WO2018184394A1 - 锦纶织物湿法转移印花用浸轧液及其配制方法 - Google Patents

锦纶织物湿法转移印花用浸轧液及其配制方法 Download PDF

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WO2018184394A1
WO2018184394A1 PCT/CN2017/113297 CN2017113297W WO2018184394A1 WO 2018184394 A1 WO2018184394 A1 WO 2018184394A1 CN 2017113297 W CN2017113297 W CN 2017113297W WO 2018184394 A1 WO2018184394 A1 WO 2018184394A1
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transfer printing
wet transfer
nylon fabric
padding liquid
agent
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PCT/CN2017/113297
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French (fr)
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黄庄芳容
张国成
左凯杰
颜怀成
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黄庄芳容
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    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/445—Use of auxiliary substances before, during or after dyeing or printing
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
    • D06P1/48—Derivatives of carbohydrates
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
    • D06P1/48—Derivatives of carbohydrates
    • D06P1/50—Derivatives of cellulose
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/62—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds with sulfate, sulfonate, sulfenic or sulfinic groups
    • D06P1/628—Compounds containing nitrogen
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
    • D06P1/642—Compounds containing nitrogen
    • D06P1/649—Compounds containing carbonamide, thiocarbonamide or guanyl groups
    • D06P1/6491—(Thio)urea or (cyclic) derivatives
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
    • D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
    • D06P1/673—Inorganic compounds
    • D06P1/67333—Salts or hydroxides
    • D06P1/67341—Salts or hydroxides of elements different from the alkaline or alkaline-earth metals or with anions containing those elements
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
    • D06P3/02—Material containing basic nitrogen
    • D06P3/04—Material containing basic nitrogen containing amide groups
    • D06P3/24—Polyamides; Polyurethanes
    • D06P3/241—Polyamides; Polyurethanes using acid dyes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
    • D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
    • D06P5/003—Transfer printing

Definitions

  • the invention belongs to the technical field of textile printing, and particularly relates to a padding liquid for wet transfer printing of nylon fabric and a preparation method thereof.
  • the traditional nylon fabric printing adopts the rotary screen and the flat screen printing.
  • the process has the following advantages: 1 full color; 2 fast production speed and low cost.
  • some problems in the production process cannot be ignored, including: 1 It is only suitable for the production of color block patterns, and is not suitable for production of halftones, transitions, etc. 2)
  • the dye utilization rate is not high, and the floating color is high. , washing and easy to stain; 3 for thin fabrics, because the patch is not strong, the production of more rickets, difficult to mass production.
  • the transfer printing process of fabrics is divided into dry transfer printing and wet transfer printing.
  • Dry transfer printing is thermal transfer printing, mainly used for transfer printing of polyester fabrics; wet transfer printing is called cold transfer in the past few years, mainly because the technology was applied to the transfer printing of cotton fabrics at the beginning of the research.
  • the cold-stacking process is also called cold transfer in order to distinguish it from thermal transfer and highlight its advantages in energy saving and emission reduction.
  • the object of the present invention is to provide a padding liquid for wet transfer printing of nylon fabrics and a method for preparing the same, which can improve the color yield and fastness of the fabric after wet transfer printing.
  • the technical solution for achieving the object of the present invention is: a padding liquid for wet transfer printing of nylon fabric, which is prepared from the following components by weight: 1% to 5% pH sustained release agent, 0.5% to 2% Ammonium sulfate, 0.5% to 2% sodium m-nitrobenzenesulfonate, 3% to 10% urea, 0.5% to 2% chelating dispersant, 1% to 3% anti-migration agent, 0.5% ⁇ 2% paste and the balance of water.
  • the above pH sustained release agent is an anionic surfactant capable of uniformly and slowly releasing an acid agent as the temperature rises.
  • the above chelate dispersant is an anionic surfactant which has a chelate dispersing action on ions such as iron, copper, magnesium and calcium.
  • the above anti-migration agent is an anionic surfactant which prevents the migration of the acid dye during drying.
  • the above paste is modified starch, guar gum, sodium alginate, long gum or sodium carboxymethylcellulose.
  • the viscosity of the above paste is preferably 500 ⁇ 20 mPa ⁇ s (1%).
  • the preparation method of the above-mentioned padding liquid for wet transfer printing of nylon fabric has the following steps:
  • the solution obtained in the step 2 is filtered with a 200 mesh screen to obtain a padding solution.
  • the positive effect of the invention is that the wet-dye transfer printing of the nylon fabric by using the padding liquid of the invention not only makes the color of the fabric saturated and plump, the color yield is high, the flower pattern has high fineness, and the washing fastness can reach 4 Above the level.
  • the padding liquid for nylon fabric wet transfer printing of the present embodiment is prepared from the following components by weight: 2.5% pH slow release agent, 1% ammonium sulfate, 2% sodium m-nitrobenzenesulfonate 3% urea, 1% chelating dispersant, 1.5% anti-migration agent, 2% paste and 87% water.
  • pH slow release agent is MEROPAN EF anionic surfactant of CHT Group of Germany; sodium m-nitrobenzenesulfonate is also known as anti-staining salt S; chelate dispersing agent is HEPTOL WZB anionic surfactant of CHT Group of Germany; anti-stroke
  • the transfer agent is MIGRASOL SAP anionic surfactant of CHT Group of Germany; the paste is guar gum with a viscosity of 500 ⁇ 5 mPa ⁇ s (1%).
  • the solution obtained in the step 2 is filtered with a 200 mesh screen to obtain a padding solution.

