CN104140296A - Polished crystal tile manufacturing method and polished crystal tile prepared through same - Google Patents

Polished crystal tile manufacturing method and polished crystal tile prepared through same Download PDF

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Publication number
CN104140296A
CN104140296A CN201410378001.XA CN201410378001A CN104140296A CN 104140296 A CN104140296 A CN 104140296A CN 201410378001 A CN201410378001 A CN 201410378001A CN 104140296 A CN104140296 A CN 104140296A
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CN
China
Prior art keywords
manufacture
pit
throwing
brilliant brick
layer
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Pending
Application number
CN201410378001.XA
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Chinese (zh)
Inventor
丘云灵
周燕
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Fengcheng Dongpeng Ceramic Co., Ltd.
Foshan Dongpeng Ceramic Co Ltd
Guangdong Dongpeng Holdings Co Ltd
Original Assignee
FENGCHENG DONGPENG CERAMIC Co Ltd
Foshan Dongpeng Ceramic Co Ltd
Guangdong Dongpeng Holdings Co Ltd
Guangdong Dongpeng Ceramic Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by FENGCHENG DONGPENG CERAMIC Co Ltd, Foshan Dongpeng Ceramic Co Ltd, Guangdong Dongpeng Holdings Co Ltd, Guangdong Dongpeng Ceramic Co Ltd filed Critical FENGCHENG DONGPENG CERAMIC Co Ltd
Priority to CN201410378001.XA priority Critical patent/CN104140296A/en
Publication of CN104140296A publication Critical patent/CN104140296A/en
Pending legal-status Critical Current

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Abstract

The invention relates to a polished crystal tile manufacturing method and a polished crystal tile prepared through the method. The method comprises the following steps that A, raw materials and ingredients are subjected to ball milling, spray granulation and then pressed to form green bricks, and the green bricks are dried; B, the dried green bricks are printed with printing ornament, and then frits are arranged; C, fixing agents are sprayed on frits to fix the frits, and strips of the frits are pressed out through a wale-typed die for adhesive pressing before the fixing agents is dried, so that pits can be formed on the frits; D, firing is conducted; E, fired semi-finished products or only the pits are respectively sprayed and coated with a layer of metallic luster coating, polishing is conducted after drying is conducted, and packaging and warehousing are conducted. Compared with an existing method that the similar types of products are manufactured through metallic luster glaze, the method has the advantages of being high in high-grade rate, low in production cost and the like, and the metallic luster ornament effect is rich and can be predesigned.

