CN105997678A - Washing and care two-in-one infant shower gel - Google Patents
Washing and care two-in-one infant shower gel Download PDFInfo
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- CN105997678A CN105997678A CN201610473889.4A CN201610473889A CN105997678A CN 105997678 A CN105997678 A CN 105997678A CN 201610473889 A CN201610473889 A CN 201610473889A CN 105997678 A CN105997678 A CN 105997678A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/49—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing heterocyclic compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The invention relates to a washing and care two-in-one infant shower gel. The washing and care two-in-one infant shower gel is prepared from, by weight, an anionic surfactant 6-10%, a nonionic surfactant 6-10%, an amphoteric ionic surfactant 6-10%, an amino acid surfactant 10-30%, an emulsifier 0.1-1%, glycerin 0.1-1%, an argania spinosa kernel extract 0.1-1%, avocado tree fruit oil 0.1-1%, citric acid 0.1-0.5%, sodium chloride 0.1-1%, disodium ethylenediamine tetraacetic acid 0.01-0.1%, methylisothiazolinone 0.05-0.1%, essence 0.005-0.2% and the balance water. The washing and care two-in-one infant shower gel is mild in nature, has very low skin and eye irritation and sensitivity, can gently clean the baby skin and effectively keep infant skin soft and smooth and has a remarkable moisturizing effect.
Description
Technical field
The present invention relates to daily chemicals technical field, be specifically related to one and wash and protect two-in-one baby shower gel.
Background technology
Along with increase and the socio-economic development paces of China's annual neonate birth quantity are accelerated, Chinese Infant and Children washing product city
Field scale constantly expands.High security, high-effect, high stability and high performance-price ratio have become current infant washing product formula
The outstanding feature of technology.
Bath product is only second to a large consumer goods of class of hair shampoo article as consumption figure in washing product, typically by several gentleness
Surfactant and a certain amount of emollient, suds booster, thickening agent, solubilizing agent, antioxidant, preservative and essence composition.
Traditional bath product majority has only played basic cleaning action and has acted on the moisturizing of part, refrigerant, antipruritic etc., it is impossible to very well
The effect playing skin protection.And bath product formula major part on the market is to develop for the skin characteristic of adult,
Therefore infant it is not particularly suited for.
The skin of infant differs widely with adult, and its skin is the thinnest, and the most sensitive, highly fragile, skin barrier function is still
Incomplete development, fails to resist the impact of external environment.Simultaneously because the brain of infant, nervous system and other organs are still
Being in the stage of development, its skin is easier to osmotic absorption chemical substance than the skin of adult, so the chemistry the least on adult's impact
The growth of infant all can be impacted by material.Therefore, the head of a family choose infant wash protect product time often special concern product
Safety, mildness and zest.
Bath product in the market can be divided into soap base type, surfactant type, compound three classes.Soap base type bath gel uses
Rear the most sticky, use in the winter time and easily produce the sensation that skin is tight, be dried, moistness is poor.Surfactant type is taken a shower
Dew mostly is anionic surfactant, owing to this type of SURFACTANT ADSORPTION is relatively strong, has soapy feeling, make people easy after crossing water
Produce the sensation not washed clean, and bigger to the zest of skin and eyes.Compound bath gel is many with plant extract, gentleness
Type surfactant compound is made, and has the advantages that clear property is good, it is easy to cross the water capacity, gentleness is moistened, represents the development trend of bath gel.
Chinese patent application 201510950299.1 discloses a kind of bath dew for baby, and this bath gel is made up of following raw material of preparing: coconut palm
Olein, cocos nucifera oil acyl methyl taurine sodium sulfonate, Flos Lonicerae, Fructus Citri Limoniae, glycerol, Methylisothiazolinone, Aloe is extracted
Thing, Lac Bovis seu Bubali, decyl glucoside, plant Flos Matricariae chamomillae, natural propolis, Olive oil quintessence and water.This bath gel character is gentle, clearly
Clean property is good, and can strengthen skin natural resistance, safe and reliable.
Summary of the invention
For solving the problem that prior art exists, it is an object of the invention to provide a kind of have clean and the washing of moist double effects
Protecting two-in-one baby shower gel, described baby shower gel character is gentle, to skin and the zest of eyes and sensitivity pole
Low, can effectively maintain the softness of infant skin and smooth, moisturizing effect is notable, and can effectively prevent infant sebum skin
Scorching, the generation of miliaria, safety is high.