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Molecular Biology (AREA)
  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Coloring (AREA)

Abstract

一种锦纶织物湿法转移印花用浸轧液及其配制方法，该浸轧液由下述重量百分比的组分配制而成：1％～5％的pH缓释剂、0.5％～2％的硫酸铵、0.5％～2％的间硝基苯磺酸钠、3％～10％的尿素、0.5％～2％的螯合分散剂、1％～3％的防泳移剂、0.5％～2％糊料以及余量的水。该浸轧液的配制方法如下：先将pH缓释剂和硫酸铵加入到水中并搅拌溶解；然后加入间硝基苯磺酸钠并搅拌溶解；接着加入尿素并搅拌溶解；再接着依次加入螯合分散剂和防泳移剂并搅拌溶解；最后缓慢加入糊料并缓慢搅拌至溶解；再过滤即得。采用所述浸轧液进行湿法转移印花不仅能够使得织物颜色饱和丰满，得色率高，而且水洗牢度可达4级以上。

Description

锦纶织物湿法转移印花用浸轧液及其配制方法 技术领域
本发明属于纺织品印花技术领域，具体涉及一种锦纶织物湿法转移印花用浸轧液及其配制方法。
背景技术
传统的锦纶织物印花采用的是圆网、平网印花，该工艺具有如下的优点：①颜色饱满；②生产速度快、成本低。但是该工艺在生产过程中存在的一些问题，也不容忽视，主要包括：①仅适合生产色块花型，对于半色调、过渡等花型不适宜生产；②染料利用率不高，浮色多、水洗易沾色；③针对薄型织物，由于贴布不牢，生产疵病多，难以量产。
织物的转移印花工艺分为干法转移印花和湿法转移印花两种。干法转移印花即热转印，主要用于涤纶织物的转移印花；湿法转移印花前几年被称为冷转印，主要因为该项技术在研究初期是针对棉织物的转移印花，且采用冷堆固色工艺，为了与热转印相区别，且凸显其在节能减排方面的优势，故也称为冷转印。
近年来通过对工艺的不断研究，湿法转移印花的应用已经扩展到了锦纶织物。但是存在湿法转移印花后的锦纶织物得色率低、牢度不高(只有3-4级)的问题。
发明内容
本发明的目的在于针对现有技术的不足，提供一种能够提高湿法转移印花后织物得色率和牢度的锦纶织物湿法转移印花用浸轧液及其配制方法。
实现本发明目的的技术方案是：一种锦纶织物湿法转移印花用浸轧液，由下述重量百分比的组分配制而成：1％～5％的pH缓释剂、0.5％～2％的硫酸铵、0.5％～2％的间硝基苯磺酸钠、3％～10％的尿素、0.5％～2％的螯合分散剂、1％～3％的防泳移剂、0.5％～2％糊料以及余量的水。
上述pH缓释剂为能够随着温度升高而均匀、缓慢释放出酸剂的阴离子表面活性剂。
上述螯合分散剂为对铁、铜、镁、钙等离子有螯合分散作用的阴离子表面活性剂。
上述防泳移剂为对酸性染料烘干时泳移有防止作用的阴离子表面活性剂。
上述糊料为改性淀粉、瓜儿豆胶、海藻酸钠、龙胶或者羧甲基纤维素钠。
上述糊料的粘度优选为500±20mPa·s(1％)。
上述锦纶织物湿法转移印花用浸轧液的配制方法，具有以下步骤：
①按照配方依次称取水、pH缓释剂、硫酸铵、间硝基苯磺酸钠、尿素、螯合分散剂、防泳移剂以及糊料待用；
②先将pH缓释剂和硫酸铵依次加入到水中，边加边搅拌至完全溶解；然后加入间硝基苯磺酸钠，边加边搅拌至完全溶解；接着加入尿素，边加边搅拌至完全溶解；再接着依次加入螯合分散剂和防泳移剂，边加边搅拌至完全溶解；最后缓慢加入糊料，边加边快速搅拌至完全溶解；
③用200目滤网过滤步骤②得到的溶液，即得浸轧液。
本发明具有的积极效果：采用本发明的浸轧液进行锦纶织物湿法转移印花，不仅能够使得织物颜色饱和丰满、均匀，得色率高，花型精细度高，而且水洗牢度可达4级以上。
具体实施方式
(实施例1)
本实施例的锦纶织物湿法转移印花用浸轧液由下述重量百分比的组分配制而成：2.5％的pH缓释剂、1％的硫酸铵、2％的间硝基苯磺酸钠、3％的尿素、1％的螯合分散剂、1.5％的防泳移剂、2％的糊料以及水87％。
其中，pH缓释剂为德国CHT集团的MEROPAN EF阴离子表面活性剂；间硝基苯磺酸钠也即防染盐S；螯合分散剂为德国CHT集团的HEPTOL WZB阴离子表面活性剂；防泳移剂为德国CHT集团的MIGRASOL SAP阴离子表面活性剂；糊料为瓜尔豆胶，其粘度为500±5mPa·s(1％)。
本实施例的锦纶织物湿法转移印花用浸轧液的配制方法具有以下步骤：
①按照配方依次称取水、pH缓释剂、硫酸铵、间硝基苯磺酸钠、尿素、螯合分散剂、防泳移剂以及糊料待用。
②先将pH缓释剂和硫酸铵依次加入到水中，高速搅拌机调至1400r/min，边加边搅拌约10min，使其完全溶解；然后加入间硝基苯磺酸钠，同样的转速下边加边搅拌约5min，使其完全溶解；接着加入尿素，同样的转速下边加边搅拌约5min，使其完全溶解；再接着依次加入螯合分散剂和防泳移剂，同样的转速下边加边搅拌约5min，使其完全溶解；最后缓慢加入糊料，将高速搅拌机转速调整为2800r/min，边加边快速搅拌约30min，使其完全溶解。
③用200目滤网过滤步骤②得到的溶液，即得浸轧液。
(实施例2～实施例5)
各实施例的浸轧液与实施例1的不同之处见表1。
表1
Figure PCTCN2017113297-appb-000001
(对比例1～对比例5)
各对比例的浸轧液与实施例1的不同之处见表2。
表2
Figure PCTCN2017113297-appb-000002
(应用例)
将各实施例和各对比例的浸轧液用于锦纶织物的湿法转移印花(具体方法参考中国专利文献CN106498769A)，检测湿法转移印花后织物的相关性能，结果见表3。
表3
Figure PCTCN2017113297-appb-000003

