross-linking polymer, sodium hyaluronate, acetylated hyaluronate, hyaluronic acid, 1 part by weight of hyaluronic acid, 2-ethylhexylglycerin, ethylhexylpentanediol, 2-ethylhexylpentanediol, 0.2 part of mixture consisting of water, 0.05 part of sodium hyaluronate, 0.5 part of p-hydroxyacetophenone and 0.0002 part of geranium savianum (PELARGONIUM GRAVEOLENS) oil; the mixture consists of 1 part of sodium hyaluronate cross-linked polymer, 1 part of sodium hyaluronate, 1 part of acetylated sodium hyaluronate, 1 part of hydrolyzed sodium hyaluronate, 1 part of 1, 2-pentanediol, 1 part of ethylhexyl glycerin and 94 parts of water in parts by weight
The humectant is selected from 6 parts of glycerol, 4 parts of butanediol, 0.3 part of panthenol, 1 part of hydroxyethyl urea and 0.5 part of 1, 2-hexanediol;
the antioxidant is 0.2 part of 3-o-ethyl ascorbic acid and 0.05 part of tocopherol (vitamin E);
the emollient is isononyl isononanoate 0.1 part;
the thickening agent is selected from 0.1 part of acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, 0.1 part of sodium polyacrylate grafted starch and 0.2 part of hydroxyethyl cellulose;
the emulsifier is selected from 0.1 part of a mixture of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
the chelating agent is 0.05 part of EDTA disodium;
the solubilizer is 0.0008 part of PEG-40 hydrogenated castor oil;
83.349 parts of solvent water.
6. The dendrobium officinale skin rejuvenation and moisturizing mask as claimed in any one of claims 3 to 5, wherein the mixture of water, glycerin, oat (AVENA SATIVA) extract, CNIDIUM MONNIERI (CNIDIUM monieri) extract, SCUTELLARIA BAICALENSIS (scutelaria BAICALENSIS) root extract, KOCHIA SCOPARIA (KOCHIA SCOPARIA) extract, SOPHORA flavescens (SOPHORA ANGUSTIFOLIA) root extract, grape (VITIS VINIFERA) seed extract, Opuntia streptacanthantha stem extract, caprylhydroxamic acid, ethylhexylglycerin, propylene glycol is 70 to 90 parts by weight of each component, preferably 75 to 85 parts by weight, more preferably 80 parts by weight of each component; 1-5 parts of glycerol, preferably 2-4 parts, more preferably 3 parts; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of oat (AVENA SATIVA) extract; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of fructus Cnidii (CNIDIUM MONNIERI) extract; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of SCUTELLARIA BAICALENSIS (scutelaria BAICALENSIS) root extract; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of Kochia SCOPARIA (KOCHIA SCOPARIA) extract; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of radix Sophorae Flavescentis (Sophora ANGUSTIFOLIA) root extract; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of grape (VITIS VINIFERA) seed extract; 1-5 parts, preferably 2-4 parts, more preferably 3 parts of stem extract of prickly pear (Opuntia Streptacantha); 0.05-0.2 part of caprylyl hydroximic acid, preferably 0.1-0.8 part, more preferably 0.6 part; 0.05-0.2 parts of ethylhexyl glycerol, preferably 0.1-0.8 parts, more preferably 0.6 parts; 0.1 to 0.5 part of propylene glycol, preferably 0.2 to 0.4 part, and more preferably 0.3 part.
7. The dendrobium officinale skin rejuvenation and repairing hydrating mask as claimed in any one of claims 1 to 5, characterized in that the dendrobium officinale extract is extracted by the following method:
(1) cleaning fresh dendrobium officinale stem leaves, airing or drying and dehydrating to be dry, and then grinding the dendrobium officinale into fine powder by using a wall breaking machine;
(2) adding the dendrobium officinale powder into a container, adding an extraction solvent, wherein the weight ratio of feed liquid is 1: 9 to 2: 8, extracting with water and glycerol (the ratio of the solvent to the water to the alcohol is 1: 1);
(3) homogenizing and stirring during leaching to make the powder material fully contact with solvent, leaching at 75-85 deg.C, preferably 80 deg.C for 1.5-3.5 hr, and cooling;
(4) cooling to below 45 ℃, adding a preservative, and filtering with 100-mesh and 220-mesh filter cloth;
(5) standing for 48 hr, collecting supernatant, and vacuum filtering with 0.8-1.2 μm microporous folding filter core to obtain herba Dendrobii extract.
8. The dendrobium officinale skin rejuvenation and repairing hydrating mask as claimed in claim 7, characterized in that the dendrobium officinale extract is extracted by the following method:
(1) cleaning fresh dendrobium officinale stem leaves, airing or drying and dehydrating to be dry, and then grinding the dendrobium officinale into fine powder by using a wall breaking machine;
(2) adding the dendrobium officinale powder into a container, adding an extraction solvent, wherein the weight ratio of feed liquid is 1: 9, extracting with water and glycerol (the ratio of the solvent to the water to the alcohol is 1: 1);
(3) homogenizing and stirring during leaching to ensure that the powder is fully contacted with the solvent, wherein the leaching temperature is 80 ℃, the leaching time is 2 hours, and the temperature is reduced;
(4) cooling to below 45 deg.C, adding antiseptic, and filtering with 200 mesh filter cloth;
standing for 48 hr, collecting supernatant, and vacuum filtering with 1 μm microporous folding filter core to obtain herba Dendrobii extract.
