CN106631159A - Preparation method of glazed bricks - Google Patents
Preparation method of glazed bricks Download PDFInfo
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- CN106631159A CN106631159A CN201510718578.5A CN201510718578A CN106631159A CN 106631159 A CN106631159 A CN 106631159A CN 201510718578 A CN201510718578 A CN 201510718578A CN 106631159 A CN106631159 A CN 106631159A
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Abstract
A preparation method of glazed bricks comprises the following steps: A, powder material is uniformly laid in a mold cavity of a lower mold of a stamping mold, and stamped and pressed by an upper mold to obtain a blank body with the surrounding edge ring structure, and a boss is arranged on the stamping surface of the upper mold, and the area of the boss is smaller than the material distribution area of the mold cavity of the lower mold, the edge surrounding ring surrounds on the surface of the blank body to form a material distribution cavity, and the blank body is transferred for later use; B, after the blank body obtained in the step A is dried, glaze is applied to the material distribution cavity, and a decoration glaze layer is formed; C, the blank body with the decoration glaze layer obtained in the step B is put into a kiln for firing and sintering; D, polishing and grinding: the sintered glazed brick is subjected to polishing and grinding, and the glazed brick with the decorative glaze layer is obtained. The thickness of the decoration glaze layer of the glazed brick prepared by the preparation method is increased, the mirror surface effect and the transparency three-dimensional sense are enhanced, and the flatness and integrity of the glaze surface are guaranteed, so that the product quality and the decoration effect of the glazed bricks can be improved.
Description
Technical field
The present invention relates to architectural pottery technical field, more particularly to a kind of preparation method of glazed tile.
Background technology
In the market for existing glazed tile is produced, because its side of base substrate four does not have surrounding edge ring and distribution cavity
Structure, therefore when decorative layer applies cloth glaze, because when glaze mobility is excessive, the thickness of glaze layer cannot spread
Thickness, its thickness generally in below 2mm, and it cannot be guaranteed that glaze surface evenness, or even during glaze is thrown, because
Worry that glaze layer is thrown away for thickness low LCL, it is difficult to the integrity for guaranteeing glaze layer and the appearance for often having ripple glaze.
The existing method being superimposed typically by technique increases the decoration glaze layer of glazed tile, but still cannot carry out
Effectively heap is thick, ultimately results in current glazed tile and there is the mirror effect of its decoration glaze layer and spend third dimension not thoroughly
Foot, the relatively simple defect of decorative effect.
The content of the invention
It is an object of the invention to propose a kind of preparation method of the glazed tile that can increase decoration glazed thickness.
It is that, up to this purpose, the present invention is employed the following technical solutions:
A kind of preparation method of glazed tile, comprises the following steps:
A, powder is uniformly layed in the die cavity of the lower mould of stamping mold, is had by upper punch pressure compacting
The base substrate of surrounding edge ring structure, the stamping surface of the upper mould is provided with boss, and the area of the boss is less than described
The cloth area of the die cavity of lower mould, the surrounding edge ring the base substrate surface loop around formed distribution cavity, transfer
Base substrate is standby;
After B, the body drying for obtaining step A, to its cloth intracavity glazing, decoration glaze layer is formed;
C, the base substrate kiln-firing with decoration glaze layer for being obtained step B, burn till;
D, polishing grinding:By the ceramic tile after burning till, polishing is polished, obtains the ceramic tile with decoration glaze layer.
Illustrate further, the base substrate to suppressing can also make base substrate obtain pattern texture by pattern decorative,
The pattern decorative is the superposition of one or more decorating methods, and the decorating method is silk-screen, cylinder, spray
Ink, cloth glaze, cloth slurry etc., carry out again charity clear frit or transparent glass-ceramics frit after pattern decorative.
Further illustrate, the height of the distribution cavity is 3-10mm.
Preferably, the polishing grinding of step D also includes cutting action, will burn till enclosing for the ceramic tile of acquisition
The cutting of side ring structure is removed.
Preferably, the glazing material in step B is marzacotto, ornamental glaze or feature glaze
In at least one.
Further illustrate, the glazing of step B be divided into two-layer or two-layer more than layering glazing.
Preferably, the base substrate after the compacting of step A is before into step B, by throwing blank process or roll process
The surface of the base substrate is provided with textured pattern.
