CN108314524A - A kind of liquid fertilizer prepared as raw material using charcoal - Google Patents
A kind of liquid fertilizer prepared as raw material using charcoal Download PDFInfo
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- CN108314524A CN108314524A CN201810205439.6A CN201810205439A CN108314524A CN 108314524 A CN108314524 A CN 108314524A CN 201810205439 A CN201810205439 A CN 201810205439A CN 108314524 A CN108314524 A CN 108314524A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05D—INORGANIC FERTILISERS NOT COVERED BY SUBCLASSES C05B, C05C; FERTILISERS PRODUCING CARBON DIOXIDE
- C05D9/00—Other inorganic fertilisers
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/90—Mixtures of one or more fertilisers with additives not having a specially fertilising activity for affecting the nitrification of ammonium compounds or urea in the soil
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G5/00—Fertilisers characterised by their form
- C05G5/20—Liquid fertilisers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A40/00—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production
- Y02A40/10—Adaptation technologies in agriculture, forestry, livestock or agroalimentary production in agriculture
- Y02A40/22—Improving land use; Improving water use or availability; Controlling erosion
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P60/00—Technologies relating to agriculture, livestock or agroalimentary industries
- Y02P60/20—Reduction of greenhouse gas [GHG] emissions in agriculture, e.g. CO2
- Y02P60/21—Dinitrogen oxide [N2O], e.g. using aquaponics, hydroponics or efficiency measures
Abstract
The invention discloses a kind of liquid fertilizers prepared as raw material using charcoal, are prepared using following steps：S1, bacterium bag, algae or water hyacinth, green gram leaf or mung bean bar, liquid people and animals liquid dung, EM bacteria agent, bentonite or river embankment mud are uniformly mixed according to following weight part ratio：1：1‑2:1‑2:4‑6：0.1‑0.15：23, it is fitted into after mixing in fermentation vat and carries out anaerobic fermentation；It filters after fermentation, obtains the first fermented liquid；S2, green wheat stalk, cornstalk are crushed, then with wheat stalk, cornstalk, the first fermented liquid according to weight part ratio 23：1‑1.5：10 15 ratio is uniformly mixed, and carries out anaerobic fermentation again；Liquid is filtered after fermentation, obtains the second fermented liquid, the first solid；S3, that the first solid in S2 is pressed into brick is spare；S4, brick are put into pyrolysis furnace and are crushed after cracking, obtain charcoal powder；S6, by potassium humate, charcoal powder, the second fermented liquid according to weight part ratio be 0.1：1‑1.5：10 18 ratio is uniformly mixed.
Description
Technical field
The present invention relates to a kind of liquid fertilizers, more particularly to a kind of liquid fertilizer prepared as raw material using charcoal.
Background technology
Gradual attention with people to quality of life, organic agronomic crop are selected by more and more people, main at present
Plant leaf, pericarp, rhizome, people and animals' liquid dung etc. is used to carry out retting, fermentation, compost to produce organic fertilizer, to keep away
The soil exempted from pollution of the chemical fertilizer to crops, soil, while damaged using chemical fertilizer before can also repairing, is come with this
Obtain organic agronomic crop, such as organic rice, organic vegetable, organic fruits, organic herbage.
And organic fertilizer is mainly by the way of solid fertilizer application at present, volume is larger, and effective nutrients is inclined under same volume
It is low, it is unfavorable for transporting, is widely applied.Certainly, part organic fertilizer also applies using liquid mode, but between organic fertilizer
A certain amount of water-soluble chemical fertilizer also have to be added in making feature wherein, cause it actually not real
Organic fertilizer, and fertilizer efficiency is shorter, can not show a candle to solid fertilizer.
In the prior art, it is desirable to as long as it improves organic fertilizer fertilizer efficiency and improves the method application of the soil organism simultaneously
Charcoal, but this life of charcoal is not soluble in water, therefore liquid fertilizer can not be applied to.
Therefore, it is applicant's understanding that it is necessary to provide a kind of liquid fertilizer prepared as raw material using charcoal, biology is utilized
Charcoal can improve fertilizer efficiency duration, and charcoal can be dissolved in water the short time after treatment, in addition entire manufacturing process as carrier
It is all made of Organic Ingredients, to ensure its original intention as organic fertilizer
Invention content
In view of the drawbacks described above of the prior art, technical problem to be solved by the invention is to provide one kind with charcoal is
Liquid fertilizer prepared by raw material.
