CN115737459A - Body cleaning composition with moisturizing, moistening and skin nourishing effects and preparation method thereof - Google Patents
Body cleaning composition with moisturizing, moistening and skin nourishing effects and preparation method thereof Download PDFInfo
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- CN115737459A CN115737459A CN202211440686.7A CN202211440686A CN115737459A CN 115737459 A CN115737459 A CN 115737459A CN 202211440686 A CN202211440686 A CN 202211440686A CN 115737459 A CN115737459 A CN 115737459A
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- 239000000203 mixture Substances 0.000 title claims abstract description 80
- 238000004140 cleaning Methods 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 230000003020 moisturizing effect Effects 0.000 title claims abstract description 14
- 230000000694 effects Effects 0.000 title claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 34
- 239000003906 humectant Substances 0.000 claims abstract description 29
- 150000001413 amino acids Chemical class 0.000 claims abstract description 26
- 239000002904 solvent Substances 0.000 claims abstract description 23
- 239000004094 surface-active agent Substances 0.000 claims abstract description 22
- 239000008367 deionised water Substances 0.000 claims abstract description 20
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 20
- 239000003963 antioxidant agent Substances 0.000 claims abstract description 14
- 230000003078 antioxidant effect Effects 0.000 claims abstract description 14
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 11
- 239000003755 preservative agent Substances 0.000 claims abstract description 10
- 230000002335 preservative effect Effects 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 8
- 239000012752 auxiliary agent Substances 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims description 101
- 230000001804 emulsifying effect Effects 0.000 claims description 66
- PEDCQBHIVMGVHV-UHFFFAOYSA-N glycerol group Chemical group OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 58
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical group C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 45
- 239000011734 sodium Substances 0.000 claims description 37
- 229910052708 sodium Inorganic materials 0.000 claims description 37
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 34
- 238000001816 cooling Methods 0.000 claims description 30
- 235000011187 glycerol Nutrition 0.000 claims description 20
- JDRSMPFHFNXQRB-CMTNHCDUSA-N Decyl beta-D-threo-hexopyranoside Chemical compound CCCCCCCCCCO[C@@H]1O[C@H](CO)C(O)[C@H](O)C1O JDRSMPFHFNXQRB-CMTNHCDUSA-N 0.000 claims description 16
- 239000002253 acid Substances 0.000 claims description 16
- 229940073499 decyl glucoside Drugs 0.000 claims description 16
- 229940080279 sodium cocoate Drugs 0.000 claims description 16
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical group OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 15
- 241001135917 Vitellaria paradoxa Species 0.000 claims description 15
- 235000018936 Vitellaria paradoxa Nutrition 0.000 claims description 15
- 229960005323 phenoxyethanol Drugs 0.000 claims description 15
- KSAVQLQVUXSOCR-UHFFFAOYSA-M sodium lauroyl sarcosinate Chemical compound [Na+].CCCCCCCCCCCC(=O)N(C)CC([O-])=O KSAVQLQVUXSOCR-UHFFFAOYSA-M 0.000 claims description 15
- WTVHAMTYZJGJLJ-UHFFFAOYSA-N (+)-(4S,8R)-8-epi-beta-bisabolol Natural products CC(C)=CCCC(C)C1(O)CCC(C)=CC1 WTVHAMTYZJGJLJ-UHFFFAOYSA-N 0.000 claims description 14
- RGZSQWQPBWRIAQ-CABCVRRESA-N (-)-alpha-Bisabolol Chemical compound CC(C)=CCC[C@](C)(O)[C@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-CABCVRRESA-N 0.000 claims description 14
- NCZPCONIKBICGS-UHFFFAOYSA-N 3-(2-ethylhexoxy)propane-1,2-diol Chemical compound CCCCC(CC)COCC(O)CO NCZPCONIKBICGS-UHFFFAOYSA-N 0.000 claims description 14
- RGZSQWQPBWRIAQ-LSDHHAIUSA-N alpha-Bisabolol Natural products CC(C)=CCC[C@@](C)(O)[C@@H]1CCC(C)=CC1 RGZSQWQPBWRIAQ-LSDHHAIUSA-N 0.000 claims description 14
- 229940036350 bisabolol Drugs 0.000 claims description 14
- HHGZABIIYIWLGA-UHFFFAOYSA-N bisabolol Natural products CC1CCC(C(C)(O)CCC=C(C)C)CC1 HHGZABIIYIWLGA-UHFFFAOYSA-N 0.000 claims description 14
- 229940100524 ethylhexylglycerin Drugs 0.000 claims description 14
- 239000001524 citrus aurantium oil Substances 0.000 claims description 11
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- 235000009470 Theobroma cacao Nutrition 0.000 claims description 4
- 238000000265 homogenisation Methods 0.000 claims description 4
- XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical group CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 claims description 3
- 239000012459 cleaning agent Substances 0.000 claims description 3
- FSYKKLYZXJSNPZ-UHFFFAOYSA-N sarcosine Chemical compound C[NH2+]CC([O-])=O FSYKKLYZXJSNPZ-UHFFFAOYSA-N 0.000 claims description 3
- 229940087291 tridecyl alcohol Drugs 0.000 claims description 3
- LXAHHHIGZXPRKQ-UHFFFAOYSA-N 5-fluoro-2-methylpyridine Chemical group CC1=CC=C(F)C=N1 LXAHHHIGZXPRKQ-UHFFFAOYSA-N 0.000 claims description 2
- 235000019480 chamomile oil Nutrition 0.000 claims description 2
- 239000010628 chamomile oil Substances 0.000 claims description 2
- 125000003900 glycosphingolipid group Chemical group 0.000 claims description 2
- 238000004519 manufacturing process Methods 0.000 claims 1
- 210000003491 skin Anatomy 0.000 abstract description 60
- 210000000434 stratum corneum Anatomy 0.000 abstract description 8
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- -1 sulfate ester Chemical class 0.000 abstract description 4
- 230000008901 benefit Effects 0.000 abstract description 2
- 238000009776 industrial production Methods 0.000 abstract description 2
- 239000002085 irritant Substances 0.000 abstract description 2
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- 239000000463 material Substances 0.000 description 40
- 230000000052 comparative effect Effects 0.000 description 34
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- 235000001014 amino acid Nutrition 0.000 description 18
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- 239000000523 sample Substances 0.000 description 15
- 239000003109 Disodium ethylene diamine tetraacetate Substances 0.000 description 13
- ZGTMUACCHSMWAC-UHFFFAOYSA-L EDTA disodium salt (anhydrous) Chemical compound [Na+].[Na+].OC(=O)CN(CC([O-])=O)CCN(CC(O)=O)CC([O-])=O ZGTMUACCHSMWAC-UHFFFAOYSA-L 0.000 description 13
- 238000007599 discharging Methods 0.000 description 13
- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 description 13
- 150000002339 glycosphingolipids Chemical class 0.000 description 13
- 238000010438 heat treatment Methods 0.000 description 13
- 229940049920 malate Drugs 0.000 description 13
- BJEPYKJPYRNKOW-UHFFFAOYSA-N malic acid Chemical compound OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 description 13