The present invention is by following technical solution to be attained in that
One is washed and is protected two-in-one baby shower gel, is made up of the raw material of preparing of following percentage by weight meter:
Anionic surfactant 6～10%, nonionic surfactant 6～10%, amphoteric ionic surfactant
6～10%, amino acid type surfactant 10～30%, emulsifying agent 0.1～1%, glycerol 0.1～1%, thorn A Gan tree core extract
0.1～1%, Butyrospermum parkii fruit fatty oil 0.1～1%, citric acid 0.1～0.5%, sodium chloride 0.1～1%, disodiumedetate
0.01～0.1%, Methylisothiazolinone 0.05～0.1%, essence 0.005～0.2%, surplus is water；
Described anionic surfactant is sodium laureth sulfate or mono sulfosuccinates；Described nonionic
Type surfactant is Coco-Glucoside or decyl glucoside；Described amphoteric ionic surfactant is that cocamidopropyl propyl amide is sweet
Dish alkali；Described amino acid type surfactant is sodium cocoyl glycinate, Disodium N-Coco acy-L-Glutamate, lauroyl collagenous amino
At least one in acid TEA salt, sodium lauroyl sarcosine；
Described emulsifying agent is the one in glycerol caprylate class, glycerol decanoate class, Natrulon H-10 esters.
Preferably, two-in-one baby shower gel is protected in described washing, and is made up of the raw material of preparing of following percentage by weight meter:
Anionic surfactant 8%, nonionic surfactant 8%, amphoteric ionic surfactant 7%, amino
Acid type surfactant 16%, emulsifying agent 0.5%, glycerol 0.5%, thorn A Gan tree core extract 0.4%, Butyrospermum parkii fruit fat
Oil 0.5%, citric acid 0.3%, sodium chloride 0.1%, disodiumedetate 0.05%, Methylisothiazolinone 0.1%,
Essence 0.01%, surplus is water；
Described anionic surfactant is mono sulfosuccinates；Described nonionic surfactant is cocoyl
Glucoside；Described amphoteric ionic surfactant is cocamido propyl betaine；Described amino acid type surfactant is coconut palm
Oleoyl Glycine sodium, Disodium N-Coco acy-L-Glutamate, lauroyl collagen amino acid TEA salt and the mixing of sodium lauroyl sarcosine
Thing；
Described emulsifying agent is Natrulon H-10 oleate.
Further, described amino acid type surfactant is sodium cocoyl glycinate, Disodium N-Coco acy-L-Glutamate, lauroyl
Collagen amino acid TEA salt, sodium lauroyl sarcosine are with (0.4～1): (0.4～1): (0.2～0.6): the weight ratio composition of (0.1～0.4).
Preferably, described amino acid type surfactant is sodium cocoyl glycinate, Disodium N-Coco acy-L-Glutamate, lauroyl glue
Original acid TEA salt, sodium lauroyl sarcosine form with the weight ratio of 0.5:0.5:0.4:0.2.
Further, described wash that to protect the pH value of two-in-one baby shower gel be 5.5～6.5.
Additionally, the present invention also provides for a kind of described washing the preparation method protecting two-in-one baby shower gel, comprise the following steps:
(1) toward addition disodiumedetate, mono sulfosuccinates in water, warming while stirring to 85 DEG C,
It is incubated 30 minutes so that it is be completely dissolved；
(2) it is cooled to 65 DEG C, adds Coco-Glucoside, cocamido propyl betaine, sodium cocoyl glycinate, cocos nucifera oil
Acyl disodium glutamate, sodium lauroyl sarcosine and Natrulon H-10 oleate, insulated and stirred 20 minutes is to being completely dissolved；
(3) it is cooled to 45 DEG C, is sequentially added into glycerol, lauroyl collagen amino acid TEA salt, stirs, carry out height
Pressure homogenizing processes, and obtains solution A；
(4) toward solution A add in advance with water dissolution citric acid completely, stir, be sequentially added into thorn A Gan tree core extraction
Thing, Butyrospermum parkii fruit fatty oil, Methylisothiazolinone, sodium chloride and essence, stir, carry out cryogenic high pressure homogenizing process,
Obtain baby shower gel.
