CN111214389A - Post-foaming makeup-removing bubble composition aerosol and preparation method thereof - Google Patents
Post-foaming makeup-removing bubble composition aerosol and preparation method thereof Download PDFInfo
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- 238000005187 foaming Methods 0.000 title claims abstract description 92
- 239000000443 aerosol Substances 0.000 title claims abstract description 83
- 239000000203 mixture Substances 0.000 title claims abstract description 80
- 238000002360 preparation method Methods 0.000 title abstract description 16
- 238000001856 aerosol method Methods 0.000 title description 2
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 44
- 229930186217 Glycolipid Natural products 0.000 claims abstract description 43
- 239000004088 foaming agent Substances 0.000 claims abstract description 42
- HVCOBJNICQPDBP-UHFFFAOYSA-N 3-[3-[3,5-dihydroxy-6-methyl-4-(3,4,5-trihydroxy-6-methyloxan-2-yl)oxyoxan-2-yl]oxydecanoyloxy]decanoic acid;hydrate Chemical compound O.OC1C(OC(CC(=O)OC(CCCCCCC)CC(O)=O)CCCCCCC)OC(C)C(O)C1OC1C(O)C(O)C(O)C(C)O1 HVCOBJNICQPDBP-UHFFFAOYSA-N 0.000 claims abstract description 40
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 claims abstract description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 28
- 150000002148 esters Chemical class 0.000 claims abstract description 27
- ZAKOWWREFLAJOT-CEFNRUSXSA-N D-alpha-tocopherylacetate Chemical compound CC(=O)OC1=C(C)C(C)=C2O[C@@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-CEFNRUSXSA-N 0.000 claims abstract description 24
- 125000005456 glyceride group Chemical group 0.000 claims abstract description 24
- WWZKQHOCKIZLMA-UHFFFAOYSA-N octanoic acid Chemical compound CCCCCCCC(O)=O WWZKQHOCKIZLMA-UHFFFAOYSA-N 0.000 claims abstract description 24
- XTJKNGLLPGBHHO-HNNXBMFYSA-N (2s)-5-(diaminomethylideneamino)-2-(dodecanoylamino)pentanoic acid Chemical compound CCCCCCCCCCCC(=O)N[C@H](C(O)=O)CCCN=C(N)N XTJKNGLLPGBHHO-HNNXBMFYSA-N 0.000 claims abstract description 23
- SAVLIIGUQOSOEP-UHFFFAOYSA-N N-octanoylglycine Chemical compound CCCCCCCC(=O)NCC(O)=O SAVLIIGUQOSOEP-UHFFFAOYSA-N 0.000 claims abstract description 23
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- 235000012730 carminic acid Nutrition 0.000 claims abstract description 18
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- 239000011259 mixed solution Substances 0.000 claims description 63
- 238000003756 stirring Methods 0.000 claims description 49
- 229940042585 tocopherol acetate Drugs 0.000 claims description 16
- LDTMPQQAWUMPKS-OWOJBTEDSA-N (e)-1-chloro-3,3,3-trifluoroprop-1-ene Chemical group FC(F)(F)\C=C\Cl LDTMPQQAWUMPKS-OWOJBTEDSA-N 0.000 claims description 14
- 238000002156 mixing Methods 0.000 claims description 14
- QUZHZFAQJATMCA-UHFFFAOYSA-N Monogalactosyldiglyceride Natural products CCC=CCC=CCC=CCCCCCCCC(=O)OCC(OC(=O)CCCCCCCC=CCC=CCC=CCC)COC1OC(CO)C(O)C(O)C1O QUZHZFAQJATMCA-UHFFFAOYSA-N 0.000 claims description 11
- 238000007789 sealing Methods 0.000 claims description 10
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- 238000001816 cooling Methods 0.000 claims description 7
- 238000010438 heat treatment Methods 0.000 claims description 7
- DGQLVPJVXFOQEV-JNVSTXMASA-N carminic acid Chemical compound OC1=C2C(=O)C=3C(C)=C(C(O)=O)C(O)=CC=3C(=O)C2=C(O)C(O)=C1[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O DGQLVPJVXFOQEV-JNVSTXMASA-N 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 2
- FROLUYNBHPUZQU-IIZJPUEISA-N (2R,3R,4S,5R)-2-(hydroxymethyl)-6-[3-[3-[(3R,4S,5R,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxypropoxy]propoxy]oxane-3,4,5-triol Chemical compound OC[C@H]1OC(OCCCOCCCOC2O[C@H](CO)[C@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@H]1O FROLUYNBHPUZQU-IIZJPUEISA-N 0.000 claims 1
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- 238000004140 cleaning Methods 0.000 abstract description 18
- 230000000694 effects Effects 0.000 abstract description 16
- ZAKOWWREFLAJOT-UHFFFAOYSA-N d-alpha-Tocopheryl acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C ZAKOWWREFLAJOT-UHFFFAOYSA-N 0.000 abstract description 8
- FOYKKGHVWRFIBD-UHFFFAOYSA-N gamma-tocopherol acetate Natural products CC(=O)OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1 FOYKKGHVWRFIBD-UHFFFAOYSA-N 0.000 abstract description 8
- 239000003755 preservative agent Substances 0.000 abstract description 5
- 230000002335 preservative effect Effects 0.000 abstract description 5
- 239000002537 cosmetic Substances 0.000 abstract description 4
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- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 1
- 239000002775 capsule Substances 0.000 abstract 1
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- 239000007789 gas Substances 0.000 abstract 1
- 238000004806 packaging method and process Methods 0.000 abstract 1
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- 230000000052 comparative effect Effects 0.000 description 27
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- 230000032683 aging Effects 0.000 description 3
- SFNALCNOMXIBKG-UHFFFAOYSA-N ethylene glycol monododecyl ether Chemical compound CCCCCCCCCCCCOCCO SFNALCNOMXIBKG-UHFFFAOYSA-N 0.000 description 3
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- WSDISUOETYTPRL-UHFFFAOYSA-N dmdm hydantoin Chemical compound CC1(C)N(CO)C(=O)N(CO)C1=O WSDISUOETYTPRL-UHFFFAOYSA-N 0.000 description 2
- 239000004519 grease Substances 0.000 description 2
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- 239000000126 substance Substances 0.000 description 2
- RYHBNJHYFVUHQT-UHFFFAOYSA-N 1,4-Dioxane Chemical compound C1COCCO1 RYHBNJHYFVUHQT-UHFFFAOYSA-N 0.000 description 1
- 208000002874 Acne Vulgaris Diseases 0.000 description 1
- 229920000298 Cellophane Polymers 0.000 description 1
- 108010066551 Cholestenone 5 alpha-Reductase Proteins 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- 208000003251 Pruritus Diseases 0.000 description 1
- 206010039792 Seborrhoea Diseases 0.000 description 1
