CN105362287A - Disinfecting shower cream for pigs - Google Patents
Disinfecting shower cream for pigs Download PDFInfo
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- CN105362287A CN105362287A CN201510945407.6A CN201510945407A CN105362287A CN 105362287 A CN105362287 A CN 105362287A CN 201510945407 A CN201510945407 A CN 201510945407A CN 105362287 A CN105362287 A CN 105362287A
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- high speed
- fenvalerate
- speed homogenization
- aqueous phase
- povidone iodine
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/74—Synthetic polymeric materials
- A61K31/785—Polymers containing nitrogen
- A61K31/787—Polymers containing nitrogen containing heterocyclic rings having nitrogen as a ring hetero atom
- A61K31/79—Polymers of vinyl pyrrolidone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/275—Nitriles; Isonitriles
- A61K31/277—Nitriles; Isonitriles having a ring, e.g. verapamil
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
- A61K47/26—Carbohydrates, e.g. sugar alcohols, amino sugars, nucleic acids, mono-, di- or oligo-saccharides; Derivatives thereof, e.g. polysorbates, sorbitan fatty acid esters or glycyrrhizin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/10—Dispersions; Emulsions
- A61K9/107—Emulsions ; Emulsion preconcentrates; Micelles
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- Life Sciences & Earth Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- General Health & Medical Sciences (AREA)
- Animal Behavior & Ethology (AREA)
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- Oil, Petroleum & Natural Gas (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
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- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention provides a disinfecting shower cream for pigs. Main effective ingredients of the disinfecting shower cream comprise S-fenvalerate and povidone iodine, wherein the weight ratio of the S-fenvalerate to the povidone iodine is 2-2.5:10-12. The main effective ingredients are prepared and processed into emulsion in water. When the disinfecting shower cream is used, 0.1 liter of the shower cream is added into every 10 liters of water, spraying and bathing are carried out on pigs for 1 minute to 2 minutes, and then bathing is carried out with clean water for 2 minutes to 3 minutes. The disinfecting shower cream has the effects of sterilization and insect expelling, is broad in bacteriocidal spectrum, good in insect expelling effect and small in irritation, and can further remove cutin and soften and moisten hairs.
Description
Technical field
The present invention relates to boar sterilization bath oil, belong to agricultural breeding field.
Background technology
Pig industry is the important industry in China's agricultural.Be supplied with important function to guarantee meat food safety, current China pig industry is just changed to Pig Industry industry by traditional pig industry, is that aquaculture model, Regional Distribution or the mode of production, production capacity are all in generation significant change.
The cultivation of sow always is the key of pig industry, supports good sow, and the object improving sow plant productivity is exactly that a sow can provide more, healthy and strong piglet in 1 year.Usually the measure of three aspects is taked: 1, shortening sows in lactation and sow are weaned to the interval time of breeding again; 2, the number of live birth of sow is improved; 3, piglet survival ratio is improved.Above-mentioned measure can improve the economic benefit of feeding mother pig.For ensureing the survival rate of piglet, enter obstetric table from pig house before sow produces before, need to carry out disinfection.To kill the pathogenic bacteria that sow is carried with it, cut off and propagate, control pathogen transmission is to piglet.Effective raising piglet survival ratio.
In purification animal body ectozoic insecticide, adopt organophosphor, organochlorine compound etc. more both at home and abroad, have the shortcoming that some are common, as different to different parasite killing effects, poor stability, corrosivity by force, have very large zest etc.Simultaneously due to the continuous variation of infectious disease pathogens and the continuous appearance of drug resistance, the Disinfection Effect of many disinfecting drugs is also deteriorated gradually.And the zest of most chemosterilant can to animal bring olfactory sensation stress, thus cause that animal is uneasy, restless, hypopnea even affects and searches for food.Therefore the scientific development of disinfectant and reasonable utilization play a key effect to plant's purification work.
S-fenvalerate is broad-spectrum highly efficient insecticide, and rapidly, power of knocking down is strong in effect, to tag, multiple cotton-plant pest-insects can be prevented and treated, as bollworm, cotten aphids etc., are widely used in the insect of control Nicotiana tabacum L., Semen sojae atricolor, Semen Maydis, fruit tree, vegetable, also can be used for the insect preventing and treating the aspect such as domestic animal and storage.The dosage form of current use mostly is 0.05%S-fenvalerate missible oil.Due to the easy contaminated environment of cream life-time service.
Moreover, existing disinfectant only has the function of sterilizing, does not possess the effect of the fur that watches for animals.