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- 229940045885 sodium lauroyl sarcosinate Drugs 0.000 description 13
- 239000006071 cream Substances 0.000 description 12
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- 238000004321 preservation Methods 0.000 description 12
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- 125000002889 tridecyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 12
- 244000060011 Cocos nucifera Species 0.000 description 9
- 235000013162 Cocos nucifera Nutrition 0.000 description 9
- 239000000344 soap Substances 0.000 description 8
- 235000020739 avocado extract Nutrition 0.000 description 7
- 239000002537 cosmetic Substances 0.000 description 7
- 239000006210 lotion Substances 0.000 description 6
- 244000183685 Citrus aurantium Species 0.000 description 5
- 235000007716 Citrus aurantium Nutrition 0.000 description 5
- 235000006708 antioxidants Nutrition 0.000 description 5
- 239000000047 product Substances 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 description 4
- 230000000844 anti-bacterial effect Effects 0.000 description 4
- 235000014113 dietary fatty acids Nutrition 0.000 description 4
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 4
- 235000019197 fats Nutrition 0.000 description 4
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- 239000000194 fatty acid Substances 0.000 description 4
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- 235000008673 Persea americana Nutrition 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
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- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 description 2
- 201000004624 Dermatitis Diseases 0.000 description 2
- 206010013786 Dry skin Diseases 0.000 description 2
- NTYJJOPFIAHURM-UHFFFAOYSA-N Histamine Chemical compound NCCC1=CN=CN1 NTYJJOPFIAHURM-UHFFFAOYSA-N 0.000 description 2
- 239000005639 Lauric acid Substances 0.000 description 2
- 244000042664 Matricaria chamomilla Species 0.000 description 2
- 235000007232 Matricaria chamomilla Nutrition 0.000 description 2
- 239000004909 Moisturizer Substances 0.000 description 2
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 description 2
- 238000010521 absorption reaction Methods 0.000 description 2
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- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 2
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- 235000019864 coconut oil Nutrition 0.000 description 2
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- 239000003599 detergent Substances 0.000 description 2
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- ANZUDYZHSVGBRF-UHFFFAOYSA-N 3-ethylnonane-1,2,3-triol Chemical compound CCCCCCC(O)(CC)C(O)CO ANZUDYZHSVGBRF-UHFFFAOYSA-N 0.000 description 1
- 208000002874 Acne Vulgaris Diseases 0.000 description 1
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- PZIRUHCJZBGLDY-UHFFFAOYSA-N Caffeoylquinic acid Natural products CC(CCC(=O)C(C)C1C(=O)CC2C3CC(O)C4CC(O)CCC4(C)C3CCC12C)C(=O)O PZIRUHCJZBGLDY-UHFFFAOYSA-N 0.000 description 1
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- SNPLKNRPJHDVJA-ZETCQYMHSA-N D-panthenol Chemical compound OCC(C)(C)[C@@H](O)C(=O)NCCCO SNPLKNRPJHDVJA-ZETCQYMHSA-N 0.000 description 1
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- CWVRJTMFETXNAD-KLZCAUPSSA-N Neochlorogenin-saeure Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O CWVRJTMFETXNAD-KLZCAUPSSA-N 0.000 description 1
- 208000006787 Port-Wine Stain Diseases 0.000 description 1
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 1
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- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 1
- 235000005764 Theobroma cacao ssp. cacao Nutrition 0.000 description 1
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- 229940114081 cinnamate Drugs 0.000 description 1
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- 229910001415 sodium ion Inorganic materials 0.000 description 1
- 229910052938 sodium sulfate Inorganic materials 0.000 description 1
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- 229940045905 sodium tallowate Drugs 0.000 description 1
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Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention provides a body cleaning composition with the effects of moisturizing, moistening and nourishing skin and a preparation method thereof, and the bath composition comprises the following components: the skin care product comprises a solvent, an oily humectant, a non-oily humectant, an amino acid surfactant, a cleanser, a skin conditioner, an emulsifier, an antioxidant auxiliary agent, a preservative and deionized water. The body cleaning composition does not contain irritant sulfate ester surfactant, and can effectively clean the skin, nourish the skin, keep the moisture of the skin stratum corneum and make the skin soft and glossy by matching the components such as oily humectant, non-oily humectant, amino acid surfactant, skin conditioner and the like. The preparation method provided by the invention has the advantages of simple process, mild condition and short time, and is beneficial to industrial production.
Description
Technical Field
The invention relates to the field of daily chemicals, in particular to a body cleaning composition with the effects of moisturizing, moistening and nourishing skin and a preparation method thereof.
Background
The shower gel is a common daily chemical washing product for bathing and belongs to a liquid cleaning agent. In recent years, with the improvement of the living standard of people, the shower gel gradually replaces the perfumed soap to become the first choice of the bathing articles of people. Meanwhile, people put forward requirements for the shower gel besides cleaning, such as moisturizing, whitening, anti-acne and other effects.
At present, soap-based components are mostly adopted in common bath cream on the market to improve the cleaning power, but the components are usually alkaline, the skin of a human body is weakly acidic, and the skin lipid layer can be damaged and the skin barrier can be weakened after the bath cream is used for a long time. Some bath cream selects sulfate surfactants to enhance the cleaning power and the foaming performance of the bath cream, but the sulfate surfactants have certain irritation to skin and eyes and are controversial in safety. Chinese patent CN107875041A provides a skin-activating and moisturizing body wash, which comprises fatty alcohol polyoxyethylene ether sodium sulfate, lauric acid, rice bran oil, safflower, avocado essential oil, a thickening agent and a preservative, wherein the body wash is added with a sulfate surfactant and lauric acid, so that the body wash has strong irritation and is easy to cause the problems of dry skin, roughness, large pores, desquamation, acne growth and the like.
Disclosure of Invention
In view of the above, the present invention provides a body cleansing composition and a method for preparing the same.
