CN105666971A - 一种压花抗菌保暖复合面料的制备方法 - Google Patents

一种压花抗菌保暖复合面料的制备方法 Download PDF

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CN105666971A
CN105666971A CN201511031727.7A CN201511031727A CN105666971A CN 105666971 A CN105666971 A CN 105666971A CN 201511031727 A CN201511031727 A CN 201511031727A CN 105666971 A CN105666971 A CN 105666971A
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黄关林
钟国能
何立锋
王健刚
汪治燕
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Ningbo Daqian Textile Co Ltd
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    • D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
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    • D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
    • D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
    • D06M13/46—Compounds containing quaternary nitrogen atoms
    • D06M13/463—Compounds containing quaternary nitrogen atoms derived from monoamines
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
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    • B—PERFORMING OPERATIONS; TRANSPORTING
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    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2307/00—Properties of the layers or laminate
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
    • B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
    • B32B2307/00—Properties of the layers or laminate
    • B32B2307/70—Other properties
    • B32B2307/714—Inert, i.e. inert to chemical degradation, corrosion
    • B32B2307/7145—Rot proof, resistant to bacteria, mildew, mould, fungi
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B32—LAYERED PRODUCTS
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Abstract

本发明公开了一种压花抗菌保暖复合面料的制备方法。采用氯异氰尿酸钠、2-羟基-4-正辛氧基二苯甲酮、十四烷基三甲基氯化铵和纳米SiO2粉体配制的混合液进行前处理工艺，对抗菌面料进行改性，然后将抗菌面料和镂空海绵通过热熔技术复合，再通过高温压花，制得压花防风透气型复合面料。本发明方法操作工艺简单，生产效率高，制得的压花抗菌保暖复合面料具备良好的抗菌性能和抗静电性，且花型种类丰富、风格独特，保暖性能和防风透气效果优良。