Summary of the invention
The present invention is directed to the deficiencies in the prior art, provide boar sterilization bath oil, the effect of tool sterilization anthelmintic, moist fur, its fungicidal spectrum is wide, and anthelminthic effect is good, and zest is little, can also remove cutin, soft and moist hair.
Technical solution of the present invention is as follows: boar sterilization bath oil, principle active component is: S-fenvalerate and povidone iodine, and wherein the weight ratio of S-fenvalerate and povidone iodine is 2-2.5:10-12.
Concrete, pig of the present invention sterilization bath oil, comprises following component: the former powder 2%-2.5% of S-fenvalerate, povidone iodine 10%-12%, solvent naphtha 150
#20%-25%, emulsifying agent 5%-15%, ethylene glycol 5%-10%, glacial acetic acid 0.01%-0.05%, deionized water supplies 100%
Described emulsifying agent is: agriculture breast 600
#b:, agriculture breast 500
#, SPAN-20/60/80 the mixing of one or more, be preferably: agriculture breast 600
#b:SPAN-60: agriculture breast 500#=2:6:2.
Be mixed with aqueous emulsion processing method as follows:
(1) former for S-fenvalerate powder is dissolved in solvent, mixing, forms oil phase;
(2) emulsifying agent is mixed with ethylene glycol and isopyknic deionized water, form surfactant phase;
(3) in aqueous phase modulation kettle, add povidone iodine, remaining deionized water, glacial acetic acid be mixed into aqueous phase;
(4) in high speed homogenization still, add surfactant phase, add oil phase gradually, high speed homogenization stirs 10 minutes; Oil phase temperature is preferably 40-60 DEG C.
(5) be then communicated with aqueous phase modulation kettle and high speed homogenization still, make aqueous phase slowly flow in high speed homogenization still; This process preferably makes high speed homogenization temperature in the kettle remain on 40-60 DEG C;
(6) after aqueous phase drops into high speed homogenization still completely, high speed homogenization is continued 30 minutes;
(7) stop stirring, be cooled to room temperature, stirring at low speed is even, sample analysis fill.
Aqueous emulsion of the present invention adopts D phase emulsion process, processes with high speed dispersion homogenizer.The prescription of aqueous emulsion is met by the aqueous emulsion indices of formulated processing of the present invention.Aqueous emulsion good stability of the present invention, (54 ± 2) DEG C heat storage 14 days, resolution ratio was less than 1%.
| Index name | Index |
| Outward appearance | Thick white working fluid |
| pH | 4-6 |
| Stability of emulsion (diluting 200 times) | Qualified |
| Heat storage stability | Qualified |
| Cold storage stability | Qualified |
Bath oil usage of the present invention: the ratio adding 0.1 liter of bath oil according to every 10 premium on currency, to pig spraying shower 1-2 minute, and then with clear water shower 2-3 minute.
The present invention's S-fenvalerate used is efficient pesticides the most frequently used in current aquaculture.It all has good killing effect to the multiple vermin of poultry and hematophagus such as demodicid mite, louse, flea, Ticks, mosquito, fly, horsefly etc., and insecticidal power is strong, and effect is high.Its pharmacological action, to tag, has stomach toxicity and repellent action concurrently.
Povidone iodine: be disinfection preservative, have killing action to various bacteria, brood cell, virus, fungus etc.Its mechanism of action is after this product contacts wound surface or affected part, depolymerization can discharge free-iodine performance bactericidal action.Feature is little to tissue irritation, is applicable to skin, mucosa infection.Can be used for the sterilization of small size skin, mucosa wound.Sterilization speed is fast, and most of antibacterial can be killed in 30 seconds, within 5 minutes, was enough to kill to individual bacteria.To mucocutaneous non-stimulated, can be used for sterilization and the treatment of body cavity, mucosa and ulcer surface.Avirulence.Not easily make microorganism produce drug resistance, not easily anaphylaxis occurs.It is lasting to use, and good stability, storage life is long.Soluble in water, easy cleaning, does not pollute or damages fabric and other article.
During aqueous emulsion of the present invention preparation, be different from traditional aqueous phase and add oil phase or oil phase adds aqueous phase, but form oil phase by S-fenvalerate and solvent; Emulsifying agent mixes with ethylene glycol and appropriate deionized water, forms surfactant phase; Povidone iodine, remaining deionized water, glacial acetic acid are mixed into aqueous phase; Three-phase is homogenizing in high speed homogenization still.First add surfactant phase, add oil phase gradually, after stirring homogenizing, finally add aqueous phase and continue homogenizing.The aqueous emulsion good stability that said method is produced, can not flocculate, coalescent and layering bleed.Drug effect is better than S-fenvalerate missible oil.
