CN106699941A - 一种萜烯树脂的制备方法 - Google Patents
一种萜烯树脂的制备方法 Download PDFInfo
- Publication number
- CN106699941A CN106699941A CN201611239688.4A CN201611239688A CN106699941A CN 106699941 A CN106699941 A CN 106699941A CN 201611239688 A CN201611239688 A CN 201611239688A CN 106699941 A CN106699941 A CN 106699941A
- Authority
- CN
- China
- Prior art keywords
- terpene resin
- solvent
- preparation
- molecular sieve
- catalyst
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000011347 resin Substances 0.000 title claims abstract description 22
- 229920005989 resin Polymers 0.000 title claims abstract description 22
- 150000003505 terpenes Chemical class 0.000 title claims abstract description 22
- 235000007586 terpenes Nutrition 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 239000003054 catalyst Substances 0.000 claims abstract description 27
- 238000006243 chemical reaction Methods 0.000 claims abstract description 25
- 239000002808 molecular sieve Substances 0.000 claims abstract description 23
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000002904 solvent Substances 0.000 claims abstract description 14
- 239000002994 raw material Substances 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 8
- 239000007822 coupling agent Substances 0.000 claims abstract description 7
- 238000005406 washing Methods 0.000 claims abstract description 7
- 230000008569 process Effects 0.000 claims abstract description 3
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Natural products CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 22
- 239000000203 mixture Substances 0.000 claims description 7
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical group [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims description 4
- 229930006722 beta-pinene Natural products 0.000 claims description 4
- 238000004821 distillation Methods 0.000 claims description 4
- 229910000077 silane Inorganic materials 0.000 claims description 4
- WTARULDDTDQWMU-UHFFFAOYSA-N β-pinene Chemical compound C1C2C(C)(C)C1CCC2=C WTARULDDTDQWMU-UHFFFAOYSA-N 0.000 claims description 4
- 125000003944 tolyl group Chemical group 0.000 claims description 2
- 230000036632 reaction speed Effects 0.000 abstract description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 4
- 239000011149 active material Substances 0.000 description 2
- 238000007792 addition Methods 0.000 description 2
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium chloride Substances Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 2
- 239000006185 dispersion Substances 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 235000019198 oils Nutrition 0.000 description 2
- 238000007086 side reaction Methods 0.000 description 2
- 239000004820 Pressure-sensitive adhesive Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 230000003712 anti-aging effect Effects 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- 150000001555 benzenes Chemical class 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 238000010538 cationic polymerization reaction Methods 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000012943 hotmelt Substances 0.000 description 1
- 230000002209 hydrophobic effect Effects 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 229920000620 organic polymer Polymers 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- CMXPERZAMAQXSF-UHFFFAOYSA-M sodium;1,4-bis(2-ethylhexoxy)-1,4-dioxobutane-2-sulfonate;1,8-dihydroxyanthracene-9,10-dione Chemical compound [Na+].O=C1C2=CC=CC(O)=C2C(=O)C2=C1C=CC=C2O.CCCCC(CC)COC(=O)CC(S([O-])(=O)=O)C(=O)OCC(CC)CCCC CMXPERZAMAQXSF-UHFFFAOYSA-M 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 150000003613 toluenes Chemical class 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F132/00—Homopolymers of cyclic compounds containing no unsaturated aliphatic radicals in a side chain, and having one or more carbon-to-carbon double bonds in a carbocyclic ring system
- C08F132/08—Homopolymers of cyclic compounds containing no unsaturated aliphatic radicals in a side chain, and having one or more carbon-to-carbon double bonds in a carbocyclic ring system having condensed rings
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/02—Carriers therefor
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F4/00—Polymerisation catalysts
- C08F4/06—Metallic compounds other than hydrides and other than metallo-organic compounds; Boron halide or aluminium halide complexes with organic compounds containing oxygen
- C08F4/10—Metallic compounds other than hydrides and other than metallo-organic compounds; Boron halide or aluminium halide complexes with organic compounds containing oxygen of alkaline earth metals, zinc, cadmium, mercury, copper or silver
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
Abstract
Description
Claims (4)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201611239688.4A CN106699941B (zh) | 2016-12-28 | 2016-12-28 | 一种萜烯树脂的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201611239688.4A CN106699941B (zh) | 2016-12-28 | 2016-12-28 | 一种萜烯树脂的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN106699941A true CN106699941A (zh) | 2017-05-24 |
CN106699941B CN106699941B (zh) | 2018-12-14 |
Family
ID=58895651
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201611239688.4A Active CN106699941B (zh) | 2016-12-28 | 2016-12-28 | 一种萜烯树脂的制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN106699941B (zh) |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1709927A (zh) * | 2005-07-08 | 2005-12-21 | 广西大学 | 无色萜烯树脂的制备方法 |
CN104119300A (zh) * | 2014-07-29 | 2014-10-29 | 浙江大学 | 一种α-蒎烯环氧化制备2,3-环氧蒎烷的方法 |
CN104211843A (zh) * | 2014-08-14 | 2014-12-17 | 广西众昌树脂有限公司 | 萜烯树脂的制备方法 |
-
2016
- 2016-12-28 CN CN201611239688.4A patent/CN106699941B/zh active Active
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1709927A (zh) * | 2005-07-08 | 2005-12-21 | 广西大学 | 无色萜烯树脂的制备方法 |
CN104119300A (zh) * | 2014-07-29 | 2014-10-29 | 浙江大学 | 一种α-蒎烯环氧化制备2,3-环氧蒎烷的方法 |
CN104211843A (zh) * | 2014-08-14 | 2014-12-17 | 广西众昌树脂有限公司 | 萜烯树脂的制备方法 |
Also Published As
Publication number | Publication date |
---|---|
CN106699941B (zh) | 2018-12-14 |
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PB01 | Publication | ||
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GR01 | Patent grant | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A preparation method of terpene resin Effective date of registration: 20220314 Granted publication date: 20181214 Pledgee: Puyang Rural Commercial Bank Co.,Ltd. Pledgor: PUYANG BINDER CHEMICAL Co.,Ltd. Registration number: Y2022980002477 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20220627 Granted publication date: 20181214 Pledgee: Puyang Rural Commercial Bank Co.,Ltd. Pledgor: PUYANG BINDER CHEMICAL Co.,Ltd. Registration number: Y2022980002477 |
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PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A kind of preparation method of terpene resin Effective date of registration: 20220815 Granted publication date: 20181214 Pledgee: Puyang Rural Commercial Bank Co.,Ltd. Pledgor: PUYANG BINDER CHEMICAL Co.,Ltd. Registration number: Y2022980012535 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20230808 Granted publication date: 20181214 Pledgee: Puyang Rural Commercial Bank Co.,Ltd. Pledgor: PUYANG BINDER CHEMICAL Co.,Ltd. Registration number: Y2022980012535 |
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PC01 | Cancellation of the registration of the contract for pledge of patent right |