CN105599401A - 一种压花防风透气型复合面料的制备方法 - Google Patents

一种压花防风透气型复合面料的制备方法 Download PDF

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CN105599401A
CN105599401A CN201511029486.2A CN201511029486A CN105599401A CN 105599401 A CN105599401 A CN 105599401A CN 201511029486 A CN201511029486 A CN 201511029486A CN 105599401 A CN105599401 A CN 105599401A
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composite material
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windproof
chemical fibre
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黄关林
钟国能
何立锋
王健刚
汪治燕
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Ningbo Daqian Textile Co Ltd
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Abstract

本发明公开了一种压花防风透气型复合面料的制备方法，采用氯异氰尿酸钠、2-羟基-4-正辛氧基二苯甲酮、十四烷基三甲基氯化铵和纳米SiO2粉体配制的混合液进行前处理工艺，对化纤面料进行改性，然后通过高温压花再和特殊的防风透气膜直接复合，制得压花防风透气型复合面料。本发明方法操作工艺简单，生产效率高，制得的复合面料花型种类丰富、抗静电性能强，风格独特，保暖性能和防风透气效果优良且面料轻薄。

Description

一种压花防风透气型复合面料的制备方法
技术领域
本发明属于纺织材料技术领域，尤其涉及一种压花防风透气型复合面料的制备方法。
背景技术
随着生活水平的提高，人们对衣物的要求越来越高，皮衣具有防风、美观、高贵、不容易脏的特点，成为春秋季节服装的主要材料之一。但是皮衣其价格较高，且质地较重，且色彩及花型变化少，满足不料人们对时尚、轻薄、舒适的追求。其后，PU革面料成为人们的一种选择，PU革面料其具有质地轻、美观、不易脏的特点，成为时装动物皮的替代品。但是传统的PU革面料，其透气性差，穿着是，身体产生的热气很难挥发出，极易产生不适感，且其表面较平整，立体感差。
化纤作为人造的高分子聚合物，在生产过程中可以预先设计其功能性。例如添加抗菌剂，使其具有抗菌功能；添加矿物微粉，使其具有低辐射功能、远红外辐射功能或抗静电功能等。这样做显然比PU革面料或改造天然纤维更容易、更经济，而且效果更显著。
目前，常规生产的化学功能性面料，花型种类少，面料厚重，防风透气效果小差，且抗辐射辐射性和抗静电性差，因此，如何提供一种花型种类丰富、防风透气及抗静电的面料以满足人们需求，势必成为当前纺织材料的发展趋势。
发明内容
本发明为解决现有技术中的上述问题，提供一种压花防风透气型复合面料的制备方法。
为实现上述目的，本发明采用以下技术方案：
本发明的提供一种压花防风透气型复合面料的制备方法，包括以下步骤：
(1)取三氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮，分别用水配制成1.2-1.5wt％的二氯异氰尿酸钠溶液和2-4wt％的2-羟基-4-正辛氧基二苯甲酮溶液，然后按重量比1：0.5-1.5混合均匀，再加入十四烷基三甲基氯化铵和纳米SiO2粉体，混合均匀，得整理液；
(2)将化纤复合面料放入步骤(1)混合均匀的整理液中，二浸二扎，轧余率70％-85％；
(3)将化纤复合面料在110-150℃下进行预烘1min，再在100-130℃下烘1min，定型，放置72小时；
(4)将定型后的化纤复合面料与防风透气膜在40-80℃下粘结复合；
(5)将复合后的化纤复合面料在190-210℃下进行压花，时间5-30s，得压花防风透气型复合面料。
进一步地，在对化纤复合面料进行复合前还包括对化纤复合面料毛坯进行以下工艺处理：预定型(180-195℃)和染色，然后再经整理液处理。
进一步地，所述步骤(1)中十四烷基三甲基氯化铵的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的3-5wt％。
进一步地，所述步骤(1)中改性纳米SiO2粉体的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的0.1-0.3wt％。
进一步地，所述改性纳米SiO2粉体的粒径为粒径为60-200nm。
进一步地，所述改性纳米SiO2粉体在加入前经硅烷偶联剂进行改性处理，优选的所述硅烷偶联剂为KH-560或KH-570。
进一步地，所述步骤(2)中化纤复合面料为全涤复合面料或锦纶复合面料或涤锦混纺复合面料，优选的所述化纤复合面料为全涤复合面料。
进一步地，所述步骤(5)中防风透气膜采用TPU材质，优选市售可得的s-3085防风透气膜。
进一步地，所述步骤(5)中粘结复合采用研泰TS9012胶水。
进一步地，所述压花防风透气型复合面料中防风透气膜的厚度为0.01-0.05mm。
本发明采用上述技术方案，与现有技术相比，具有如下技术效果：
本发明的压花防风透气型复合面料选用产能高且成本低的常规结构的化纤面料，采用特殊前处理工艺，如采用抗静电剂十四烷基三甲基氯化铵与纳米SiO2粉体结合能够有效提高面料的抗静电性能，且抗静电更持久，通过对化纤面料进行改性，然后通过高温压花再和特殊的防风透气膜直接复合，操作工艺简单生产效率高。本发明面料花型种类丰富，抗静电性能强，风格独特，保暖性能和防风透气效果优良且面料轻薄。
具体实施方式
本发明提供了一种生产效率高，花型种类丰富和保暖性能好的压花防风透气型复合面料的制备方法。
下面通过具体实施例对本发明进行详细和具体的介绍，以使更好的理解本发明，但是下述实施例并不限制本发明范围。
实施例1压花防风透气型复合面料的制备
(1)取三氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮，分别用水配制成1.2wt％的二氯异氰尿酸钠溶液和2wt％的2-羟基-4-正辛氧基二苯甲酮溶液，然后按重量比1：0.5混合均匀，再加入十四烷基三甲基氯化铵和经KH-560改性后的纳米SiO2粉体，混合均匀，得整理液；
其中，十四烷基三甲基氯化铵的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的5wt％；改性纳米SiO2粉体的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的0.1wt％。
(2)将化纤复合面料放入步骤(1)混合均匀的整理液中，二浸二扎，轧余率75％。
(3)将化纤复合面料在140℃下进行预烘1min，再在120℃下烘1min，定型；
(4)将定型后的化纤复合面料与0.02mm的防风透气膜在60℃下采用研泰TS9012胶水粘结复合；
(5)将复合后的化纤复合面料在200℃下进行压花，时间20s，得压花防风透气型复合面料。
本实施例1制得的压花防风透气型复合面料经10-20次水洗烘干后防风透气膜不脱落，达到了耐克的测试标准。
实施例2
(1)取三氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮，分别用水配制成1.5wt％的二氯异氰尿酸钠溶液和3wt％的2-羟基-4-正辛氧基二苯甲酮溶液，然后按重量比1：1混合均匀，再加入十四烷基三甲基氯化铵和经KH-560改性后的纳米SiO2粉体，混合均匀，得整理液；
其中，十四烷基三甲基氯化铵的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的5wt％；改性纳米SiO2粉体的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的0.1wt％。
(2)将化纤复合面料放入步骤(1)混合均匀的整理液中，二浸二扎，轧余率80％。
(3)将化纤复合面料在110℃下进行预烘1min，再在130℃下烘1min，定型；
(4)将定型后的化纤复合面料与0.02mm的防风透气膜在60℃下采用研泰TS9012胶水粘结复合；
(5)将复合后的化纤复合面料在200℃下进行压花，时间20s，得压花防风透气型复合面料。
本实施例2制得的压花防风透气型复合面料经20-30次水洗烘干后防风透气膜不脱落，达到了耐克的测试标准。
实施例3
(1)取三氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮，分别用水配制成1.5wt％的二氯异氰尿酸钠溶液和4wt％的2-羟基-4-正辛氧基二苯甲酮溶液，然后按重量比1：1.5混合均匀，再加入十四烷基三甲基氯化铵和经KH-560改性后纳米SiO2粉体，混合均匀，得整理液；
其中，十四烷基三甲基氯化铵的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的5wt％；改性纳米SiO2粉体的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的0.1wt％。
(2)将化纤复合面料放入步骤(1)混合均匀的整理液中，二浸二扎，轧余率85％；
(3)将化纤复合面料在150℃下进行预烘1min，再在100℃下烘1min，定型；
(4)将定型后的化纤复合面料与0.02mm的防风透气膜在60℃下采用研泰TS9012胶水粘结复合；
(5)将复合后的化纤复合面料在200℃下进行压花，时间30s，得压花防风透气型复合面料。
本实施3例制得的压花防风透气型复合面料经20-30次水洗烘干后防风透气膜不脱落，达到了耐克的测试标准。
以上对本发明的具体实施例进行了详细描述，但其只是作为范例，本发明并不限制于以上描述的具体实施例。对于本领域技术人员而言，任何对本发明进行的等同修改和替代也都在本发明的范畴之中。因此，在不脱离本发明的精神和范围下所作的均等变换和修改，都应涵盖在本发明的范围内。