Description

A kind of manufacture method of throwing brilliant brick and products thereof
Technical field
The present invention relates to ceramic tile manufacturing technology field, especially relate to a kind of manufacture method of throwing brilliant brick and products thereof.
Background technology
Throwing brilliant brick is devitrified glass to be compounded in to the ceramic tile in printed layer after adobe surface printing, between base substrate and glass-ceramic layer, is provided with pattern, and glass-ceramic layer can protect pattern to present good decorative effect by refraction and the transmission of light simultaneously.Because decoration, high temperature under its glaze burn till, glaze exquisiteness, noble magnificent, belong to high-grade decorative product, be more and more subject to liking of human consumer, thereby market sales volume is increasing.
For the abundant decorative effect of throwing brilliant brick, the brilliant brick product of throwing with metalluster progressively occurs, but prior art is while being combined with due to metal glaze and frit, produces melting meeting and allow metal glaze spread out under frit high temperature, and metal ion is difficult to assemble, be just difficult to produce metalluster.Therefore existing company fixture has the brilliant brick yield rate of throwing of metalluster low, and production cost is high, and waste is serious.
Summary of the invention
The object of the invention is to propose a kind of manufacture method of throwing brilliant brick, it can solve the problem that prior art is difficult to produce metalluster, and process stabilizing, and yield rate is high.
For reaching this object, the present invention by the following technical solutions:
A manufacture method of throwing brilliant brick, step comprises successively:
A, ceramic powder compacting is formed to adobe dry;
B, in dried adobe printing ornament, then cloth frit;
C, spray fixing agent are fixed frit, and extrude lines at the mould of the not dry front burr with moulding of fixing agent, make frit layer occur pit; Or first adopt the mould of burr to extrude lines, then spray fixing agent;
D, burn till;
E, on the work in-process that bake, or only in pit, spraying layer of metal gloss paint, polishing after drying, packaging warehouse-in.
Described printing ornament in described step B is screen printing, roller printing, one or more combinations in ink-jet printed.Certainly, preferably screen printing and ink-jet printed combining, is difficult to process the layout that gray scale is higher because ink-jet printed, mode by screen printing complementary color can finely address this problem, and then obtaining high gray scale, resolving power is high, the effect of pattern exquisiteness.
The PVA solution that described fixing agent in described step C is 0.01%-0.1%.Can certainly select the aqueous solution of carboxymethyl cellulose.
Described pit depth in described step C is 1-4mm, is preferably 2-3mm.Cross shallowly, in the time of melting, because the glassy phase of frit melting flows and pit is filled and led up, in the time of polishing, also can damage the metallized coating at pit simultaneously; Cross deeply, easily damage printed layer pattern.
Described metallized coating fineness in described step e is more than or equal to 300 orders.Coating fineness is excessively slightly not easy with glass-ceramic layer compound, easily layering.
Described metallized coating viscosity in described step e is 200-500cps.Suitable viscosity is also for metallized coating can be applied preferably, and compound in glass-ceramic layer.
Described oven dry in described step e for to dry 10-20 minute at 200-300 DEG C.By drying, can allow metallized coating fixing on brick face rapidly, and it is better compound that metallized coating and brick face are done.
Described metallized coating fraction of coverage in described step e is 7.5-9m 2/ kg.Fraction of coverage is too low, and metalluster is not obvious, and fraction of coverage is too high, and the coating forming is thicker, in follow-up use, easily ftractures.
Compared with prior art, the present invention's precompressed before firing forms pit, and metallic paint is sprayed in pit, matt after having avoided the metal glaze that brings firing front upper metal glaze in prior art to disperse to fire, the problem bad with frit adaptability, resultant metal texture is strong, glossiness is high, and metal can be mutually compound with crystallite texture, the harmony of brick face, expressive force is strong.And yield rate raising, manufacturing cost also decreases.
Another object of the present invention is to propose the brilliant brick of a kind of throwing of being manufactured by aforesaid method, and it from bottom to top comprises end base layer, ornament layer and glass coating successively.
Further, in the brilliant brick of throwing of manufacturing at aforesaid method, base layer thickness of the described end is 8-10mm.
Further, in the brilliant brick of throwing of manufacturing at aforesaid method, described decorative layer thickness 0.1-0.5mm.
Further, in the brilliant brick of throwing of manufacturing at aforesaid method, described glass coating thickness 0.5-3mm.
Further, in the brilliant brick of throwing of manufacturing at aforesaid method, on described glass coating, be provided with pit.
Further, in the brilliant brick of throwing of manufacturing at aforesaid method, described pit depth is 1-4mm.
