CN1068762C - Traditional Chinese medicine seed dressing agent and method for preparing same - Google Patents
Traditional Chinese medicine seed dressing agent and method for preparing same Download PDFInfo
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- CN1068762C CN1068762C CN97100468A CN97100468A CN1068762C CN 1068762 C CN1068762 C CN 1068762C CN 97100468 A CN97100468 A CN 97100468A CN 97100468 A CN97100468 A CN 97100468A CN 1068762 C CN1068762 C CN 1068762C
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Abstract
The present invention relates to a seed-dressing agent prepared from traditional Chinese medicines and a preparation method thereof, which comprises the water-boiled liquid of stramonium, rhododendron molle, raw pinellia tuber, stemona root, etc. and the ethanol soaked liquid of the stramonium, gleditsiae, croton, lightyellow sophora root, etc. The preparation method is to mix the water-boiled liquid and the ethanol soaked liquid together in the weight proportion of 100: (4 to 6). The seed-dressing agent of the present invention can effectively inhibit the spores and the hyphae of bacteria, such as the bacteria of gummy stem blight, bipolaris pityrosporion ovale, fusarium, fusarium solani, etc. in the seeds of vegetables, melons, maize, wheat, peas, etc. or in soil; the present invention has the characteristics of wide spectrum, high efficiency and low toxicity, and no waste water, waste gas or waste slag is generated in the process of the preparation.
Description
The present invention relates to a kind of agricultural chemicals, especially utilize seed dressing of Chinese medicine preparation and preparation method thereof.
Agricultural seed dressing is a kind of important agricultural chemicals.After the peasant mixes seed and seed dressing thoroughly prior to seeding, broadcast and bury.Use the purpose of seed dressing to be to kill or suppress harmful bacterium that seed is given in the self-contained or soil infection of seed, seed is normally germinateed and grow up strong and sturdy.The seed dressing that uses is furans pellet, the U.S. top grade of Japanese match of producing that the U.S. produces at present, is chemicals, for hypertoxic class medicine, seriously endangers the person poultry safety.These medicament synthesis technique complexity, the production cost height, and also the sterilization yield-to-weight ratio is lower, and relatively poor to the inhibition effect of harmful bacterium spore and mycelia, the seed that causes can not germinate, though some seed germinates, because of the effect of harmful bacterium, the seedlings of cereal crops also can die of illness.According to statistics, very big harm up to 35-45%, is brought to agricultural production without the seedlings of cereal crops lethality of dressing seed in some area.
Application number is that the inventor has announced a kind of Pesticide with Chinese medicinal material and preparation method thereof in 95115505.9 the Chinese patent application.Wherein, the Chinese medicine that uses of insecticide as datura, give birth to ten plurality of Chinese such as the tuber of pinellia, the tuber of stemona through poach or alcohol-pickled forming.This medicament is a kind of excellent insecticide, though certain bactericidal action is also arranged, as the control to cucumber downy mildew etc., effect is splendid, and with the what seed dressing, bactericidal effect is also not obvious, haves much room for improvement.
The objective of the invention is at application number is on the basis of 95115505.9 patent applications, improves, and provides a kind of preparation to have broad spectrum activity, high efficiency and hypotoxic Chinese medicine seed dressing and preparation method thereof.
The purpose of invention is achieved in that the Chinese medicine seed dressing comprises the water cooking liquid of following medicine:
Datura 200-600g Chinese azalea 300-500g
Give birth to tuber of pinellia 400-600g tuber of stemona 400-600g
Chinese prickly ash or Zanthoxylum simulans 200-400g verdigris or industrial sulphuric acid copper 200-500g
Sulphur 500-800g lilac daphne 200-400g
Capsicum 300-400g quicklime 150-300g
Chinese honey locust 300-400g
Water consumption is 7-8 a times of drug weight.The Chinese medicine seed dressing is characterised in that the alcohol-pickled liquid that also comprises following medicine:
Datura 16-40g Chinese azalea 16-50g
Give birth to tuber of pinellia 35-65g Chinese prickly ash or Zanthoxylum simulans 5-15g
Dried venom of toads 0.5-1.5g Chinese blister beetle 10-35g
Chinese honey locust 5-15g crotons 15-40g
Monkshood 50-80g Dalmatian chrysanthemum 15-35g
Kuh-seng 50-80g lilac daphne 30-50g
Return tail 15-30g wartwort 20-35g
Thunder godvine 50-80g alcohol consumption is 4.5-5 a times of drug weight.
