CN108499614B - 一种改性镍催化材料制备中枢神经系统用药物中间体的方法 - Google Patents
一种改性镍催化材料制备中枢神经系统用药物中间体的方法 Download PDFInfo
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- CN108499614B CN108499614B CN201810396983.3A CN201810396983A CN108499614B CN 108499614 B CN108499614 B CN 108499614B CN 201810396983 A CN201810396983 A CN 201810396983A CN 108499614 B CN108499614 B CN 108499614B
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- benzoic acid
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- zirconium dioxide
- cesium
- catalytic material
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0201—Impregnation
- B01J37/0205—Impregnation in several steps
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
- B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
- B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
- B01J23/78—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with alkali- or alkaline earth metals
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/02—Impregnation, coating or precipitation
- B01J37/0201—Impregnation
- B01J37/0209—Impregnation involving a reaction between the support and a fluid
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/08—Heat treatment
- B01J37/082—Decomposition and pyrolysis
- B01J37/088—Decomposition of a metal salt
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
- B01J37/16—Reducing
- B01J37/18—Reducing with gases containing free hydrogen
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/14—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof
- C07C227/16—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton from compounds containing already amino and carboxyl groups or derivatives thereof by reactions not involving the amino or carboxyl groups
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
Abstract
Description
序列 | 催化剂 | 转化率/% | 选择性/% |
1 | Cat/200 | 56.6 | — |
2 | Cat/300 | 73.6 | 99.2 |
3 | Cat/400 | 99.9 | 99.3 |
4 | Cat/500 | 100 | 99.3 |
5 | Cat/600 | 98.9 | 99.3 |
6 | Cat/700 | 97.2 | 99.2 |
序列 | 催化剂 | 转化率/% | 选择性/% |
1 | Cat/500-A | 100 | 98.4 |
2 | Cat/500-B | 96.7 | 98.6 |
3 | 雷尼镍 | 99.8 | 97.9 |
Claims (4)
Priority Applications (1)
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CN201810396983.3A CN108499614B (zh) | 2018-04-28 | 2018-04-28 | 一种改性镍催化材料制备中枢神经系统用药物中间体的方法 |
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CN201810396983.3A CN108499614B (zh) | 2018-04-28 | 2018-04-28 | 一种改性镍催化材料制备中枢神经系统用药物中间体的方法 |
Publications (2)
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CN108499614A CN108499614A (zh) | 2018-09-07 |
CN108499614B true CN108499614B (zh) | 2021-06-04 |
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CN201810396983.3A Expired - Fee Related CN108499614B (zh) | 2018-04-28 | 2018-04-28 | 一种改性镍催化材料制备中枢神经系统用药物中间体的方法 |
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Families Citing this family (1)
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CN109336775A (zh) * | 2018-11-09 | 2019-02-15 | 安徽省化工研究院 | 一种2,4-二氯-5-异丙氧基苯胺的合成方法 |
Citations (11)
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EP1262232A1 (en) * | 2001-05-22 | 2002-12-04 | Mitsubishi Gas Chemical Company, Inc. | Catalysts and process for producing aromatic amines |
CN1424304A (zh) * | 2002-12-12 | 2003-06-18 | 厦门市先端科技有限公司 | 苯胺、苯酚及其衍生物的制备方法 |
CN1439456A (zh) * | 2003-04-08 | 2003-09-03 | 天津大学 | 用于间二硝基苯液相加氢制间苯二胺的催化剂及制备方法 |
CN1458140A (zh) * | 2003-05-04 | 2003-11-26 | 厦门市先端科技有限公司 | 苯胺及其衍生物的制备方法 |
CN1485131A (zh) * | 2002-09-26 | 2004-03-31 | 中国科学院大连化学物理研究所 | 用于甲苯合成苯甲醛和苯甲醇的催化剂及制法和用途 |
EP1934167A2 (en) * | 2006-07-26 | 2008-06-25 | Teva Pharmaceutical Industries Ltd. | Processes for the synthesis of o-desmethylvenlafaxine |
CN101239957A (zh) * | 2008-03-13 | 2008-08-13 | 江都市新华化工有限公司 | 一种n-甲基哌嗪的合成方法 |
CN102993116A (zh) * | 2012-12-04 | 2013-03-27 | 常州大学 | 一种苯并噁嗪类激动剂的制备方法 |
CN105080548A (zh) * | 2014-05-08 | 2015-11-25 | 中国石油化工股份有限公司 | 一种提高镍系液相加氢催化剂选择性和稳定性的方法 |
CN106187887A (zh) * | 2016-07-01 | 2016-12-07 | 上海工程技术大学 | 4‑羟基喹啉‑3‑甲酸的制备方法 |
CN107597157A (zh) * | 2017-10-31 | 2018-01-19 | 张法军 | 一种用于制备抗肿瘤药物中间体的固体酸催化剂及其制备方法 |
-
2018
- 2018-04-28 CN CN201810396983.3A patent/CN108499614B/zh not_active Expired - Fee Related
Patent Citations (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP1262232A1 (en) * | 2001-05-22 | 2002-12-04 | Mitsubishi Gas Chemical Company, Inc. | Catalysts and process for producing aromatic amines |
CN1485131A (zh) * | 2002-09-26 | 2004-03-31 | 中国科学院大连化学物理研究所 | 用于甲苯合成苯甲醛和苯甲醇的催化剂及制法和用途 |
CN1424304A (zh) * | 2002-12-12 | 2003-06-18 | 厦门市先端科技有限公司 | 苯胺、苯酚及其衍生物的制备方法 |
CN1439456A (zh) * | 2003-04-08 | 2003-09-03 | 天津大学 | 用于间二硝基苯液相加氢制间苯二胺的催化剂及制备方法 |
CN1458140A (zh) * | 2003-05-04 | 2003-11-26 | 厦门市先端科技有限公司 | 苯胺及其衍生物的制备方法 |
EP1934167A2 (en) * | 2006-07-26 | 2008-06-25 | Teva Pharmaceutical Industries Ltd. | Processes for the synthesis of o-desmethylvenlafaxine |
CN101239957A (zh) * | 2008-03-13 | 2008-08-13 | 江都市新华化工有限公司 | 一种n-甲基哌嗪的合成方法 |
CN102993116A (zh) * | 2012-12-04 | 2013-03-27 | 常州大学 | 一种苯并噁嗪类激动剂的制备方法 |
CN105080548A (zh) * | 2014-05-08 | 2015-11-25 | 中国石油化工股份有限公司 | 一种提高镍系液相加氢催化剂选择性和稳定性的方法 |
CN106187887A (zh) * | 2016-07-01 | 2016-12-07 | 上海工程技术大学 | 4‑羟基喹啉‑3‑甲酸的制备方法 |
CN107597157A (zh) * | 2017-10-31 | 2018-01-19 | 张法军 | 一种用于制备抗肿瘤药物中间体的固体酸催化剂及其制备方法 |
Non-Patent Citations (2)
Title |
---|
"Hydrogenation and hydrodeoxygenation of difurfurylidene acetone to liquid alkanes over Raney Ni and the supported Pt catalysts";Yuping Li et al.;《Applied Energy》;20150314;第160卷;第990-998页 * |
"Ni 基催化剂上邻-硝基氯苯加氢反应的研究";熊峻;《中国优秀硕士学位论文全文数据库 工程科技Ⅰ辑》;20070715(第01期);B014-81 * |
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