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- 238000005238 degreasing Methods 0.000 description 1
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- 229910021641 deionized water Inorganic materials 0.000 description 1
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Classifications
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/04—Dispersions; Emulsions
- A61K8/046—Aerosols; Foams
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
- A61K8/315—Halogenated hydrocarbons
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
- A61P17/00—Drugs for dermatological disorders
- A61P17/10—Anti-acne agents
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/008—Preparations for oily skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/30—Characterized by the absence of a particular group of ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/596—Mixtures of surface active compounds
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Dermatology (AREA)
- Chemical & Material Sciences (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
- Organic Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Emergency Medicine (AREA)
- Dispersion Chemistry (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to a post-foaming makeup-removing bubble composition aerosol and a preparation method thereof. The invention adopts the technical form of binary capsule valve packaging aerosol, and is prepared from glycolipid, caprylic/capric glyceride polyglycerol-10 esters, dipropylene glycol, a post-foaming agent, lauroyl arginine ethyl ester HCl, caprylyl glycine, xanthan gum, cochineal, tocopheryl acetate, hydroxyethyl cellulose, essence, nitrogen and water. The post-foaming makeup removing bubble composition aerosol provided by the invention uses a natural cleaning component, namely glycolipid, and has a certain water replenishing effect while cleaning efficiently, and after the aerosol is used, the skin is moisturized and oil is controlled for a long time, so that the aerosol has three functions of makeup removing, skin care and oil control; and the product does not contain flammable propellant gas, realizes a safe aerosol technology, has a self-foaming characteristic, does not contain a traditional preservative, and realizes multiple breakthroughs of the product in use performance, skin feel and mildness.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a post-foaming makeup-removing bubble composition aerosol and a preparation method thereof.
Background
The makeup removing products in the current market can be divided into makeup removing oil, makeup removing cream, makeup removing liquid, makeup removing cream and the like according to a system, wherein the makeup removing oil and the makeup removing cream are oil-based systems, the makeup removing performance is good, and the makeup removing products have good cleaning effects on common lipsticks, foundation foundations, mascaras and the like, but the makeup removing products of the oil-based systems have sticky and greasy skin feeling after makeup removal, and need to be cleaned for the second time by using other products to remove the sticky and greasy oil bases. The makeup removing and cleaning effects of the makeup removing liquid and the makeup removing milk are relatively weak, and the makeup such as mascara and the like is usually difficult to clean completely, so that the makeup removing and cleaning lotion has the advantage of better skin feel. The makeup removing product is also available on the market in the form of makeup removing bubbles, but the makeup removing product for cleaning the face usually needs to be added with a large amount of surfactant with high irritation to obtain a good makeup removing effect, so that the skin barrier can be unbalanced and damaged after the makeup removing product is used, and the conditions of allergy, pruritus, dryness, desquamation and the like can be caused. And the irritation risk brought by traditional antisepsis such as cason, DMDMH and the like is also an important embodiment influencing the use experience of products.
In summary, the makeup removing products on the market at present have advantages and disadvantages. Therefore, the method has important practical significance in developing makeup removing products with excellent makeup removing performance, moisturizing and oil and skin controlling feeling, mildness and safety, fun of playing and convenience in use.
Patent document CN201510915655.6 discloses a mild makeup removing cream without emulsifier and a preparation method thereof, wherein the formula of the mild makeup removing cream comprises, by weight, 5-20% of grease, 6-15% of humectant, 0.2-3.0% of suspension stabilizer, 2-10% of natural lignocellulose porous particles with the mesh number of 90-150 and the balance of deionized water. Although the cleansing cream disclosed by the invention is mild and non-irritating, the formula of the cleansing cream contains a large amount of grease, secondary cleaning is needed after cleansing, and the skin is easily greasy after long-time use.
Therefore, the technical problems of sticky and greasy skin after makeup removal, poor makeup removal and cleaning effect, high irritation and the like generally exist in the prior art.
Disclosure of Invention
In order to overcome the defects of the prior art, the invention aims to provide a post-foaming makeup removing bubble composition aerosol and a preparation method thereof. The post-foaming makeup removing bubble composition aerosol provided by the invention is used for cleaning and removing makeup by using natural saccharides, is combined with the wetting and cleaning of polyglycerol, provides excellent makeup removing performance, has the characteristic of long-acting oil control, has a reddish appearance, does not contain a preservative, is mild and non-irritating, can form foam without rubbing, is convenient to use, has good cleaning capability and good moisturizing and oil control performances, and has considerable practical use experience.