Further, in the brilliant brick of throwing of manufacturing at aforesaid method, the internal surface of described pit has metalluster layer.
Further, in the brilliant brick of throwing of manufacturing at aforesaid method, described pit size, deep mixed.
Brief description of the drawings
Fig. 1 is the schematic cross-section that carries out unfired brick structure variation in process of the manufacture method of the brilliant brick of throwing of one of them embodiment of the present invention.
Drawing reference numeral: 1-end base layer 1; 2-printed layer; 3-frit layer; 31-pit; 4-glass coating; 5-metalluster layer.
Embodiment
Further illustrate technical scheme of the present invention below by embodiment.
Embodiment 1
As shown in Figure 1, it from bottom to top comprises that end base layer 1, printed layer 2 and glass coating 4, glass coating surface arrangement have pit 31 to the brilliant brick of a kind of throwing successively, has layer of metal gloss layer 5 on described pit 31 surfaces.
Referring to the appended flow process signal of Fig. 1; Select the ceramic tile that preparation specification is 1000 × 1000mm, its blank raw material is for known taking feldspar, clay, sand etc. as main raw material in the industry, be aided with again other auxiliary materials such as talcum, certainly, can also add according to actual needs a zirconium silicate brightening or coloured ceramic body stain.
Particularly, with reference to Fig. 1, its manufacture method comprises the steps:
A, feed proportioning ball milling is carried out after mist projection granulating to (ceramic powder) compacting form adobe the dry end base layer 1 that forms;
B, first form frit layer 3 by forming the rear cloth frit of printed layer 2 by spray ink Printing stamp again after screen printing; Here the frit that used is preferably transparent or semitransparent frit, and what select in the present embodiment is clear frit;
The PVA solution fixing agent of C, spray content 0.01% is fixed, and extrudes lines at the mould of the not dry front burr with moulding of fixing agent, makes clear frit layer occur the deep mixed of degree of depth 1-4mm, pit 31 not of uniform size;
D, burn till; Under oxidizing atmosphere, in roller kiln, burn till with 1100~1250 DEG C, firing period is 90-120 minute;
E, be 500cps in the interior spraying one deck of work in-process pit 31 fineness 300 mesh screen residues 0, the viscosity that bake, spraying fraction of coverage 9m 2the metallized coating of/kg is dried polishing after 10 minutes at 280 DEG C, packaging warehouse-in.
Certainly, also can be on whole brick face metallize gloss paint, by top layer jettisoning, only retain the interior part of pit 31 by polishing.Just can waste like this metallized coating.
Metallized coating described here refers to by fluoro-resin, high-quality color stuffing, auxiliary agent, solidifying agent etc. and forms; Wherein contain lemel, therefore have metalluster, different metal group branches present different colours, and for example aluminium or silver can present silver color or silver gray, and gold can present golden yellow.
By regulating known parameter (base substrate cloth amount, stamp is the consumption of stamp-pad ink used and ink, the consumption of frit charity etc., these parameters are that those skilled in the art can carry out suitably adjusting as required), at the bottom of the brilliant brick of throwing of the present embodiment after firing, base layer 1 thickness is 8mm, printed layer 2 thickness are 0.3mm, and glass coating 4 thickness are 0.5mm.
The present embodiment precompressed before firing forms pit 31, and metallic paint is sprayed in pit 31, matt after having avoided the metal glaze that brings firing front upper metal glaze in prior art to disperse to fire, the problem bad with frit adaptability, resultant metal texture is strong, and glossiness is high, and metal can be mutually compound with crystallite texture, the harmony of brick face, expressive force is strong.
Produce the brilliant brick of throwing with metalluster effect by this method, excellence rate is more than 85%; And adopt traditional method of executing metal-lustrous glaze, and because the dissemination of frit in the time of melting obtains product effect and cannot reach expection, excellence rate is only 40% left and right, and waste is serious, and production cost is high.
Embodiment 2
With reference to accompanying drawing 1, in this enforcement, manufacturing specification is the brilliant brick of throwing of 1000 × 1000mm, and its manufacturing process in turn includes the following steps:
A, feed proportioning ball milling is carried out to compacting after mist projection granulating form adobe the dry end base layer 1 that forms;
B, form the rear cloth clear frit of printed layer 2 by roller printing and form clear frit layer 3;
The PVA solution fixing agent of C, spray content 0.1% is fixed, and extrudes lines at the mould of the not dry front burr with moulding of fixing agent, makes frit layer 3 occur the deep mixed of degree of depth 1-3mm, pit 31 not of uniform size;
D, burn till; Under oxidizing atmosphere, in roller kiln, burn till with 1100~1250 DEG C, firing period is 90-120 minute;
E, be 200cps in the interior spraying one deck of work in-process pit 31 fineness 300 mesh screen residues 0, the viscosity that bake, spraying fraction of coverage 7.5m 2the metallized coating of/kg is dried polishing after 20 minutes at 200 DEG C, packaging warehouse-in.
