CN106614820A - Composition for preventing and treating anthracnose of spinach - Google Patents

Composition for preventing and treating anthracnose of spinach Download PDF

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Publication number
CN106614820A
CN106614820A CN201611041236.5A CN201611041236A CN106614820A CN 106614820 A CN106614820 A CN 106614820A CN 201611041236 A CN201611041236 A CN 201611041236A CN 106614820 A CN106614820 A CN 106614820A
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China
Prior art keywords
parts
composition
preventing
spinach
portions
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CN201611041236.5A
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Chinese (zh)
Inventor
戴加国
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Wa Chicken Breeding Farmers' Professional Cooperatives In Bengbu City
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Wa Chicken Breeding Farmers' Professional Cooperatives In Bengbu City
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Priority to CN201611041236.5A priority Critical patent/CN106614820A/en
Publication of CN106614820A publication Critical patent/CN106614820A/en
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    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/40Liliopsida [monocotyledons]
    • A01N65/42Aloeaceae [Aloe family] or Liliaceae [Lily family], e.g. aloe, veratrum, onion, garlic or chives

Abstract

The invention discloses a composition for preventing and treating anthracnose of spinach, and belongs to the technical field of pesticide. The composition is prepared from the following materials: fructus cannabis, morinda officinalis, silybum marianum, radix polygonati officinalis, folium artemisiae argyi, pomegranate bark, microcos paniculata, grape seeds, wild chrysanthemum flowers, ovate leaf holly bark and auxiliaries. The components of the composition are matched reasonably, the prepared traditional Chinese medicine has stable quality, bactericidal active components are diversified, the fact that pathogenic bacteria generate medicine resistance can be effectively avoided, medicine residue and damage to the environment are avoided, the prevention and treatment rate reaches above 90 percent, the use value is high, and the vitamin content of the cultivated spinach is remarkably increased.