In order to achieve the purpose, the technical scheme of the invention is as follows:
a post-foaming makeup-removing bubble composition aerosol comprises the following components in parts by weight:
10-20 parts of glycolipid, 8-20 parts of caprylic/capric glyceride polyglycerol-10 esters, 5-15 parts of dipropylene glycol, 3-8 parts of post-foaming agent, 0.7-1.5 parts of lauroyl arginine ethyl ester HCl, 0.1-0.5 part of caprylyl glycine, 0.3-0.8 part of xanthan gum, 0.3-0.9 part of cochineal, 0.3-0.7 part of tocopherol acetate, 0.1-0.5 part of hydroxyethyl cellulose, 0.1-0.3 part of essence, 0.1-1 part of nitrogen and 40-60 parts of water.
Further, the post-foaming makeup-removing bubble composition aerosol comprises the following components in parts by weight: 12-17 parts of glycolipid, 8-12 parts of caprylic/capric glyceride polyglycerol-10 esters, 6-10 parts of dipropylene glycol, 4-7 parts of post-foaming agent, 1-1.3 parts of lauroyl arginine ethyl ester HCl, 0.1-0.3 part of caprylyl glycine, 0.4-0.7 part of xanthan gum, 0.7-0.9 part of cochineal carmine, 0.4-0.6 part of tocopherol acetate, 0.2-0.4 part of hydroxyethyl cellulose, 0.1-0.2 part of essence, 0.3-0.6 part of nitrogen and 50-60 parts of water.
Furthermore, the post-foaming makeup removing bubble composition aerosol comprises the following components in parts by weight: 15 parts of glycolipid, 10 parts of caprylic/capric glyceride polyglycerol-10 esters, 8 parts of dipropylene glycol, 6 parts of post-foaming agent, 1.2 parts of lauroyl arginine ethyl ester HCl, 0.2 part of caprylyl glycine, 0.6 part of xanthan gum, 0.8 part of cochineal carmine, 0.45 part of tocopherol acetate, 0.3 part of hydroxyethyl cellulose, 0.2 part of essence, 0.5 part of nitrogen and 57 parts of water.
Furthermore, the glycolipid in the post-foaming makeup removing bubble composition aerosol consists of fucoidin, mono-galactosyl diglyceride and di-galactosyl diglyceride according to the mass ratio of 2-5:1-3: 4-7.
Further, a post-foaming agent in the post-foaming makeup removing bubble composition aerosol is trans-1-chloro-3, 3, 3-trifluoropropene.
The invention also provides a preparation method of the post-foaming makeup-removing bubble composition aerosol, which specifically comprises the following steps:
s1, mixing 50% of dipropylene glycol with the formula amount of xanthan gum and hydroxyethyl cellulose, and stirring for 10-20min at the rotation speed of 200rpm to obtain a mixed solution A;
s2, adding the water with the formula amount and the mixed solution A prepared in the step S1 into a reaction kettle, heating to 80-85 ℃, and stirring for 15-25min under the condition that the rotation speed is 200rpm to prepare a mixed solution B;
s3, adding the glycolipid and the caprylic/capric glyceride polyglycerol-10 ester into the mixed solution B prepared in the step S2, and stirring for 15-25min at the rotation speed of 300rpm to prepare a mixed solution C;
s4, mixing 50% of dipropylene glycol, tocopherol acetate and caprylyl glycine according to the formula amount, and stirring for 10min at the rotation speed of 200rpm to obtain a mixed solution D;
s5, adding the mixed solution D obtained in the step S4 into the mixed solution C obtained in the step S3, and stirring for 10min under the condition that the rotating speed is 350rpm to obtain a mixed solution E;
s6, cooling the mixed liquid E prepared in the step S5 to below 45 ℃, adding cochineal, essence and lauroyl arginine ethyl ester HCl, stirring for 10min at the rotation speed of 400rpm, adding a rear foaming agent, continuously stirring for 10-20min, and finally filling nitrogen for sealing to obtain the product.
Compared with the prior art, the invention has the following advantages:
(1) the post-foaming cleansing bubble composition aerosol provided by the invention uses non-petroleum-derived cleaning components, such as glycolipids and caprylic/capric glyceride polyglycerol-10 esters, and does not contain dioxane risk of ethylene oxide; the glycolipid is prepared by fermenting sugar in 100%, is biodegradable in 100%, is clean in high efficiency, can well moisten skin, is compatible with caprylic/capric glyceride polyglycerol-10 esters for use, realizes washing and protecting, is environment-friendly, and promotes sustainable development;
(2) the post-foaming makeup removing bubble composition aerosol provided by the invention realizes the convenience of use through a post-foaming form without adding water for rubbing bubbles. The rear foaming agent is trans-1-chloro-3, 3, 3-trifluoropropene, the boiling point of the rear foaming agent is lower than the normal body temperature of a human body, and the rear foaming agent can be naturally foamed into cleansing foam under the action of the normal body temperature of the human body, but if the addition amount of the rear foaming agent is not suitable for the proportion of other cleaning components, the normal moisturizing function of skin can be damaged, so that the cleansing foam prepared by the inventor does not damage the structures of normal lipid-containing components such as a water lipid membrane and the like kept by the skin by groping the compounding proportion of the rear foaming agent and other active component surfactants, can spontaneously generate rich and fine foam, has good foam stability, and has good functions of cleaning the skin and maintaining the moisturizing of the skin;
(3) the post-foaming makeup removing bubble composition aerosol provided by the invention has the advantages that the skin is moist and not tight after being used, the long-acting oil control effect can be achieved, the product is compounded with caprylyl glycine, the oil-water balance of the skin can be effectively adjusted, the 5 α reductase activity is inhibited, the sebum secretion is reduced, the long-acting oil control effect is realized, the skin is moist and not greasy after being used, and the oily skin, the whelk and acne skin are improved;
(4) the post-foaming makeup removing bubble composition aerosol provided by the invention does not use the traditional preservative (such as DMDMH preservative with formaldehyde release, cason and the like which are verified by multiple European tests to have irritation, sensitization and the like on skin), the existing formula realizes the mildness and stability of the formula without the preservative by compounding and synergism and using lauroyl arginine ethyl ester HCl.