Preferably, the glazing material in step B be marzacotto, the stamping mold used in step A
The stamping surface of upper mould be additionally provided with textured pattern.
Preferably, before the glazing in step B or during glazing, to cloth intracavity add molten grain or
Ornament, the ornament be burn till after do not burn the decoration particle of mistake.
The distribution cavity is provided with boundary projection, and forms multiple cloth point chambers, institute by the boundary bulge clearance
State the raised height of boundary highly consistent with surrounding edge ring.
Beneficial effects of the present invention:In the glazed tile production of the present invention, the thickness of glaze layer is by cloth during glazing
The height in chamber determines there is certain thickness decoration glaze layer by applying to obtain, it is ensured that the flatness of glaze,
Thickness increase due to decorating glaze layer, enhances the mirror effect of decorative layer and spends third dimension thoroughly, and is throwing
Light is thrown away when polishing without having to worry about glaze layer, it is ensured that the integrity of glaze layer, reduces the appearance of ripple glaze, significantly
Raising ceramic tile product quality and decorative effect.
Description of the drawings
Fig. 1 is the structural representation of the stamping mold of one embodiment of the invention and base substrate;
Fig. 2 is a kind of structural representation of glazed tile of the invention;
Fig. 3 is the structural representation of the glazed tile of multiple embodiments of the invention;
Fig. 4 is a kind of production preparation flow figure of glazed tile of one embodiment of the invention;
Fig. 5 is a kind of production preparation flow figure of glazed tile of one embodiment of the invention;
Wherein:Stamping mold 1, lower mould 11, upper mould 12, base substrate 2, surrounding edge ring 21, distribution cavity 22, point
Boundary's projection 23, cloth point chamber 24, textured pattern 25 decorates glaze layer 3.
Specific embodiment
Further illustrate technical scheme below in conjunction with the accompanying drawings and by specific embodiment.
As shown in figure 1, a kind of preparation method of glazed tile, comprises the following steps:
A, powder is uniformly layed in the die cavity of the lower mould 11 of stamping mold 1, is suppressed by the punching press of upper mould 12
The base substrate 2 with the structure of surrounding edge ring 21 is obtained, the stamping surface of the upper mould 12 is provided with boss, the boss
Area less than the lower mould 11 die cavity cloth area, table of the surrounding edge ring 21 in the base substrate 2
Face ring is standby around distribution cavity 22, transfer base substrate 2 is formed;
B, by step A obtain base substrate 2 be dried after, the glazing into its distribution cavity 22, formed decoration glaze layer
3;
C, the kiln-firing of base substrate 2 with decoration glaze layer 3 for being obtained step B, burn till;
D, polishing grinding:By the ceramic tile after burning till, polishing is polished, obtains the ceramic tile with decoration glaze layer.
In the glazed tile production of the present invention, the base substrate 2 for using has surrounding edge ring 21 and the structure of distribution cavity 22,
The thickness of glaze layer is determined by the height of distribution cavity 22 during glazing, with existing no surrounding edge ring and cloth cavity configuration
Common base substrate compare, the thickness of the glazing layer of common base substrate is maximum to be less than 2mm, and itself and glaze
Proportion or mobility have greatly relatedness, and when glaze mobility is excessive, the thickness of glaze layer cannot spread at all
Thickness, its thickness typically can only achieve 1mm, and in the preparation method of the present invention prepared acquisition glaze layer, its
The proportion or mobility of the minimum thickness and glaze itself of glaze layer is uncorrelated, only with distribution cavity 22 or surrounding edge ring 21
Height correlation, glaze is limited to by surrounding edge ring 21 in the distribution cavity 22 that formed, by charity acquisition
With certain thickness decoration glaze layer 3, because the height of surrounding edge ring 21 is higher than pattern texture peak in surrounding edge
Height, glazing is poured in fluid form in distribution cavity 22, due to the phase between action of gravity and liquid
Melting property, can be very good the glaze surface evenness that ensure that a level;Again by the base substrate 2 with decoration glaze layer 3
The ceramic tile with decoration glaze layer 3 can be obtained after kiln-firing, polishing grinding.The thickness of decoration glaze layer 3 increases
Greatly, enhance the mirror effect of decorative layer and spend third dimension thoroughly, in addition, the thickness of decoration glaze layer increases, throw
Light is thrown away when polishing without having to worry about glaze layer, it is ensured that the integrity of glaze layer, reduces the appearance of ripple glaze, it is ensured that
The flatness in brick face, greatly improves the product quality and decorative effect of ceramic tile.