The technical scheme of the invention is as follows:
a body cleaning composition with the effects of moisturizing, moistening and nourishing skin comprises the following components in parts by weight: 2 to 5 portions of solvent, 0.5 to 2 portions of oily humectant, 0.3 to 1 portion of non-oily humectant, 15 to 30 portions of amino acid surfactant, 3 to 7 portions of cleanser, 1 to 3 portions of skin conditioner, 0.3 to 1 portion of emulsifier, 0.03 to 0.1 portion of antioxidant additive, 0.5 to 1.5 portions of preservative and 50 to 71 portions of deionized water.
Further, the body cleaning composition comprises the following components in parts by weight: 3 parts of solvent, 1 part of oily humectant, 0.5 part of non-oily humectant, 18 parts of amino acid surfactant, 4 parts of cleanser, 2.5 parts of skin conditioner, 0.5 part of emulsifier, 0.05 part of antioxidant auxiliary agent, 1 part of preservative and 69 parts of deionized water.
Further, the body cleansing composition according to the above, wherein the solvent is glycerin;
the oily humectant is selected from Butyrospermum parkii fruit extract and/or cacao seed fat;
the non-oily humectant is glycosphingolipid humectant;
the amino acid surfactant is selected from one or more of sodium cocoamidopropionate, sodium cocoyl amino acid, sodium cocoyl malic amino acid, cocoyl sarcosine, sodium lauroyl sarcosine and sodium lauroyl oat amino acid;
the cleanser is one or more selected from decyl glucoside, sodium cocoate, and coco acid;
the skin conditioner is selected from one or more of neroli oil, bisabolol, and chamomile oil;
the emulsifier is tridecyl alcohol polyether-9;
the antioxidant is citric acid;
the antioxidant additive is EDTA disodium;
the preservative is selected from phenoxyethanol and/or ethylhexyl glycerin.
The present invention also provides a method of preparing a body cleansing composition according to any of the preceding claims, comprising the steps of:
s1, sequentially putting a solvent, an amino acid surfactant, a cleaning agent, a non-oily humectant, an emulsifier, an antioxidant auxiliary agent and an antioxidant into an emulsifying pot, stirring and dissolving uniformly, then putting deionized water, and stirring and homogenizing until all components are uniformly dispersed;
s2, maintaining stirring, and keeping the temperature of the mixture obtained in the S1;
s3, continuously stirring the mixture obtained in the step S2, cooling to 45 ℃, adding an oily humectant, a skin conditioner and a preservative, and uniformly stirring;
and S4, continuously stirring the mixture obtained in the step S3, and cooling to 35 ℃ to obtain the body cleaning composition.
Further, in the above preparation method, in step S1, the stirring homogenization temperature is 80 to 90 ℃, the stirring rotation speed is 25 rpm, and the homogenization time is 5 minutes.
Further, in the above preparation method, in step S2, the stirring speed is 35 rpm, and the heat preservation time is 10 minutes.
Further, in the above preparation method, in step S3, the stirring speed is 35 rpm, and the stirring time is 5 minutes.
The chemical name of the solvent glycerol selected by the invention is glycerol, and the glycerol is colorless transparent viscous liquid, odorless and sweet. It is the earliest and common humectant used in cosmetics. The glycerol molecule contains three-OH groups, and hydrogen bonds are formed with water molecules to bind water, so that good moisture absorption and moisture retention effects are achieved. Has obvious moistening effect on human skin and hair, and can increase the solubility of other components in the cosmetic. Glycerin is widely used in various cosmetics to supplement moisture to the skin stratum corneum, regulate the physiological action of the skin, keep the skin healthy, and improve the feeling of use.
Among the oily moisturizers that can be used in the present invention, the extract of the fruit of Butyrospermum PARKII (Butyrupium PARKII): the skin moisturizing cream is extracted from the fruit of the avocado, the mass fraction of unsaponifiable matters in the avocado extract is as high as 9-13%, and the natural moisturizing factors in the avocado extract and the moisturizing agent extracted from sebaceous glands have the same components, so that the avocado extract is a natural vitamin A cream, and is considered to be the most effective natural skin moisturizing agent and conditioning agent. The avocado extract contains cinnamate, and can be used in sunscreen cosmetic for preventing skin injury caused by ultraviolet irradiation, and natural latex in avocado fat can prevent skin allergy caused by sunlight irradiation. The avocado extract can promote cell regeneration and capillary circulation, and can be used in skin care products for preventing and delaying skin aging. The avocado extract has strong water locking capacity and good affinity to skin, so that the avocado extract can be applied to hair products such as dry shampoo and the like. The vitamin A in the shea butter has important improvement effect on removing a plurality of skin defects such as wrinkles, eczema and the like.
Cocoa (Theobroma CACAO) seed fat is excellent basic oil for cosmetics, and has effects of nourishing skin and penetrating well. It can promote skin metabolism, and has anti-aging effect in combination with its antioxidant effect; can inhibit histamine release, and has anti-allergy and relieving effects; has inhibitory effect on metalloprotease, and has anti-inflammatory effect.
The glycosphingolipid non-oily humectant can effectively improve the adhesive force of keratinocytes, enable the cells to be tightly combined and reduce the water loss.
In the amino acid surfactant adopted by the invention, sodium cocoamido propionate has good capabilities of decontamination, emulsification, solubilization, foam stabilization, wetting, infiltration and the like, and has excellent capabilities of skin refreshing, moisturizing and conditioning. Under the acidic condition, the antistatic and bactericidal coating also has antistatic and bactericidal capabilities. Good compatibility and hard water resistance, and is a mild amino acid surfactant. Has excellent compatibility with skin and hair, and is very suitable for preparing non-sulfate system formula.
The sodium cocoyl malate comes from natural plants, has strong foamability, is soft and rich in foam, is mild to eyes and skin, is mild and clean, and enables the skin to be as young as the skin is and elastic.
Sodium lauroyl sarcosinate is an anionic amino acid surfactant, and has the characteristics of low toxicity, low irritation, good biodegradability, good compatibility, antibacterial property, corrosion resistance and the like. It has the characteristics of both fatty acid soap and alkyl sulfonate, and has good foamability and affinity to skin and hair; the amide group forms a specific association, has chelating and antioxidant properties, has good skin permeability, and can inhibit the permeation of potentially irritating solutes such as sodium ions through human skin, thereby preventing skin roughness after use.
Among the detergents which can be used in the invention, decyl glucoside is a novel nonionic surfactant APG, has the characteristics of common nonionic and anionic surfactants, and has the characteristics of low surface tension, excellent detergency, wetting power, excellent foaming performance and the like.