Claims (8)

1.一种压花防风透气型复合面料的制备方法，其特征在于，包括以下步骤：
(1)取三氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮，分别用水配制成1.2-1.5wt％的二氯异氰尿酸钠溶液和2-4wt％的2-羟基-4-正辛氧基二苯甲酮溶液，然后按重量比1：0.5-1.5混合均匀，再加入十四烷基三甲基氯化铵和纳米SiO2粉体，混合均匀，得整理液；
(2)将化纤复合面料放入步骤(1)混合均匀的整理液中，二浸二扎，轧余率70％-85％；
(3)将化纤复合面料在110-150℃下进行预烘1min，再在100-130℃下烘1min，定型；
(4)将定型后的化纤复合面料与防风透气膜在40-80℃下粘结复合；
(5)将复合后的化纤复合面料在190-210℃下进行压花，时间5-30s，得压花防风透气型复合面料。
2.根据权利要求1所述的复合面料的制备方法，其特征在于，所述步骤(1)中十四烷基三甲基氯化铵的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的3-5wt％。
3.根据权利要求1所述的复合面料的制备方法，其特征在于，所述步骤(1)中改性纳米SiO2粉体的加入量为二氯异氰尿酸钠和2-羟基-4-正辛氧基二苯甲酮混合溶液的0.1-0.3wt％。
4.根据权利要求3所述的复合面料的制备方法，其特征在于，所述改性纳米SiO2粉体的粒径为60-200nm。
5.根据权利要求4所述的复合面料的制备方法，其特征在于，所述改性纳米SiO2粉体在加入前经硅烷偶联剂进行改性处理。
6.根据权利要求1所述的复合面料的制备方法，其特征在于，所述步骤(2)中化纤复合面料为全涤复合面料或锦纶复合面料或涤锦混纺复合面料。
7.根据权利要求1所述的复合面料的制备方法，其特征在于，所述步骤(5)中防风透气膜采用TPU材质。
8.根据权利要求1所述的复合面料的制备方法，其特征在于，所述步骤(5)中粘结复合采用研泰TS9012胶水。
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