Further description, the height of the distribution cavity 22 is 3-10mm.The setting of the height of distribution cavity 22
The thickness of decoration glaze layer is determined, therefore the height of distribution cavity is set in 3-10mm, it is ensured that decoration glaze layer
Charity thickness, enhances the mirror effect of decoration glaze layer and spends third dimension thoroughly.
Further description, the polishing grinding of step D also includes cutting action, will burn till acquisition
The structure of surrounding edge ring 21 cutting of ceramic tile is removed.Ceramic tile is set to be prepared into the porcelain similar to the glazed tile structure in market
Brick, its difference is ceramic tile prepared by the present invention, the thickness of the thickness of its decorative layer than original glazed tile
It is big, and the product qualified rate of its production is higher, reduces the appearance of substandard products.
Further description, the glazing material in step B is marzacotto, ornamental glaze or work(
At least one in energy property glaze.Because clear frit has certain light transmission, clear frit is selected to carry out glazing,
Can make brick face that there is certain three-dimensional transparent effect, increased the decorative effect in brick face.
Further description, the glazing of step B be divided into two-layer or two-layer more than layering glazing.Enter
The layering glazing of row two-layer or multilamellar, on the one hand ensures the thickness of glaze layer, it is ensured that the integrity of glaze layer;It is another
Aspect improves the saturating degree third dimension and three-dimensional transparent effect of decoration glaze layer, reduces the appearance of ripple glaze, also protects
The flatness in card brick face.
Further description, step A compacting after base substrate 2 before into step B, by pattern decorative
The surface of the base substrate 2 is provided with textured pattern 25.The pattern decorative is one or more decorating methods
Superposition, the decorating method be silk-screen, cylinder, ink-jet, cloth glaze, cloth slurry etc., after pattern decorative again
Carry out charity clear frit or transparent glass-ceramics frit.
Further description, the glazing material in step B is marzacotto, used in step A
The stamping surface of the upper mould 12 of stamping mold 1 is additionally provided with textured pattern.
Throwing base after the textured pattern design or compacting of the stamping surface of upper mould 12 is processed, and has billet surface
Textured pattern, with reference to certain thickness decoration glaze layer 3, the enhanced visual effect for burning till rear brick face is abundant
The decorative effect of glazed tile.
Further description, before the glazing in step B or during glazing, into distribution cavity 22
Add molten grain or ornament.Add molten grain or ornament using in glaze layer, can increase brick face decorative layer it is many
Sample, so as to improve its decorative effect.
Further description, the ornament be burn till after do not burn the decoration particle of mistake.In distribution cavity 22
Add and melt in solid form grain or ornament, covered by the parcel of clear frit, define the dress of adequate thickness
Decorations layer.Wherein, ornament can be burn till after do not burn the decoration particle of mistake, alternatively mica sheet etc., molten grain can
Think the frit grains different from glaze color, make decoration glaze layer that there is the decorative effect of succinum, form succinum glaze
Layer, glaze is glittering and translucent as succinum, realizes the visual effect as succinum, its thickness up to 3mm or
The glaze layer of more than 3mm, is different from the full throwing glaze of main flow on market, the thick throwing product such as glaze or thin crystallite, increases newly
Ceramic tile with decorative effect as succinum, and it is in process of production, can be prepared according to different demands and be obtained
Obtain different succinum glaze effects, device effect very abundant.
Further description, the distribution cavity 22 is provided with boundary raised 23, and by the boundary raised 23
Interval forms multiple cloth point chambers 24, and the height of the boundary raised 23 is highly consistent with surrounding edge ring 21.
Boundary raised 23 is provided with the inside of distribution cavity 22 and forms multiple cloth point chambers 24, be capable of achieving the cloth of different cavity,
Realize the glazed tile with splicing effect.Boundary raised 23 is provided with the inside of distribution cavity 22 form multiple clothes
Divide chamber 24, be capable of achieving the cloth of different cavity, realize the devitrified glass ceramic tile with splicing effect, in addition, also
Its stitching portion can be cut, brick body is split, be suitable for it is various sizes of install and use, demarcate
Raised 33 design makes its cutting not affect brick face decorative effect.
