CN109790026B - 球状氮化硼微粉、其制造方法及使用了其的导热树脂组合物 - Google Patents

球状氮化硼微粉、其制造方法及使用了其的导热树脂组合物 Download PDF

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CN109790026B
CN109790026B CN201780060965.1A CN201780060965A CN109790026B CN 109790026 B CN109790026 B CN 109790026B CN 201780060965 A CN201780060965 A CN 201780060965A CN 109790026 B CN109790026 B CN 109790026B
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boron nitride
fine powder
spherical boron
nitride fine
group
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CN109790026A (zh
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竹田豪
谷口佳孝
小熊武美
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Denka Co Ltd
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Denka Co Ltd
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    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
    • C01B21/064—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with boron
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/04—Ingredients treated with organic substances
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
    • C01B21/064—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with boron
    • C01B21/0646—Preparation by pyrolysis of boron and nitrogen containing compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/38—Boron-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K9/00—Use of pretreated ingredients
    • C08K9/04—Ingredients treated with organic substances
    • C08K9/06—Ingredients treated with organic substances with silicon-containing compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L101/00—Compositions of unspecified macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/85—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by XPS, EDX or EDAX data
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/80—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70
    • C01P2002/89—Crystal-structural characteristics defined by measured data other than those specified in group C01P2002/70 by mass-spectroscopy
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/30—Particle morphology extending in three dimensions
    • C01P2004/32—Spheres
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/38—Boron-containing compounds
    • C08K2003/382—Boron-containing compounds and nitrogen
    • C08K2003/385—Binary compounds of nitrogen with boron
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K3/00—Use of inorganic substances as compounding ingredients
    • C08K3/01—Use of inorganic substances as compounding ingredients characterized by their specific function
    • C08K3/013—Fillers, pigments or reinforcing additives
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
    • C08K7/00—Use of ingredients characterised by shape
    • C08K7/16—Solid spheres
    • C08K7/18—Solid spheres inorganic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2203/00—Applications
    • C08L2203/20—Applications use in electrical or conductive gadgets

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Inorganic Chemistry (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
CN201780060965.1A 2016-10-21 2017-08-31 球状氮化硼微粉、其制造方法及使用了其的导热树脂组合物 Active CN109790026B (zh)

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Application Number Priority Date Filing Date Title
JP2016-207061 2016-10-21
JP2016207061 2016-10-21
PCT/JP2017/031352 WO2018074077A1 (fr) 2016-10-21 2017-08-31 Poudre fine de nitrure de bore sphérique, son procédé de production et composition de résine thermoconductrice l'utilisant

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CN109790026A CN109790026A (zh) 2019-05-21
CN109790026B true CN109790026B (zh) 2023-03-28

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US (1) US10752503B2 (fr)
EP (1) EP3530614A4 (fr)
JP (1) JP7037494B2 (fr)
KR (1) KR102360935B1 (fr)
CN (1) CN109790026B (fr)
TW (1) TWI746636B (fr)
WO (1) WO2018074077A1 (fr)

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CN109790025B (zh) * 2016-10-07 2023-05-30 电化株式会社 氮化硼块状粒子、其制造方法及使用了其的导热树脂组合物
WO2020196644A1 (fr) * 2019-03-27 2020-10-01 デンカ株式会社 Particules de nitrure de bore en vrac, composition de résine thermoconductrice et élément de dissipation de chaleur
JP6978707B2 (ja) * 2019-07-16 2021-12-08 ダイキン工業株式会社 回路基板用樹脂組成物、回路基板用成形体、回路基板用積層体及び回路基板
WO2021111910A1 (fr) * 2019-12-06 2021-06-10 デンカ株式会社 Particules de nitrure de bore et leur procédé de production
WO2021230096A1 (fr) * 2020-05-15 2021-11-18 富士フイルム株式会社 Méthode de production de particules de nitrure de bore modifiées, particules de nitrure de bore modifiées, composition pour former un matériau thermoconducteur, matériau thermoconducteur, feuille thermoconductrice et dispositif avec couche thermoconductrice
CN112048270B (zh) * 2020-09-09 2022-04-12 苏州巨峰电气绝缘系统股份有限公司 高导热环氧复合材料及其制备方法与应用
CN112029151B (zh) * 2020-09-09 2022-04-15 苏州巨峰电气绝缘系统股份有限公司 高导热微纳氮化硼粒子及其制备方法与应用
CN114426757B (zh) * 2022-01-20 2023-05-09 国网河北省电力有限公司电力科学研究院 一种树脂材料及其制备方法