The present invention has following beneficial effect:
1, the present inventor study find by after composite with povidone iodine for S-fenvalerate compared with single dose, have obvious synergistic function to the control of insect, significantly improve prevention effect.
2, for animal body surface sterilization, have and drive away ectozoal effect, various virus can be killed fast, antibacterial, spore, mycoplasma, fungus etc.Very high killing rate is had to the various parasite of body surface (as demodicid mite, flea, louse etc.).
3, to people and animals, harmless, non-stimulated, safety and environmental protection.Alternative high-toxic pesticide, reduces environmental pollution and pesticide residues.Reduce and produce and use cost.
4, the present invention has clean fur, removes cuticular effect.
Detailed description of the invention
Below in conjunction with embodiment and test example, the present invention will be further described.
Embodiment 1, one boar sterilization bath oil, comprises following component: the former powder 2% of S-fenvalerate, povidone iodine 10%, solvent naphtha 150
#20%, emulsifying agent 10%, ethylene glycol 5%, glacial acetic acid 0.01, deionized water supplies 100%.
Described emulsifying agent is: agriculture breast 600
#b:SPAN-60: agriculture breast 500#=2:6:2
Be mixed with aqueous emulsion processing method as follows:
(1) former for S-fenvalerate powder is dissolved in solvent, mixing, forms oil phase;
(2) emulsifying agent is mixed with ethylene glycol and isopyknic deionized water, form surfactant phase;
(3) in aqueous phase modulation kettle, add povidone iodine, remaining deionized water, glacial acetic acid be mixed into aqueous phase;
(4) in high speed homogenization still, add surfactant phase, add oil phase gradually, oil phase temperature is 50 DEG C, and high speed homogenization stirs 10 minutes;
(5) be then communicated with aqueous phase modulation kettle and high speed homogenization still, make aqueous phase slowly flow in high speed homogenization still; This process, high speed homogenization temperature in the kettle remains on 50 DEG C;
(6) after aqueous phase drops into high speed homogenization still completely, high speed homogenization is continued 30 minutes;
(7) stop stirring, be cooled to room temperature, stirring at low speed is even, sample analysis fill.
Embodiment 2, one boar sterilization bath oil, comprise following component: the former powder 2.5% of S-fenvalerate, povidone iodine 12%, solvent naphtha 150#25%, emulsifying agent 15%, ethylene glycol 10%, glacial acetic acid 0.05%, deionized water supplies 100%.
Described emulsifying agent is: agriculture breast 600#B: agriculture breast 500#=1:1.
Be mixed with aqueous emulsion processing method as follows:
(1) former for S-fenvalerate powder is dissolved in solvent, mixing, forms oil phase;
(2) emulsifying agent is mixed with ethylene glycol and isopyknic deionized water, form surfactant phase;
(3) in aqueous phase modulation kettle, add povidone iodine, remaining deionized water, glacial acetic acid be mixed into aqueous phase;
(4) in high speed homogenization still, add surfactant phase, add oil phase gradually, oil phase temperature is 45 DEG C, and high speed homogenization stirs 12 minutes;
(5) be then communicated with aqueous phase modulation kettle and high speed homogenization still, make aqueous phase slowly flow in high speed homogenization still; This process, high speed homogenization temperature in the kettle remains on 50 DEG C;
(6) after aqueous phase drops into high speed homogenization still completely, high speed homogenization is continued 25 minutes;
(7) stop stirring, be cooled to room temperature, stirring at low speed is even, sample analysis fill.
Embodiment 3, one boar sterilization bath oil, comprises following component: the former powder 2% of S-fenvalerate, povidone iodine 10%, solvent naphtha 150
#22%, emulsifying agent 10%, ethylene glycol 8%, glacial acetic acid 0.03%, deionized water supplies 100%.
Emulsifying agent is: SPAN-20:SPAN-60:SPAN-80=1:1:1.
Be mixed with aqueous emulsion processing method as follows:
(1) former for S-fenvalerate powder is dissolved in solvent, mixing, forms oil phase;
(2) emulsifying agent is mixed with ethylene glycol and isopyknic deionized water, form surfactant phase;
(3) in aqueous phase modulation kettle, add povidone iodine, remaining deionized water, glacial acetic acid be mixed into aqueous phase;
(4) in high speed homogenization still, add surfactant phase, add oil phase gradually, oil phase temperature is 60 DEG C, and high speed homogenization stirs 15 minutes;
(5) be then communicated with aqueous phase modulation kettle and high speed homogenization still, make aqueous phase slowly flow in high speed homogenization still; This process, high speed homogenization temperature in the kettle remains on 60 DEG C;
(6) after aqueous phase drops into high speed homogenization still completely, high speed homogenization is continued 35 minutes;
(7) stop stirring, be cooled to room temperature, stirring at low speed is even, sample analysis fill.
