CN107083698A - 锦纶织物湿法转移印花用浸轧液及其配制方法 - Google Patents

锦纶织物湿法转移印花用浸轧液及其配制方法 Download PDF

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CN107083698A
CN107083698A CN201710224376.4A CN201710224376A CN107083698A CN 107083698 A CN107083698 A CN 107083698A CN 201710224376 A CN201710224376 A CN 201710224376A CN 107083698 A CN107083698 A CN 107083698A
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黄庄芳容
张国成
左凯杰
颜怀成
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Changzhou New Wide Knitting & Dyeing Co Ltd
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Abstract

本发明公开了一种锦纶织物湿法转移印花用浸轧液及其配制方法，该浸轧液由下述重量百分比的组分配制而成：1%～5%的pH缓释剂、0.5%～2%的硫酸铵、0.5%～2%的间硝基苯磺酸钠、3%～10%的尿素、0.5%～2%的螯合分散剂、1%～3%的防泳移剂、0.5%～2%糊料以及余量的水。该浸轧液的配制方法如下：先将pH缓释剂和硫酸铵加入到水中并搅拌溶解；然后加入间硝基苯磺酸钠并搅拌溶解；接着加入尿素并搅拌溶解；再接着依次加入螯合分散剂和防泳移剂并搅拌溶解；最后缓慢加入糊料并缓慢搅拌至溶解；再过滤即得。采用本发明的浸轧液进行湿法转移印花不仅能够使得织物颜色饱和丰满，得色率高，而且水洗牢度可达4级以上。

Description

锦纶织物湿法转移印花用浸轧液及其配制方法
技术领域
本发明属于纺织品印花技术领域，具体涉及一种锦纶织物湿法转移印花用浸轧液及其配制方法。
背景技术
传统的锦纶织物印花采用的是圆网、平网印花，该工艺具有如下的优点：①颜色饱满；②生产速度快、成本低。但是该工艺在生产过程中存在的一些问题，也不容忽视，主要包括：①仅适合生产色块花型，对于半色调、过渡等花型不适宜生产；②染料利用率不高，浮色多、水洗易沾色；③针对薄型织物，由于贴布不牢，生产疵病多，难以量产。
织物的转移印花工艺分为干法转移印花和湿法转移印花两种。干法转移印花即热转印，主要用于涤纶织物的转移印花；湿法转移印花前几年被称为冷转印，主要因为该项技术在研究初期是针对棉织物的转移印花，且采用冷堆固色工艺，为了与热转印相区别，且凸显其在节能减排方面的优势，故也称为冷转印。
近年来通过对工艺的不断研究，湿法转移印花的应用已经扩展到了锦纶织物。但是存在湿法转移印花后的锦纶织物得色率低、牢度不高（只有3-4级）的问题。
发明内容
本发明的目的在于针对现有技术的不足，提供一种能够提高湿法转移印花后织物得色率和牢度的锦纶织物湿法转移印花用浸轧液及其配制方法。
实现本发明目的的技术方案是：一种锦纶织物湿法转移印花用浸轧液，由下述重量百分比的组分配制而成：1%～5%的pH缓释剂、0.5%～2%的硫酸铵、0.5%～2%的间硝基苯磺酸钠、3%～10%的尿素、0.5%～2%的螯合分散剂、1%～3%的防泳移剂、0.5%～2%糊料以及余量的水。
上述pH缓释剂为能够随着温度升高而均匀、缓慢释放出酸剂的阴离子表面活性剂。
上述螯合分散剂为对铁、铜、镁、钙等离子有螯合分散作用的阴离子表面活性剂。
上述防泳移剂为对酸性染料烘干时泳移有防止作用的阴离子表面活性剂。
上述糊料为改性淀粉、瓜儿豆胶、海藻酸钠、龙胶或者羧甲基纤维素钠。
上述糊料的粘度优选为500±20mPa·s（1%）。
上述锦纶织物湿法转移印花用浸轧液的配制方法，具有以下步骤：
①按照配方依次称取水、pH缓释剂、硫酸铵、间硝基苯磺酸钠、尿素、螯合分散剂、防泳移剂以及糊料待用；
②先将pH缓释剂和硫酸铵依次加入到水中，边加边搅拌至完全溶解；然后加入间硝基苯磺酸钠，边加边搅拌至完全溶解；接着加入尿素，边加边搅拌至完全溶解；再接着依次加入螯合分散剂和防泳移剂，边加边搅拌至完全溶解；最后缓慢加入糊料，边加边快速搅拌至完全溶解；
③用200目滤网过滤步骤②得到的溶液，即得浸轧液。
本发明具有的积极效果：采用本发明的浸轧液进行锦纶织物湿法转移印花，不仅能够使得织物颜色饱和丰满、均匀，得色率高，花型精细度高，而且水洗牢度可达4级以上。
具体实施方式
（实施例1）
本实施例的锦纶织物湿法转移印花用浸轧液由下述重量百分比的组分配制而成：2.5%的pH缓释剂、1%的硫酸铵、2%的间硝基苯磺酸钠、3%的尿素、1%的螯合分散剂、1.5%的防泳移剂、2%的糊料以及水87%。
其中，pH缓释剂为德国CHT集团的MEROPAN EF阴离子表面活性剂；间硝基苯磺酸钠也即防染盐S；螯合分散剂为德国CHT集团的HEPTOL WZB阴离子表面活性剂；防泳移剂为德国CHT集团的MIGRASOL SAP阴离子表面活性剂；糊料为瓜尔豆胶，其粘度为500±5mPa·s（1%）。
本实施例的锦纶织物湿法转移印花用浸轧液的配制方法具有以下步骤：
①按照配方依次称取水、pH缓释剂、硫酸铵、间硝基苯磺酸钠、尿素、螯合分散剂、防泳移剂以及糊料待用。
②先将pH缓释剂和硫酸铵依次加入到水中，高速搅拌机调至1400r/min，边加边搅拌约10min，使其完全溶解；然后加入间硝基苯磺酸钠，同样的转速下边加边搅拌约5min，使其完全溶解；接着加入尿素，同样的转速下边加边搅拌约5min，使其完全溶解；再接着依次加入螯合分散剂和防泳移剂，同样的转速下边加边搅拌约5min，使其完全溶解；最后缓慢加入糊料，将高速搅拌机转速调整为2800r/min，边加边快速搅拌约30min，使其完全溶解。
③用200目滤网过滤步骤②得到的溶液，即得浸轧液。
（实施例2～实施例5）
各实施例的浸轧液与实施例1的不同之处见表1。
表1
实施例1 实施例2 实施例3 实施例4 实施例5
pH缓释剂 2.5% 1.5% 5% 4% 3%
硫酸铵 1% 0.5% 2% 1.6% 1.2%
间硝基苯磺酸钠 2% 0.5% 1% 1% 1.3%
尿素 3% 5% 10% 8% 6%
螯合分散剂 1% 1.3% 2% 0.5% 0.8%
防泳移剂 1.5% 2.5% 1% 2% 3%
糊料 2% 0.5% 1.2% 1.3% 1.4%
水 87% 88.2% 77.8% 81.6% 83.3%
（对比例1～对比例5）
各对比例的浸轧液与实施例1的不同之处见表2。
表2
实施例1 对比例1 对比例2 对比例3 对比例4 对比例5
pH缓释剂 2.5% - 2.5% 2.5% 2.5% 2.5%
硫酸铵 1% 1% 1% 1% 1% -
间硝基苯磺酸钠 2% 2% 2% - 2% 2%
尿素 3% 3% - 3% 3% 3%
螯合分散剂 1% 1% 1% 1% 1% 1%
防泳移剂 1.5% 1.5% 1.5% 1.5% - 1.5%
糊料 2% 2% 2% 2% 2% 2%
水 87% 89.5% 90% 89% 88.5% 88%
（应用例）
将各实施例和各对比例的浸轧液用于锦纶织物的湿法转移印花（具体方法参考中国专利文献CN106498769A），检测湿法转移印花后织物的相关性能，结果见表3。
表3
织物 染料 水洗牢度 颜色 得色率 花型
实施例1 锦纶织物 酸性染料 5级 饱和丰满 高 精细度高
实施例2 锦纶织物 酸性染料 4-5级 饱和丰满 高 精细度高
实施例3 锦纶织物 酸性染料 4-5级 饱和丰满 高 精细度高
实施例4 锦纶织物 酸性染料 5级 饱和丰满 高 精细度高
实施例5 锦纶织物 酸性染料 4-5级 饱和丰满 高 精细度高
对比例1 锦纶织物 酸性染料 2-3级 颜色灰暗 低 精细度差
对比例2 锦纶织物 酸性染料 3-4级 颜色灰暗 偏低 精细度高
对比例3 锦纶织物 酸性染料 4级 颜色不均匀 偏低 精细度高
对比例4 锦纶织物 酸性染料 4级 饱和丰满但不均匀 高 精细度高
对比例5 锦纶织物 酸性染料 3级 饱和丰满但颜色稍暗 低 精细度高