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CN101157770A (zh) * 2006-10-08 2008-04-09 通用电气公司 增强的氮化硼组合物和用其制备的组合物
WO2012027194A2 (fr) * 2010-08-25 2012-03-01 Saint-Gobain Ceramics And Plastics, Inc. Nitrure de bore à particules métalliques attachées, ses procédés de fabrication et ses utilisations
CN103958400A (zh) * 2011-11-29 2014-07-30 三菱化学株式会社 氮化硼凝聚粒子、含有该粒子的组合物、及具有包含该组合物的层的三维集成电路
CN105026312A (zh) * 2013-03-07 2015-11-04 电气化学工业株式会社 氮化硼粉末及含有该氮化硼粉末的树脂组合物
CN105980298A (zh) * 2014-02-12 2016-09-28 电化株式会社 球状氮化硼微粒及其制造方法

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US6348179B1 (en) 1999-05-19 2002-02-19 University Of New Mexico Spherical boron nitride process, system and product of manufacture
US7445797B2 (en) * 2005-03-14 2008-11-04 Momentive Performance Materials Inc. Enhanced boron nitride composition and polymer-based compositions made therewith
US6652822B2 (en) 2001-05-17 2003-11-25 The Regents Of The University Of California Spherical boron nitride particles and method for preparing them
JP3851951B2 (ja) 2002-12-05 2006-11-29 独立行政法人物質・材料研究機構 サブミクロンサイズの窒化ホウ素球状粒子の製造方法
JP5689985B2 (ja) 2012-06-27 2015-03-25 水島合金鉄株式会社 凹部付きｂｎ球状焼結粒子およびその製造方法ならびに高分子材料
WO2014005683A1 (fr) 2012-07-05 2014-01-09 Vaximm Ag Vaccin à adn, destiné à être utilisé chez des patients atteints de cancer du pancréas
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KR101389889B1 (ko) 2012-09-25 2014-04-30 김동현 체형보정기능 및 인체보온기능을 갖는 의류
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CN101157770A (zh) * 2006-10-08 2008-04-09 通用电气公司 增强的氮化硼组合物和用其制备的组合物
WO2012027194A2 (fr) * 2010-08-25 2012-03-01 Saint-Gobain Ceramics And Plastics, Inc. Nitrure de bore à particules métalliques attachées, ses procédés de fabrication et ses utilisations
CN103958400A (zh) * 2011-11-29 2014-07-30 三菱化学株式会社 氮化硼凝聚粒子、含有该粒子的组合物、及具有包含该组合物的层的三维集成电路
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CN105980298A (zh) * 2014-02-12 2016-09-28 电化株式会社 球状氮化硼微粒及其制造方法

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JP7037494B2 (ja) 2022-03-16
KR20190071686A (ko) 2019-06-24
US10752503B2 (en) 2020-08-25
EP3530614A4 (fr) 2020-04-29
WO2018074077A1 (fr) 2018-04-26
JPWO2018074077A1 (ja) 2019-08-15
KR102360935B1 (ko) 2022-02-09
CN109790026A (zh) 2019-05-21
TW201815666A (zh) 2018-05-01
TWI746636B (zh) 2021-11-21
EP3530614A1 (fr) 2019-08-28
US20200048091A1 (en) 2020-02-13

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