To achieve the above object, the present invention provides a kind of liquid fertilizer prepared as raw material using charcoal, use is following
It is prepared by step：
S1, by bacterium bag (the exhaust gas bacterium bag for breeding mushroom), algae or water hyacinth, green gram leaf or mung bean bar, liquid people
Animal manure water (liquid of urine or solid-liquid after storage), EM bacteria agent (" the prosperous EM of soil fertility " microbial inoculum can be used), bentonite or river embankment
Mud is uniformly mixed according to following weight part ratio：1：1-2:1-2:4-6：0.1-0.15：2-3 is fitted into after mixing in fermentation vat
Anaerobic fermentation is carried out, at 20-40 DEG C, fermentation time is not less than 20 days for fermentation temperature control；Liquid is filtered after fermentation, is obtained
The first fermented liquid is obtained, while the bulky grain sundries in solid being removed, obtains mud；Rich in nitrogen member in first fermented liquid
Element and other trace elements；
Wherein algae or water hyacinth, green gram leaf or mung bean bar break into paste or starch and reuse preferably with beater, in this way may be used
To effectively improve its fermentation efficiency.
S2, green wheat stalk, milled powders of cornstalk are broken to grain size be 1-2cm particle, then with wheat stalk, cornstalk,
First fermented liquid is according to weight part ratio 2-3：1-1.5：The ratio of 10-15 is uniformly mixed, and is placed again into fermentation vat and is carried out
Anaerobic fermentation, fermentation fermentation temperature control is at 20-30 DEG C, and fermentation time was at 10-15 days；After fermentation by liquid filtering (Gu
Liquid detaches), obtain the second fermented liquid, the first solid；Organic matter is rich in second fermented liquid, can be effectively increased fertilizer efficiency,
Improve soil.Preferably, green wheat stalk, cornstalk crush again after cooked, are greatly improved fermentation efficiency in this way.
S3, the first solid in S2 is lyophilized to water content less than 1%, then with volume ratio 5:1 ratio is pressed into size
It is spare for long 5cm, width 5cm, the brick of high 3cm；Fertilizer efficiency in the first solid, inorganic salts can be effectively prevent by way of freeze-drying
It is lost in.
S4, it the brick in S3 is put into pyrolysis furnace is slowly warming up to 300-400 DEG C, 3-4 hour progress anaerobics is kept to split
Solution, then cools to room temperature, and obtains compound bio charcoal；And the charcoal of acquisition is crushed to the biology that grain size is not more than 0.3cm
Carbon powder；Preferably, heating rate is 20-25 DEG C/min；After containing a large amount of decompose inside compound bio charcoal after everfermentation
Inorganic salts, and after Pintsch process is at charcoal, in the pore of charcoal, a large amount of inorganic salts and its can be adhered on surface
It is dissolved in the substance of water and this charcoal is very loose, and this inorganic salts can be dissolved in water, when being mixed with water,
Charcoal can carry out the mixing of short time by these inorganic salts and water, not soluble in water and lead to it always to solve charcoal
The case where causing equably to apply fertilizer is suspended on the water surface.
S5, it will be ground into bone ash powder of the grain size no more than 0.3cm after the high-temperature firings such as animal bone, eggshell, fires temperature
Degree is 700-1000 DEG C, is then 1 according to weight ratio by bone ash powder and the second fermented liquid:The ratio of 1-1.5 mixes, and obtains
Wet type bone ash；
It is according to weight ratio by wet type bone ash, poultry dung, CM101 fermenting agents (Gymboree leavening, anaerobic type) again
4-5:5-6：The ratio of 0.4-0.6 is uniformly mixed, and adjusts mixture, so that its moisture content is maintained at 60~65%, PH and is adjusted to 6-8
(adjusting acidity by the way that the second fermented liquid is added, preferentially meet pH value, moisture content can suitably increase), is put into hermetically sealed can in 30-
Anaerobic fermentation 40 days or more in 40 DEG C；Then take out water and stirring of the addition with mixture weight portion rate in fermentation tank for 2-4
Uniformly, to dilute the mixture to ferment in fermentation tank, after leaching liquid, third fermented liquid is obtained；In third fermented liquid
It is preferable phosphate fertilizer rich in P elements.Due to containing a large amount of nutrients in the second fermented liquid, therefore after being inoculated with CM101 fermenting agents,
Its nutrient can make the rapid increment of CM101 fermenting agents, and to improve fermentation efficiency and effect, while part retains the second fermentation
The nutrient of liquid.