(5) The post-foaming makeup removing bubble composition aerosol provided by the invention realizes that the product has a transparent red appearance through a natural colorant and does not contain traditional artificial pigments.
Detailed Description
The present invention will be further described below by way of specific embodiments, but the present invention is not limited to only the following examples. Various modifications can be made by those skilled in the art based on the basic idea of the invention, but it is within the scope of the invention as long as it does not depart from the basic idea of the invention.
The reagents used in the invention are all common and practical and can be purchased from conventional reagent production and sale companies.
Example 1 Aerosol post-foaming Makeup-removing bubble composition
A post-foaming makeup-removing bubble composition aerosol comprises the following components in parts by weight: 12 parts of glycolipid, 8 parts of caprylic/capric glyceride polyglycerol-10 esters, 6 parts of dipropylene glycol, 4 parts of post-foaming agent, 1 part of lauroyl arginine ethyl ester HCl, 0.1 part of caprylyl glycine, 0.4 part of xanthan gum, 0.7 part of cochineal, 0.4 part of tocopheryl acetate, 0.2 part of hydroxyethyl cellulose, 0.1 part of essence, 0.3 part of nitrogen and 50 parts of water.
The glycolipid in the post-foaming makeup-removing bubble composition aerosol is composed of fucoidin, mono-galactosyl diglyceride and di-galactosyl diglyceride according to the mass ratio of 2:1: 4. The post-foaming agent in the post-foaming makeup removing bubble composition aerosol is trans-1-chloro-3, 3, 3-trifluoropropene.
The preparation method of the post-foaming makeup removing bubble composition aerosol specifically comprises the following steps:
s1, mixing 50% of dipropylene glycol with the formula amount of xanthan gum and hydroxyethyl cellulose, and stirring for 10min at the rotation speed of 200rpm to obtain a mixed solution A;
s2, adding the water with the formula amount and the mixed solution A prepared in the step S1 into a reaction kettle, heating to 80 ℃, and stirring for 15min at the rotation speed of 200rpm to prepare a mixed solution B;
s3, adding the glycolipid and the caprylic/capric glyceride polyglycerol-10 ester into the mixed solution B prepared in the step S2, and stirring for 15min at the rotation speed of 300rpm to prepare a mixed solution C;
s4, mixing 50% of dipropylene glycol, tocopherol acetate and caprylyl glycine according to the formula amount, and stirring for 10min at the rotation speed of 200rpm to obtain a mixed solution D;
s5, adding the mixed solution D obtained in the step S4 into the mixed solution C obtained in the step S3, and stirring for 10min under the condition that the rotating speed is 350rpm to obtain a mixed solution E;
s6, cooling the mixed liquid E prepared in the step S5 to below 45 ℃, adding cochineal, essence and lauroyl arginine ethyl ester HCl, stirring for 10min at the rotation speed of 400rpm, adding a rear foaming agent, continuously stirring for 10min, and finally filling nitrogen for sealing to obtain the product.
Example 2 post-foaming cleansing bubble composition aerosol
A post-foaming makeup-removing bubble composition aerosol comprises the following components in parts by weight: 13 parts of glycolipid, 9 parts of caprylic/capric glyceride polyglycerol-10 esters, 7 parts of dipropylene glycol, 5 parts of post-foaming agent, 1.15 parts of lauroyl arginine ethyl ester HClI, 0.15 part of caprylyl glycine, 0.5 part of xanthan gum, 0.75 part of cochineal, 0.5 part of tocopheryl acetate, 0.25 part of hydroxyethyl cellulose, 0.15 part of essence, 0.4 part of nitrogen and 55 parts of water.
The glycolipid in the post-foaming makeup-removing bubble composition aerosol is composed of fucoidin, mono-galactosyl diglyceride and di-galactosyl diglyceride according to the mass ratio of 3:2: 5. The post-foaming agent in the post-foaming makeup removing bubble composition aerosol is trans-1-chloro-3, 3, 3-trifluoropropene.
The preparation method of the post-foaming makeup removing bubble composition aerosol specifically comprises the following steps:
s1, mixing 50% of dipropylene glycol with the formula amount of xanthan gum and hydroxyethyl cellulose, and stirring for 14min at the rotation speed of 200rpm to obtain a mixed solution A;
s2, adding the water with the formula amount and the mixed solution A prepared in the step S1 into a reaction kettle, heating to 81 ℃, and stirring for 18min at the rotation speed of 200rpm to prepare a mixed solution B;
s3, adding the glycolipid and the caprylic/capric acid glyceride polyglycerol-10 ester into the mixed solution B prepared in the step S2, and stirring for 18min at the rotation speed of 300rpm to prepare mixed solution C;
s4, mixing 50% of dipropylene glycol, tocopherol acetate and caprylyl glycine according to the formula amount, and stirring for 10min at the rotation speed of 200rpm to obtain a mixed solution D;
s5, adding the mixed solution D obtained in the step S4 into the mixed solution C obtained in the step S3, and stirring for 10min under the condition that the rotating speed is 350rpm to obtain a mixed solution E;
s6, cooling the mixed liquid E prepared in the step S5 to below 45 ℃, adding cochineal, essence and lauroyl arginine ethyl ester HCl, stirring for 10min at the rotation speed of 400rpm, adding a rear foaming agent, continuously stirring for 13min, and finally filling nitrogen for sealing to obtain the product.
Example 3 post-foaming cleansing bubble composition Aerosol
A post-foaming makeup-removing bubble composition aerosol comprises the following components in parts by weight: 15 parts of glycolipid, 10 parts of caprylic/capric glyceride polyglycerol-10 esters, 8 parts of dipropylene glycol, 6 parts of post-foaming agent, 1.2 parts of lauroyl arginine ethyl ester HCl, 0.2 part of caprylyl glycine, 0.6 part of xanthan gum, 0.8 part of cochineal, 0.45 part of tocopheryl acetate, 0.3 part of hydroxyethyl cellulose, 0.2 part of essence, 0.5 part of nitrogen and 57 parts of water.