Embodiment 4, one boar sterilization bath oil, comprise following component: the former powder 2.2% of S-fenvalerate, povidone iodine 11, solvent naphtha 150#23%, emulsifying agent 12%, ethylene glycol 7%, glacial acetic acid 0.04%, deionized water supplies 100%.
Described emulsifying agent is, agriculture breast 500#:SPAN-20:SPAN60=1:2:3.
Be mixed with aqueous emulsion processing method as follows:
(1) former for S-fenvalerate powder is dissolved in solvent, mixing, forms oil phase;
(2) emulsifying agent is mixed with ethylene glycol and isopyknic deionized water, form surfactant phase;
(3) in aqueous phase modulation kettle, add povidone iodine, remaining deionized water, glacial acetic acid be mixed into aqueous phase;
(4) in high speed homogenization still, add surfactant phase, add oil phase gradually, oil phase temperature is 55 DEG C, and high speed homogenization stirs 12 minutes;
(5) be then communicated with aqueous phase modulation kettle and high speed homogenization still, make aqueous phase slowly flow in high speed homogenization still; This process, high speed homogenization temperature in the kettle remains on 55 DEG C;
(6) after aqueous phase drops into high speed homogenization still completely, high speed homogenization is continued 28 minutes;
(7) stop stirring, be cooled to room temperature, stirring at low speed is even, sample analysis fill.
Test one, Disinfection Effect testing experiment of the present invention
1, experimental technique
Test with reference to " disinfectant for animals identification experiment technical specification " (Ministry of Agriculture) method, adopt bacterial suspension quantitative method, test strain is escherichia coli, staphylococcus aureus.Specific experiment step is as follows:
(1), after the bacterium liquid count plate prepared, be diluted to containing bacterium 10 with the phosphate buffer of 0.3M
6-10
7the test organisms liquid of individual/milliliter.
(2) test group: draw 0.1 milliliter of bacterium liquid and mix with test disinfectant solution 0.9 milliliter.Be placed in 20 DEG C of water-baths to act on to the stipulated time.Draw above-mentioned bacterium medicine mixed liquor 0.1ml, add the mixing of 0.9ml nertralizer as test sample.
(3) matched group: replace disinfectant solution with 0.03M phosphate buffer is identical with step 2 processing method.
(4) by test group and matched group and after 10 minutes, carry out count plate, calculate sterilizing rate.
Sterilizing rate=(matched group bacterium number-test group bacterium number)/matched group bacterium number × 100%.
2, result of the test
Disinfectant of the present invention the results are shown in Table 1 to escherichia coli, staphylococcus aureus sterilize experiment.From table 1 data, for escherichia coli, disinfectant of the present invention is for escherichia coli, and 1:500 is diluted in 1 minute sterilizing rate 99.99%, just can reach sterilization requirement.Matched group bacterium number 1.61 × 10
7cfu/ml.
For staphylococcus aureus, 1:100 is diluted in 1 minute sterilizing rate 99.99%, just can reach sterilization requirement.Matched group bacterium number 9.7 × 10
7cfu/ml.
Table 1 disinfectant of the present invention is to escherichia coli, staphylococcus aureus sterilize experiment result
Test two, insecticidal effect testing experiment of the present invention
1, test method
By disinfectant of the present invention, carry out contrast bactericidal assay with two kinds of commercial insecticide.Two kinds of commercial insecticide are respectively: ivermectin, S-fenvalerate.
(1) laboratory animal
Female KM mice, 25-30g, standard microscopy turns out to be the positive kunming mice 40 of epizoite louse, is divided into ivermectin group at random, S-fenvalerate group, disinfectant high dose group of the present invention and low dose group.Separately establish a blank group, for not infecting the female KM mice of louse.Often organize 10 mices.
(2) processing method
Ivermectin group 0.5% ivermectin, S-fenvalerate group 0.05%S-fenvalerate carries out spray and uses; Spray-dip is carried out in high dose group 1:100 dilution of the present invention, and spray-dip is carried out in low dose group 1:200 dilution of the present invention.Above four groups with the continuous dipping in interval in 2 days 3 times, secondary daily inspection insecticidal effect.Observe 30 days.Matched group distilled water spray-dip.
Each group of test mice fed standard chow, free diet, cage tool, bedding and padding etc. are disinfected, and are strictly on guard against cross infection for each group.