S6, it is according to weight part ratio by potassium humate, charcoal powder, the second fermented liquid, third fermented liquid
0.1：1-1.5：10-18:The ratio of 4-8 is uniformly mixed, and obtains liquid fertilizer.In use, then 30-60 times of dilution is applied fertilizer
.Note that since charcoal is not soluble in water, therefore preferably complete to apply in liquid fertilizer has configured 5-20 minutes after configuration is good
Best side is stirred when fertilizer and fertilising, in order to avoid charcoal is precipitated, is caused the charcoal in liquid fertilizer uneven, is influenced fertilizer
Effect.
Since potassium humate, third fermented liquid, charcoal powder are alkalinity (PH is more than 7), the second fermented liquid is acid
Property (PH be less than 7), therefore its PH also has different variations after its different proportion is mixed, and generally for acid soil, can match
Alkalinity is set to improve its soil environment；In addition for partial alkaline soil, it can be configured to acidity, with to improve its soil ring
Border.
Simultaneously as potassium humate, charcoal powder, the second fermented liquid, third fermented liquid mainly pass through organic matter
Fertilizer efficiency is discharged, therefore its acid-base property influences less its fertilizer efficiency.Unlike inorganic fertilizer such as urea etc., mixes and can seriously affect with alkalinity
Its fertilizer efficiency.
Preferably, the potassium humate in S6 may be used the charcoal powder prepared in S4 and be made, and specific steps are such as
Under：
S61, charcoal powder is added in the nitric acid that mass percent is 12-20%, and ensures salpeter solution temperature level
In 80-90 DEG C, ultrasonic oscillation is aoxidized for 2-3 hours, is then adjusted solution PH to 5-7 using ammonium hydroxide, is filtered, obtains
The second solid is obtained, and the second solid is lyophilized；
S62, the potassium hydroxide solution that mass percent is 1-2% is added in the second solid, surpassed in the environment of 85-90 DEG C
Sound wave shock 1-2 hours；Then it uses ammonium hydroxide to adjust pH value to 9-11, stirs 1-2 hours, be then filtered, obtain the 5th
Liquid；
S63, the 5th liquid is stood 20 hours or more, removes supernatant, obtain solidliquid mixture；
S64, the solidliquid mixture in S63 is heated, until moisture evaporation, the solid left is potassium humate, finally
Potassium humate is crushed to grain size and is not more than 0.3cm.
Certainly, the potassium humate that the present invention uses can directly purchase finished product.
Further include following content in S6：Potassium humate, charcoal powder, the second fermented liquid, third fermented liquid are pressed
It is 0.02 according to weight fraction ratio：1：4:1.5 ratio mixing, stirs 1-2 hours, so that charcoal is fully absorbed its nutrient, then
Solid is filtered, third solid is obtained；
Third solid is mixed with the mud prepared in S1 so that mud is rolled in outside charcoal powder and forms protective layer, so
After dry, to obtain the 4th solid, the 4th solid be graininess (the 4th solid is ground into grain size and is located at 0.1-0.3 ㎝'s
Particle, the too small mobility that can influence liquid fertilizer is too big that liquid fertilizer can be caused just not applied fertilizer with the mode of sprinkling,
It is caused not have the mobility of liquid fertilizer substantially).This mode can increase the density of the 4th solid, when in use,
It can be suspended in liquid fertilizer (similar to the suspended particulate being added in milk tea), so that entire liquid fertilizer is more equal
It is even, additionally, due to having mud coating, can make charcoal powder nutrient obtain sustained release function, extend nutrient stop when
Between.
The proportioning of liquid fertilizer is in final S6：Potassium humate, the 4th solid, the second fermented liquid, third fermented liquid
According to weight part ratio 0.1：1-1.5：10-18:4-8.
The beneficial effects of the invention are as follows：
1, liquid fertilizer of the invention is all made of organic material, can be effectively prevent chemical fertilizer pollution plant, be made
It is always that organic mode is applied fertilizer to obtain plant.
2, liquid fertilizer of the invention can be that the growth of plant carries rich in nutriments such as the required nitrogen of plant, phosphorus, potassium
For enough nutrients, its yield is improved.