Embodiment 1
As shown in figure 4, a kind of preparation method of glazed tile:
A, as shown in figure 1, powder is uniformly layed in the die cavity of the lower mould 11 of stamping mold 1, by upper
The punching press of mould 12 compacting obtains the base substrate 2 with surrounding edge ring 21 and structure, and the stamping surface of the upper mould 12 is arranged
There is boss, the area of the boss is less than the cloth area of the die cavity of the lower mould 11, the surrounding edge ring 21
In the surface loop of the base substrate 2 around distribution cavity 22 is formed, the height of its distribution cavity 22 is 6mm, shifts base
Body 2 is standby;
B, the base substrate 2 that step A is obtained is dried after, carry out applying clear frit into its distribution cavity 22, respectively
The layering glazing of 3 times is carried out, its each glazed thickness is 2mm, obtain transparent decoration glaze layer 3;
C, the kiln-firing of base substrate 2 with decoration glaze layer 3 for being obtained step B, burn till;
D, polishing grinding:By the ceramic tile after burning till, polishing is polished, is obtained with printing opacity glaze layer effect
Ceramic tile, as shown in Figure 2.
It is to be appreciated that in step B, in addition to charity marzacotto is selected, it is also an option that decoration
The glazing material of property glaze or feature glaze.
Embodiment 2
A kind of preparation method of the ceramic tile of the printing opacity glaze layer effect with textured pattern:
A, powder is uniformly layed in the die cavity of the lower mould 11 of stamping mold 1, the stamping mold 1 for using
The stamping surface of upper mould 12 be provided with textured pattern, obtained by the punching press of upper mould 12 compacting and there is surrounding edge ring
21 and the base substrate 2 of structure, the stamping surface of the upper mould 12 is provided with boss, and the area of the boss is less than institute
State the cloth area of the die cavity of lower mould 11, the surrounding edge ring 21 the base substrate 2 surface loop around forming cloth
Material chamber 22, the height of its distribution cavity 22 is 8mm, is equipped with the surface of the base substrate 2 by roll process
Textured pattern 25, transfer base substrate 2 is standby;
B, the base substrate 2 that step A is obtained is dried after, carry out applying clear frit into its distribution cavity 22, respectively
The layering glazing of 2 times is carried out, its each glazed thickness is 4mm, obtain transparent decoration glaze layer 3;
C, the kiln-firing of base substrate 2 with decoration glaze layer 3 for being obtained step B, burn till;
D, polishing grinding:By the ceramic tile after burning till, polishing is polished, obtains the printing opacity with textured pattern
The ceramic tile of glaze layer effect.
Embodiment 3
A kind of preparation method of the ceramic tile of the nontransparent glaze layer effect without surrounding edge ring 21:
A, powder is uniformly layed in the die cavity of the lower mould 11 of stamping mold 1, is suppressed by the punching press of upper mould 12
The base substrate 2 with surrounding edge ring 21 and structure is obtained, the stamping surface of the upper mould 12 is provided with boss, described convex
, less than the cloth area of the die cavity of the lower mould 11, the surrounding edge ring 21 is in the base substrate 2 for the area of platform
Around distribution cavity 22 is formed, the height of its distribution cavity 22 is 8mm to surface loop, and transfer base substrate 2 is standby;
B, the base substrate 2 that step A is obtained is dried after, common nontransparent glaze is applied into its distribution cavity 22, point
The layering glazing of 2 times is not carried out, its each glazed thickness is 4mm, obtain decorating glaze layer 3;
C, the kiln-firing of base substrate 2 with decoration glaze layer 3 for being obtained step B, burn till;
D, cutting and polishing grinding:By the ceramic tile after burning till, its surrounding edge ring 21 is cut into removal, re-polishing
Polishing, obtains the ceramic tile of the nontransparent glaze layer effect without surrounding edge ring 21, as shown in Figure 2.