Further, high pressure homogenize in described step (3) processes particularly as follows: at 40～45 DEG C, under conditions of 60～80MPa
Homogenizing 3～6min.
Further, cryogenic high pressure homogenizing in described step (4) processes particularly as follows: at 15 DEG C, the condition of 40～50MPa
Lower homogenizing 5～10min；Then homogenizing 2～4min under conditions of 15～20MPa.
Thorn A Gan tree core extract of the present invention is commercially available prod (being purchased from Chemyunion, article No. CN072-0518),
Described thorn A Gan tree core extract contains abundant vitamin E and unsaturated fatty acid, has stronger oxidation resistance,
There is anti-sebum, anti-acne and effect of calm skin simultaneously, the lipid barrier of skin can be repaired.
Described Butyrospermum parkii fruit fatty oil is commercially available prod (being purchased from Li Meida Fine Chemical Co., Ltd, article No. ZJF-01200420),
It contains fat and fatty acid etc., has potent moist moisturizing effect, has stronger absorbability to ultraviolet, have good
Skin protection, anti-sunlight function, additionally, containing substantial amounts of not saponification composition, make skin soft, smooth.
Essence of the present invention is selected exclusively for child's safe essence used for cosmetic, meets IFRA standard.Described essence can
To select Flos Matricariae chamomillae, Flos Inulae, lavandula angustifolia odor type, there is help infant and loosen just before going to bed, the feature releived, it is possible to
To select fruital odor type, such as Fructus Fragariae Ananssae, fragrant citrus, Fructus Musae etc., fresh and sweet berry breath, soft aroma and, a kind of comfortable to people
Sensation.Essence of the present invention is preferably Flos Matricariae chamomillae, Flos Inulae, lavandula angustifolia odor type, but is not limited solely to described selection.
Compared with prior art, present invention have an advantage that
(1) of the present invention washing is protected two-in-one baby shower gel and is contained several amino acids surfactant, and character is gentle,
Extremely low to skin and the zest of eyes and sensitivity, to baby's more safety care, make the most pearlescent gentleness of baby's skin pure
Only, and by adding thorn A Gan tree core extract, Butyrospermum parkii fruit fatty oil adacrya formula, ultimate attainment pure, careful foam, gentle
Ground cleaning baby's skin.
(2) of the present invention wash that to protect two-in-one baby shower gel be micro-acid pH, close to baby's sebum film acidity, more
Adding pro-skin, moisten moisturizing again, can effectively maintain the softness of infant skin and smooth, moisturizing effect is notable, and can be the most pre-
Anti-Infant acrodermatitis, the generation of miliaria, safety is high.
(3) material such as surfactant, emulsifying agent is carried out high pressure homogenize process by the present invention in advance at a higher temperature, makes
Emulsifying agent and surfactant refine fully, dissolve and mix, and beneficially bath gel produces and enriches and the foam of exquisiteness, improves
Dirt-removing power；Use cryogenic high pressure homogenizing to process technique to be prepared, make surfactant rapid adsorption extract in thorn A Gan tree core
Thing, the interface between Butyrospermum parkii fruit fatty oil and water, form spatial stability layer, prevent from stinging the vitamin in A Gan tree core extract
The oil-phase component conglomerates such as E, unsaturated fatty acid and Butyrospermum parkii fruit fatty oil, are formed dispersed, clear appearance, stream
The bath gel that dynamic property is good, low temperature also advantageously improves the stability of bath gel.
Detailed description of the invention
Further describe the present invention below by way of detailed description of the invention, but the present invention is not limited only to following example.
Embodiment 1 washes the preparation protecting two-in-one baby shower gel
Two-in-one baby shower gel is protected in washing of the embodiment of the present invention 1, is made up of the raw material of preparing of following percentage by weight meter:
Mono sulfosuccinates 8%, Coco-Glucoside 8%, cocamido propyl betaine 7%, the sweet ammonia of cocos nucifera oil acyl
Acid sodium 5%, Disodium N-Coco acy-L-Glutamate 5%, lauroyl collagen amino acid TEA salt 4%, sodium lauroyl sarcosine 2%,
Natrulon H-10 oleate 0.5%, glycerol 0.5%, thorn A Gan tree core extract 0.4%, Butyrospermum parkii fruit fatty oil 0.5%, Fructus Citri Limoniae
Acid 0.3%, sodium chloride 0.1%, disodiumedetate 0.05%, Methylisothiazolinone 0.1%, Flos Matricariae chamomillae essence 0.01%,
Surplus is water.