Description

A kind of composition of preventing and treating spinach anthracnose
Technical field
The invention belongs to technical field of pesticide, and in particular to a kind of composition of preventing and treating spinach anthracnose.
Background technology
Spinach(Spinacia oleracea L.)Also known as Persian dish, red root vegetables, parrot dish etc., category Chenopodiaceae spinach category, one Year raw herbaceous plant.Plant is high, and up to 1 meter, root is coniform, redly, less for white, leaf halberd shape to avette, emerald green, entirely Edge has minority tooth shape sliver.Spinach has the title of " nutrition model student ", it rich in carotenoid, vitamin C, vitamin K, Mineral matter(Calcareous, irony etc.), the various nutrients such as Co-Q10.With blood-nourishing, hemostasis, the moon is held back, the effect moisturized.Can prevent and treat Bleeding from five sense organs or subcutaneous tissue, has blood in stool, scurvy, quenches one's thirst and draws drink, defecate not smooth etc..Spinach originates in Iran, and China generally cultivates, and is extremely common vegetables One of.
Anthracnose is a kind of disease common when spinach is planted, if preventing and treating is unfavorable to cause significantly underproduction consequence.It is now to adopt more Prevented and treated with chemical pesticide preparation, but medicament residue can be caused, also have pollution to environment, it is long-term to apply also produce disease resistance.Have People attempts being prevented and treated with Chinese herbal medicine, but he arranges in pairs or groups it is unreasonable the problems such as, cause prevent and treat effect on driving birds is not good.
The content of the invention
The present invention is intended to provide a kind of composition of preventing and treating spinach anthracnose.
The present invention is achieved through the following technical solutions:
A kind of composition of preventing and treating spinach anthracnose, is made up of the material of following weight portion:
10 ~ 14 parts of fructus cannabis, 8 ~ 12 parts of Morinda officinalis, 4 ~ 7 portions of milk thistles, 6 ~ 9 portions of radix polygonati officinalis, 14 ~ 16 portions of tarragons, 5 ~ 7 parts of granatums, 3 ~ 6 parts of buzhayes, 2 ~ 4 parts of grape pips, 5 ~ 8 parts of mother chrysanthemums, 3 ~ 5 parts of iron holly barks, 2 ~ 4 parts of auxiliary agents;The auxiliary agent is by following weight The material of part is made:3 ~ 5 parts of tourmaline, 4 ~ 6 parts of serpentines, 2 ~ 4 parts of stone needles.
Preferably, it is made up of the material of following weight portion:
12 parts of fructus cannabis, 10 parts of Morinda officinalis, 5 portions of milk thistles, 8 portions of radix polygonati officinalis, 15 portions of tarragons, 6 parts of granatums, 5 parts of buzhayes, 3 parts Grape pip, 6 parts of mother chrysanthemums, 4 parts of iron holly barks, 3 parts of auxiliary agents;The auxiliary agent is made up of the material of following weight portion:4 parts of tourmaline, 5 Part serpentine, 3 parts of stone needles.
A kind of preparation method of the composition of preventing and treating spinach anthracnose, comprises the steps:
(1)It is put in the marmite for filling wheat bran after fructus cannabis, granatum and grape pip are mixed, the temperature in heating holding pot is 96 ~ 100 DEG C, take out after the 32 ~ 36min of process that constantly stir-fries, 120 mesh are crossed after then being crushed, and to obtain mixture A standby;
(2)Tarragon, buzhaye and mother chrysanthemum are put in the acetum that mass fraction is 5% after 0.5 ~ 1h of immersion treatment jointly Take out, clear water rinses rear drying and crushing well and crosses 100 mesh to obtain mixture B standby;
(3)It is put in the marmite for filling the seed of Job's tears after Morinda officinalis, milk thistle, radix polygonati officinalis and iron holly bark are mixed, heating is kept in pot Temperature is 110 ~ 115 DEG C, is taken out after the 28 ~ 32min of process that constantly stir-fries, and 150 mesh are crossed after then being crushed, and to obtain mixture C standby With;
(4)Mixture A obtained by above-mentioned steps, mixture B, mixture C are mixed jointly, the body of 12 times of its gross mass is placed into Fraction is that in 80% ethanol solution, it is 5.0 ~ 6.0 to adjust solution ph, keeps solution temperature to be 90 ~ 95 DEG C, constantly backflow 6 ~ 7h of extraction, then filters extract, and extract is transferred in vacuum decompressioning and concentrating tank, and the temperature for controlling to distill is 55 ~ 60 DEG C, obtain concentrated extract standby;
(5)Temperature will be put into after tourmaline, serpentine and stone needle jointly mixing for 1 ~ 2h of calcination processing under conditions of 400 ~ 440 DEG C After take out, 600 mesh sieves are crossed after crushing, and to obtain auxiliary agent standby;
(6)By step(4)300 mesh are crossed after the concentrated extract drying and crushing of gained, then same step(5)The auxiliary agent of gained is common After being well mixed.
Further, step(4)Described in vacuum decompressioning and concentrating tank in vacuum degree control be 0.01 ~ 0.015MPa.
Further, step(6)In to temperature during concentrated extract dried process be 70 ~ 75 DEG C.
The present invention has the advantages that:
The present invention has carried out rational collocation on the basis of substantial amounts of practical studies to Chinese herbal medicine not of the same race, and first it is carried out Corresponding frying, acidleach etc. are processed, and can reduce harmful toxic matter composition, improve the property of medicine, improve mutual effect, and just Operate in follow-up alcohol extracting;The auxiliary agent of addition has good infrared, ultrasonic, negative ions radiation characteristic, can promote the suction of spinach Characteristic is received, strengthens the physique of spinach, strengthen the performance of the efficacy of a drug, improve overall prevention effect.In the common with cooperation of each composition With under, the obtained Chinese medicine stay in grade of the present invention, fungicide active ingredient is various, can be prevented effectively from germ and produce drug resistance, together When do not result in again medicament residue, harm environment, control rate is up to more than 90%, and use value is higher, and in the spinach for educating dimension life The content of element is improved significantly.