The ratio of water cooking liquid and alcohol-pickled liquid weight is 100: 4-6, this medicament are light yellow, and its Baume degrees is 1.08-1.10 ° of B_.Medicine in water cooking liquid and the alcohol-pickled liquid can be the several times of above-mentioned consumption.
The compound method of seed dressing is as follows: the seed dressing according to the present invention's preparation is mixed by a certain percentage by medicine water cooking liquid and alcohol-pickled liquid, and concrete preparation method is as follows:
A. the water cooking liquid medicine is formed
Datura 200-600g Chinese azalea 300-500g
Give birth to tuber of pinellia 400-600g tuber of stemona 400-600g
Chinese prickly ash or Zanthoxylum simulans 200-400g verdigris or industrial sulphuric acid copper 200-500g
Sulphur 500-800g lilac daphne 200400g
Capsicum 300-400g quicklime 150-300g
Chinese honey locust 300-400g
B. the method for making of water cooking liquid
In heating container, add said medicine weight 7-8 water doubly, heat after 40-60 ℃, above-mentioned medicine is after crushed added continue heating in this heating container, use slow fire after boiling again instead and boil 60-100 minute, and after annealing, cooling, the elimination dregs of a decoction, soup are stand-by water cooking liquid.Can be back in the heating container or directly after the water vapour cooling that produces in the decoct medicinal herbs process and add in the water cooking liquid that finally obtains, as the part of water cooking liquid.The compound method of seed dressing is characterized in that the preparation method of alcohol-pickled liquid:
A. medicine is formed
Datura 16-40g Chinese azalea 16-50g gives birth to tuber of pinellia 35-65g
Chinese prickly ash or Zanthoxylum simulans 5-15g dried venom of toads 0.5-1.5g Chinese blister beetle 10-35g
Chinese honey locust 5-15g crotons 15-40g monkshood 50-80g
Dalmatian chrysanthemum 15-35g kuh-seng 50-80g lilac daphne 30-50g
Return tail 15-30g wartwort 20-35g thunder godvine 50-80g
B. the method for making of alcohol-pickled liquid
Above-mentioned medicine through pulverizing is placed in the closed container, add drug weight 4.5-5 industrial alcohol doubly, soaked 20-30 days, filter the dregs of a decoction, filtrate is stand-by alcohol-pickled liquid.
Above-mentioned water cooking liquid of making and alcohol-pickled liquid mix, and are final products, and water cooking liquid is 100 with the ratio of alcohol-pickled liquid: 4-6.
In the preparation also can be by the several times preparation of medicine composition separately in water cooking liquid and the alcohol-pickled liquid.Water and alcohol consumption be other multiple of drug weight also.So, just change the ratio of water cooking liquid and alcohol-pickled liquid and the Baume degrees of seed dressing.
Seed dressing according to the present invention's development is liquid seed dressing, and the preparation water cooking liquid and the alcohol-pickled liquid gained dregs of a decoction still contain certain effective ingredient, they can be mixed as the pulvis seed dressing.