Preparation method:
(1) toward addition disodiumedetate, mono sulfosuccinates in water, warming while stirring to 85 DEG C,
It is incubated 30 minutes so that it is be completely dissolved；
(2) it is cooled to 65 DEG C, adds Coco-Glucoside, cocamido propyl betaine, sodium cocoyl glycinate, cocos nucifera oil
Acyl disodium glutamate, sodium lauroyl sarcosine and Natrulon H-10 oleate, insulated and stirred 20 minutes is to being completely dissolved；
(3) it is cooled to 45 DEG C, is sequentially added into glycerol, lauroyl collagen amino acid TEA salt, stirs, at 45 DEG C,
Homogenizing 5min under conditions of 70MPa, obtains solution A；
(4) toward solution A add in advance with water dissolution citric acid completely, stir, be sequentially added into thorn A Gan tree core extraction
Thing, Butyrospermum parkii fruit fatty oil, Methylisothiazolinone, sodium chloride and essence, stir, at 15 DEG C, and the bar of 45MPa
Homogenizing 8min under part；Then homogenizing 3min under conditions of 15MPa, obtains baby shower gel.
Embodiment 2 washes the preparation protecting two-in-one baby shower gel
Two-in-one baby shower gel is protected in washing of the embodiment of the present invention 2, is made up of the raw material of preparing of following percentage by weight meter:
Mono sulfosuccinates 6%, decyl glucoside 10%, cocamido propyl betaine 7%, the sweet ammonia of cocos nucifera oil acyl
Acid sodium 6%, Disodium N-Coco acy-L-Glutamate 5%, lauroyl collagen amino acid TEA salt 3% and sodium lauroyl sarcosine 2%,
Natrulon H-10 oleate 0.6%, glycerol 0.4%, thorn A Gan tree core extract 0.6%, Butyrospermum parkii fruit fatty oil 0.4%, Fructus Citri Limoniae
Acid 0.4%, sodium chloride 0.2%, disodiumedetate 0.06%, Methylisothiazolinone 0.1%, lavandula angustifolia essence 0.01%,
Surplus is water.
Preparation method is with embodiment 1.
Embodiment 3 washes the preparation protecting two-in-one baby shower gel
Two-in-one baby shower gel is protected in washing of the embodiment of the present invention 3, is made up of the raw material of preparing of following percentage by weight meter:
Mono sulfosuccinates 10%, Coco-Glucoside 6%, cocamido propyl betaine 7%, cocos nucifera oil acyl are sweet
Propylhomoserin sodium 7%, Disodium N-Coco acy-L-Glutamate 5%, lauroyl collagen amino acid TEA salt 2% and sodium lauroyl sarcosine 2%,
Natrulon H-10 oleate 0.6%, glycerol 0.4%, thorn A Gan tree core extract 0.4%, Butyrospermum parkii fruit fatty oil 0.6%, Fructus Citri Limoniae
Acid 0.3%, sodium chloride 0.2%, disodiumedetate 0.04%, Methylisothiazolinone 0.1%, Flos Inulae essence 0.01%,
Surplus is water.
Preparation method is with embodiment 1.
Comparative example 1 washes the preparation protecting two-in-one baby shower gel
Two-in-one baby shower gel is protected in washing of comparative example 1 of the present invention, is made up of the raw material of preparing of following percentage by weight meter:
Mono sulfosuccinates 8%, Coco-Glucoside 8%, cocamido propyl betaine 7%, the sweet ammonia of cocos nucifera oil acyl
Acid sodium 4%, Disodium N-Coco acy-L-Glutamate 4%, lauroyl collagen amino acid TEA salt 4%, sodium lauroyl sarcosine 4%,
Natrulon H-10 oleate 0.5%, glycerol 0.5%, thorn A Gan tree core extract 0.4%, Butyrospermum parkii fruit fatty oil 0.5%, Fructus Citri Limoniae
Acid 0.3%, sodium chloride 0.1%, disodiumedetate 0.05%, Methylisothiazolinone 0.1%, Flos Matricariae chamomillae essence 0.01%,
Surplus is water.
