CN106009487B - 一种酚醛树脂基复合材料的制备方法 - Google Patents
一种酚醛树脂基复合材料的制备方法 Download PDFInfo
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- CN106009487B CN106009487B CN201610531363.7A CN201610531363A CN106009487B CN 106009487 B CN106009487 B CN 106009487B CN 201610531363 A CN201610531363 A CN 201610531363A CN 106009487 B CN106009487 B CN 106009487B
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- calcium sulfate
- oyster shell
- shell whiting
- phenolic resin
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- 239000002131 composite material Substances 0.000 title claims abstract description 32
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N phenol group Chemical group C1(=CC=CC=C1)O ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 title claims description 21
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 claims abstract description 68
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims abstract description 54
- 241000276489 Merlangius merlangus Species 0.000 claims abstract description 52
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 claims abstract description 38
- 229910000077 silane Inorganic materials 0.000 claims abstract description 38
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 33
- 229920001568 phenolic resin Polymers 0.000 claims abstract description 26
- 239000013078 crystal Substances 0.000 claims abstract description 24
- 239000005011 phenolic resin Substances 0.000 claims abstract description 23
- KXGFMDJXCMQABM-UHFFFAOYSA-N 2-methoxy-6-methylphenol Chemical compound [CH]OC1=CC=CC([CH])=C1O KXGFMDJXCMQABM-UHFFFAOYSA-N 0.000 claims abstract description 22
- 150000001875 compounds Chemical class 0.000 claims abstract description 21
- 238000001035 drying Methods 0.000 claims abstract description 19
- 238000007731 hot pressing Methods 0.000 claims abstract description 19
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 19
- 238000003756 stirring Methods 0.000 claims abstract description 19
- 239000002351 wastewater Substances 0.000 claims abstract description 19
- 239000002002 slurry Substances 0.000 claims abstract description 11
- 239000000725 suspension Substances 0.000 claims abstract description 11
- 238000000227 grinding Methods 0.000 claims abstract description 10
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 32
- 239000008367 deionised water Substances 0.000 claims description 23
- 229910021641 deionized water Inorganic materials 0.000 claims description 23
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 18
- 230000004048 modification Effects 0.000 claims description 12
- 238000012986 modification Methods 0.000 claims description 12
- 239000012065 filter cake Substances 0.000 claims description 9
- 238000001291 vacuum drying Methods 0.000 claims description 8
- 239000000843 powder Substances 0.000 claims description 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N 1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylic acid Chemical compound C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims 1
- 239000007822 coupling agent Substances 0.000 claims 1
- 235000015170 shellfish Nutrition 0.000 claims 1
- 239000011734 sodium Substances 0.000 claims 1
- 229910052708 sodium Inorganic materials 0.000 claims 1
- 238000005406 washing Methods 0.000 abstract description 9
- 238000001816 cooling Methods 0.000 abstract 3
- 238000001914 filtration Methods 0.000 abstract 2
- 235000013824 polyphenols Nutrition 0.000 description 22
- 235000019441 ethanol Nutrition 0.000 description 7
- 238000005452 bending Methods 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 239000004033 plastic Substances 0.000 description 3
- 229920003023 plastic Polymers 0.000 description 3
- 239000004927 clay Substances 0.000 description 2
- 239000004035 construction material Substances 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000011159 matrix material Substances 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 229920005989 resin Polymers 0.000 description 2
- 239000011347 resin Substances 0.000 description 2
- 229920000818 Catalin Polymers 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- OKPNYGAWTYOBFZ-UHFFFAOYSA-N Pirenoxine Chemical compound C12=NC3=CC=CC=C3OC2=CC(=O)C2=C1C(=O)C=C(C(=O)O)N2 OKPNYGAWTYOBFZ-UHFFFAOYSA-N 0.000 description 1
- 208000037656 Respiratory Sounds Diseases 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 229910000019 calcium carbonate Inorganic materials 0.000 description 1