Coconut oil acid is a fatty acid, which is generally a generic name for mixtures of fatty acids derived from coconut oil. Sodium cocoate is a salt that it saponifies with sodium hydroxide. Cocoate/sodium cocoate is often formulated with sodium tallowate into soaps, detergents and surfactants. Fatty acids can maintain the elasticity of cells, they can promote cell membrane function and skin health.
Among the skin conditioners which can be used in the invention, bitter orange (CITRUS AURANTIUM AMARA) flower oil can relieve and moisten skin, so that the skin is soft and bright.
Bisabolol is also called l-enol, and is a thick oily liquid, which is the main component of chamomile essential oil. It has effects in promoting absorption of other beneficial components, relieving inflammation, sterilizing, and promoting skin wound healing. In addition, the skin-nourishing cream is rich in natural humectant panthenol, can effectively preserve moisture, enables the skin to recover vitality from the inside, and achieves the purpose of nourishing the skin.
Flos Matricariae Chamomillae (CHAMOMILLA RECUTITA) flower oil contains volatile oil, flavonoids, amino acids, chlorogenic acid and trace elements, and has sunscreen, antibacterial, antioxidant, antiinflammatory, soothing, and antiallergic effects. It can prevent pachylosis, protect epidermal mucosa from bacteria, regulate water and oil balance of skin, and delay skin aging.
The invention has the following beneficial effects: the body cleaning composition does not contain an irritant sulfate ester surfactant, and can effectively clean the skin, nourish the skin, keep the moisture of the skin stratum corneum and make the skin soft and glossy by matching the components such as an oily humectant, a non-oily humectant, an amino acid surfactant, a skin conditioner and the like. The preparation method provided by the invention has the advantages of simple process, mild condition and short time, and is beneficial to industrial production.
Detailed Description
The experimental methods used in the following examples are all conventional methods unless otherwise specified; the reagents, materials and the like used in the following examples are all commercially available products or can be prepared by known methods unless otherwise specified. Experimental procedures without specific conditions noted in the following examples, molecular cloning is generally performed according to conventional conditions such as Sambrook et al: conditions described in a Laboratory Manual (New York: cold spring harbor Laboratory Press, 1989), or according to the manufacturer's recommendations.
Example 1
(1) Dispersing solvent: weighing 3 parts by weight of glycerol, 10 parts by weight of sodium cocoamidopropionate, 3 parts by weight of sodium cocoyl malate, 5 parts by weight of sodium lauroyl sarcosinate, 2 parts by weight of decyl glucoside, 1 part by weight of sodium cocoate, 1 part by weight of cocoanut acid, 0.5 part by weight of glycosphingolipids, 0.5 part by weight of tridecyl polyether-9, 0.05 part by weight of disodium EDTA and 0.05 part by weight of citric acid, putting into an emulsifying pot, stirring and dissolving uniformly, adding 69 parts by weight of deionized water, heating to 90 ℃, keeping at 80 ℃, stirring and homogenizing for 5 minutes until all components are uniformly dispersed, and stirring at the rotating speed of 25 revolutions per minute;
(2) Preserving heat: keeping the temperature of the mixture in the emulsifying pot for 10 minutes;
(3) Mixing and homogenizing: continuously stirring the materials in the emulsifying pot, cooling to 45 ℃, weighing 2 parts by weight of neroli oil, 0.5 part by weight of bisabolol, 1 part by weight of shea butter fruit extract, 0.5 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerin, putting the weighed materials into the emulsifying pot, stirring at the rotating speed of 35 revolutions per minute for 5 minutes, and uniformly mixing;
(4) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35 deg.C to obtain the body cleaning composition.
Example 2
(1) Dispersing solvent: weighing 2 parts by weight of glycerol, 9 parts by weight of sodium cocoyl amino acid, 2 parts by weight of cocoyl sarcosine, 4 parts by weight of sodium lauroyl avenamide, 1.5 parts by weight of decyl glucoside, 1 part by weight of sodium cocoyl amino acid, 0.5 part by weight of coco acid, 0.3 part by weight of glycosphingolipids, 0.3 part by weight of tridecyl alcohol polyether-9, 0.03 part by weight of disodium EDTA and 0.03 part by weight of citric acid, adding 71 parts by weight of deionized water after stirring and dissolving uniformly, heating to 90 ℃, keeping at 80 ℃, stirring and homogenizing for 5 minutes until all components are uniformly dispersed, and stirring at the rotating speed of 25 r/min;
(2) And (3) heat preservation: keeping the temperature of the mixture in the emulsifying pot for 10 minutes;
(3) Mixing and homogenizing: continuously stirring the materials in the emulsifying pot, cooling to 45 ℃, weighing 2 parts by weight of bitter orange flower oil, 1 part by weight of mother chrysanthemum oil, 2 parts by weight of cocoa seed fat, 0.2 part by weight of phenoxyethanol and 0.3 part by weight of ethylhexyl glycerin, putting the materials into the emulsifying pot, stirring at the rotating speed of 35 revolutions per minute for 5 minutes, and uniformly mixing;
(4) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35 deg.C to obtain the body cleaning composition.
Example 3
(1) Dispersing solvent: weighing 5 parts by weight of glycerol, 15 parts by weight of sodium cocoamidopropionate, 7 parts by weight of sodium cocoyl malate, 8 parts by weight of sodium lauroyl sarcosinate, 4 parts by weight of decyl glucoside, 1 part by weight of sodium cocoate, 2 parts by weight of cocoanut acid, 1 part by weight of glycosphingolipids, 1 part by weight of tridecyl polyether-9, 0.1 part by weight of disodium EDTA and 0.1 part by weight of citric acid, putting the mixture into an emulsifying pot, stirring and dissolving the mixture uniformly, adding 50 parts by weight of deionized water, heating the mixture to 90 ℃, keeping the temperature at 80 ℃, stirring and homogenizing the mixture for 5 minutes until all components are uniformly dispersed, and stirring the rotation speed of the stirring to 25 revolutions per minute;
(2) And (3) heat preservation: keeping the temperature of the mixture in the emulsifying pot for 10 minutes;
(3) Mixing and homogenizing: continuously stirring the materials in the emulsifying pot, cooling to 45 ℃, weighing 0.5 part by weight of bitter orange flower oil, 0.5 part by weight of bisabolol, 0.5 part by weight of shea butter fruit extract, 1 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerin, putting the materials into the emulsifying pot, stirring at the rotating speed of 35 revolutions per minute for 5 minutes, and uniformly mixing;
(4) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35 deg.C to obtain the body cleaning composition.