Preparation method is with the difference of embodiment 1 with embodiment 1, this comparative example, and described amino acid type surfactant is coconut palm
Oleoyl Glycine sodium, Disodium N-Coco acy-L-Glutamate, lauroyl collagen amino acid TEA salt, sodium lauroyl sarcosine are with 1:1:1:1
Weight ratio composition.
Comparative example 2 washes the preparation protecting two-in-one baby shower gel
The washing of comparative example 2 of the present invention protect two-in-one baby shower gel to prepare raw material composition same as in Example 1 with proportioning；District
Not being, the step (3) in preparation method does not carry out high pressure homogenize process, particularly as follows:
Preparation method:
(1) toward addition disodiumedetate, mono sulfosuccinates in water, warming while stirring to 85 DEG C,
It is incubated 30 minutes so that it is be completely dissolved；
(2) it is cooled to 65 DEG C, adds Coco-Glucoside, cocamido propyl betaine, sodium cocoyl glycinate, cocos nucifera oil
Acyl disodium glutamate, sodium lauroyl sarcosine and Natrulon H-10 oleate, insulated and stirred 20 minutes is to being completely dissolved；
(3) it is cooled to 45 DEG C, is sequentially added into glycerol, lauroyl collagen amino acid TEA salt, stirs, obtain molten
Liquid A；
(4) toward solution A add in advance with water dissolution citric acid completely, stir, be sequentially added into thorn A Gan tree core extraction
Thing, Butyrospermum parkii fruit fatty oil, Methylisothiazolinone, sodium chloride and essence, stir, at 15 DEG C, and the bar of 45MPa
Homogenizing 8min under part；Then homogenizing 3min under conditions of 15MPa, obtains baby shower gel.
Comparative example 3 washes the preparation protecting two-in-one baby shower gel
The washing of comparative example 3 of the present invention protect two-in-one baby shower gel to prepare raw material composition same as in Example 1 with proportioning；District
Not being, the step (4) in preparation method does not carry out cryogenic high pressure homogenizing process, particularly as follows:
Preparation method:
(1) toward addition disodiumedetate, mono sulfosuccinates in water, warming while stirring to 85 DEG C,
It is incubated 30 minutes so that it is be completely dissolved；
(2) it is cooled to 65 DEG C, adds Coco-Glucoside, cocamido propyl betaine, sodium cocoyl glycinate, cocos nucifera oil
Acyl disodium glutamate, sodium lauroyl sarcosine and Natrulon H-10 oleate, insulated and stirred 20 minutes is to being completely dissolved；
(3) it is cooled to 45 DEG C, is sequentially added into glycerol, lauroyl collagen amino acid TEA salt, stirs, at 45 DEG C,
Homogenizing 5min under conditions of 70MPa, obtains solution A；
(4) toward solution A add in advance with water dissolution citric acid completely, stir, be sequentially added into thorn A Gan tree core extraction
Thing, Butyrospermum parkii fruit fatty oil, Methylisothiazolinone, sodium chloride and essence, stir, obtain baby shower gel.
Comparative example 4 washes the preparation protecting two-in-one baby shower gel
The washing of comparative example 4 of the present invention protect two-in-one baby shower gel to prepare raw material composition same as in Example 1 with proportioning；District
Not being, the step (3) in preparation method does not carry out high pressure homogenize process and step (4) does not carry out cryogenic high pressure homogenizing process,
Particularly as follows:
Preparation method:
(1) toward addition disodiumedetate, mono sulfosuccinates in water, warming while stirring to 85 DEG C,
It is incubated 30 minutes so that it is be completely dissolved；
(2) it is cooled to 65 DEG C, adds Coco-Glucoside, cocamido propyl betaine, sodium cocoyl glycinate, cocos nucifera oil
Acyl disodium glutamate, sodium lauroyl sarcosine and Natrulon H-10 oleate, insulated and stirred 20 minutes is to being completely dissolved；
(3) it is cooled to 45 DEG C, is sequentially added into glycerol, lauroyl collagen amino acid TEA salt, stirs, obtain molten
Liquid A；
(4) toward solution A add in advance with water dissolution citric acid completely, stir, be sequentially added into thorn A Gan tree core extraction
Thing, Butyrospermum parkii fruit fatty oil, Methylisothiazolinone, sodium chloride and essence, stir, obtain baby shower gel.