3, liquid fertilizer of the invention uses carrier of the charcoal as fertilizer, absorbs fertilizer by the pore in charcoal
Material, can extend fertilizer efficiency time, and charcoal can also absorb in soil by charcoal slow release fertilizer again after fertilising
Heavy metal, locking soil in organic matter, to improve soil.
4, the charcoal manufacture raw material of this law first passes through fermentation, is then cracked into charcoal again, can solve charcoal
It is not soluble in water and swim in the problem on the water surface.In actual use, it is several uniformly to mix its charcoal in 20 minutes for liquid fertilizer
It is uniformly mixed with liquid, the uniformity coefficient of charcoal when can effectively improve fertilising ensures fertilizer efficiency everywhere.
5, the EM bacteria agent that the present invention uses, also has a large amount of photosynthetic bacteria group, it can utilize the solar thermal energy that soil receives
Or using ultraviolet light as the energy, the hydrogen in the hydrogen sulfide and hydrocarbon in soil is separated, becomes harmful substance to be harmless
Substance, and with the secretion, organic matter, pernicious gas of plant root (hydrogen sulfide etc.) and carbon dioxide, nitrogen etc. for matrix, synthesis
Carbohydrate, amino acid, vitamins, nitrogen compound and physiological activator etc. are rich soil and promotion animal and plant growth
The main force.The metabolite of photosynthetic bacteria either directly absorbed by plant or as other microbial reproductions nutrient, it is photosynthetic
If bacterium can be proliferated, other beneficial microbes can be also proliferated.To effectively improve soil environment.
6, contain a large amount of nutrients in the solid that the present invention generates, can be used as base manure, entire manufacturing process is without discarded produce
It is raw, it is very environmentally friendly.
7, liquid fertilizer of the invention is in fertilising, and potassium humate, charcoal powder, the can be adjusted according to actual conditions
Two fermented liquids, third fermented liquid proportioning, it is to need to need phosphorus more when more nitrogen, result such as to come into leaves, and user can root
It is adjusted, is used very flexibly according to actual conditions.
Specific implementation mode
With reference to embodiment, the invention will be further described：
Embodiment one：
A kind of liquid fertilizer prepared as raw material using charcoal, is prepared using following steps：
S1, by bacterium bag, algae, green gram leaf, liquid people and animals liquid dung, EM bacteria agent, bentonite or river embankment mud according to following heavy
Amount portion rate uniformly mixes：1：1.5:1.5:5：0.15：2, it is fitted into after mixing in fermentation vat and carries out anaerobic fermentation, fermentation temperature control
System is at 30 DEG C, fermentation time 20 days；Liquid is filtered after fermentation, obtains the first fermented liquid；Wherein algae or water hyacinth,
Green gram leaf or mung bean bar are broken into paste or starched using beater to be reused.
S2, green wheat stalk, milled powders of cornstalk are broken to grain size be 1.5cm particle, then with wheat stalk, cornstalk,
First fermented liquid is according to weight part ratio 2：1.5：12 ratio is uniformly mixed, and is placed again into progress anaerobism hair in fermentation vat
Ferment, fermentation fermentation temperature control is at 25 DEG C, and fermentation time was at 10 days；Liquid is filtered into (separation of solid and liquid) after fermentation, is obtained
Second fermented liquid, the first solid；
S3, the first solid in S2 is lyophilized to water content less than 1%, then with volume ratio 5:1 ratio is pressed into size
It is spare for long 5cm, width 5cm, the brick of high 3cm；
S4, it the brick in S3 is put into pyrolysis furnace is slowly warming up to 300 DEG C, keep carrying out anaerobic cracking in 4 hours, then
It is cooled to room temperature, obtains compound bio charcoal；And the charcoal of acquisition is crushed to the charcoal powder that grain size is not more than 0.3cm；
Heating rate is 20-25 DEG C/min；
S5, bone ash powder of the grain size no more than 0.3cm will be ground into after the high-temperature firings such as fish-bone, sheep bone, pig bone, eggshell,
Firing temperature is 700-1000 DEG C, then mixes bone ash powder and the second fermented liquid according to the ratio that weight ratio is 1-1.5,
Obtain wet type bone ash；
It is again 4 according to weight ratio by wet type bone ash, poultry dung, CM101 fermenting agents:5：0.5 ratio is uniformly mixed,
Mixture is adjusted, so that its moisture content is maintained at 60~65%, PH and adjusts to 6-8, be put into hermetically sealed can the anaerobic fermentation in 30-40 DEG C
40 days；It then takes out the water that addition is 3 with mixture weight portion rate in fermentation tank and stirs evenly, sent out with diluting in fermentation tank
The mixture of ferment obtains third fermented liquid after leaching liquid；
S6, it is according to weight fraction ratio by potassium humate, charcoal powder, the second fermented liquid, third fermented liquid
0.02：1：4:1.5 ratio mixing, stirs 1-2 hours, so that charcoal is fully absorbed its nutrient, then filter solid, obtain
Third solid；
Third solid is mixed with the mud prepared in S1 so that mud is rolled in outside charcoal powder and forms protective layer, so
After dry, to obtain the 4th solid, the 4th solid be graininess.