The glycolipid in the post-foaming makeup-removing bubble composition aerosol is composed of fucoidin, mono-galactosyl diglyceride and di-galactosyl diglyceride according to the mass ratio of 4:3: 5. The post-foaming agent in the post-foaming makeup removing bubble composition aerosol is trans-1-chloro-3, 3, 3-trifluoropropene.
The preparation method of the post-foaming makeup removing bubble composition aerosol specifically comprises the following steps:
s1, mixing 50% of dipropylene glycol with the formula amount of xanthan gum and hydroxyethyl cellulose, and stirring for 16min at the rotation speed of 200rpm to obtain a mixed solution A;
s2, adding the water with the formula amount and the mixed solution A prepared in the step S1 into a reaction kettle, heating to 83 ℃, and stirring for 20min at the rotation speed of 200rpm to prepare a mixed solution B;
s3, adding the glycolipid and the caprylic/capric acid glyceride polyglycerol-10 ester into the mixed solution B prepared in the step S2, and stirring for 20min at the rotation speed of 300rpm to prepare a mixed solution C;
s4, mixing 50% of dipropylene glycol, tocopherol acetate and caprylyl glycine according to the formula amount, and stirring for 10min at the rotation speed of 200rpm to obtain a mixed solution D;
s5, adding the mixed solution D obtained in the step S4 into the mixed solution C obtained in the step S3, and stirring for 10min under the condition that the rotating speed is 350rpm to obtain a mixed solution E;
s6, cooling the mixed liquid E prepared in the step S5 to below 45 ℃, adding cochineal, essence and lauroyl arginine ethyl ester HCl, stirring for 10min at the rotation speed of 400rpm, adding a rear foaming agent, continuing stirring for 15min, and finally filling nitrogen for sealing to obtain the product.
Example 4 Aerosol post-foaming Makeup-removing bubble composition
A post-foaming makeup-removing bubble composition aerosol comprises the following components in parts by weight: 16 parts of glycolipid, 11 parts of caprylic/capric glyceride polyglycerol-10 esters, 9 parts of dipropylene glycol, 6.5 parts of post-foaming agent, 1.25 parts of lauroyl arginine ethyl ester HCl, 0.25 part of caprylyl glycine, 0.65 part of xanthan gum, 0.85 part of cochineal carmine, 0.55 part of tocopherol acetate, 0.35 part of hydroxyethyl cellulose, 0.12 part of essence, 0.55 part of nitrogen and 59 parts of water.
The glycolipid in the post-foaming makeup-removing bubble composition aerosol is composed of fucoidin, mono-galactosyl diglyceride and di-galactosyl diglyceride according to the mass ratio of 2:3: 7. The post-foaming agent in the post-foaming makeup removing bubble composition aerosol is trans-1-chloro-3, 3, 3-trifluoropropene.
The preparation method of the post-foaming makeup removing bubble composition aerosol specifically comprises the following steps:
s1, mixing 50% of dipropylene glycol with the formula amount of xanthan gum and hydroxyethyl cellulose, and stirring for 18min at the rotation speed of 200rpm to obtain a mixed solution A;
s2, adding the water with the formula amount and the mixed solution A prepared in the step S1 into a reaction kettle, heating to 84 ℃, and stirring for 23min at the rotation speed of 200rpm to prepare a mixed solution B;
s3, adding the glycolipid and the caprylic/capric acid glyceride polyglycerol-10 ester into the mixed solution B prepared in the step S2, and stirring for 23min at the rotation speed of 300rpm to prepare mixed solution C;
s4, mixing 50% of dipropylene glycol, tocopherol acetate and caprylyl glycine according to the formula amount, and stirring for 10min at the rotation speed of 200rpm to obtain a mixed solution D;
s5, adding the mixed solution D obtained in the step S4 into the mixed solution C obtained in the step S3, and stirring for 10min under the condition that the rotating speed is 350rpm to obtain a mixed solution E;
s6, cooling the mixed liquid E prepared in the step S5 to below 45 ℃, adding cochineal, essence and lauroyl arginine ethyl ester HCl, stirring for 10min at the rotation speed of 400rpm, adding a rear foaming agent, continuously stirring for 17min, and finally filling nitrogen for sealing to obtain the product.
Example 5 Aerosol post-foaming Makeup-removing bubble composition
A post-foaming makeup-removing bubble composition aerosol comprises the following components in parts by weight: 17 parts of glycolipid, 12 parts of caprylic/capric glyceride polyglycerol-10 esters, 10 parts of dipropylene glycol, 7 parts of post-foaming agent, 1.3 parts of lauroyl arginine ethyl ester HClI, 0.3 part of caprylyl glycine, 0.7 part of xanthan gum, 0.9 part of cochineal, 0.6 part of tocopheryl acetate, 0.4 part of hydroxyethyl cellulose, 0.17 part of essence, 0.6 part of nitrogen and 60 parts of water.
The glycolipid in the post-foaming makeup-removing bubble composition aerosol is composed of fucoidin, mono-galactosyl diglyceride and di-galactosyl diglyceride according to the mass ratio of 5:2: 6. The post-foaming agent in the post-foaming makeup removing bubble composition aerosol is trans-1-chloro-3, 3, 3-trifluoropropene.