(3) method of inspection
Carry out inspection insecticidal effect after each medication, with pincet to inside the groin of mice, face both sides, forelimb, pull off the feather of after ear, be placed on microscopy on the slide that drips and have normal saline and live louse.
Two, experimental result
After each group of medication, effect is in table 2.
Table 2 the present invention and ivermectin, lambda-cyhalothrin kill louse effectiveness comparison
As can be seen from Table 2, in above-mentioned test, 0.5% ivermectin delousing poor effect is still moderate or low invasion and attack after twice spray-dip.0.05%S-fenvalerate treatment pediculosis determined curative effect, after a spray-dip, delousing rate just reaches 84.6%.After twice spray-dip, continuous observation has no movable louse in 30 days.Low dose group medication insecticidal effect of 1:200 dilution of the present invention is better, and after twice, killing rate reaches 100%, and effect is better than 0.5% ivermectin.High dose group medication of the present invention killing rate just reaches more than 92%, and effect is better than 0.5% ivermectin and 0.05%S-fenvalerate, and depilation, ulcer, incrustation, skin sclerosis etc. do not appear in mouse skin.The present invention's high concentration also has no animal dead and intoxicating phenomenon.Blank group does not infect louse all the time, meets expected results.The active constituent content S-fenvalerate of high dose group of the present invention is 0.02%, and lower than 0.05%S-fenvalerate, effect is better than 0.05%S-fenvalerate.May be due to S-fenvalerate and povidone iodine composite after, there is synergistic function between component.
Claims (5)
1. boar sterilization bath oil, it is characterized in that, principle active component is: S-fenvalerate and povidone iodine, and wherein the weight ratio of S-fenvalerate and povidone iodine is 2-2.5:10-12.
2. pig as claimed in claim 1 sterilization bath oil, is characterized in that, comprise following component: the former powder 2%-2.5% of S-fenvalerate, povidone iodine 10%-12%, solvent naphtha 150
#20%-25%, emulsifying agent 5%-15%, ethylene glycol 5%-10%, glacial acetic acid 0.01%-0.05%, deionized water supplies 100%.
3. pig as claimed in claim 2 sterilization bath oil, it is characterized in that, described emulsifying agent is: agriculture breast 600
#b, agriculture breast 500
#, SPAN-20/60/80 the mixing of one or more.
4. pig as claimed in claim 3 sterilization bath oil, it is characterized in that, described emulsifying agent is: agriculture breast 600
#b:SPAN-60: agriculture breast 500#=2:6:2.
5. claim 1-4 arbitrary described pig sterilization bath oil, it is characterized in that, formulated method is as follows:
(1) former for S-fenvalerate powder is dissolved in solvent, mixing, forms oil phase;
(2) emulsifying agent is mixed with ethylene glycol and isopyknic deionized water, form surfactant phase;
(3) in aqueous phase modulation kettle, add povidone iodine, remaining deionized water, glacial acetic acid be mixed into aqueous phase;
(4) in high speed homogenization still, add surfactant phase, add oil phase gradually, high speed homogenization stirs;
(5) be then communicated with aqueous phase modulation kettle and high speed homogenization still, make aqueous phase slowly flow in high speed homogenization still;
(6) after aqueous phase drops into high speed homogenization still completely, continue high speed homogenization and stir;
(7) stop stirring, sample analysis fill.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510945407.6A CN105362287B (en) | 2015-12-17 | 2015-12-17 | One boar sterilization bath oil |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510945407.6A CN105362287B (en) | 2015-12-17 | 2015-12-17 | One boar sterilization bath oil |
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| CN105362287B CN105362287B (en) | 2017-12-29 |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107873637A (en) * | 2017-11-13 | 2018-04-06 | 李劲松 | A kind of three-dimensional integrated pig expelling intestinal parasites method |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102935082A (en) * | 2012-11-19 | 2013-02-20 | 穆永才 | Drug for external use for preventing and treating scabies |
| CN104523748A (en) * | 2015-01-05 | 2015-04-22 | 四川悦康源通药业有限公司 | Compound iodine disinfectant and preparation method and application thereof |
-
2015
- 2015-12-17 CN CN201510945407.6A patent/CN105362287B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102935082A (en) * | 2012-11-19 | 2013-02-20 | 穆永才 | Drug for external use for preventing and treating scabies |
| CN104523748A (en) * | 2015-01-05 | 2015-04-22 | 四川悦康源通药业有限公司 | Compound iodine disinfectant and preparation method and application thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107873637A (en) * | 2017-11-13 | 2018-04-06 | 李劲松 | A kind of three-dimensional integrated pig expelling intestinal parasites method |
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