By potassium humate, the 4th solid, the second fermented liquid, third fermented liquid according to weight part ratio be 0.1：1：
15:4 ratio is uniformly mixed, and obtains liquid fertilizer.
Embodiment two
A kind of liquid fertilizer prepared as raw material using charcoal, is prepared using following steps：
S1, by bacterium bag, water hyacinth, mung bean bar, liquid people and animals liquid dung, EM bacteria agent, bentonite or river embankment mud according to following
Weight part ratio uniformly mixes：1：2:2:6：0.15：2.5, be fitted into after beater breaks into slurries after mixing in fermentation vat into
Row anaerobic fermentation, fermentation temperature control is at 20-40 DEG C, fermentation time 30 days；Liquid is filtered after fermentation, obtains the first hair
Zymotic fluid body；
S2, green wheat stalk, milled powders of cornstalk are broken to grain size be 1-2cm particle, then with wheat stalk, cornstalk,
First fermented liquid is according to weight part ratio 3：1：15 ratio is uniformly mixed, and is placed again into fermentation vat and is carried out anaerobic fermentation,
Fermentation temperature control ferment at 20-30 DEG C, fermentation time was at 15 days；Liquid is filtered after fermentation, obtains the second zymotic fluid
Body, the first solid；
S3, the first solid in S2 is lyophilized to water content less than 1%, then with volume ratio 5:1 ratio is pressed into size
It is spare for long 5cm, width 5cm, the brick of high 3cm；
S4, it the brick in S3 is put into pyrolysis furnace is slowly warming up to 400 DEG C, keep carrying out anaerobic cracking in 3 hours, then
It is cooled to room temperature, obtains compound bio charcoal；And the charcoal of acquisition is crushed to the charcoal powder that grain size is not more than 0.3cm；
Heating rate is 20 DEG C/min；
S5, it will be ground into bone ash powder of the grain size no more than 0.3cm after the high-temperature firings such as animal bone, eggshell, fires temperature
Degree is 700-1000 DEG C, then mixes bone ash powder and the second fermented liquid according to the ratio that weight ratio is 1.5-1.5, obtains
Wet type bone ash；
It is again 4-5 according to weight ratio by wet type bone ash, poultry dung, CM101 fermenting agents:5-6：The ratio of 0.4-0.6
It is uniformly mixed, adjusts mixture, so that its PH is adjusted to 6-8, be put into hermetically sealed can anaerobic fermentation 60 in 30-40 DEG C；Then it takes
Go out the water that addition is 4 with mixture weight portion rate in fermentation tank and stirs evenly, to dilute the mixture to ferment in fermentation tank,
After leaching liquid, third fermented liquid is obtained；
S6, it is according to weight fraction ratio by potassium humate, charcoal powder, the second fermented liquid, third fermented liquid
0.02：1：4:1.5 ratio mixing, stirs 1-2 hours, so that charcoal is fully absorbed its nutrient, then filter solid, obtain
Third solid；
Third solid is mixed with the mud prepared in S1 so that mud is rolled in outside charcoal powder and forms protective layer, so
After dry, to obtain the 4th solid, the 4th solid be graininess.
By potassium humate, the 4th solid, the second fermented liquid, third fermented liquid according to weight part ratio be 0.1：1：
18:4 ratio is uniformly mixed, and obtains liquid fertilizer.