Seed dressing according to the present invention's development, prove through the related research units animal experiment, its toxicity is produced the red and Japan product Sai Meite seed dressing of furans well below the U.S., in production, dilution medicament and seed dressing process the person is safe from harm, the rice shoot that grows after the seed dressing seed dressing according to the present invention's development is to the harm of fowl poultry nothing.Laboratory test proves simultaneously, under room temperature (about 25 ℃) condition, and soup dilution back seed dressing 8-51 hour, as shown in the table to the inhibition effect of various bacterium spore germinations:
| Diluted concentration (times liquid) | Category | Bacterial classification | Germination rate % | Inhibiting rate % |
| 50 control groups | Pumpkin | The didymella bryoniae spore | 0 71 | 100 |
| 60 control groups | Wheat | The Bipolaris sacchari spore | 5.4 14.3 | 62.2 |
| Diluted concentration (times liquid) | Category | Bacterial classification | Germination rate % | Inhibiting rate % |
| 50 control groups | Wheat | The sickle-like bacteria spore | 5.2 50.9 | 89.8 |
| 60 control groups | Pea | The Fusarium solani spore | 0 85.4 | 100 |
| 50 control groups | Corn | The sickle-like bacteria spore | 28.5 82.7 | 65.5 |
Annotate: " control group " is the sterile water seed dressing
Times liquid number is meant that sterile water is the multiple of seed dressing
As seen from the above table, according to the seed dressing of the present invention preparation the didymella bryoniae spore and the Fusarium solani spore of pumpkin, pea suppressed best results, spore germination rate is zero, and also very high to corn, wheat sickle-like bacteria spore inhibiting rate, spore germination rate only is the 10.2-37.8% of control group.Seed dressing to melon didymella bryoniae spore, phytophthora capsici spore, wheat and corn sickle-like bacteria spore, pea Fusarium solani percentage mycelial inhibition up to 68.0%-94.6%.This effect is enough to guarantee that through producing proof seed is not subjected to bacterium infringement and all germinations, grows up strong and sturdy, and does not find the rice shoot of dying of illness because of the infringement of bacterium.
The invention has the advantages that: the raw materials used wide material sources of seed dressing, all originate in China, seed dressing has the obvious suppression effect to didymella bryoniae spore, Bipolaris sacchari spore, Fusarium solani spore and sickle-like bacteria spore and the mycelia of various seeds, and the seed that has these germs is respectively cereal crops such as greengroceries such as various melon and capsicums such as pumpkin, watermelon, eggplant, tomato and pea, corn, wheat.Simultaneously, during seed dressing and through the rice shoot that seed dressing grows the people livestock and poultry are not all had harm, safety is very strong.Therefore, this seed dressing has broad spectrum activity, high efficiency and hypotoxicity, safety.The production cost of preparation seed dressing is low, and method is simple, and production unit can be " three do not have " factory of no waste water,waste gas and industrial residue, helps environmental protection.
Specify Chinese medicine seed dressing of the present invention and preparation method thereof below in conjunction with embodiment.
First embodiment
1. the preparation of water cooking liquid
Datura 200g Chinese azalea 300g gives birth to tuber of pinellia 400g
Tuber of stemona 400g Chinese prickly ash 200g industrial sulphuric acid copper 200g
Sulphur 500g lilac daphne 200g capsicum 300g
Quicklime 150g Chinese honey locust 300g
Said medicine is crushed to less than 2mm standby.Add water 23kg and be heated to 40-60 ℃ in heating container, put into the said medicine that crushes, heating is boiled again, and then change slow fire and boil to 100 minutes, annealing again, cooling, the filter method dregs of a decoction, filtrate is the part of medicine of the present invention---water cooking liquid.Decoct medicinal herbs gained water vapour adds after cooling off in the water cooking liquid, as the part of water cooking liquid.
2. the preparation of alcohol-pickled liquid
Datura 35g Chinese azalea 45g gives birth to tuber of pinellia 60g
Chinese prickly ash 10g dried venom of toads 1g Chinese blister beetle 30g
Chinese honey locust 10g crotons 35g monkshood 70g
Dalmatian chrysanthemum 30g kuh-seng 70g lilac daphne 45g
Return tail 30g wartwort 30g thunder godvine 70g
Said medicine is crushed to less than being placed in the closed container behind the 2mm and injecting industrial alcohol 2.7kg, soaks the elimination dregs of a decoction after 30 days, and filtrate is another part of seed dressing of the present invention---alcohol-pickled liquid.
3. be that water cooking liquid and alcohol-pickled liquid mix and is medicine of the present invention with above-mentioned two kinds of soups---the Chinese medicine seed dressing.The ratio of water cooking liquid and alcohol-pickled liquid weight is 100: 4.