The metallized coating of selecting in this enforcement is golden metallic luster coating.Certainly,, in application, in order to obtain the more effect of horn of plenty, the metallized coating collocation of multiple color can be used.
By regulating known parameter, brilliant its end base layer 1 thickness of brick of the throwing of the present embodiment is 10mm; Printed layer 2 thickness 0.1mm; Glass coating 4 thickness are 3mm.
It is 87% that the metalluster that after burning prepared by statistics this method is thrown brilliant brick excellence rate.
Embodiment 3
With reference to accompanying drawing 1, in this enforcement, manufacturing specification is the brilliant brick of throwing of 1000 × 1000mm, and its manufacturing process in turn includes the following steps:
A, feed proportioning ball milling is carried out to compacting after mist projection granulating form adobe the dry end base layer 1 that forms;
B, form the rear cloth clear frit of printed layer 2 by spray ink Printing stamp, roller printing, screen printing successively and form clear frit layer 3;
The PVA solution fixing agent of C, spray content 0.08% is fixed, and extrudes lines at the mould of the not dry front burr with moulding of fixing agent, makes frit layer occur the deep mixed of degree of depth 1-4mm, pit 31 not of uniform size;
D, burn till; Under oxidizing atmosphere, in roller kiln, burn till with 1100~1250 DEG C, firing period is 90-120 minute;
E, in the work in-process pit baking, spray one deck fineness 450 mesh screen residues 0, viscosity is 400cps, spraying fraction of coverage 8m 2the metallized coating of/kg is dried polishing after 15 minutes at 250 DEG C, packaging warehouse-in.
Its end base layer 1 thickness is 9mm; Printed layer 2 thickness 0.5mm, glass coating 4 thickness are 1.5mm.
Embodiment 4
With reference to accompanying drawing 1, in this enforcement, manufacturing specification is the brilliant brick of throwing of 1000 × 1000mm, and its manufacturing process in turn includes the following steps:
A, feed proportioning ball milling is carried out to compacting after mist projection granulating form adobe the dry end base layer 1 that forms;
B, form the rear cloth clear frit of printed layer 2 by spray ink Printing stamp and form clear frit layer 3;
The mould of the burr of C, use moulding extrudes lines, makes frit layer 3 occur the deep mixed of degree of depth 1-3mm, pit 31 not of uniform size; The PVA solution fixing agent that sprays again content 0.07% is fixed;
D, burn till; Under oxidizing atmosphere, in roller kiln, burn till with 1100~1250 DEG C, firing period is 90-120 minute;
E, in the work in-process pit baking, spray one deck fineness 350 mesh screen residues 0, viscosity is 380cps, spraying fraction of coverage 8.5m 2the metallized coating of/kg is dried polishing after 20 minutes at 280 DEG C, packaging warehouse-in.
The metalluster that after burning prepared by statistics this method is thrown brilliant brick excellence rate and is exceeded 75%.
Embodiment 5
With reference to accompanying drawing 1, in this enforcement, manufacturing specification is the brilliant brick of throwing of 1000 × 1000mm, and its manufacturing process in turn includes the following steps:
A, feed proportioning ball milling is carried out to compacting after mist projection granulating form adobe the dry end base layer 1 that forms;
B, form the rear cloth clear frit of printed layer 2 by roller printing and form clear frit layer 3;
The PVA solution fixing agent of C, spray content 0.05% is fixed, and extrudes lines at the mould of the not dry front burr with moulding of fixing agent, makes frit layer 3 occur the deep mixed of degree of depth 2-4mm, pit 31 not of uniform size;
D, burn till; Under oxidizing atmosphere, in roller kiln, burn till with 1100~1250 DEG C, firing period is 90-120 minute;
E, in the work in-process pit baking, spray one deck fineness 350 mesh screen residues 0, viscosity is 380cps, spraying fraction of coverage 8m 2the metallized coating of/kg is dried polishing after 15 minutes at 280 DEG C, packaging warehouse-in.
The present invention is after charity frit, become lines in frit layer top roll swaging, after burning till, metallize gloss paint at brick face or in the pit of depression lines only roll extrusion being formed again, acquisition has the brilliant brick product of throwing of metalluster, dissemination to metal-lustrous glaze during because of frit melting when having solved traditional technology and using metal-lustrous glaze, and be difficult to obtain the technical problem of metalluster effect.
The advantages such as it is high that the brilliant brick of throwing that the solution of the present invention is prepared metal lustre decorative effect has excellence rate, and production cost is low, and metal lustre decorative effect is abundant, can design in advance.
In above embodiment, the metallized coating using is all purchased from Ding Xusheng novel material Science and Technology Ltd. of Foshan City, needs explanation here, and the analogous products that other company produces on the market can be suitable for.
Know-why of the present invention has below been described in conjunction with specific embodiments.These are described is in order to explain principle of the present invention, and can not be interpreted as by any way limiting the scope of the invention.Based on explanation herein, those skilled in the art does not need to pay performing creative labour can associate other embodiment of the present invention, within these modes all will fall into protection scope of the present invention.