Embodiment three
A kind of liquid fertilizer prepared as raw material using charcoal, is prepared using following steps：
S1, by bacterium bag, water hyacinth, mung bean bar, liquid people and animals liquid dung, EM bacteria agent, bentonite or river embankment mud according to following
Weight part ratio uniformly mixes：1：2:2:6：0.15：3, it is fitted into after mixing in fermentation vat and carries out anaerobic fermentation, fermentation temperature control
At 20-40 DEG C, fermentation time 40 days；Liquid is filtered after fermentation, obtains the first fermented liquid；
S2, green wheat stalk, milled powders of cornstalk are broken to grain size be 1-2cm particle, then with wheat stalk, cornstalk,
First fermented liquid is according to weight part ratio 2.5：1：10 ratio is uniformly mixed, and is placed again into progress anaerobism hair in fermentation vat
Ferment, fermentation fermentation temperature control is at 20-30 DEG C, and fermentation time was at 10-15 days；Liquid is filtered after fermentation, obtains second
Fermented liquid, the first solid；
S3, the first solid in S2 is lyophilized to water content less than 1%, then with volume ratio 5:1 ratio is pressed into size
It is spare for long 5cm, width 5cm, the brick of high 3cm；
S4, it the brick in S3 is put into pyrolysis furnace is slowly warming up to 400 DEG C, keep carrying out anaerobic cracking in 4 hours, then
It is cooled to room temperature, obtains compound bio charcoal；And the charcoal of acquisition is crushed to the charcoal powder that grain size is not more than 0.3cm；
Heating rate is 25 DEG C/min；
S5, it will be ground into bone ash powder of the grain size no more than 0.3cm after the high-temperature firings such as animal bone, eggshell, fires temperature
Degree is 700-1000 DEG C, is then 1 according to weight ratio by bone ash powder and the second fermented liquid:1.5 ratio mixing, obtains wet
Formula bone ash；
It is again 4-5 according to weight ratio by wet type bone ash, poultry dung, CM101 fermenting agents:5-6：The ratio of 0.4-0.6
It is uniformly mixed, adjusts mixture, so that its moisture content is maintained at 60~65%, PH and adjust to 6-8, be put into hermetically sealed can at 30-40 DEG C
Interior anaerobic fermentation 60 days；It then takes out the water that addition is 2 with mixture weight portion rate in fermentation tank and stirs evenly, with dilution
The mixture to ferment in fermentation tank obtains third fermented liquid after leaching liquid；
S6, it is according to weight fraction ratio by potassium humate, charcoal powder, the second fermented liquid, third fermented liquid
0.02：1：4:1.5 ratio mixing, stirs 1-2 hours, so that charcoal is fully absorbed its nutrient, then filter solid, obtain
Third solid；
Third solid is mixed with the mud prepared in S1 so that mud is rolled in outside charcoal powder and forms protective layer, so
After dry, to obtain the 4th solid, the 4th solid be graininess.
By potassium humate, the 4th solid, the second fermented liquid, third fermented liquid according to weight part ratio be 0.1：1.5：
18:4 ratio is uniformly mixed, and is obtained liquid fertilizer, is then applied fertilizer.
Test group：
Wheat test data
Object is summer rice, and the liquid fertilizer of setting clear water control group and the present invention carry out fertilizer treatment, and selection is same
Area, growing way almost consistent wheat, best planting site is adjacent, experimental field selects Sichuan Chengdu, sowing, April at the beginning of 4 months by the end of March
Bottom early May transplanting.It is applied fertilizer respectively using the liquid fertilizer of embodiment one to three.
The fertilising process of each fertilizer：
Base manure before rice transplantation, sprays after being diluted with water 30 times using 20 kilograms per acre of liquid fertilizer；Control group sprays
Same clear water；
Tillering fertilizer is applied after rice transplanting when two weeks, is sprayed after being diluted with water 30 times using 25 kilograms per acre of liquid fertilizer；
Control group sprays same clear water；
Ear manuer is divided into and promotees fertilizers for potted flowers and guarantor's fertilizers for potted flowers；Promoting fertilizers for potted flowers was applied in cob idiophase to the Floret differentiation phase, using per acre
30 kilograms of liquid fertilizer sprays after being diluted with water 30 times；Control group sprays same clear water；
Protecting fertilizers for potted flowers was applied slightly before in pollen cell meiophase, was diluted with water using 30 kilograms per acre of liquid fertilizer
It is sprayed with water after 30 times；Control group sprays same clear water；
Granulated fertilizer is applied after going out fringe, is diluted with water after 30 times using 15 kilograms per acre of liquid fertilizer and is sprayed with water for 5~10 days
It spills；Control group sprays same clear water.