Embodiment 4
As shown in figure 5, a kind of preparation method of the ceramic tile with succinum visual effect:
A, powder is uniformly layed in the die cavity of the lower mould 11 of stamping mold 1, is suppressed by the punching press of upper mould 12
The base substrate 2 with surrounding edge ring 21 and structure is obtained, the stamping surface of the upper mould 12 is provided with boss, described convex
, less than the cloth area of the die cavity of the lower mould 11, the surrounding edge ring 21 is in the base substrate 2 for the area of platform
Around distribution cavity 22 is formed, the height of its distribution cavity 22 is 6mm to surface loop, and transfer base substrate 2 is standby;
B, by step A obtain base substrate 2 be dried after, carry out ground floor into its distribution cavity 22 and apply clear frit,
Ground floor glazed thickness is 2mm, dispenses some molten grains at random in ground floor glaze layer, is carried out again after having dispensed
Clear frit is applied, makes molten grain be located at the inside of whole clearing glaze layer, obtain decoration glaze layer 3;
C, the kiln-firing of base substrate 2 with decoration glaze layer 3 for being obtained step B, burn till;
D, polishing grinding:By the ceramic tile after burning till, polishing is polished, is obtained with succinum visual effect
Ceramic tile, as shown in Figure 2.
Embodiment 5
A kind of preparation method of the glazed tile with splicing effect:
A, powder is uniformly layed in the die cavity of the lower mould 11 of stamping mold 1, the stamping mold 1 for using
The stamping surface of upper mould 12 be provided with textured pattern, obtained by the punching press of upper mould 12 compacting and there is surrounding edge ring
21 and the base substrate 2 of structure, the stamping surface of the upper mould 12 is provided with boss, and the area of the boss is less than institute
State the cloth area of the die cavity of lower mould 11, the surrounding edge ring 21 the base substrate 2 surface loop around forming cloth
Material chamber 22, the height of its distribution cavity 22 is 8mm, and the distribution cavity 22 is partitioned into ripple by boundary raised 23
The cloth of shape shape point chamber 24, the height of the boundary raised 23 is highly consistent with surrounding edge ring 21, by throwing
Blank process is equipped with textured pattern 25 on the surface of the base substrate 2, and transfer base substrate 2 is standby;
B, by step A obtain base substrate 2 be dried after, carry out applying clear frit into its cloth point chamber 24, divide
The layering glazing of 2 times is not carried out, its each glazed thickness is 4mm, obtain transparent decoration glaze layer 3;
C, the kiln-firing of base substrate 2 with decoration glaze layer 3 for being obtained step B, burn till;
D, polishing grinding:By the ceramic tile after burning till, polishing is polished, obtains the throwing glaze with splicing effect
Brick.
Supplementary notes, the boundary raised 23, can be with addition to the cloth point chamber 24 for being partitioned into contoured shape
The cloth point chamber 24 of the various shapes such as grid, hydrosphere, polygon is formed, it is combined with the textured pattern 25,
The glazed tile with splicing effect is realized, the decoration multiformity of glazed tile is increased, as shown in Figure 3.
Further description, the design of its boundary raised 23, by the preparation of a ceramic tile, follow-up paving makes
Used time, segmentation can be carried out to it and be used, strong adaptability.
The know-why of the present invention is described above in association with specific embodiment.These descriptions are intended merely to explain this
The principle of invention, and can not by any way be construed to limiting the scope of the invention.Based on herein
Explain, those skilled in the art associates other tools of the present invention by need not paying performing creative labour
Body embodiment, these modes are fallen within protection scope of the present invention.
Claims (9)
1. a kind of preparation method of glazed tile, it is characterised in that:Comprise the following steps:
A, powder is uniformly layed in the die cavity of the lower mould of stamping mold, is had by upper punch pressure compacting
The base substrate of surrounding edge ring structure;The stamping surface of the upper mould is provided with boss, and the area of the boss is less than described
The cloth area of the die cavity of lower mould, the surrounding edge ring the base substrate surface loop around formed distribution cavity, transfer
Base substrate is standby;
After B, the body drying for obtaining step A, to its cloth intracavity glazing, decoration glaze layer is formed;
C, the base substrate kiln-firing with decoration glaze layer for being obtained step B, burn till;
D, polishing grinding:By the ceramic tile after burning till, polishing is polished, obtains the ceramic tile with decoration glaze layer.
2. a kind of preparation method of glazed tile according to claim 1, it is characterised in that:The distribution cavity
Height be 3-10mm.
3. a kind of preparation method of glazed tile according to claim 1, it is characterised in that:Step D
Polishing grinding also include cutting action, will burn till the ceramic tile of acquisition surrounding edge ring structure cutting remove.