The preparation method of the post-foaming makeup removing bubble composition aerosol specifically comprises the following steps:
s1, mixing 50% of dipropylene glycol with the formula amount of xanthan gum and hydroxyethyl cellulose, and stirring for 20min at the rotation speed of 200rpm to obtain a mixed solution A;
s2, adding the water with the formula amount and the mixed solution A prepared in the step S1 into a reaction kettle, heating to 85 ℃, and stirring for 25min at the rotation speed of 200rpm to prepare a mixed solution B;
s3, adding the glycolipid and the caprylic/capric glyceride polyglycerol-10 ester into the mixed solution B prepared in the step S2, and stirring for 25min at the rotation speed of 300rpm to prepare a mixed solution C;
s4, mixing 50% of dipropylene glycol, tocopherol acetate and caprylyl glycine according to the formula amount, and stirring for 10min at the rotation speed of 200rpm to obtain a mixed solution D;
s5, adding the mixed solution D obtained in the step S4 into the mixed solution C obtained in the step S3, and stirring for 10min under the condition that the rotating speed is 350rpm to obtain a mixed solution E;
s6, cooling the mixed liquid E prepared in the step S5 to below 45 ℃, adding cochineal, essence and lauroyl arginine ethyl ester HCl, stirring for 10min at the rotation speed of 400rpm, adding a rear foaming agent, continuously stirring for 20min, and finally filling nitrogen for sealing to obtain the product.
Comparative example 1 post-foaming cleansing foam composition aerosol
A post-foaming makeup-removing bubble composition aerosol comprises the following components in parts by weight: 12.75 parts of glycolipid, 42.25 parts of laureth-42.25 parts of caprylic/capric glyceride polyglycerol-10 esters, 8 parts of dipropylene glycol, 6 parts of post-foaming agent, 1.2 parts of lauroyl arginine ethyl ester HCl, 0.2 part of caprylyl glycine, 0.6 part of xanthan gum, 0.8 part of cochineal carmine, 0.45 part of tocopherol acetate, 0.3 part of hydroxyethyl cellulose, 0.2 part of essence, 0.5 part of nitrogen and 57 parts of water.
The glycolipid in the post-foaming makeup-removing bubble composition aerosol is composed of fucoidin, mono-galactosyl diglyceride and di-galactosyl diglyceride according to the mass ratio of 4:3: 5. The post-foaming agent in the post-foaming makeup removing bubble composition aerosol is trans-1-chloro-3, 3, 3-trifluoropropene.
The preparation method of the post-foaming makeup removing bubble composition aerosol is similar to that of the example 3.
The comparative example differs from example 3 in that laureth-4 is used instead of 15% of the glycolipid.
Comparative example 2 post-foaming cleansing foam composition aerosol
A post-foaming makeup-removing bubble composition aerosol comprises the following components in parts by weight: 15 parts of glycolipid, 10 parts of PEG-7 glyceryl cocoate, 8 parts of dipropylene glycol, 6 parts of post-foaming agent, 1.2 parts of lauroyl arginine ethyl ester HCl, 0.2 part of caprylyl glycine, 0.6 part of xanthan gum, 0.8 part of cochineal, 0.45 part of tocopheryl acetate, 0.3 part of hydroxyethyl cellulose, 0.2 part of essence, 0.5 part of nitrogen and 57 parts of water.
The glycolipid in the post-foaming makeup-removing bubble composition aerosol is composed of fucoidin, mono-galactosyl diglyceride and di-galactosyl diglyceride according to the mass ratio of 4:3: 5. The post-foaming agent in the post-foaming makeup removing bubble composition aerosol is trans-1-chloro-3, 3, 3-trifluoropropene.
The preparation method of the post-foaming makeup removing bubble composition aerosol is similar to the embodiment 3.
This comparative example differs from example 3 in that PEG-7 glyceryl cocoate was used in place of the caprylic/capric glyceride polyglyceryl-10 esters in this comparative example.
Comparative example 3 post-foaming cleansing foam composition aerosol
A post-foaming makeup-removing bubble composition aerosol comprises the following components in parts by weight: 15 parts of glycolipid, 10 parts of caprylic/capric glyceride polyglycerol-10 esters, 8 parts of dipropylene glycol, 8 parts of post-foaming agent, 1.2 parts of lauroyl arginine ethyl ester HCl, 0.2 part of caprylyl glycine, 0.6 part of xanthan gum, 0.8 part of cochineal, 0.45 part of tocopheryl acetate, 0.3 part of hydroxyethyl cellulose, 0.2 part of essence, 0.5 part of nitrogen and 57 parts of water.
The glycolipid in the post-foaming makeup-removing bubble composition aerosol is composed of fucoidin, mono-galactosyl diglyceride and di-galactosyl diglyceride according to the mass ratio of 4:3: 5. The post-foaming agent in the post-foaming makeup removing bubble composition aerosol is trans-1-chloro-3, 3, 3-trifluoropropene.
The preparation method of the post-foaming makeup removing bubble composition aerosol is similar to that of the example 3.
This comparative example differs from example 3 in that the amount of post-foaming agent used in this comparative example is 8 parts.
Comparative example 3 post-foaming cleansing foam composition aerosol
A post-foaming makeup-removing bubble composition aerosol comprises the following components in parts by weight: 15 parts of glycolipid, 10 parts of caprylic/capric glyceride polyglycerol-10 esters, 8 parts of dipropylene glycol, 6 parts of post-foaming agent, 1.2 parts of lauroyl arginine ethyl ester HCl, 0.2 part of caprylyl glycine, 0.6 part of xanthan gum, 0.8 part of cochineal, 0.3 part of hydroxyethyl cellulose, 0.2 part of essence, 0.5 part of nitrogen and 57 parts of water.
The glycolipid in the post-foaming makeup-removing bubble composition aerosol is composed of fucoidin, mono-galactosyl diglyceride and di-galactosyl diglyceride according to the mass ratio of 4:3: 5. The post-foaming agent in the post-foaming makeup removing bubble composition aerosol is trans-1-chloro-3, 3, 3-trifluoropropene.