Related data is measured after rice maturation, makes following table：
| Fertilizer | Mass of 1000 kernel (g) | Number of grain per ear |
| Clear water | 25.391 | 104.1 |
| Embodiment one | 26.386 | 165.3 |
| Embodiment two | 26.411 | 164.8 |
| Embodiment three | 26.513 | 166.2 |
The native coming year after being planted using embodiment one to three is broadcast again in same time, same rice paddy seed
Kind, it applies fertilizer as clear water, related data is measured after rice maturation, make following table：
It can be obtained by upper table, the liquid fertilizer using the present invention can effectively make increasing production of rice, and can be effectively improved
Soil quality, fertilizer efficiency can extended residual in the soil, that is, the content of the soil organism, nutrient can be increased.
Place is not described in detail by the present invention, is the known technology of those skilled in the art.
The preferred embodiment of the present invention has been described in detail above.It should be appreciated that those skilled in the art without
It needs creative work according to the present invention can conceive and makes many modifications and variations.Therefore, all technologies in the art
Personnel are available by logical analysis, reasoning, or a limited experiment on the basis of existing technology under this invention's idea
Technical solution, all should be in the protection domain being defined in the patent claims.
Claims (10)
1. a kind of liquid fertilizer prepared as raw material using charcoal, which is characterized in that prepared using following steps：
S1, bacterium bag, algae or water hyacinth, green gram leaf or mung bean bar, liquid people and animals liquid dung, EM bacteria agent, bentonite or river embankment are become silted up
Mud is uniformly mixed according to following weight part ratio：1：1-2:1-2:4-6：0.1-0.15：2-3, be fitted into after mixing in fermentation vat into
Row anaerobic fermentation, at 20-40 DEG C, fermentation time is not less than 20 days for fermentation temperature control；Liquid is filtered after fermentation, is obtained
First fermented liquid, while the bulky grain sundries in solid being removed, obtain mud；
S2, green wheat stalk, milled powders of cornstalk are broken to the particle that grain size is 1-2cm, then with wheat stalk, cornstalk, first
Fermented liquid is according to weight part ratio 2-3：1-1.5：The ratio of 10-15 is uniformly mixed, and is placed again into fermentation vat and is carried out anaerobism
Fermentation, fermentation fermentation temperature control is at 20-30 DEG C, and fermentation time was at 10-15 days；Liquid is filtered after fermentation, obtains the
Two fermented liquids, the first solid；
S3, the first solids treatment in S2 to water content is less than 1%, then with volume ratio 5:It is length that 1 ratio, which is pressed into size,
5cm, width 5cm, the brick of high 3cm are spare；
S4, it the brick in S3 is put into pyrolysis furnace is slowly warming up to 300-400 DEG C, keep progress anaerobic cracking in 3-4 hour, so
Postcooling obtains compound bio charcoal to room temperature；And the charcoal of acquisition is crushed to the biological powdered carbon that grain size is not more than 0.3cm
End；
S6, by potassium humate, charcoal powder, the second fermented liquid according to weight part ratio be 0.1：1-1.5：The ratio of 10-18
Example is uniformly mixed, and obtains liquid fertilizer.
2. the liquid fertilizer according to claim 1 prepared as raw material using charcoal, which is characterized in that
Further include following content in S6：By potassium humate, charcoal powder, the second fermented liquid, third fermented liquid according to weight
It is 0.02 to measure score ratio：1：4:1.5 ratio mixing, stirs 1-2 hours, so that charcoal is fully absorbed its nutrient, then will consolidate
Body filters, and obtains third solid；
Third solid is mixed with the mud prepared in S1 so that mud is rolled in outside charcoal powder and forms protective layer, then dries
Dry, to obtain the 4th solid, graininess is made in the 4th solid；
Then the 4th solid is substituted into charcoal powder in S6, is mixed with potassium humate, charcoal powder, the second fermented liquid
Conjunction prepares liquid fertilizer.