Comparative example 1
(1) Dispersing solvent: weighing 3 parts by weight of glycerol, 10 parts by weight of sodium cocoamidopropionate, 3 parts by weight of sodium cocoyl malate, 5 parts by weight of sodium lauroyl sarcosinate, 2 parts by weight of decyl glucoside, 1 part by weight of sodium cocoate, 1 part by weight of cocoanut acid, 0.5 part by weight of glycosphingolipids, 0.5 part by weight of tridecyl polyether-9, 0.05 part by weight of disodium EDTA and 0.05 part by weight of citric acid, putting into an emulsifying pot, stirring and dissolving uniformly, adding 69 parts by weight of deionized water, heating to 90 ℃, keeping at 80 ℃, stirring and homogenizing for 5 minutes until all components are uniformly dispersed, and stirring at the rotating speed of 25 revolutions per minute;
(2) And (3) heat preservation: keeping the temperature of the mixture in the emulsifying pot for 10 minutes;
(3) Mixing and homogenizing: continuously stirring the materials in the emulsifying pot, cooling to 45 ℃, weighing 3 parts by weight of bitter orange flower oil, 1 part by weight of bisabolol, 3 parts by weight of shea butter fruit extract, 0.5 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerin, putting the materials into the emulsifying pot, stirring at the rotating speed of 35 revolutions per minute for 5 minutes, and uniformly mixing;
(4) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35 deg.C to obtain the body cleaning composition.
Comparative example 2
(1) Dispersing solvent: weighing 3 parts by weight of glycerol, 10 parts by weight of sodium cocoamidopropionate, 3 parts by weight of sodium cocoyl malate, 5 parts by weight of sodium lauroyl sarcosinate, 2 parts by weight of decyl glucoside, 1 part by weight of sodium cocoate, 1 part by weight of cocoanut acid, 0.5 part by weight of glycosphingolipids, 0.5 part by weight of tridecyl polyether-9, 0.05 part by weight of disodium EDTA and 0.05 part by weight of citric acid, putting into an emulsifying pot, stirring and dissolving uniformly, adding 69 parts by weight of deionized water, heating to 90 ℃, keeping at 80 ℃, stirring and homogenizing for 5 minutes until all components are uniformly dispersed, and stirring at the rotating speed of 25 revolutions per minute;
(2) And (3) heat preservation: keeping the temperature of the mixture in the emulsifying pot for 10 minutes;
(3) Mixing and homogenizing: continuously stirring the materials in the emulsifying pot, cooling to 45 ℃, weighing 0.3 part by weight of neroli oil, 0.2 part by weight of bisabolol, 0.2 part by weight of shea butter extract, 0.5 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerin, putting the weighed materials into the emulsifying pot, stirring at the rotating speed of 35 revolutions per minute for 5 minutes, and uniformly mixing;
(4) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35 deg.C to obtain the body cleaning composition.
Comparative example 3
(1) Dispersing solvent: weighing 7 parts by weight of glycerol, 10 parts by weight of sodium cocoamidopropionate, 3 parts by weight of sodium cocoyl malate, 5 parts by weight of sodium lauroyl sarcosinate, 2 parts by weight of decyl glucoside, 1 part by weight of sodium cocoate, 1 part by weight of cocoanut acid, 0.5 part by weight of glycosphingolipids, 0.5 part by weight of tridecyl polyether-9, 0.05 part by weight of disodium EDTA and 0.05 part by weight of citric acid, putting into an emulsifying pot, stirring and dissolving uniformly, adding 80 parts by weight of deionized water, heating to 90 ℃, keeping at 80 ℃, stirring and homogenizing for 5 minutes until all components are uniformly dispersed, and stirring at 25 revolutions per minute;
(2) And (3) heat preservation: keeping the temperature of the mixture in the emulsifying pot for 10 minutes;
(3) Mixing and homogenizing: continuously stirring the materials in the emulsifying pot, cooling to 45 ℃, weighing 2 parts by weight of neroli oil, 0.5 part by weight of bisabolol, 1 part by weight of shea butter fruit extract, 0.5 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerin, putting the weighed materials into the emulsifying pot, stirring at the rotating speed of 35 revolutions per minute for 5 minutes, and uniformly mixing;
(4) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35 deg.C to obtain the body cleaning composition.
Comparative example 4
(1) Dispersing solvent: weighing 1 part by weight of glycerol, 10 parts by weight of sodium cocoamidopropionate, 3 parts by weight of sodium cocoyl malate, 5 parts by weight of sodium lauroyl sarcosinate, 2 parts by weight of decyl glucoside, 1 part by weight of sodium cocoate, 1 part by weight of cocoanut acid, 0.5 part by weight of glycosphingolipids, 0.5 part by weight of tridecyl polyether-9, 0.05 part by weight of disodium EDTA and 0.05 part by weight of citric acid, putting into an emulsifying pot, stirring and dissolving uniformly, adding 40 parts by weight of deionized water, heating to 90 ℃, keeping at 80 ℃, stirring and homogenizing for 5 minutes until all components are uniformly dispersed, and stirring at the rotating speed of 25 revolutions per minute;
(2) And (3) heat preservation: keeping the temperature of the mixture in the emulsifying pot for 10 minutes;
(3) Mixing and homogenizing: continuously stirring the materials in the emulsifying pot, cooling to 45 ℃, weighing 2 parts by weight of neroli oil, 0.5 part by weight of bisabolol, 1 part by weight of shea butter fruit extract, 0.5 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerin, putting the weighed materials into the emulsifying pot, stirring at the rotating speed of 35 revolutions per minute for 5 minutes, and uniformly mixing;
(4) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35 deg.C to obtain the body cleaning composition.
Comparative example 5
(1) Dispersing solvent: weighing 3 parts by weight of glycerol, 10 parts by weight of sodium cocoamidopropionate, 3 parts by weight of sodium cocoyl malate, 5 parts by weight of sodium lauroyl sarcosinate, 2 parts by weight of decyl glucoside, 1 part by weight of sodium cocoate, 1 part by weight of cocoanut acid, 0.5 part by weight of glycosphingolipids, 1.5 parts by weight of tridecyl polyether-9, 0.05 part by weight of disodium EDTA and 0.05 part by weight of citric acid, putting into an emulsifying pot, stirring and dissolving uniformly, adding 69 parts by weight of deionized water, heating to 90 ℃, keeping at 80 ℃, stirring and homogenizing for 5 minutes until all components are uniformly dispersed, and stirring at the rotating speed of 25 revolutions per minute;
(2) And (3) heat preservation: keeping the temperature of the mixture in the emulsifying pot for 10 minutes;
(3) Mixing and homogenizing: continuously stirring the materials in the emulsifying pot, cooling to 45 ℃, weighing 2 parts by weight of neroli oil, 0.5 part by weight of bisabolol, 1 part by weight of shea butter fruit extract, 0.5 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerin, putting the weighed materials into the emulsifying pot, stirring at the rotating speed of 35 revolutions per minute for 5 minutes, and uniformly mixing;
(4) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35 deg.C to obtain the body cleaning composition.