Claims (6)

  1. 一种锦纶织物湿法转移印花用浸轧液，其特征在于由下述重量百分比的组分配制而成：1％～5％的pH缓释剂、0.5％～2％的硫酸铵、0.5％～2％的间硝基苯磺酸钠、3％～10％的尿素、0.5％～2％的螯合分散剂、1％～3％的防泳移剂、0.5％～2％糊料以及余量的水。
  2. 根据权利要求1所述的锦纶织物湿法转移印花用浸轧液，其特征在于：所述pH缓释剂为能够随着温度升高而均匀、缓慢释放出酸剂的阴离子表面活性剂。
  3. 根据权利要求1所述的锦纶织物湿法转移印花用浸轧液，其特征在于：所述螯合分散剂为对铁、铜、镁、钙离子有螯合分散作用的阴离子表面活性剂。
  4. 根据权利要求1所述的锦纶织物湿法转移印花用浸轧液，其特征在于：上述防泳移剂为对酸性染料烘干时泳移有防止作用的阴离子表面活性剂。
  5. 根据权利要求1所述的锦纶织物湿法转移印花用浸轧液，其特征在于：上述糊料为改性淀粉、瓜儿豆胶、海藻酸钠、龙胶或者羧甲基纤维素钠。
  6. 根据权利要求1至5之一所述的锦纶织物湿法转移印花用浸轧液的配制方法，具有以下步骤：
    ①按照配方依次称取水、pH缓释剂、硫酸铵、间硝基苯磺酸钠、尿素、螯合分散剂、防泳移剂以及糊料待用；
    ②先将pH缓释剂和硫酸铵依次加入到水中，边加边搅拌至完全溶解；然后加入间硝基苯磺酸钠，边加边搅拌至完全溶解；接着加入尿素，边加边搅拌至完全溶解；再接着依次加入螯合分散剂和防泳移剂，边加边搅拌至完全溶解；最后缓慢加入糊料，边加边快速搅拌至完全溶解；
    ③用200目滤网过滤步骤②得到的溶液，即得浸轧液。
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