Test example one, the present invention wash the stability test protecting two-in-one baby shower gel
The bath gel prepared embodiment of the present invention 1-3 and comparative example 1-4 respectively carries out heat-resisting, resistance to freezing test, and result see table.
Table 1 present invention washes the Stability Determination result protecting two-in-one baby shower gel
| Group | -20 DEG C of freexing tolerance energy | 45 DEG C of heat resistances |
| Embodiment 1 | Do not freeze, not stratified | Not stratified, invariant color |
| Embodiment 2 | Do not freeze, not stratified | Not stratified, invariant color |
| Embodiment 3 | Do not freeze, not stratified | Not stratified, invariant color |
| Comparative example 1 | Do not freeze, not stratified | Not stratified, invariant color |
| Comparative example 2 | Do not freeze, layering occurs | Not stratified, invariant color |
| Comparative example 3 | Do not freeze, layering occurs | Layering, invariant color occur |
| Comparative example 4 | Do not freeze, layering occurs | Layering, invariant color occur |
As seen from the above table, what embodiment of the present invention 1-3 prepared wash protects two-in-one infant bath and is exposed at 45 DEG C and-20 DEG C of equal nothings are sunk
Form sediment, without variable color, without lamination appearance, show that the present invention washes and protect two-in-one infant bath and be exposed under high temperature and cryogenic conditions all
There is good stability.Wherein, each component in amino acid surfactant with etc. weight ratio composition, bath gel is stablized
Property impact little.In advance the material such as surfactant, emulsifying agent is carried out high pressure homogenize process at a higher temperature, be conducive to
Improve the freexing tolerance energy of bath gel；Cryogenic high pressure homogenizing processes the heat resistance that can improve bath gel further, improves bath gel steady
Qualitative.
Test example two, the present invention wash and protect the foaming power of two-in-one baby shower gel and compare
The bath gel that embodiment of the present invention 1-3 and comparative example 1-4 prepare is added water and makes the diluent of 5 times, use ROSS
The foam volume of bath gel diluent measured by foam meter, and result see table.
Table 2 present invention washes the foaming capacity measurement result protecting two-in-one baby shower gel
| Group | At once foam height (cm) | Foam height (cm) after 5min | Foamy appearance |
| Embodiment 1 | 23.5 | 23.5 | Fine and smooth |
| Embodiment 2 | 23.3 | 23.3 | Fine and smooth |
| Embodiment 3 | 23.2 | 23.2 | Fine and smooth |
| Comparative example 1 | 19.2 | 19.2 | Thick |
| Comparative example 2 | 17.3 | 17.1 | Thick |
| Comparative example 3 | 17.6 | 17.5 | Thick |
| Comparative example 4 | 16.0 | 16.2 | Thick |
As seen from the above table, two-in-one baby shower gel foaming abundancy, exquisiteness are protected in washing that embodiment of the present invention 1-3 prepares, and surely
Fixed.And the minimizing of two-in-one baby shower gel foam volume is protected in washing that comparative example 1-4 prepares, and foam is thick, shows aminoacid table
Each component in the activating agent of face, with suitable weight ratio composition, is conducive to improving the foam performance of bath gel；In advance by surface activity
The material such as agent, emulsifying agent carries out high pressure homogenize process at a higher temperature, make emulsifying agent and surfactant refine fully,
Dissolve and mixing, beneficially bath gel produce and enrich and the foam of exquisiteness；Cryogenic high pressure homogenizing processes can improve bath gel further
Foaminess.
Test example three, the present invention wash the Ocular irritation test protecting two-in-one baby shower gel
Screen 35 healthy white New Zealand to grow up rabbit, body weight 2～2.5kg.It is divided into embodiment 1-3 group, comparative example 1-4 group,
Often group 5, the bath gel prepared toward the lower eyelid instillation corresponding embodiment of 0.1mL and the comparative example of often group rabbit images of left and right eyes respectively
Stock solution, makes rabbit eyes closed 1s, uses normal saline flushing after 30s again；Observe and record tested at 24h, 48h, 72h respectively
The irritant reaction of rear rabbit cornea, iris or conjunctiva, result see table.
Table 3 present invention washes the Ocular irritation result of the test protecting two-in-one baby shower gel
As seen from the above table, two-in-one baby shower gel is protected in prepared the washing of embodiment of the present invention 1-3 does not has zest, peace to eye
Quan Xinggao.The bath gel that comparative example 1-4 prepares can cause conjunctiva secretions occur, and eye exists slight zest.