9. A preparation method of a dendrobium officinale skin-tendering repairing and moisturizing mask is characterized by comprising the following steps:
mixing raw materials of butanediol, p-hydroxyacetophenone, 1, 2-hexanediol and a proper amount of solvent, heating to 45-55 ℃, and pre-dissolving to form a phase B;
mixing raw materials of glycerol, panthenol, erythritol, hydroxyethyl urea, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, sodium polyacrylate grafted starch, sodium hyaluronate, hydroxyethyl cellulose and a proper amount of solvent, heating to 85-90 ℃, homogenizing, stirring, dispersing uniformly, and cooling to about 50 ℃ to form a phase A;
step three, adding phase C into phase A, homogenizing and dispersing uniformly; the phase C comprises sunflower (Helianthus ANNUUS) seed oil, isononyl isononanoate, tocopherol (vitamin E), and emulsifier composed of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
step four, adding the dispersed phase B into the mixture formed in the step three, uniformly stirring, and cooling to below 45 ℃;
step five, adding the phase D and the solubilized phase E into the mixture formed in the step four, and uniformly stirring; the D phase comprises herba Dendrobii (Dendrobium CANDIDUM) extract, 3-o-ethyl ascorbic acid, tetrahydro-methyl pyrimidinecarboxylic acid, a mixture of water, glycerol, oat (AVENA SATIVA) extract, fructus Cnidii (CNIDIUM MONNIERI) extract, radix Scutellariae (SCUTELLARIA BAICALENSIS) root extract, fructus Kochiae (KOCHIA SCOPARIA) extract, radix Sophorae Flavescentis (SOPHORA ANTIFOLIA) root extract, fructus Vitis Viniferae (VITIS VINIFERA) seed extract, radix et caulis Opuntiae Dillenii (Opuntia Streptacantha) stem extract, caprylyl hydroximic acid, ethylhexyl glycerol, propylene glycol, a mixture of sodium hyaluronate cross-linked polymer, sodium hyaluronate, sodium acetylated hyaluronate, hydrolyzed sodium hyaluronate, 1, 2-pentanediol, ethylhexyl glycerol, a mixture of water, and a mixture of EDTA and disodium; said E phase comprises PEG-40 hydrogenated castor oil and geranium oil (Pelargonium GRAVEOLENS);
and F, filtering and discharging after the product formed in the fifth step is qualified in inspection.
10. The preparation method of the dendrobium officinale skin rejuvenation and repairing water mask as claimed in claim 9, wherein the method comprises the following steps:
mixing raw materials of butanediol, p-hydroxyacetophenone, 1, 2-hexanediol and a proper amount of solvent, heating to 50 ℃, and pre-dissolving to form a phase B;
mixing raw materials of glycerol, panthenol, erythritol, hydroxyethyl urea, acrylic acid (ester)/C10-30 alkanol acrylate cross-linked polymer, sodium polyacrylate grafted starch, sodium hyaluronate, hydroxyethyl cellulose and a proper amount of solvent, heating to 88 ℃, homogenizing, stirring, dispersing uniformly, and cooling to about 50 ℃ to form a phase A;
step three, adding phase C into phase A, homogenizing and dispersing uniformly; the phase C comprises sunflower (Helianthus ANNUUS) seed oil, isononyl isononanoate, tocopherol (vitamin E), and emulsifier composed of sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane and laureth-7;
step four, adding the dispersed phase B into the mixture formed in the step three, uniformly stirring, and cooling to below 45 ℃;
step five, adding the phase D and the solubilized phase E into the mixture formed in the step four, and uniformly stirring; the D phase comprises herba Dendrobii (Dendrobium CANDIDUM) extract, 3-o-ethyl ascorbic acid, tetrahydro-methyl pyrimidinecarboxylic acid, a mixture of water, glycerol, oat (AVENA SATIVA) extract, fructus Cnidii (CNIDIUM MONNIERI) extract, radix Scutellariae (SCUTELLARIA BAICALENSIS) root extract, fructus Kochiae (KOCHIA SCOPARIA) extract, radix Sophorae Flavescentis (SOPHORA ANTIFOLIA) root extract, fructus Vitis Viniferae (VITIS VINIFERA) seed extract, radix et caulis Opuntiae Dillenii (Opuntia Streptacantha) stem extract, caprylyl hydroximic acid, ethylhexyl glycerol, propylene glycol, a mixture of sodium hyaluronate cross-linked polymer, sodium hyaluronate, sodium acetylated hyaluronate, hydrolyzed sodium hyaluronate, 1, 2-pentanediol, ethylhexyl glycerol, a mixture of water, and a mixture of EDTA and disodium; said E phase comprises PEG-40 hydrogenated castor oil and geranium oil (Pelargonium GRAVEOLENS);
and F, filtering and discharging after the product formed in the fifth step is qualified in inspection.
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| CN113693981A (en) * | 2021-08-26 | 2021-11-26 | 广州百颜汇化妆品有限公司 | Careful moisturizing lotion and preparation method thereof |
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