4. a kind of preparation method of glazed tile according to claim 1, it is characterised in that:Step B
In glazing material be at least one in marzacotto, ornamental glaze or feature glaze.
5. a kind of preparation method of glazed tile according to claim 4, it is characterised in that:Step B
Glazing be divided into two-layer or two-layer more than layering glazing.
6. a kind of preparation method of glazed tile according to claim 4, it is characterised in that:Step A is suppressed
Base substrate afterwards is provided with by throwing blank process or roll process before into step B on the surface of the base substrate
Textured pattern.
7. a kind of preparation method of glazed tile according to claim 4, it is characterised in that:Step B
In glazing material be marzacotto, the stamping surface of the upper mould of the stamping mold used in step A is additionally provided with
Textured pattern.
8. a kind of preparation method of glazed tile according to claim 1 or 6 or 7, it is characterised in that:
Before glazing in step B or during glazing, to cloth intracavity molten grain or ornament are added.
9. a kind of preparation method of glazed tile according to claim 1, it is characterised in that:The distribution cavity
It is provided with boundary raised, and multiple cloth point chambers is formed by the boundary bulge clearance.
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CN108298953A (en) * | 2018-01-31 | 2018-07-20 | 佛山市金牛陶瓷有限公司 | The reeded polished bricks production technology of burnishing surface band, mould structure and polished bricks |
CN110451802A (en) * | 2019-08-15 | 2019-11-15 | 蒙娜丽莎集团股份有限公司 | A kind of mica sheet decorative porcelain glazed tile and preparation method thereof |
CN110981552A (en) * | 2019-12-17 | 2020-04-10 | 佛山欧神诺陶瓷有限公司 | Cera flava-imitated ceramic tile and preparation method thereof |
CN110981553A (en) * | 2019-12-17 | 2020-04-10 | 佛山欧神诺陶瓷有限公司 | Transparent amber-like ceramic tile and preparation method thereof |
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CN101747020A (en) * | 2009-06-22 | 2010-06-23 | 陈满坚 | Fambe glaze-polished brick and production method thereof |
CN102775074A (en) * | 2012-08-13 | 2012-11-14 | 广东金牌陶瓷有限公司 | Method for producing microcrystal glass ceramics composite board |
CN104108958A (en) * | 2014-08-01 | 2014-10-22 | 佛山市东鹏陶瓷有限公司 | Microcrystalline glass-ceramic composite panel manufacturing method and product thereof |
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CN1537709A (en) * | 2003-04-17 | 2004-10-20 | 潮 何 | Production technology of polished brick with embedded pattern polished brick manufactural using said technology |
CN101497521A (en) * | 2008-12-25 | 2009-08-05 | 萧华 | Technique of preparing glaze color convexo-concave texture ornamental porcelain brick |
CN101747020A (en) * | 2009-06-22 | 2010-06-23 | 陈满坚 | Fambe glaze-polished brick and production method thereof |
CN102775074A (en) * | 2012-08-13 | 2012-11-14 | 广东金牌陶瓷有限公司 | Method for producing microcrystal glass ceramics composite board |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN108298953A (en) * | 2018-01-31 | 2018-07-20 | 佛山市金牛陶瓷有限公司 | The reeded polished bricks production technology of burnishing surface band, mould structure and polished bricks |
CN110451802A (en) * | 2019-08-15 | 2019-11-15 | 蒙娜丽莎集团股份有限公司 | A kind of mica sheet decorative porcelain glazed tile and preparation method thereof |
CN110451802B (en) * | 2019-08-15 | 2022-02-11 | 蒙娜丽莎集团股份有限公司 | Mica sheet decorative ceramic glazed brick and preparation method thereof |
CN110981552A (en) * | 2019-12-17 | 2020-04-10 | 佛山欧神诺陶瓷有限公司 | Cera flava-imitated ceramic tile and preparation method thereof |
CN110981553A (en) * | 2019-12-17 | 2020-04-10 | 佛山欧神诺陶瓷有限公司 | Transparent amber-like ceramic tile and preparation method thereof |
CN110981553B (en) * | 2019-12-17 | 2021-12-17 | 佛山欧神诺陶瓷有限公司 | Transparent amber-like ceramic tile and preparation method thereof |
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Application publication date: 20170510 |