Claims (6)

1.一种锦纶织物湿法转移印花用浸轧液，其特征在于由下述重量百分比的组分配制而成：1%～5%的pH缓释剂、0.5%～2%的硫酸铵、0.5%～2%的间硝基苯磺酸钠、3%～10%的尿素、0.5%～2%的螯合分散剂、1%～3%的防泳移剂、0.5%～2%糊料以及余量的水。
2.根据权利要求1所述的锦纶织物湿法转移印花用浸轧液，其特征在于：所述pH缓释剂为能够随着温度升高而均匀、缓慢释放出酸剂的阴离子表面活性剂。
3.根据权利要求1所述的锦纶织物湿法转移印花用浸轧液，其特征在于：所述螯合分散剂为对铁、铜、镁、钙离子有螯合分散作用的阴离子表面活性剂。
4.根据权利要求1所述的锦纶织物湿法转移印花用浸轧液，其特征在于：上述防泳移剂为对酸性染料烘干时泳移有防止作用的阴离子表面活性剂。
5.根据权利要求1所述的锦纶织物湿法转移印花用浸轧液，其特征在于：上述糊料为改性淀粉、瓜儿豆胶、海藻酸钠、龙胶或者羧甲基纤维素钠。
6.根据权利要求1至5之一所述的锦纶织物湿法转移印花用浸轧液的配制方法，具有以下步骤：
①按照配方依次称取水、pH缓释剂、硫酸铵、间硝基苯磺酸钠、尿素、螯合分散剂、防泳移剂以及糊料待用；
②先将pH缓释剂和硫酸铵依次加入到水中，边加边搅拌至完全溶解；然后加入间硝基苯磺酸钠，边加边搅拌至完全溶解；接着加入尿素，边加边搅拌至完全溶解；再接着依次加入螯合分散剂和防泳移剂，边加边搅拌至完全溶解；最后缓慢加入糊料，边加边快速搅拌至完全溶解；
③用200目滤网过滤步骤②得到的溶液，即得浸轧液。
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