Comparative example 6
(1) Dispersing solvent: weighing 3 parts by weight of glycerol, 10 parts by weight of sodium cocoamidopropionate, 3 parts by weight of sodium cocoyl malate, 5 parts by weight of sodium lauroyl sarcosinate, 2 parts by weight of decyl glucoside, 1 part by weight of sodium cocoate, 1 part by weight of coco acid, 0.5 part by weight of glycosphingolipids, 0.1 part by weight of tridecyl polyether-9, 0.05 part by weight of disodium EDTA and 0.05 part by weight of citric acid, putting the components into an emulsifying pot, stirring and dissolving uniformly, adding 69 parts by weight of deionized water, heating to 90 ℃, keeping at 80 ℃, stirring and homogenizing for 5 minutes until all components are uniformly dispersed, and stirring at the rotation speed of 25 revolutions per minute;
(2) And (3) heat preservation: keeping the temperature of the mixture in the emulsifying pot for 10 minutes;
(3) Mixing and homogenizing: continuously stirring the materials in the emulsifying pot, cooling to 45 ℃, weighing 2 parts by weight of neroli oil, 0.5 part by weight of bisabolol, 1 part by weight of shea butter fruit extract, 0.5 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerin, putting the weighed materials into the emulsifying pot, stirring at the rotating speed of 35 revolutions per minute for 5 minutes, and uniformly mixing;
(4) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35 deg.C to obtain the body cleaning composition.
Comparative example 7
(1) Dispersing solvent: weighing 3 parts by weight of glycerol, 7 parts by weight of sodium cocoamidopropionate, 2 parts by weight of sodium cocoyl malate, 1 part by weight of sodium lauroyl sarcosinate, 2 parts by weight of decyl glucoside, 1 part by weight of sodium cocoate, 1 part by weight of coco acid, 0.5 part by weight of glycosphingolipids, 0.5 part by weight of tridecyl polyether-9, 0.05 part by weight of disodium EDTA and 0.05 part by weight of citric acid, putting the components into an emulsifying pot, stirring and dissolving uniformly, adding 69 parts by weight of deionized water, heating to 90 ℃, keeping at 80 ℃, stirring and homogenizing for 5 minutes until all components are uniformly dispersed, and stirring at the rotation speed of 25 revolutions per minute; the formula has less amino acid surfactant.
(2) And (3) heat preservation: keeping the temperature of the mixture in the emulsifying pot for 10 minutes;
(3) Mixing and homogenizing: continuously stirring the materials in the emulsifying pot, cooling to 45 ℃, weighing 2 parts by weight of neroli oil, 0.5 part by weight of bisabolol, 1 part by weight of shea butter fruit extract, 0.5 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerin, putting the weighed materials into the emulsifying pot, stirring at the rotating speed of 35 revolutions per minute for 5 minutes, and uniformly mixing;
(4) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35 deg.C to obtain the body cleaning composition.
Comparative example 8
(1) Dispersing solvent: weighing 3 parts by weight of glycerol, 10 parts by weight of sodium cocoamidopropionate, 3 parts by weight of sodium cocoyl malate, 5 parts by weight of sodium lauroyl sarcosinate, 2 parts by weight of decyl glucoside, 1 part by weight of sodium cocoate, 1 part by weight of cocoanut acid, 0.5 part by weight of tridecyl polyether-9.5, 0.05 part by weight of disodium EDTA and 0.05 part by weight of citric acid, putting into an emulsifying pot, stirring and dissolving uniformly, adding 69 parts by weight of deionized water, heating to 90 ℃, keeping at 80 ℃, stirring and homogenizing for 5 minutes until all components are uniformly dispersed, and stirring at the rotating speed of 25 revolutions per minute; the formula lacks a non-oily humectant.
(2) And (3) heat preservation: keeping the temperature of the mixture in the emulsifying pot for 10 minutes;
(3) Mixing and homogenizing: continuously stirring the materials in the emulsifying pot, cooling to 45 ℃, weighing 2 parts by weight of neroli oil, 0.5 part by weight of bisabolol, 1 part by weight of shea butter fruit extract, 0.5 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerin, putting the weighed materials into the emulsifying pot, stirring at the rotating speed of 35 revolutions per minute for 5 minutes, and uniformly mixing;
(4) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35 deg.C to obtain the body cleaning composition.
Comparative example 9
(1) Dispersing solvent: weighing 3 parts by weight of glycerol, 10 parts by weight of sodium cocoamidopropionate, 3 parts by weight of sodium cocoyl malate, 5 parts by weight of sodium lauroyl sarcosinate, 2 parts by weight of decyl glucoside, 1 part by weight of sodium cocoate, 1 part by weight of cocoanut acid, 0.5 part by weight of glycosphingolipids, 0.5 part by weight of tridecyl polyether-9, 0.05 part by weight of disodium EDTA and 0.05 part by weight of citric acid, putting into an emulsifying pot, stirring and dissolving uniformly, adding 69 parts by weight of deionized water, heating to 90 ℃, keeping at 80 ℃, stirring and homogenizing for 5 minutes until all components are uniformly dispersed, and stirring at the rotating speed of 25 revolutions per minute;
(2) Preserving heat: keeping the temperature of the mixture in the emulsifying pot for 10 minutes;
(3) Mixing and homogenizing: continuously stirring the materials in the emulsifying pot, cooling to 45 ℃, weighing 2 parts by weight of neroli oil, 0.5 part by weight of bisabolol, 0.5 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerin, putting the weighed materials into the emulsifying pot, stirring at the rotating speed of 35 revolutions per minute for 5 minutes, and uniformly mixing; the formula lacks an oily humectant.
(4) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35 deg.C to obtain the body cleaning composition.