3. the liquid fertilizer according to claim 1 or 2 prepared as raw material using charcoal, which is characterized in that S4 and S6 it
Between further include S5：It will be ground into bone ash powder of the grain size no more than 0.3cm after the high-temperature firings such as animal bone, eggshell, fires temperature
Degree is 700-1000 DEG C, is then 1 according to weight ratio by bone ash powder and the second fermented liquid:The ratio of 1-1.5 mixes, and obtains
Wet type bone ash；
It is again 4-5 according to weight ratio by wet type bone ash, poultry dung, CM101 fermenting agents:5-6：The ratio of 0.4-0.6 mixes
Uniformly, mixture is adjusted, so that its moisture content is maintained at 60~65%, PH and adjusts to 6-8, be put into hermetically sealed can the anaerobism in 30-40 DEG C
Ferment 40 days or more；It then takes out the water that addition and mixture weight portion rate in fermentation tank are 2-4 and stirs evenly, with dilution
The mixture to ferment in fermentation tank obtains third fermented liquid after leaching liquid.
4. the liquid fertilizer according to claim 3 prepared as raw material using charcoal, which is characterized in that S6 includes following
Content：By potassium humate, the 4th solid, the second fermented liquid, third fermented liquid according to weight part ratio be 0.1：1-1.5：
10-18：The ratio of 4-8 is uniformly mixed, and obtains liquid fertilizer.
5. the liquid fertilizer according to claim 1 prepared as raw material using charcoal, which is characterized in that algae in S1 or
Water hyacinth, green gram leaf or mung bean bar break into paste using beater or slurry reuses.
6. the liquid fertilizer according to claim 1 prepared as raw material using charcoal, which is characterized in that the heating speed in S4
Degree is 20-25 DEG C/min.
7. the liquid fertilizer according to claim 1 prepared as raw material using charcoal, which is characterized in that the humic acid in S6
Potassium making step is as follows：
S61, charcoal powder is added in the nitric acid that mass percent is 12-20%, and ensures that salpeter solution temperature is located at 80-
90 DEG C, ultrasonic oscillation is aoxidized for 2-3 hours, is then adjusted solution PH to 5-7 using ammonium hydroxide, is filtered, and obtains the
Two solids, and the second solid is lyophilized；
S62, the potassium hydroxide solution that mass percent is 1-2%, ultrasonic wave in the environment of 85-90 DEG C is added in the second solid
Concussion 1-2 hours；Then it uses ammonium hydroxide to adjust pH value to 9-11, stirs 1-2 hours, be then filtered, obtain the 5th liquid；
S63, the 5th liquid is stood 20 hours or more, removes supernatant, obtain solidliquid mixture；
S64, the solidliquid mixture in S63 is heated, until moisture evaporation, the solid left is potassium humate, finally will be rotten
It grows sour potassium and is crushed to grain size no more than 0.3cm.
8. the liquid fertilizer according to claim 1 prepared as raw material using charcoal, which is characterized in that green Wheat Straw in S2
Stalk, cornstalk crush again after cooked.
9. the liquid fertilizer according to claim 4 prepared as raw material using charcoal, which is characterized in that liquid fertilizer uses
Time is that configuration was completed in 5-20 minutes.
10. the liquid fertilizer according to claim 4 prepared as raw material using charcoal, which is characterized in that liquid fertilizer is dilute
It is used after releasing 30-60 times.
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Cited By (5)
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| CN110627035A (en) * | 2019-10-16 | 2019-12-31 | 天津大学 | Method for preparing biochar by pretreating biomass through anaerobic fermentation |
| US11124461B2 (en) | 2019-07-04 | 2021-09-21 | Incitec Pivot Limited | Fertilizer |
| CN113501733A (en) * | 2021-08-09 | 2021-10-15 | 安徽省司尔特肥业股份有限公司 | Special functional bio-organic fertilizer for hickory and preparation method thereof |
| CN114349578A (en) * | 2021-12-16 | 2022-04-15 | 山西欣普旺农业科技有限公司 | Method for producing special fertilizer for solanaceous vegetables by using traditional Chinese medicine residues |
| CN117466678A (en) * | 2023-12-25 | 2024-01-30 | 内蒙古公田农业科技有限责任公司 | Organic-inorganic compound fertilizer with biomass charcoal as matrix |
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| CN117466678A (en) * | 2023-12-25 | 2024-01-30 | 内蒙古公田农业科技有限责任公司 | Organic-inorganic compound fertilizer with biomass charcoal as matrix |
| CN117466678B (en) * | 2023-12-25 | 2024-03-15 | 内蒙古公田农业科技有限责任公司 | Organic-inorganic compound fertilizer with biomass charcoal as matrix |
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