Description

一种压花抗菌保暖复合面料的制备方法
技术领域
本发明属于纺织材料技术领域，尤其涉及一种压花抗菌保暖复合面料的制备方法。
背景技术
随着生活水平的提高，人们对衣物的要求越来越高，功能性服装面料有防风、防水、速干、防紫外线和不容易脏的特点，成为春秋季节户外运动服装的主要材料之一。户外运动功能性面料制作的服装，以休闲时尚为主，讲究做工精细，手感柔软，穿着舒适，适用于旅游、野外活动等。
目前常规功能性面料的生产，一般使用复杂提花织机织造，面料生产过程中夹层喂入涤纶长丝填充，操作复杂，生产效率低，面料洗水过程中，夹层的涤纶丝容易出现漏丝严重影响服用性能。在穿着时，其透气性差，身体产生的热气很难挥发出，容易滋生病菌，使穿着者产生不适感，且其表面较平整，立体感差。同时存在质地较重，色彩及花型变化少，满足不料人们对时尚、舒适的追求。因此，如何提供一种花型种类丰富、透气保暖以及抗菌的的面料以满足人们需求，势必成为当前纺织材料的发展趋势。
发明内容
本发明为解决现有技术中的上述问题，提供一种压花抗菌保暖复合面料的制备方法。
为实现上述目的，本发明采用以下技术方案：
本发明的提供一种压花抗菌保暖复合面料的制备方法，包括以下步骤：
(1)取三氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮，分别用水配制成2-4wt％的二氯异氰尿酸钠溶液和1-3wt％的2-羟基-4-正辛氧基二苯甲酮溶液，然后按重量比1：1-2混合均匀，再加入十四烷基三甲基氯化铵和纳米SiO2粉体，混合均匀，得整理液；
(2)将抗菌面料放入步骤(1)混合均匀的整理液中，二浸二扎，轧余率70％-85％；
(3)将化纤复合面料在110-150℃下进行预烘1min，再在100-130℃下烘1min，定型；
(4)将定型后的抗菌面料与镂空海绵在40-80℃下热熔复合，得内外两层为抗菌面料、中间层为镂空海绵的复合面料；
(5)将上述复合后的面料在190-220℃下进行压花，时间5-30s，得压花抗菌保暖复合面料。
进一步地，所述步骤(1)中十四烷基三甲基氯化铵的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的3-5wt％。
进一步地，所述步骤(1)中改性纳米SiO2粉体的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的0.1-0.3wt％。
进一步地，所述改性纳米SiO2粉体的粒径为粒径为60-200nm。
进一步地，所述改性纳米SiO2粉体在加入前经硅烷偶联剂进行改性处理，优选的所述硅烷偶联剂为KH-560或KH-570。
进一步地，所述步骤(2)中抗菌面料为涤纶或尼龙或腈纶，所述抗菌面料还可以选用天然纤维面料或化纤复合面料，如纯棉复合面料，全涤复合面料或锦纶复合面料等。
进一步地，所述步骤(4)中镂空海绵的厚度为0.2-0.4cm，优选的镂空海绵的厚度为0.3cm。
进一步地，所述步骤(4)中热熔复合步骤采用研泰TS9012胶水。
本发明采用上述技术方案，与现有技术相比，具有如下技术效果：
本发明制备方法是将抗菌面料和镂空海绵通过热熔技术复合，操作简便和生产效率高，由于海绵具有优异的吸湿透气性，良好的保暖性以及可塑性能，复合后的面料风格独特，保暖性能优于常规织造面料同时洗水牢度强。本发明方法采用在与镂空海绵进行复合前对抗菌面料进行改性处理，使制得的复合面料具备良好的抗菌性能和抗静电性，相比常规的生产方法，生产效率高，花型种类丰富、保暖效果更好。
具体实施方式
本发明提供了一种生产效率高，花型种类丰富，抗菌性能和保暖性能优良的压花抗菌保暖复合面料的制备方法。
下面通过具体实施例对本发明进行详细和具体的介绍，以使更好的理解本发明，但是下述实施例并不限制本发明范围。
实施例1压花抗菌保暖复合面料的制备
(1)取三氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮，分别用水配制成2wt％的二氯异氰尿酸钠溶液和2wt％的2-羟基-4-正辛氧基二苯甲酮溶液，然后按重量比1：1.5混合均匀，再加入十四烷基三甲基氯化铵和经KH-560改性后的纳米SiO2粉体，混合均匀，得整理液；
其中，十四烷基三甲基氯化铵的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的5wt％；改性纳米SiO2粉体的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的0.1wt％。
(2)将纯棉复合面料放入步骤(1)混合均匀的整理液中，二浸二扎，轧余率75％；
(3)将化纤复合面料在120℃下进行预烘1min，再在130℃下烘1min，定型；
(4)将定型后的纯棉复合面料与取镂空海绵在60℃热熔复合，得内外两层为纯棉复合面料、中间层为镂空海绵的抗菌复合面料；
(5)将上述复合后的面料在190℃下进行压花，时间20s，得压花抗菌保暖复合面料。
本实施例1制得的压花抗菌保暖复合面料经10-20次水洗烘干后面料层与海绵层不脱落，达到了耐克的测试标准。
实施例2压花抗菌保暖复合面料的制备
(1)取三氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮，分别用水配制成2wt％的二氯异氰尿酸钠溶液和3wt％的2-羟基-4-正辛氧基二苯甲酮溶液，然后按重量比1：2混合均匀，再加入十四烷基三甲基氯化铵和经KH-560改性后的纳米SiO2粉体，混合均匀，得整理液；
其中，十四烷基三甲基氯化铵的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的5wt％；改性纳米SiO2粉体的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的0.1wt％。
(2)将全涤复合面料放入步骤(1)混合均匀的整理液中，二浸二扎，轧余率85％；
(3)将化纤复合面料在150℃下进行预烘1min，再在130℃下烘1min，定型；
(4)将定型后的全涤复合面料与镂空海绵在80℃下热熔复合，得内外两层为全涤复合面料、中间层为镂空海绵的抗菌复合面料；
(5)将上述复合后的面料在220℃下进行压花，时间20s，得压花抗菌保暖复合面料。
本实施例2制得的压花抗菌保暖复合面料经30-40次水洗烘干后面料层与海绵层不脱落，达到了耐克的测试标准。
实施例3压花抗菌保暖复合面料的制备
(1)取三氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮，分别用水配制成4wt％的二氯异氰尿酸钠溶液和3wt％的2-羟基-4-正辛氧基二苯甲酮溶液，然后按重量比1：1混合均匀，再加入十四烷基三甲基氯化铵和经KH-560改性后的纳米SiO2粉体，混合均匀，得整理液；
其中，十四烷基三甲基氯化铵的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的5wt％；改性纳米SiO2粉体的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的0.1wt％。
(2)将锦纶复合面料放入步骤(1)混合均匀的整理液中，二浸二扎，轧余率85％；
(3)将化纤复合面料在140℃下进行预烘1min，再在120℃下烘1min，定型；
(4)将定型后的锦纶复合面料与镂空海绵在80℃下热熔复合，得内外两层为全涤复合面料、中间层为镂空海绵的抗菌复合面料；
(5)将上述复合后的面料在220℃下进行压花，时间20s，得压花抗菌保暖复合面料。
本实施例3制得的压花抗菌保暖复合面料经30-40次水洗烘干后面料层与海绵层不脱落，达到了耐克的测试标准。
以上对本发明的具体实施例进行了详细描述，但其只是作为范例，本发明并不限制于以上描述的具体实施例。对于本领域技术人员而言，任何对本发明进行的等同修改和替代也都在本发明的范畴之中。因此，在不脱离本发明的精神和范围下所作的均等变换和修改，都应涵盖在本发明的范围内。