Specific embodiment
Embodiment 1
A kind of composition of preventing and treating spinach anthracnose, is made up of the material of following weight portion:
10 parts of fructus cannabis, 8 parts of Morinda officinalis, 4 parts of milk thistles, 6 parts of radix polygonati officinalis, 14 parts of tarragons, 5 parts of granatums, 3 parts of buzhayes, 2 parts of Portugals Grape seed, 5 parts of mother chrysanthemums, 3 parts of iron holly barks, 2 parts of auxiliary agents;The auxiliary agent is made up of the material of following weight portion:3 parts of tourmaline, 4 parts Serpentine, 2 parts of stone needles.
A kind of preparation method of the composition of preventing and treating spinach anthracnose, comprises the steps:
(1)It is put in the marmite for filling wheat bran after fructus cannabis, granatum and grape pip are mixed, the temperature in heating holding pot is 98 ~ 100 DEG C, take out after the process 35min that constantly stir-fries, 120 mesh are crossed after then being crushed, and to obtain mixture A standby;
(2)Tarragon, buzhaye and mother chrysanthemum are put in the acetum that mass fraction is 5% jointly and are taken after immersion treatment 0.8h Go out, clear water rinses rear drying and crushing well and crosses 100 mesh to obtain mixture B standby;
(3)It is put in the marmite for filling the seed of Job's tears after Morinda officinalis, milk thistle, radix polygonati officinalis and iron holly bark are mixed, heating is kept in pot Temperature is 110 ~ 112 DEG C, is taken out after the process 30min that constantly stir-fries, and 150 mesh are crossed after then being crushed, and to obtain mixture C standby;
(4)Mixture A obtained by above-mentioned steps, mixture B, mixture C are mixed jointly, the body of 12 times of its gross mass is placed into Fraction is that in 80% ethanol solution, it is 5.5 ~ 6.0 to adjust solution ph, keeps solution temperature to be 93 DEG C, constantly backflow extraction 6.5h, then filters extract, and extract is transferred in vacuum decompressioning and concentrating tank, and the temperature for controlling to distill is 58 DEG C, obtains dense Contracting extract is standby;
(5)Temperature will be put into after tourmaline, serpentine and stone needle jointly mixing to take after calcination processing 1.5h under conditions of 420 DEG C Go out, 600 mesh sieves are crossed after crushing, and to obtain auxiliary agent standby;More preferably, synergy is more preferable for the radiation characteristic of each material after calcination processing;
(6)By step(4)300 mesh are crossed after the concentrated extract drying and crushing of gained, then same step(5)The auxiliary agent of gained is common After being well mixed.
Further, step(4)Described in vacuum decompressioning and concentrating tank in vacuum degree control be 0.01MPa.
Further, step(6)In to temperature during concentrated extract dried process be 73 DEG C.
Embodiment 2
A kind of composition of preventing and treating spinach anthracnose, is made up of the material of following weight portion:
12 parts of fructus cannabis, 10 parts of Morinda officinalis, 5 portions of milk thistles, 8 portions of radix polygonati officinalis, 15 portions of tarragons, 6 parts of granatums, 5 parts of buzhayes, 3 parts Grape pip, 6 parts of mother chrysanthemums, 4 parts of iron holly barks, 3 parts of auxiliary agents;The auxiliary agent is made up of the material of following weight portion:4 parts of tourmaline, 5 Part serpentine, 3 parts of stone needles.Remaining method and step is with embodiment 1.
Embodiment 3
A kind of composition of preventing and treating spinach anthracnose, is made up of the material of following weight portion:
14 parts of fructus cannabis, 12 parts of Morinda officinalis, 7 portions of milk thistles, 9 portions of radix polygonati officinalis, 16 portions of tarragons, 7 parts of granatums, 6 parts of buzhayes, 4 parts Grape pip, 8 parts of mother chrysanthemums, 5 parts of iron holly barks, 4 parts of auxiliary agents;The auxiliary agent is made up of the material of following weight portion:5 parts of tourmaline, 6 Part serpentine, 4 parts of stone needles.Remaining method and step is with embodiment 1.
Comparative example 1
This comparative example 1 saves compared with Example 1, in preparation process step(1)、(2)、(3), i.e., each composition do not entered The special pretreatment of row, method and step all same in addition.
Comparative example 2
This comparative example 2 compared with Example 2, does not contain auxiliary agent in its composition, method and step all same in addition.
Control group 1
The existing chemical agent for the preventing and treating of spinach anthracnose.
Control group 2
The existing Chinese medicine for the preventing and treating of spinach anthracnose.
In order to contrast effect of the present invention, from " spinach is miscellaneous No. 10 " kind spinach as plantation research object, by experimental plot point For eight pieces, one group as blank control group, remaining is prevented and treated respectively with the corresponding reagent of above-mentioned seven kinds of modes, and statistics is continuous The prevention effect of 3 years, correction data is as shown in table 1 below:
Table 1
First Year relative control effect rate(%) Second Year relative control effect rate(%) 3rd year relative control effect rate(%)
Embodiment 1 92 91 92
Embodiment 2 93 93 92
Embodiment 3 90 91 91
Comparative example 1 79 78 80
Comparative example 2 75 73 74
Control group 1 90 82 78
Control group 2 68 65 66
By upper table 1 as can be seen that the obtained Chinese medicine of the present invention is preferable for the prevention effect of spinach anthracnose, and Long-Time Service Also be not in problem that chemical agent effect is gradually reduced, do not pollute the environment again, use value is higher.
The ripe spinach that embodiment 2, comparative example 1, comparative example 2, control group 1 and control group 2 are produced is carried out Quality Detection, correction data is as shown in table 2 below:
Table 2
Vitamin C content in spinach(mg/100g) Vitamin C content in spinach(mg/100g)
Embodiment 2 59.4 3.22
Comparative example 1 41.2 2.11
Comparative example 2 37.6 1.82
Control group 1 28.1 1.47
Control group 2 30.2 1.56
There is special lifting effect to the content of spinach vitamin by can be seen that the made composition of the present invention in upper table 2, changing Its edibility has been apt to it, added benefit is higher.