Claims (10)

1. a manufacture method of throwing brilliant brick, is characterized in that, step comprises successively:
A, ceramic powder compacting is formed to adobe dry;
B, in dried adobe printing ornament, then cloth frit;
C, spray fixing agent are fixed frit, and extrude lines at the mould of the not dry front burr with moulding of fixing agent, make frit layer occur pit; Or first adopt the mould of burr to extrude lines, then spray fixing agent;
D, burn till;
E, on the whole surface of the work in-process that bake, or only in pit, spray layer of metal gloss paint, polishing after drying, packaging warehouse-in.
2. a kind of manufacture method of throwing brilliant brick according to claim 1, is characterized in that: the described printing ornament in described step B is one or more combinations in screen printing, roller printing, spray ink Printing stamp.
3. a kind of manufacture method of throwing brilliant brick according to claim 1, is characterized in that: the PVA solution that the described fixing agent in described step C is 0.01%-0.1%.
4. a kind of manufacture method of throwing brilliant brick according to claim 1, is characterized in that: the described pit depth in described step C is 1-4mm.
5. a kind of manufacture method of throwing brilliant brick according to claim 1, is characterized in that: the described metallized coating fineness in described step e is more than or equal to 300 orders.
6. a kind of manufacture method of throwing brilliant brick according to claim 1, is characterized in that: the described metallized coating viscosity in described step e is 200-500cps.
7. a kind of manufacture method of throwing brilliant brick according to claim 1, is characterized in that: the described oven dry in described step e for to dry 10-20 minute at 200-300 DEG C.
8. a kind of manufacture method of throwing brilliant brick according to claim 1, is characterized in that: the described metallized coating fraction of coverage in described step e is 7.5-9m 2/ kg.
9. according to the product of a kind of manufacture method manufacturing of throwing brilliant brick described in any one in claim 1-8, it is characterized in that: it from bottom to top comprises end base layer, printed layer and glass coating successively; Described glass coating is provided with pit, and the internal surface of described pit is provided with metalluster layer.
10. product according to claim 9 is characterized in that: base layer thickness of the described end is 8-10mm; Described decorative layer thickness 0.1-0.5mm; Described glass depth 0.5-3mm; Described pit depth is 1-4mm.
CN201410378001.XA 2014-08-01 2014-08-01 Polished crystal tile manufacturing method and polished crystal tile prepared through same Pending CN104140296A (en)

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104909828A (en) * 2015-06-19 2015-09-16 浙江根根陶瓷有限公司 Inner wall crystal-polishing mirror surface ceramic chip and manufacturing method thereof
CN105218171A (en) * 2015-09-22 2016-01-06 浙江根根陶瓷有限公司 A kind of manufacture method with metal glossy layer inner wall ceramic chip
CN106320622A (en) * 2016-08-08 2017-01-11 佛山市东鹏陶瓷有限公司 Ceramic tile formed by dry pressure slip casting and production method thereof
CN107902905A (en) * 2017-11-29 2018-04-13 佛山市华力达材料科技有限公司 A kind of production technology of ceramic tile
CN107902900A (en) * 2017-11-15 2018-04-13 蒙娜丽莎集团股份有限公司 Wrap up shape dry granular glaze, parcel shape dry granular glaze cloth ashlar brick and preparation method thereof

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1644559A (en) * 2004-10-13 2005-07-27 陈满坚 Metal plated and polished ceramic products and their manufacture
CN101497521A (en) * 2008-12-25 2009-08-05 萧华 Technique of preparing glaze color convexo-concave texture ornamental porcelain brick
CN102390931A (en) * 2011-08-02 2012-03-28 佛山石湾鹰牌陶瓷有限公司 Method for manufacturing once calcined glass ceramic brick

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1644559A (en) * 2004-10-13 2005-07-27 陈满坚 Metal plated and polished ceramic products and their manufacture
CN101497521A (en) * 2008-12-25 2009-08-05 萧华 Technique of preparing glaze color convexo-concave texture ornamental porcelain brick
CN102390931A (en) * 2011-08-02 2012-03-28 佛山石湾鹰牌陶瓷有限公司 Method for manufacturing once calcined glass ceramic brick

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104909828A (en) * 2015-06-19 2015-09-16 浙江根根陶瓷有限公司 Inner wall crystal-polishing mirror surface ceramic chip and manufacturing method thereof
CN104909828B (en) * 2015-06-19 2017-04-05 浙江根根陶瓷有限公司 A kind of interior wall throws brilliant minute surface ceramics and its manufacture method
CN105218171A (en) * 2015-09-22 2016-01-06 浙江根根陶瓷有限公司 A kind of manufacture method with metal glossy layer inner wall ceramic chip
CN106320622A (en) * 2016-08-08 2017-01-11 佛山市东鹏陶瓷有限公司 Ceramic tile formed by dry pressure slip casting and production method thereof
CN106320622B (en) * 2016-08-08 2019-01-04 佛山市东鹏陶瓷有限公司 A kind of Ceramic Tiles and its production method of dry-pressing injection forming
CN107902900A (en) * 2017-11-15 2018-04-13 蒙娜丽莎集团股份有限公司 Wrap up shape dry granular glaze, parcel shape dry granular glaze cloth ashlar brick and preparation method thereof
CN107902900B (en) * 2017-11-15 2021-03-19 蒙娜丽莎集团股份有限公司 Wrapped dry particle glaze, wrapped dry particle glaze cloth stone-like brick and preparation method thereof
CN107902905A (en) * 2017-11-29 2018-04-13 佛山市华力达材料科技有限公司 A kind of production technology of ceramic tile

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