Claims (8)

1.一种压花抗菌保暖复合面料的制备方法，其特征在于，包括以下步骤：
(1)取三氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮，分别用水配制成2-4wt％的二氯异氰尿酸钠溶液和1-3wt％的2-羟基-4-正辛氧基二苯甲酮溶液，然后按重量比1：1-2混合均匀，再加入十四烷基三甲基氯化铵和纳米SiO2粉体，混合均匀，得整理液；
(2)将抗菌面料放入步骤(1)混合均匀的整理液中，二浸二扎，轧余率70％-85％；
(3)将化纤复合面料在110-150℃下进行预烘1min，再在100-130℃下烘1min，定型；
(4)将定型后的抗菌面料与镂空海绵在40-80℃下热熔复合，得内外两层为抗菌面料、中间层为镂空海绵的复合面料；
(5)将上述复合后的面料在190-220℃下进行压花，时间5-30s，得压花抗菌保暖复合面料。
2.根据权利要求1所述的复合面料的制备方法，其特征在于，所述步骤(1)中十四烷基三甲基氯化铵的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的3-5wt％。
3.根据权利要求1所述的复合面料的制备方法，其特征在于，所述步骤(1)中改性纳米SiO2粉体的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的0.1-0.3wt％。
4.根据权利要求3所述的复合面料的制备方法，其特征在于，所述改性纳米SiO2粉体的粒径为粒径为60-200nm。
5.根据权利要求4所述的复合面料的制备方法，其特征在于，所述改性纳米SiO2粉体在加入前经硅烷偶联剂进行改性处理。
6.根据权利要求1所述的复合面料的制备方法，其特征在于，所述步骤(2)中抗菌面料为涤纶或尼龙或腈纶。
7.根据权利要求1所述的复合面料的制备方法，其特征在于，所述步骤(4)中镂空海绵的厚度为0.2-0.4cm。
8.根据权利要求1所述的复合面料的制备方法，其特征在于，所述步骤(4)中热熔复合步骤采用研泰TS9012胶水。
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