Claims (5)

1. it is a kind of preventing and treating spinach anthracnose composition, it is characterised in that be made up of the material of following weight portion:
10 ~ 14 parts of fructus cannabis, 8 ~ 12 parts of Morinda officinalis, 4 ~ 7 portions of milk thistles, 6 ~ 9 portions of radix polygonati officinalis, 14 ~ 16 portions of tarragons, 5 ~ 7 parts of granatums, 3 ~ 6 parts of buzhayes, 2 ~ 4 parts of grape pips, 5 ~ 8 parts of mother chrysanthemums, 3 ~ 5 parts of iron holly barks, 2 ~ 4 parts of auxiliary agents;The auxiliary agent is by following weight The material of part is made:3 ~ 5 parts of tourmaline, 4 ~ 6 parts of serpentines, 2 ~ 4 parts of stone needles.
2. it is according to claim 1 it is a kind of preventing and treating spinach anthracnose composition, it is characterised in that by following weight portion Material is made:
12 parts of fructus cannabis, 10 parts of Morinda officinalis, 5 portions of milk thistles, 8 portions of radix polygonati officinalis, 15 portions of tarragons, 6 parts of granatums, 5 parts of buzhayes, 3 parts Grape pip, 6 parts of mother chrysanthemums, 4 parts of iron holly barks, 3 parts of auxiliary agents;The auxiliary agent is made up of the material of following weight portion:4 parts of tourmaline, 5 Part serpentine, 3 parts of stone needles.
3. it is a kind of it is as claimed in claim 1 or 2 preventing and treating spinach anthracnose composition preparation method, it is characterised in that bag Include following steps:
(1)It is put in the marmite for filling wheat bran after fructus cannabis, granatum and grape pip are mixed, the temperature in heating holding pot is 96 ~ 100 DEG C, take out after the 32 ~ 36min of process that constantly stir-fries, 120 mesh are crossed after then being crushed, and to obtain mixture A standby;
(2)Tarragon, buzhaye and mother chrysanthemum are put in the acetum that mass fraction is 5% after 0.5 ~ 1h of immersion treatment jointly Take out, clear water rinses rear drying and crushing well and crosses 100 mesh to obtain mixture B standby;
(3)It is put in the marmite for filling the seed of Job's tears after Morinda officinalis, milk thistle, radix polygonati officinalis and iron holly bark are mixed, heating is kept in pot Temperature is 110 ~ 115 DEG C, is taken out after the 28 ~ 32min of process that constantly stir-fries, and 150 mesh are crossed after then being crushed, and to obtain mixture C standby With;
(4)Mixture A obtained by above-mentioned steps, mixture B, mixture C are mixed jointly, the body of 12 times of its gross mass is placed into Fraction is that in 80% ethanol solution, it is 5.0 ~ 6.0 to adjust solution ph, keeps solution temperature to be 90 ~ 95 DEG C, constantly backflow 6 ~ 7h of extraction, then filters extract, and extract is transferred in vacuum decompressioning and concentrating tank, and the temperature for controlling to distill is 55 ~ 60 DEG C, obtain concentrated extract standby;
(5)Temperature will be put into after tourmaline, serpentine and stone needle jointly mixing for 1 ~ 2h of calcination processing under conditions of 400 ~ 440 DEG C After take out, 600 mesh sieves are crossed after crushing, and to obtain auxiliary agent standby;
(6)By step(4)300 mesh are crossed after the concentrated extract drying and crushing of gained, then same step(5)The auxiliary agent of gained is common After being well mixed.
4. it is according to claim 3 it is a kind of preventing and treating spinach anthracnose composition preparation method, it is characterised in that step (4)Described in vacuum decompressioning and concentrating tank in vacuum degree control be 0.01 ~ 0.015MPa.
5. it is according to claim 3 it is a kind of preventing and treating spinach anthracnose composition preparation method, it is characterised in that step (6)In to temperature during concentrated extract dried process be 70 ~ 75 DEG C.
CN201611041236.5A 2016-11-24 2016-11-24 Composition for preventing and treating anthracnose of spinach Pending CN106614820A (en)