Test example four, the present invention wash the acute skin irritation test protecting two-in-one baby shower gel
The Cavia porcellus of 56 regular grade of screening, body weight 200～250g.It is divided into embodiment 1～3 groups, comparative example 1-4 group, often group 8,
Before test, 12h is by guinea pig back left and right side unhairing, and unhairing scope is 3cm × 3cm.Respectively toward often organizing plucked skin on the left of Cavia porcellus
Coat the bath gel stock solution that the corresponding embodiment of 0.5mL and comparative example prepare on skin, then fixed with nonirritant adhesive tape and binder,
Coat 0.5mL normal saline on the plucked skin in right side as comparison, use blocking test, after 2h, understand washing one's hair of residual with warm water
Bath lotion stock solution, observes the dermoreaction of 24h, 48h, 72h recipient site, and result see table.
Table 4 present invention washes the acute skin irritation test result protecting two-in-one baby shower gel
| Group | Stimulate phenomenon | Conclusion |
| Embodiment 1 | Without erythema, without edema | Nonirritant |
| Embodiment 2 | Without erythema, without edema | Nonirritant |
| Embodiment 3 | Without erythema, without edema | Nonirritant |
| Comparative example 1 | Without erythema, without edema | Nonirritant |
| Comparative example 2 | There is slight erythema, without edema | Minimal irritation |
| Comparative example 3 | There is slight erythema, without edema | Minimal irritation |
| Comparative example 4 | There is slight erythema, without edema | Minimal irritation |
As seen from the above table, washing that embodiment of the present invention 1-3 and comparative example 1 prepare protects two-in-one baby shower gel to guinea pig skin
Nonirritant, safety is high, and the bath gel that comparative example 2-4 prepares can cause guinea pig skin slight erythema occur, exists light
Micro-zest, this may with material not through high pressure homogenize process or (and) cryogenic high pressure homogenizing processes, and causes material dispersion
Uneven and cause local excitation relevant.
Test example five, the present invention wash the skin effect evaluation protecting two-in-one baby shower gel
Choose 80 women trial volunteers, age 18～22 years old, be divided into embodiment 1-3 group and comparative example 1 group, often group 20,
The bath gel that each group trial volunteer uses corresponding embodiment and comparative example to prepare respectively is taken a shower, and uses moisture of skin after 2 weeks
Analyzer and skin elasticity analyzer measure skin moisture content and the skin elasticity of trial volunteer respectively, and advance with test
Row compares.All experimenters prohibit the use of any skin care item and cosmetics during testing, and result see table.
Table 5 present invention washes the moistening effect evaluation protecting two-in-one baby shower gel to skin
Note: compare with before test,*P ＜ 0.05.
Table 6 present invention washes and protects two-in-one baby shower gel to skin elasticity effect assessment
Note: compare with before test,*P ＜ 0.05.
From upper table 5, what embodiment of the present invention 1-3 prepared wash protects two-in-one baby shower gel and has skin and preferably lock water
Moisture-keeping functions, can dramatically increase skin moisture content, and effect is better than comparative example 1.
R2 represents the entire change of skin elasticity, and R2 represents the degree of packing of skin.From upper table 6, the embodiment of the present invention
Prepared the washing of 1-3 is protected two-in-one baby shower gel and is remarkably improved skin elasticity, and effect is better than comparative example 1.
Below it is only the preferred embodiment of the present invention, it is noted that above-mentioned preferred implementation is not construed as the present invention
Restriction, protection scope of the present invention should be as the criterion with claim limited range.Ordinary skill for the art
For personnel, without departing from the spirit and scope of the present invention, it is also possible to make some improvements and modifications, these improvements and modifications
Also should be regarded as protection scope of the present invention.
