CN109315654A - 一种无糖型金银花甘露的生产方法 - Google Patents
一种无糖型金银花甘露的生产方法 Download PDFInfo
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Abstract
本发明公开了一种无糖型金银花甘露的生产方法，它包括以下步骤：将柠檬酸、苹果酸、抗坏血酸、山梨醇、木糖醇、甜叶菊苷及金银花原汁用水溶解，搅拌后静置6‑24h，取上清液，先用板框压滤，然后向滤液中加入复合澄清剂，搅拌后静置4‑20h，最后用超声波反渗透过滤，滤液装瓶后灭菌，即得。本发明不仅能有效去除金银花甘露中的沉淀物，延长产品的贮藏期，产品常温下保质期达到24个月，产品达到无糖型，与没有采用静置、板框压滤、澄清和超声波反渗透过滤特定的联合技术相比，绿原酸等功能活性成分含量提高30－60％，提高产品的营养价值和风味口感，从而增强了产品的综合竞争力。
Description
技术领域
本发明属于食品饮料加工领域，具体涉及一种无糖型金银花甘露的制备 方法。
背景技术
金银花甘露具有清热解毒、利胆保肝、增强免疫、降脂减肥等多种医疗 和保健用途，而且饮用方便，口感好，因此受到很多消费者的欢迎。现有金 银花甘露的生产大多是将金银花提取后得到的原汁与蜂蜜、蔗糖等调味剂混 合，然后通过沉降、过滤等方式除去部分杂质而得到。由于金银花含有很多 大分子、不稳定成分，导致产品在运输、贮存期间容易发生絮凝、沉淀，从 而导致产品的质量下降。
关于无糖型饮料的生产技术已有专利报道，中国发明专利申请号CN201710214367.7，公开了一种无糖型青钱柳饮料制备工艺,包括以下步骤： (1)青钱柳叶粉碎：粉碎至40-120目；(2)一次超声波控温提取；(4)二次超 高压提取；(5)将一次提取液和二次提取液混合,得到青钱青钱柳提取混合液； (6)调味,向青钱青钱柳提取混合液中添加木糖醇和β-环糊精；(7)过滤,将调 配好的饮料通过超滤膜过滤系统,进一步去除饮料中的细小杂质；(8)灭菌： 将饮料进行灭菌；(9)灌装：无菌灌装。本发明的优点是口感良好,且活动成 分提取率高、生物活性好；中国发明专利申请号CN201510353909.X公开了一 种无糖型生脉饮口服液,其次公开了所述的无糖型生脉饮口服液的制备方法, 其步骤如下：a)称取红参、麦冬和五味子并混合粉碎成粗粉,向粗粉中加入3-5 倍质量的乙醇,浸泡24-48h,渗漉,收集4000-5000ml渗漉液,减压浓缩至约 200-300ml,加水稀释,将稀释液搅匀并加入pH调节剂调至pH值为6.5-8.0, 然后置于4-8℃条件下冷藏48-72h；b)将冷藏后的稀释液置于4-8℃条件下以 10000-15000rpm的转速离心20-30min,向离心得到的上清液中先加防腐剂,再 加水至1000ml,然后用pH调节剂调节pH值至6.5-7.5,再加入缓冲剂,搅匀灌封,灭菌,即得。采用本发明公开的方法不仅使得稀释液的过滤效果好,而且过 滤速度快,同时制备得到的生脉饮口感好和稳定性非常好,可以进行大规模的 产业化生产；中国发明专利申请号CN201510128745.0一种无糖型芒果酸饮料 及其生产方法，其特征在于：包括如下步骤：(1)护色：将芒果的果肉片浸泡 在含0.2-1.0％食盐和0.2-1.0％抗坏血酸的混合液中5-30分钟；(2)循环打浆： 将经护色后的果肉片,分成若干小份,先取其中一小份加入0.2-1.0％抗坏血酸 的水溶液进行打浆,直至完全变成均匀的浆液,过滤得到芒果汁,再加入另一 小份芒果继续打浆,依次循环,获得浓度为20-50％的芒果汁；(3)加酶：向每千 克芒果汁中添加0.01-0.2％蛋白酶；(4)静置澄清：将加酶后的芒果汁静置, 离心去除沉淀,得到澄清芒果汁；(5)调配：每100重量份的澄清芒果汁添加 低聚果糖2-40重量份、三氯蔗糖0.005-0.03重量份作为甜味剂及菌种发 酵的营养成分,然后加热灭菌后,降温至35-45℃；(6)接种与厌氧发酵：加热 灭菌的芒果汁接种2-5％嗜热链球菌和2-5％双歧杆菌的菌液进行混合发酵,密 封进行厌氧发酵6-24h；(7)灭菌与罐装：发酵后芒果汁离心去除菌体,加热煮 沸灭菌,按每100重量份芒果汁的添加荸荠皮提取液5-20重量份,然后罐装保 存。
为了提高产品的稳定性，延长贮存期，CN 108201047A、CN 103271401A 等专利文献都采用了微孔滤膜过滤的方式，但这种方式只能除去部分大分子 物质，不能除去一些分子量相对较小且不稳定的成分，导致产品稳定性仍然 很差。为此，CN 105211440A、CN106360219A等专利文献采用了酶解技术， 即通过加入果胶酶、纤维素酶等对金银花提取物进行酶解，将大分子酶解成 小分子，从而提高产品的质量稳定性。但是这种方法又会使活性物质在酶解 过程中遭到破坏，从而降低产品的营养价值和口感。
发明内容