The preparation method of the post-foaming makeup removing bubble composition aerosol is similar to that of the example 3.
This comparative example differs from example 3 in that no tocopheryl acetate was added to the comparative example.
Test example I Performance test of Aerosol composition for post-foaming cleansing bubble
1. Test materials: the post-foaming cleansing foam composition aerosols prepared in examples 1 to 5 and comparative examples 1 to 4;
2. the test method comprises the following steps: selecting 180 female subjects with healthy skin, wherein the female subjects are 20-40 years old and are randomly divided into 9 groups of 20 persons; selecting healthy skin with the inner side of arm of 5cm × 6cm for each group of subjects, uniformly applying eyebrow pencil, lipstick and mascara with the area of 3cm × 1cm, then respectively applying the aerosol of the post-foaming makeup removing bubble composition prepared in examples 1-5 and comparative examples 1-4 with the diameter of 0.5-0.8cm, observing the foam generation condition, wiping with cotton cloth after 20s, and respectively recording the self-foaming time, the foam condition, the number of times of wiping to complete cleaning and the skin feeling after washing;
3. the test results are shown in table 1.
TABLE 1 results of aerosol performance test of post-foaming cleansing foam composition
As can be seen from the above Table 1, the cleansing foam composition aerosol prepared in the embodiments 1 to 5 of the present invention has the advantages of short self-foaming time, easy rinsing, obvious cleaning effect, good skin feel after rinsing, and moistening without tightness, wherein the self-foaming time is the shortest and the comprehensive performance is the best embodiment of the present invention in the embodiment 3;
compared with example 3, in comparative example 1, the laureth-4 is used instead of the glycolipid, so that the makeup removing and cleaning effect of comparative example 1 is greatly weakened, the self-foaming time is also reduced, the degreasing force is obviously enhanced, and the skin feel is dry and tight. In comparative example 2, classic water-soluble oil PEG-7 glyceryl cocoate is used for replacing caprylic/capric glyceride polyglycerol-10 esters, the rest components are unchanged, the cleansing effect of the prepared sample is obviously weakened, and meanwhile, the effect of slowing down the self-foaming time is influenced. In the comparative example 3, the addition amount of the surfactant is unchanged, the addition amount of the trans-1-chloro-3, 3, 3-trifluoropropene is increased, the self-foaming time of the prepared makeup removing bubble is obviously shortened, the bubble is slightly sticky, the bubble needs to be washed clean for many times, the cleaning effect is obvious, but the skin after washing is moderately dry and tight; in comparative example 4, the antioxidant tocopherol acetate was not added, the ratio of the remaining ingredients was not changed, and the oil control effect was not good for 8 hours. Therefore, the glycolipid, caprylic/capric glyceride polyglycerol-10 esters and dipropylene glycol are compounded in a proper proportion and are simultaneously synergistic with 1-chloro-3, 3, 3-trifluoropropene, and the prepared makeup removing bubble has the advantages of short self-foaming time, excellent makeup removing function, good skin feel after washing, no tightness and lasting oil control.
Test example two, acute skin irritation test of aerosol of post-foaming cleansing bubble composition
1. Test materials: the post-foaming cleansing foam composition aerosols prepared in examples 1 to 5 and comparative examples 1 to 3;
2. the test method comprises the following steps: according to the skin irritation/corrosivity test method of the ' cosmetic safety technical specification ' 2015 edition of the ministry of health of the people's republic of China, 160 general-grade New Zealand rabbits qualified for quarantine are averagely divided into 8 groups, and each group of the New Zealand rabbits is provided with ten males and females for skin irritation test. Before the test, the hair on both sides of the spine of the experimental animal is cut off, and the hair removing range is about 3cm multiplied by 3cm respectively. Approximately 0.5g of the post-foaming cleansing foam prepared in each of examples 1-5 and comparative examples 1-3 was applied to the left skin of the animal, covered with two layers of gauze (2.5 cm. times.2.5 cm) and a layer of cellophane or the like, and secured with a non-irritating adhesive tape and bandage. The other side of the skin served as a control. The application time is 2h by adopting a sealing test. After the test is finished, the residual test substance is removed by warm water or a non-irritant solvent. And observing skin reaction of the smearing part for 1, 24, 48 and 72h after removing the test substance, grading the skin reaction, performing comprehensive evaluation by using the average value of the integral of the tested animal, and judging the skin irritation intensity according to the highest integral average value of each observation time point of 24, 48 and 72 h.
3. Skin irritation response scores are shown in table 2; skin irritation intensity was graded as shown in table 3; the test results are shown in Table 4.
TABLE 2 skin irritation response score
TABLE 3 skin irritation Strength grading
| Integral mean value | Strength of |
| 0—＜0.5 | Has no irritation |
| 0.5—＜2.0 | Light irritation |
| 2.0—＜6.0 | Middle irritation |
| 6.0—8.0 | Strong irritation |
TABLE 4 results of the Aerosol acute skin irritation test for post-foaming cleansing foam compositions
As can be seen from the test results in the table, the aerosol of the post-foaming cleansing foam composition prepared in the examples 1 to 5 of the present invention is non-irritant and meets the requirement that the integral mean value is lower than 0.5. The integral mean value of example 3 is 0, and the irritation is lowest at the same ratio and is most mild to human skin.
Comparing example 3 with comparative examples 2 and 3, it can be seen that the integral mean of irritation is lower in example 3 under the same proportion of glycolipids, indicating that the effect of glycolipids on the protection of skin barrier function and the reduction of critical micelle concentration in the formulation of the present invention, exerts an irritation reducing effect.