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107372623A (en) * 2017-08-01 2017-11-24 河南柏裕植物免疫科技有限公司 Bitter rot or anthracnose of grape vaccine
CN108056117A (en) * 2017-12-23 2018-05-22 全椒县潘林园林葡萄专业合作社 A kind of control method of bitter rot or anthracnose of grape
CN108849996A (en) * 2018-07-25 2018-11-23 松桃鑫山农业科技开发有限公司 A method of preventing radix pseudostellariae leaf spot
CN110786199A (en) * 2019-11-26 2020-02-14 宾川县云福农副产品加工有限责任公司 Citrus planting method

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102784350A (en) * 2012-08-07 2012-11-21 孙雅儒 Mite killing bactericide and preparation method of mite killing bactericide
CN104982469A (en) * 2015-06-26 2015-10-21 安徽禾众农业科技有限公司 Method for controlling strawberry anthracnose

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102784350A (en) * 2012-08-07 2012-11-21 孙雅儒 Mite killing bactericide and preparation method of mite killing bactericide
CN104982469A (en) * 2015-06-26 2015-10-21 安徽禾众农业科技有限公司 Method for controlling strawberry anthracnose

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107372623A (en) * 2017-08-01 2017-11-24 河南柏裕植物免疫科技有限公司 Bitter rot or anthracnose of grape vaccine
CN108056117A (en) * 2017-12-23 2018-05-22 全椒县潘林园林葡萄专业合作社 A kind of control method of bitter rot or anthracnose of grape
CN108849996A (en) * 2018-07-25 2018-11-23 松桃鑫山农业科技开发有限公司 A method of preventing radix pseudostellariae leaf spot
CN110786199A (en) * 2019-11-26 2020-02-14 宾川县云福农副产品加工有限责任公司 Citrus planting method

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Application publication date: 20170510