本发明的目的是针对上述缺陷，提供一种无糖型金银花甘露的的制备方 法，该方法通过联合采用静置、板框压滤、澄清和超声波反渗透过滤等技术， 从而提高无糖型金银花甘露感官品质，保留维生素C等营养物质，延长产品 的贮藏期。
上述目的是通过以下技术方案实现的：
一种无糖型金银花甘露的制备方法，包括以下步骤：
将柠檬酸、苹果酸、抗坏血酸、山梨醇、木糖醇及甜叶菊苷用水溶解， 然后加入金银花原汁，搅拌后静置6-24h，取上清液，先用板框压滤，然后向 滤液中加入复合澄清剂，搅拌后静置4-20h，最后用超声波反渗透过滤，反渗 透过滤液装瓶后灭菌，即得，
所述复合澄清剂由蒙脱石、单宁、明胶及壳聚糖组成，质量比为(1-5): (0.5-3):(0.5-3):(0.5-3)；
所述个原料的重量份数为：
优选地，所述蒙脱石、单宁、明胶及壳聚糖的质量比为2:1:1:1。
优选地，所述复合澄清剂的加入量为板框压滤后滤液重量的4-14％。
优选地，所述超声波反渗透过滤膜截留分子量为10-100kDa，反渗透工作 压力0.5-0.9Mpa,超声波功率5-25KHz。
本发明的有益效果是：
1)本发明采用了采用静置、板框压滤、澄清和超声波反渗透过滤特定的 联合技术，金银花的利用率达到100％，与没有采用静置、板框压滤、澄清和 超声波反渗透过滤特定的联合技术相比，绿原酸等功能活性成分含量提高30 －60％。
2)本发明制得的无糖型金银花甘露稳定性好，常温下(25℃)保质期达 到24个月。
3)本发明制得的是无糖型(糖≤0.5g/100ml)金银花甘露，口感、色泽 好，营养丰富，老少咸宜，且特别适合糖尿病人和肥胖病人。高产品的营养 价值和风味口感，从而增强了产品的综合竞争力，本发明还具有生产效率高、 成本低等优点。
具体实施方式
下面结合具体实施例对本发明进行详细说明。
实施例1
取水100公斤、金银花原汁17.5公斤，柠檬酸0.3公斤，苹果酸0.3公斤， 抗坏血酸0.3公斤，山梨醇2.1公斤，木糖醇2.1公斤及甜叶菊苷2.1公斤， 混合均匀。取混合溶液搅拌后静置15h，取上清液，先用板框压滤，然后向滤 液中加入复合澄清剂(蒙脱石、单宁、明胶及壳聚糖＝2:1:1:1)，复合澄清剂加 入量为滤液重量的9％，搅拌后静置12h，最后用截留分子量为55kDa、反渗 透工作压力0.7Mpa及超声波功率15KHz的超声波反渗透过滤，反渗透过滤 液装瓶后灭菌，即得产品，产品常温下(25℃)保质期达到24个月，产品达 到无糖型(糖≤0.5g/100ml)。
实施例2
取水100公斤、金银花原汁5公斤，柠檬酸0.1公斤，苹果酸0.1公斤， 抗坏血酸0.1公斤，山梨醇0.2公斤，木糖醇0.2公斤及甜叶菊苷0.2公斤， 混合均匀。取混合溶液搅拌后静置6h，取上清液，先用板框压滤，然后向滤 液中加入复合澄清剂(蒙脱石、单宁、明胶及壳聚糖＝2:1:1:1)，复合澄清剂加 入量为滤液重量的4％，搅拌后静置12h，最后用截留分子量为10kDa、反渗 透工作压力0.5Mpa及超声波功率5KHz的超声波反渗透过滤，反渗透过滤液 装瓶后灭菌，即得产品，产品常温下(25℃)保质期达到24个月，产品达到 无糖型(糖≤0.5g/100ml)。
实施例3
取水100公斤、金银花原汁30公斤，柠檬酸0.5公斤，苹果酸0.5公斤， 抗坏血酸0.5公斤，山梨醇4公斤，木糖醇4公斤及甜叶菊苷4公斤，混合均 匀。取混合溶液搅拌后静置24h，取上清液，先用压板压滤，然后向滤液中加 入复合澄清剂(蒙脱石、单宁、明胶及壳聚糖＝2:1:1:1)，复合澄清剂加入量为 滤液重量的14％，搅拌后静置12h，最后用截留分子量为100kDa、反渗透工 作压力0.9Mpa及超声波功率25KHz的超声波反渗透过滤，反渗透过滤液装 瓶后灭菌，即得产品，产品常温下(25℃)保质期达到24个月，产品达到无 糖型(糖≤0.5g/100ml)。
Claims (4)
1.一种无糖型金银花甘露的生产方法，其特征在于：包括以下步骤：
将柠檬酸、苹果酸、抗坏血酸、山梨醇、木糖醇及甜叶菊苷用水溶解，然后加入金银花原汁，搅拌后静置6-24h，取上清液，先用板框压滤，然后向滤液中加入复合澄清剂，搅拌后静置4-20h，最后用超声波反渗透过滤，反渗透过滤液装瓶后灭菌，即得，
所述复合澄清剂由蒙脱石、单宁、明胶及壳聚糖组成，质量比为(1-5):(0.5-3):(0.5-3):(0.5-3)；
所述个原料的重量份数为：
2.如权利要求1所述的无糖型金银花甘露的生产方法，其特征在于：所述蒙脱石、单宁、明胶及壳聚糖的质量比为2:1:1:1。
3.如权利要求1所述的无糖型金银花甘露的生产方法，其特征在于：所述复合澄清剂的加入量为板框压滤后滤液重量的4-14％。
4.如权利要求1所述的无糖型金银花甘露的生产方法，其特征在于：所述超声波反渗透过滤膜截留分子量为10-100kDa，反渗透工作压力0.5-0.9Mpa，超声波功率5-25KHz。
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