Compared with example 3, in comparative example 1, the irritation is greatly increased to be medium irritation by using laureth-4 instead of glycolipid, which shows that the glycolipid has good performance in makeup removing effect and mildness. Comparative example 2 PEG-7 glyceryl cocoate was used instead of caprylic/capric glyceride polyglycerol-10 esters, the increase in irritation being mild. The addition amount of the post-foaming agent is increased in comparative example 3, the integral mean value of the prepared post-foaming makeup removing bubbles is obviously increased and exceeds the range of 0-0.5, and the irritation of the comparative example 3 is evaluated to be light irritation according to a skin irritation/corrosion test scoring system of a cosmetic safety technical specification 2015 edition. The addition of the post-foaming agent is explained, and the irritation of the post-foaming agent is increased after a certain proportion is exceeded.
Test example III accelerated aging test of Aerosol composition for post-foaming cleansing bubble
1. Test materials: post-foaming cleansing bubbles prepared in example 3 and comparative example 4;
2. the test method comprises the following steps: respectively carrying out positive, transverse and inverted placing on test samples in-8 +/-2 ℃ and 43 +/-2 ℃ temperature environments, standing for 90 days, then returning to normal temperature, and observing the appearance, self-foaming and sealing performance of the product after 24 hours.
3. The test results are shown in Table 5.
TABLE 5 accelerated aging test results for post-foaming cleansing foam composition aerosols
As can be seen from Table 5, example 3, which was verified by the three accelerated aging tests described above, showed a normal appearance, a normal self-foaming speed and a good sealing performance, whereas comparative example 4, which did not contain the antioxidant tocopherol acetate, showed a fading of the natural colorant cochineal when stored at 43. + -. 2 ℃ for 90 days.
The foregoing embodiments are merely illustrative of the principles and utilities of the present invention and are not intended to limit the invention. Those skilled in the art will recognize that changes may be made to the embodiments described above without departing from the spirit and scope of the invention. Therefore, it is intended that all equivalent modifications or changes which can be made by those skilled in the art without departing from the technical spirit of the present invention are covered by the claims of the present invention.
Claims (5)
1. The post-foaming makeup-removing bubble composition aerosol is characterized by comprising the following components in parts by weight: 10-20 parts of glycolipid, 8-20 parts of caprylic/capric glyceride polyglycerol-10 esters, 5-15 parts of dipropylene glycol, 3-8 parts of post-foaming agent, 0.7-1.5 parts of lauroyl arginine ethyl ester HCl, 0.1-0.5 part of caprylyl glycine, 0.3-0.8 part of xanthan gum, 0.3-0.9 part of cochineal, 0.3-0.7 part of tocopherol acetate, 0.1-0.5 part of hydroxyethyl cellulose, 0.1-0.3 part of essence, 0.1-1 part of nitrogen and 40-60 parts of water.
2. The aerosol post-foaming cleansing bubble composition of claim 1, comprising the following components in parts by weight: 15 parts of glycolipid, 10 parts of caprylic/capric glyceride polyglycerol-10 esters, 8 parts of dipropylene glycol, 6 parts of post-foaming agent, 1.2 parts of lauroyl arginine ethyl ester HCl, 0.2 part of caprylyl glycine, 0.6 part of xanthan gum, 0.8 part of cochineal carmine, 0.45 part of tocopherol acetate, 0.3 part of hydroxyethyl cellulose, 0.2 part of essence, 0.5 part of nitrogen and 57 parts of water.
3. The aerosol post-foaming cleansing bubble composition of claim 2, wherein the glycolipid consists of fucoidan, monogalactosyl diglyceride, digalactosyl diglyceride in a mass ratio of 2-5:1-3: 4-7.
4. The aerosol post-foaming cleansing bubble composition of claim 2, wherein the post-foaming agent is trans-1-chloro-3, 3, 3-trifluoropropene.
5. A method for preparing the aerosol of post-foaming cleansing bubble composition according to any one of claims 1-4, comprising the steps of:
s1, mixing 50% of dipropylene glycol with the formula amount of xanthan gum and hydroxyethyl cellulose, and stirring for 10-20min at the rotation speed of 200rpm to obtain a mixed solution A;
s2, adding the water with the formula amount and the mixed solution A prepared in the step S1 into a reaction kettle, heating to 80-85 ℃, and stirring for 15-25min under the condition that the rotation speed is 200rpm to prepare a mixed solution B;
s3, adding the glycolipid and the caprylic/capric glyceride polyglycerol-10 ester into the mixed solution B prepared in the step S2, and stirring for 15-25min at the rotation speed of 300rpm to prepare a mixed solution C;
s4, mixing 50% of dipropylene glycol, tocopherol acetate and caprylyl glycine according to the formula amount, and stirring for 10min at the rotation speed of 200rpm to obtain a mixed solution D;
s5, adding the mixed solution D obtained in the step S4 into the mixed solution C obtained in the step S3, and stirring for 10min under the condition that the rotating speed is 350rpm to obtain a mixed solution E;
s6, cooling the mixed liquid E prepared in the step S5 to below 45 ℃, adding cochineal, essence and lauroyl arginine ethyl ester HCl, stirring for 10min at the rotation speed of 400rpm, adding a rear foaming agent, continuously stirring for 10-20min, and finally filling nitrogen for sealing to obtain the product.
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Cited By (2)
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| CN116099397A (en) * | 2023-01-16 | 2023-05-12 | 广东省粤东技师学院 | Bubble water and preparation method thereof |
| WO2024127300A1 (en) * | 2022-12-16 | 2024-06-20 | L'oreal | Micellar bi-phase makeup spray in a non-aerosol fine mist packaging |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2024127300A1 (en) * | 2022-12-16 | 2024-06-20 | L'oreal | Micellar bi-phase makeup spray in a non-aerosol fine mist packaging |
| CN116099397A (en) * | 2023-01-16 | 2023-05-12 | 广东省粤东技师学院 | Bubble water and preparation method thereof |
| CN116099397B (en) * | 2023-01-16 | 2023-10-24 | 广东省粤东技师学院 | Bubble water and preparation method thereof |
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