Comparative example 10
(1) Dispersing solvent: weighing 3 parts by weight of glycerol, 10 parts by weight of sodium cocoamidopropionate, 3 parts by weight of sodium cocoyl malate, 5 parts by weight of sodium lauroyl sarcosinate, 2 parts by weight of decyl glucoside, 1 part by weight of sodium cocoate, 1 part by weight of coco acid, 0.5 part by weight of glycosphingolipids, 0.5 part by weight of tridecyl polyether-9, 0.05 part by weight of disodium EDTA and 0.05 part by weight of citric acid, putting the components into an emulsifying pot, stirring and dissolving uniformly, adding 69 parts by weight of deionized water, heating to 90 ℃, keeping at 80 ℃, stirring and homogenizing for 5 minutes until all components are uniformly dispersed, and stirring at the rotation speed of 25 revolutions per minute;
(2) And (3) heat preservation: keeping the temperature of the mixture in the emulsifying pot for 10 minutes;
(3) Mixing and homogenizing: continuously stirring the materials in the emulsifying pot, cooling to 45 ℃, weighing 1 part by weight of the shea butter extract, 0.5 part by weight of phenoxyethanol and 0.5 part by weight of ethylhexyl glycerol, putting the materials into the emulsifying pot, stirring at the rotating speed of 35 revolutions per minute for 5 minutes, and uniformly mixing; the formula lacks a skin conditioner.
(4) Discharging: continuously stirring the materials in the emulsifying pot, and cooling to 35 deg.C to obtain the body cleaning composition.
Performance testing
(1) Sensory index
The body cleansing compositions prepared in examples 1 to 3 and comparative examples 1 to 10 were subjected to sensory comparison with the standard products at room temperature, and the appearance and color were visually observed, and the fragrance was smelled.
TABLE 1 sensory indices of body cleansing compositions obtained by the respective preparation Processes
As shown in the table above, the body cleansing compositions prepared in the examples and comparative examples have similar sensory attributes and are uniform white pastes having orange flower fragrance.
(2) Stability of
The body cleaning compositions prepared in the examples and the comparative examples are respectively placed in a constant temperature refrigerator at minus 18 to minus 10 ℃ and an electric heating constant temperature air blast drying oven at 48 +/-1 ℃, kept for 48 hours and then taken out, the room temperature is recovered, and the layering condition is observed.
Table 2 stability of body cleansing compositions obtained by different preparation processes
Stability affects the length of time the body cleansing composition is stored in different environments. As shown in the above table, the body cleansing compositions prepared in examples 1 to 3 and comparative examples 7 to 10 did not delaminate at high and low temperatures; comparative examples 1-6 showed delamination after low temperature treatment and high temperature treatment. The reason is presumed to be: comparative examples 1 and 4 have a high oil-water ratio; comparative examples 2 and 3 have a low oil-water ratio; comparative example 5 too much emulsifier; comparative example 6 too little emulsifier.
(3) Viscosity of the oil
The body cleansing compositions prepared in the examples and comparative examples were tested for viscosity at 25 ℃ according to the regulations of the national standard GB/T15357, with 10000-15000 being a pass interval.
Table 3 viscosity of body cleansing composition obtained by different preparation process
The viscosity affects the use feeling of the body cleaning composition, and the viscosity is too low to be easily attached to the skin; too high viscosity and difficult cleaning. As shown in the above table, the body-cleansing compositions prepared in examples 1 to 3 and comparative examples 7 to 10 had viscosities ranging from 10000 to 15000, the body-cleansing compositions prepared in comparative examples 1, 4 and 6 had viscosities less than 10000, and the body-cleansing compositions prepared in comparative examples 2, 3 and 5 had viscosities greater than 15000. The above test results show that the body cleansing compositions prepared in comparative examples 1, 4, and 6 are less likely to adhere to the skin during use, compared to other preparation processes; the body cleansing compositions prepared in comparative examples 2, 3, 5 were not easily washed off during use.
(4) Centrifugal test
The body cleaning compositions prepared in the examples and the comparative examples were subjected to centrifugal test according to the specification of the national standard GB/T29665, and were not delaminated when rotated at 3000r/min for 30 minutes, and were judged to be acceptable.
TABLE 4 centrifuge test results for body cleansing compositions obtained by different preparation procedures
The centrifugal separation experiment is a key means for testing the stability and shelf life of cream emulsion cosmetics. As shown in the above table, the body cleansing compositions prepared in examples 1 to 3 and comparative examples 7 to 10 did not delaminate after centrifugation, while the body cleansing compositions prepared in comparative examples 1 to 6 delaminated after centrifugation. The above results indicate that the body cleansing compositions prepared in comparative examples 1 to 6 had poor stability and long storage time.
(5) Efficacy assessment
(1) Reagents and instrumentation:
body cleansing compositions prepared in examples and comparative examples; stratum corneum moisture content test probe Corneometer CM815, skin moisture loss test probe Tewameter TM300, skin oil test probe Sebumeter SM815, courage + Khazaka, germany, 50829koln, germany.
(2) Test objects:
70 healthy people, half of men and women, 20-45 years old, no serious systemic diseases, no immunodeficiency or autoimmune diseases, no active allergic diseases, no serious allergic history to cosmetics, no hormone medicines and immunosuppressive agents used in nearly 1 month, no influence on the judgment of test results due to scars, pigments, atrophy, nevus flammeus or other flaws on skin test parts, no participation in other clinical tests, use of tested objects according to the regulations, complete data and sign of informed consent of volunteers before the test.
(3) The test method comprises the following steps:
initial value: the temperature is 21 +/-1 ℃ and the humidity is 40-60 percent. According to a random principle, the skin on the flexed side of the left arm or the skin on the flexed side of the right arm of 30 volunteers is randomly selected as a blank group A, and the skin on the flexed side of the other arm is selected as an experimental group B.
And (3) testing the cleaning force: marking 3 corresponding positions of the left and right forearms of the subject at the flexion side with 3 × 3cm 2 And (3) testing areas, wherein each area is at least 1-1.5 cm apart, and the left and right corresponding positions are randomly arranged as blank areas and sample areas. And (3) smearing 0.018g of special grease at the corresponding position of the left and right arms, and after an initial value is tested, respectively cleaning the blank area and the sample area for 20 circles by using clear water and shower gel in a looping manner and completely washing. Blank areas A1, A2 and A3 are washed by clear water, and sample areas B1, B2 and B3 are respectively washed by soap-based bath lotion, amino acid bath lotion and cream bath lotion.
Before each test, the testee sits statically for at least 20min in a constant temperature and humidity environment (21 +/-1) DEG C and under the humidity of 40-60%, the positions of the areas A1, A2, A3, B1, B2 and B3 of the testee are tested by a measurer by using a skin oil test probe, and the skin oil value is recorded. The test of the same subject must be completed by the same tester by using the same instrument, and the test probe should be cleaned between two measurements.