- IKRMZAOEXULJQX-UHFFFAOYSA-N calcium;3,7-dioxido-2,4,6,8,9-pentaoxa-1,3,5,7-tetraborabicyclo[3.3.1]nonane Chemical compound [Ca+2].O1B([O-])OB2OB([O-])OB1O2 IKRMZAOEXULJQX-UHFFFAOYSA-N 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- XFQYJNINHLZMIU-UHFFFAOYSA-N cataline Natural products CN1CC(O)C2=CC(OC)=C(OC)C3=C2C1CC1=C3C=C(OC)C(OC)=C1 XFQYJNINHLZMIU-UHFFFAOYSA-N 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 239000000805 composite resin Substances 0.000 description 1
- 239000012777 electrically insulating material Substances 0.000 description 1
- 239000002657 fibrous material Substances 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 238000007373 indentation Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- -1 phenolic aldehyde Chemical class 0.000 description 1
- 229910052615 phyllosilicate Inorganic materials 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 238000004080 punching Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 229920001187 thermosetting polymer Polymers 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K13/00—Use of mixtures of ingredients not covered by one single of the preceding main groups, each of these compounds being essential
- C08K13/06—Pretreated ingredients and ingredients covered by the main groups C08K3/00 - C08K7/00
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/04—Ingredients treated with organic substances
- C08K9/06—Ingredients treated with organic substances with silicon-containing compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C43/00—Compression moulding, i.e. applying external pressure to flow the moulding material; Apparatus therefor
- B29C43/32—Component parts, details or accessories; Auxiliary operations
- B29C43/58—Measuring, controlling or regulating
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K5/00—Use of organic ingredients
- C08K5/04—Oxygen-containing compounds
- C08K5/09—Carboxylic acids; Metal salts thereof; Anhydrides thereof
- C08K5/098—Metal salts of carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
- C08K7/02—Fibres or whiskers
- C08K7/04—Fibres or whiskers inorganic
- C08K7/08—Oxygen-containing compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/02—Ingredients treated with inorganic substances
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/04—Ingredients treated with organic substances
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C43/00—Compression moulding, i.e. applying external pressure to flow the moulding material; Apparatus therefor
- B29C43/32—Component parts, details or accessories; Auxiliary operations
- B29C43/58—Measuring, controlling or regulating
- B29C2043/5808—Measuring, controlling or regulating pressure or compressing force
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29C—SHAPING OR JOINING OF PLASTICS; SHAPING OF MATERIAL IN A PLASTIC STATE, NOT OTHERWISE PROVIDED FOR; AFTER-TREATMENT OF THE SHAPED PRODUCTS, e.g. REPAIRING
- B29C43/00—Compression moulding, i.e. applying external pressure to flow the moulding material; Apparatus therefor
- B29C43/32—Component parts, details or accessories; Auxiliary operations
- B29C43/58—Measuring, controlling or regulating
- B29C2043/5816—Measuring, controlling or regulating temperature
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/24—Acids; Salts thereof
- C08K3/26—Carbonates; Bicarbonates
- C08K2003/265—Calcium, strontium or barium carbonate
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3045—Sulfates
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2203/00—Applications
- C08L2203/30—Applications used for thermoforming
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- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Phenolic Resins Or Amino Resins (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
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CN201610531363.7A CN106009487B (zh) | 2015-03-24 | 2015-03-24 | 一种酚醛树脂基复合材料的制备方法 |
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CN201610531363.7A CN106009487B (zh) | 2015-03-24 | 2015-03-24 | 一种酚醛树脂基复合材料的制备方法 |
CN201510130001.2A CN104725769B (zh) | 2015-03-24 | 2015-03-24 | 一种酚醛树脂基复合材料的制备方法 |
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CN201610531589.7A Expired - Fee Related CN106009488B (zh) | 2015-03-24 | 2015-03-24 | 一种酚醛树脂基复合材料的制取方法 |
CN201610531761.9A Active CN106009489B (zh) | 2015-03-24 | 2015-03-24 | 酚醛树脂基复合材料的制造方法 |