Second embodiment
1. the preparation of water cooking liquid
Datura 400g Chinese azalea 400g gives birth to tuber of pinellia 500g
Tuber of stemona 500g Chinese prickly ash 300g industrial sulphuric acid copper 350g
Sulphur 650g lilac daphne 300g capsicum 350g
Quicklime 230g Chinese honey locust 350g
Decoct medicinal herbs water consumption 33kg, other method of producing aqua is with first embodiment.
2. the preparation of alcohol-pickled liquid
Datura 20g Chinese azalea 30g gives birth to tuber of pinellia 50g
Zanthoxylum simulans 10g dried venom of toads 1g Chinese blister beetle 20g
Chinese honey locust 10g crotons 30g monkshood 70g
Dalmatian chrysanthemum 20g kuh-seng 60g lilac daphne 40g
Return tail 20g wartwort 25g thunder godvine 65g
Said medicine is crushed to less than behind the 2mm, and all the other processing methods are with first embodiment.Wherein the industrial alcohol consumption is 2.2kg.
3, be that water cooking liquid and alcohol-pickled liquid mix and is medicine of the present invention-Chinese medicine seed dressing with above-mentioned two kinds of soups.Water cooking liquid and alcohol-pickled liquid weight ratio are 100: 5.
The 3rd embodiment
1. the preparation of water cooking liquid
Datura 500g Chinese azalea 450g gives birth to tuber of pinellia 550g
Tuber of stemona 500g Chinese prickly ash 350g verdigris 500g
Sulphur 500g lilac daphne 300g capsicum 350g
Quicklime 250g Chinese honey locust 350g
Said medicine is crushed to less than 2mm, and all the other processing methods are with first embodiment, wherein decoct medicinal herbs water 35kg.
2. the preparation of alcohol-pickled liquid
Datura 20g Chinese azalea 30g gives birth to tuber of pinellia 40g
Zanthoxylum simulans 10g dried venom of toads 1g Chinese blister beetle 20g
Chinese honey locust 10g crotons 25g monkshood 60g
Dalmatian chrysanthemum 20g kuh-seng 60g lilac daphne 35g
Return tail 20g wartwort 20g thunder godvine 60g
Said medicine is crushed to less than 2mm, and all the other processing methods are with first embodiment, and wherein the industrial alcohol consumption is 2kg.
3, be that water cooking liquid and alcohol-pickled liquid mix and is medicine-seed dressing of the present invention with above-mentioned two kinds of soups, the ratio of water cooking liquid and alcohol immersion liquid weight is 100: 6.
The seed dressing of above-mentioned three embodiment preparation, for light yellow, its Baume degrees is 1.08-1.10 ° of B_, and soup is 2: 1000 with the ratio of seed weight during use, and soup need dilute before the seed dressing, and thinner ratio is a soup: water=1: 20-60 (weight ratio).Seed dressing according to above embodiment preparation also can dilute the rice shoot filling root that 100-150 doubly is used for not using seed dressing, so that kill the bacterium on soil and the rice shoot root.
Liquid seed dressing according to the foregoing description preparation can make cereal crops obtain bigger amount of increase in production.With the corn is example, sickle-like bacteria spore harm in the self-contained or soil of corn seed is the most serious, according to statistics, the area that has makes corn rice shoot lethality up to 35-45% because of the destruction of this bacterium, causes the underproduction at least 30%, after using this seed dressing, both can kill the sickle-like bacteria spore, can promote the root system development growth again, and make the corn survival rate reach 100%.In other words, under the same conditions, use this seed dressing can increase production more than 30%, this is that present any seed dressing is incomparable.Utilization is according to the applicable seed dressing of carrying greengrocery, melon and fruit class and the cereal crops such as corn, wheat of multiple germ of seed dressing of the present invention's development, characteristics with broad spectrum activity, high efficiency and low toxicity, safety, therefore the present invention has reached and has given the phase purpose, has finished the invention task.