Moisture retention test: marking 3 corresponding positions of the left and right forearms of the subject at the flexion side with 3 × 3cm 2 And (3) testing areas, wherein each area is at least 1-1.5 cm apart, and the left and right corresponding positions are randomly arranged as blank areas and sample areas. And (5) after testing the initial value, respectively using clear water and shower gel to loop and clean the blank area and the sample area for 20 circles, and completely washing the blank area and the sample area. Blank areas C1, C2 and C3 are washed by clear water, and sample areas D1, D2 and D3 are respectively washed by soap base bath lotion, amino acid bath lotion and cream bath lotion.
Before each test, a test subject sits statically for at least 20min at a constant temperature and humidity of 21 +/-1 ℃ and a humidity of 40-60%, a measurer uses a test probe for testing the moisture content of the stratum corneum and a test probe for testing the positions of C1, C2, C3, D1, D2 and D3 areas of the test subject through the epidermal water loss amount, and records the moisture content value of the stratum corneum and the trans-epidermal water loss amount value. The test of the same subject must be done by the same tester using the same instrument, and the test probe should be cleaned between measurements.
(4) And (3) data analysis: JMP professional statistical software is adopted for analysis, and P <0.05 indicates that the difference has statistical significance.
(5) And (3) testing results: the test results are shown in the following table.
TABLE 5 skin oil, moisture content of horny layer and change rate of trans-epidermal water loss (%), of body cleansing compositions obtained by different preparation methods
"+" indicates p <0.05 compared to control body wash.
The contrast bath cream is a common soap-based bath cream. As shown in the above table, the body cleansing compositions prepared in examples 1 to 3 and comparative examples 1 to 6 slightly increased the degree of reduction of skin oil content compared to the control body wash, and significantly reduced the degree of reduction of stratum corneum moisture content and transdermal water loss while ensuring cleansing power, and were able to effectively moisturize the skin. The body cleansing composition prepared in comparative example 7 had a significantly lower reduction in skin oil content than the conventional soap-based body wash due to the lower amount of amino acid surfactant. Comparative examples 8-10 produced body cleansing compositions having a slightly lower reduction in stratum corneum moisture content and transdermal water loss than the control body wash, but did not have a significant difference, i.e., insufficient moisturizing power, due to the lack of non-oily moisturizers, and skin conditioners, respectively, of the three groups of comparative examples.
Although embodiments of the present application have been shown and described above, it is understood that the above embodiments are exemplary and should not be construed as limiting the present application, and that changes, modifications, substitutions and alterations in the above embodiments may be made by those of ordinary skill in the art within the scope of the present application.
Claims (7)
1. A body cleaning composition with the effects of moisturizing, moistening and nourishing skin comprises the following components in parts by weight: 2 to 5 portions of solvent, 0.5 to 2 portions of oily humectant, 0.3 to 1 portion of non-oily humectant, 15 to 30 portions of amino acid surfactant, 3 to 7 portions of cleanser, 1 to 3 portions of skin conditioner, 0.3 to 1 portion of emulsifier, 0.03 to 0.1 portion of antioxidant auxiliary agent, 0.5 to 1.5 portions of preservative and 50 to 71 portions of deionized water.
2. The body cleansing composition according to claim 1, comprising the following components in parts by weight: 3 parts of solvent, 1 part of oily humectant, 0.5 part of non-oily humectant, 18 parts of amino acid surfactant, 4 parts of cleanser, 2.5 parts of skin conditioner, 0.5 part of emulsifier, 0.05 part of antioxidant auxiliary agent, 1 part of preservative and 69 parts of deionized water.
3. Body cleansing composition according to claim 1 or 2, characterized in that the solvent is glycerol;
the oily humectant is selected from Butyrospermum parkii extract and/or cocoa seed fat;
the non-oily humectant is a glycosphingolipid humectant;
the amino acid surfactant is selected from one or more of sodium cocoamidopropionate, sodium cocoyl amino acid, sodium cocoyl malic amino acid, cocoyl sarcosine, sodium lauroyl sarcosine and sodium lauroyl oat amino acid;
the cleanser is one or more selected from decyl glucoside, sodium cocoate and cocoic acid;
the skin conditioner is selected from one or more of neroli oil, bisabolol and chamomile oil;
the emulsifier is tridecyl alcohol polyether-9;
the antioxidant is citric acid;
the antioxidant auxiliary agent is EDTA disodium;
the preservative is selected from phenoxyethanol and/or ethylhexyl glycerin.
4. A method of making a body cleansing composition according to any of claims 1-3 comprising the steps of:
s1, sequentially putting a solvent, an amino acid surfactant, a cleaning agent, a non-oily humectant, an emulsifier, an antioxidant auxiliary agent and an antioxidant into an emulsifying pot, stirring and dissolving uniformly, then putting deionized water, and stirring and homogenizing until all components are uniformly dispersed;
s2, maintaining stirring, and keeping the temperature of the mixture obtained in the S1;
s3, continuously stirring the mixture obtained in the step S2, cooling to 45 ℃, adding an oily humectant, a skin conditioner and a preservative, and uniformly stirring;
and S4, continuously stirring the mixture obtained in the step S3, and cooling to 35 ℃ to obtain the body cleaning composition.
5. The preparation method according to claim 4, wherein in the step S1, the stirring homogenization temperature is 80-90 ℃, the stirring rotation speed is 25 rpm, and the homogenization time is 5 minutes.
6. The method according to claim 4, wherein in the step S2, the stirring speed is 35 rpm, and the holding time is 10 minutes.
7. The method according to claim 4, wherein in the step S3, the stirring speed is 35 rpm, and the stirring time is 5 minutes.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105997678A (en) * | 2016-06-22 | 2016-10-12 | 广州科玛生物科技股份有限公司 | Washing and care two-in-one infant shower gel |
| CN107998028A (en) * | 2017-12-25 | 2018-05-08 | 深圳市芭格美生物科技有限公司 | A kind of shower cream and preparation method thereof |
| CN111743808A (en) * | 2019-03-29 | 2020-10-09 | 和和有限公司 | Antibacterial moistening whitening shower gel |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105997678A (en) * | 2016-06-22 | 2016-10-12 | 广州科玛生物科技股份有限公司 | Washing and care two-in-one infant shower gel |
| CN107998028A (en) * | 2017-12-25 | 2018-05-08 | 深圳市芭格美生物科技有限公司 | A kind of shower cream and preparation method thereof |
| CN111743808A (en) * | 2019-03-29 | 2020-10-09 | 和和有限公司 | Antibacterial moistening whitening shower gel |
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