Claims (7)
1. wash and protect two-in-one baby shower gel for one kind, it is characterised in that described bath gel is by the preparation of following percentage by weight meter
Raw material forms:
Anionic surfactant 6～10%, nonionic surfactant 6～10%, amphoteric ionic surfactant
6～10%, amino acid type surfactant 10～30%, emulsifying agent 0.1～1%, glycerol 0.1～1%, thorn A Gan tree core extract
0.1～1%, Butyrospermum parkii fruit fatty oil 0.1～1%, citric acid 0.1～0.5%, sodium chloride 0.1～1%, disodiumedetate
0.01～0.1%, Methylisothiazolinone 0.05～0.1%, essence 0.005～0.2%, surplus is water；
Described anionic surfactant is sodium laureth sulfate or mono sulfosuccinates；Described nonionic
Type surfactant is Coco-Glucoside or decyl glucoside；Described amphoteric ionic surfactant is that cocamidopropyl propyl amide is sweet
Dish alkali；Described amino acid type surfactant is sodium cocoyl glycinate, Disodium N-Coco acy-L-Glutamate, lauroyl collagenous amino
At least one in acid TEA salt, sodium lauroyl sarcosine；
Described emulsifying agent is the one in glycerol caprylate class, glycerol decanoate class, Natrulon H-10 esters.
The most according to claim 1 washing protects two-in-one baby shower gel, it is characterised in that described bath gel is by following heavy
The raw material of preparing of amount percentages forms:
Anionic surfactant 8%, nonionic surfactant 8%, amphoteric ionic surfactant 7%, amino
Acid type surfactant 16%, emulsifying agent 0.5%, glycerol 0.5%, thorn A Gan tree core extract 0.4%, Butyrospermum parkii fruit fat
Oil 0.5%, citric acid 0.3%, sodium chloride 0.1%, disodiumedetate 0.05%, Methylisothiazolinone 0.1%,
Essence 0.01%, surplus is water；
Described anionic surfactant is mono sulfosuccinates；Described nonionic surfactant is cocoyl
Glucoside；Described amphoteric ionic surfactant is cocamido propyl betaine；Described amino acid type surfactant is coconut palm
Oleoyl Glycine sodium, Disodium N-Coco acy-L-Glutamate, lauroyl collagen amino acid TEA salt and the mixing of sodium lauroyl sarcosine
Thing；
Described emulsifying agent is Natrulon H-10 oleate.
The most according to claim 2 washing protects two-in-one baby shower gel, it is characterised in that live in described amino acid pattern surface
Property agent is sodium cocoyl glycinate, Disodium N-Coco acy-L-Glutamate, lauroyl collagen amino acid TEA salt, Hamposyl L
Sodium is with (0.4～1): (0.4～1): (0.2～0.6): the weight ratio composition of (0.1～0.4).
The most according to claim 3 washing protects two-in-one baby shower gel, it is characterised in that live in described amino acid pattern surface
Property agent is sodium cocoyl glycinate, Disodium N-Coco acy-L-Glutamate, lauroyl collagen amino acid TEA salt, Hamposyl L
Sodium forms with the weight ratio of 0.5:0.5:0.4:0.2.
5. one kind prepare as described in claim 1-4 is arbitrary wash the method protecting two-in-one baby shower gel, it is characterised in that
Comprise the following steps:
(1) toward addition disodiumedetate, mono sulfosuccinates in water, warming while stirring to 85 DEG C,
It is incubated 30 minutes so that it is be completely dissolved；
(2) it is cooled to 65 DEG C, adds Coco-Glucoside, cocamido propyl betaine, sodium cocoyl glycinate, cocos nucifera oil
Acyl disodium glutamate, sodium lauroyl sarcosine and Natrulon H-10 oleate, insulated and stirred 20 minutes is to being completely dissolved；
(3) it is cooled to 45 DEG C, is sequentially added into glycerol, lauroyl collagen amino acid TEA salt, stirs, carry out height
Pressure homogenizing processes, and obtains solution A；
(4) toward solution A add in advance with water dissolution citric acid completely, stir, be sequentially added into thorn A Gan tree core extraction
Thing, Butyrospermum parkii fruit fatty oil, Methylisothiazolinone, sodium chloride and essence, stir, carry out cryogenic high pressure homogenizing process,
Obtain baby shower gel.
The most according to claim 5 wash the preparation method protecting two-in-one baby shower gel, it is characterised in that described step
(3) high pressure homogenize in processes particularly as follows: at 40～45 DEG C, under conditions of 60～80MPa homogenizing 3～6min.
The most according to claim 5 wash the preparation method protecting two-in-one baby shower gel, it is characterised in that described step
(4) the cryogenic high pressure homogenizing in processes particularly as follows: at 15 DEG C, under conditions of 40～50MPa homogenizing 5～10min；Then exist
Homogenizing 2～4min under conditions of 15～20MPa.
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