CN201610531363.7A Active CN106009487B (zh) | 2015-03-24 | 2015-03-24 | 一种酚醛树脂基复合材料的制备方法 |
CN201610531352.9A Active CN106009485B (zh) | 2015-03-24 | 2015-03-24 | 一种酚醛树脂基复合材料的制作方法 |
CN201610531358.6A Active CN106147120B (zh) | 2015-03-24 | 2015-03-24 | 酚醛树脂基复合材料的制作方法 |
CN201610531345.9A Active CN106084640B (zh) | 2015-03-24 | 2015-03-24 | 一种酚醛树脂基复合材料的制造方法 |
CN201610531360.3A Active CN106009486B (zh) | 2015-03-24 | 2015-03-24 | 酚醛树脂基复合材料的制备方法 |
CN201510130001.2A Active CN104725769B (zh) | 2015-03-24 | 2015-03-24 | 一种酚醛树脂基复合材料的制备方法 |
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CN201610531761.9A Active CN106009489B (zh) | 2015-03-24 | 2015-03-24 | 酚醛树脂基复合材料的制造方法 |
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CN201610531358.6A Active CN106147120B (zh) | 2015-03-24 | 2015-03-24 | 酚醛树脂基复合材料的制作方法 |
CN201610531345.9A Active CN106084640B (zh) | 2015-03-24 | 2015-03-24 | 一种酚醛树脂基复合材料的制造方法 |
CN201610531360.3A Active CN106009486B (zh) | 2015-03-24 | 2015-03-24 | 酚醛树脂基复合材料的制备方法 |
CN201510130001.2A Active CN104725769B (zh) | 2015-03-24 | 2015-03-24 | 一种酚醛树脂基复合材料的制备方法 |
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Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
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CN106928648B (zh) * | 2017-04-20 | 2020-05-22 | 北京石油化工学院 | 一种晶须增强增韧无卤阻燃酚醛泡沫塑料及其制备方法 |
CN107760122B (zh) * | 2017-10-24 | 2020-08-11 | 广东工业大学 | 一种外墙用干粉涂料及其制备方法 |
CN108034220A (zh) * | 2018-01-25 | 2018-05-15 | 杨秀枝 | 一种低介电常数电子复合材料的制备方法及其应用 |
CN108904889A (zh) * | 2018-07-31 | 2018-11-30 | 合肥华盖生物科技有限公司 | 一种骨用仿生材料的制备方法 |
CN109337112B (zh) * | 2018-09-14 | 2021-06-04 | 晋江瑞碧科技有限公司 | 硫酸钙晶须/密胺树脂空心球材料的制备方法及其用途 |
CN109134941A (zh) * | 2018-10-05 | 2019-01-04 | 张青美 | 改性蛤蜊壳粉及其在橡胶材料中的应用 |
CN108911690A (zh) * | 2018-10-17 | 2018-11-30 | 合肥隆扬环保科技有限公司 | 一种节能环保型保温材料及其制备方法 |
CN111825885A (zh) * | 2019-04-15 | 2020-10-27 | 王叶训 | 纳米贝壳粉塑料锭的制作方法 |
CN112480715A (zh) * | 2020-12-08 | 2021-03-12 | 深圳市锦昊辉实业发展有限公司 | 一种改性重质碳酸钙及其制备方法、应用 |
CN115140751B (zh) * | 2022-07-29 | 2023-06-30 | 山东理工大学 | 高纯氢氧化铝的制备方法 |
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CN1392196A (zh) * | 2001-06-18 | 2003-01-22 | 中国科学院化学研究所 | 一种酚醛树脂/粘土纳米复合材料的制备方法 |
CN1475520A (zh) * | 2002-08-15 | 2004-02-18 | 孙建宁 | 贝壳微粉填料及其用途 |
CN102212204A (zh) * | 2011-05-16 | 2011-10-12 | 刘立文 | 一种改性无水硫酸钙及其制备方法 |
CN102816500A (zh) * | 2012-09-10 | 2012-12-12 | 浙江大学 | 一种抗霉的环氧树脂组合物 |
CN102924864A (zh) * | 2012-11-27 | 2013-02-13 | 北京立高防水工程有限公司 | 改性环保酚醛保温材料及其制备方法 |
CN103571246A (zh) * | 2013-10-28 | 2014-02-12 | 浙江大学舟山海洋研究中心 | 一种替代玻璃鳞片用于海洋重防腐涂料的贝壳珍珠层片层材料的制备方法 |
CN103571235A (zh) * | 2013-10-28 | 2014-02-12 | 浙江大学舟山海洋研究中心 | 一种棱柱状生物碳酸钙的制备方法 |
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2015
- 2015-03-24 CN CN201610531589.7A patent/CN106009488B/zh not_active Expired - Fee Related
- 2015-03-24 CN CN201610531761.9A patent/CN106009489B/zh active Active
- 2015-03-24 CN CN201610531363.7A patent/CN106009487B/zh active Active
- 2015-03-24 CN CN201610531352.9A patent/CN106009485B/zh active Active
- 2015-03-24 CN CN201610531358.6A patent/CN106147120B/zh active Active
- 2015-03-24 CN CN201610531345.9A patent/CN106084640B/zh active Active
- 2015-03-24 CN CN201610531360.3A patent/CN106009486B/zh active Active
- 2015-03-24 CN CN201510130001.2A patent/CN104725769B/zh active Active
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CN1392196A (zh) * | 2001-06-18 | 2003-01-22 | 中国科学院化学研究所 | 一种酚醛树脂/粘土纳米复合材料的制备方法 |
CN1475520A (zh) * | 2002-08-15 | 2004-02-18 | 孙建宁 | 贝壳微粉填料及其用途 |
CN102212204A (zh) * | 2011-05-16 | 2011-10-12 | 刘立文 | 一种改性无水硫酸钙及其制备方法 |
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CN102924864A (zh) * | 2012-11-27 | 2013-02-13 | 北京立高防水工程有限公司 | 改性环保酚醛保温材料及其制备方法 |
CN103571246A (zh) * | 2013-10-28 | 2014-02-12 | 浙江大学舟山海洋研究中心 | 一种替代玻璃鳞片用于海洋重防腐涂料的贝壳珍珠层片层材料的制备方法 |
CN103571235A (zh) * | 2013-10-28 | 2014-02-12 | 浙江大学舟山海洋研究中心 | 一种棱柱状生物碳酸钙的制备方法 |
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CN106147120A (zh) | 2016-11-23 |
CN106009486A (zh) | 2016-10-12 |
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CN106009485B (zh) | 2017-10-31 |
CN104725769B (zh) | 2016-08-24 |
CN106009487A (zh) | 2016-10-12 |
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CN106084640B (zh) | 2017-10-31 |
CN106147120B (zh) | 2017-10-31 |
CN106009488B (zh) | 2017-10-31 |
CN106009489A (zh) | 2016-10-12 |
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