Claims (2)
1, a kind of Chinese medicine seed dressing, form by the water cooking liquid of following medicine:
Datura 200-600g Chinese azalea 300-500g
Give birth to tuber of pinellia 400-600g tuber of stemona 400-600g
Chinese prickly ash or Zanthoxylum simulans 200-400g verdigris or industrial sulphuric acid copper 200-500g
Sulphur 500-800g lilac daphne 200-400g
Capsicum 300-400g quicklime 150-300g
Chinese honey locust 300-400g
Water consumption is 7-8 a times of drug weight, is made up of the alcohol-pickled liquid of following medicine:
Datura 16-40g Chinese azalea 16-50g
Give birth to tuber of pinellia 35-65g Chinese prickly ash or Zanthoxylum simulans 5-15g
Dried venom of toads 0.5-1.5g Chinese blister beetle 10-35g
Chinese honey locust 5-15g crotons 15-40g
Monkshood 50-80g Dalmatian chrysanthemum 15-35g
Kuh-seng 50-80g lilac daphne 30 1 50g
Return tail 15-30 wartwort 20-35g
Thunder godvine 50-80g alcohol consumption is 4.5-5 a times of drug weight
The ratio of above-mentioned water cooking liquid and alcohol-pickled liquid weight is 100: 4-6, color is light yellow, Baume degrees 1.08-1.10 ° Be.
2, a kind of preparation method of Chinese medicine seed dressing:
(1) medicine of water cooking liquid is formed:
Datura 200-600g Chinese azalea 300-500g
Give birth to tuber of pinellia 400-600g tuber of stemona 400-600g
Chinese prickly ash or Zanthoxylum simulans 200-400g verdigris or industrial sulphuric acid copper 200-500g
Sulphur 500-800g lilac daphne 200-400g
Capsicum 300-400g quicklime 150-300g
Chinese honey locust 300-400g
(2) method for making of water cooking liquid:
In heating container, add said medicine weight 7-8 water doubly, heat to 40-60 ℃, to put into this heating container through the medicine of pulverizing, after the continuation heating is boiled 60-100 minute, annealing, cooling, the elimination dregs of a decoction, soup is water cooking liquid, is back in the heating container after the water vapour cooling that produces in the decoct medicinal herbs process or direct the adding in the final water cooking liquid that obtains, as the part of water cooking liquid; The preparation method of alcohol-pickled liquid:
(1) medicine is formed:
Datura 16-40g Chinese azalea 16-50g
Give birth to tuber of pinellia 35-65g Chinese prickly ash or Zanthoxylum simulans 5-15g
Dried venom of toads 0.5-1.5g Chinese blister beetle 10-35g
Chinese honey locust 5-15g crotons 15-40g
Monkshood 50-80g Dalmatian chrysanthemum 15-35g
Kuh-seng 50-80g lilac daphne 30-50g
Return tail 15-30 wartwort 20-35g
Thunder godvine 50-80g
(2) method for making of alcohol-pickled liquid:
Place in the closed container through the medicine of pulverizing above-mentioned, and add drug weight 4.5-5 industrial alcohol doubly, soaked 20-30 days, filter the dregs of a decoction, filtrate is stand-by alcohol-pickled liquid; The water cooking liquid and the alcohol-pickled liquid that are obtained by said method are 100 with weight ratio: the ratio of 4-6 mixes and is the liquid seed dressing that obtains according to this method.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN97100468A CN1068762C (en) | 1997-02-18 | 1997-02-18 | Traditional Chinese medicine seed dressing agent and method for preparing same |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN97100468A CN1068762C (en) | 1997-02-18 | 1997-02-18 | Traditional Chinese medicine seed dressing agent and method for preparing same |
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| Publication Number | Publication Date |
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| CN1191079A CN1191079A (en) | 1998-08-26 |
| CN1068762C true CN1068762C (en) | 2001-07-25 |
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| CN97100468A Expired - Fee Related CN1068762C (en) | 1997-02-18 | 1997-02-18 | Traditional Chinese medicine seed dressing agent and method for preparing same |
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| CN1191079A (en) | 1998-08-26 |
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