CN105362287B - One boar sterilization bath oil - Google Patents
One boar sterilization bath oil Download PDFInfo
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- CN105362287B CN105362287B CN201510945407.6A CN201510945407A CN105362287B CN 105362287 B CN105362287 B CN 105362287B CN 201510945407 A CN201510945407 A CN 201510945407A CN 105362287 B CN105362287 B CN 105362287B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/74—Synthetic polymeric materials
- A61K31/785—Polymers containing nitrogen
- A61K31/787—Polymers containing nitrogen containing heterocyclic rings having nitrogen as a ring hetero atom
- A61K31/79—Polymers of vinyl pyrrolidone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/275—Nitriles; Isonitriles
- A61K31/277—Nitriles; Isonitriles having a ring, e.g. verapamil
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K47/00—Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
- A61K47/06—Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
- A61K47/26—Carbohydrates, e.g. sugar alcohols, amino sugars, nucleic acids, mono-, di- or oligo-saccharides; Derivatives thereof, e.g. polysorbates, sorbitan fatty acid esters or glycyrrhizin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/10—Dispersions; Emulsions
- A61K9/107—Emulsions ; Emulsion preconcentrates; Micelles
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Abstract
The present invention provides boar sterilization bath oil, and principle active component is：S fenvalerates and PVP-I, the wherein weight of S fenvalerates and PVP-I ratio are 2 2.5:10‑12.It is processed as aqueous emulsion.The ratio of 0.1 liter of bath oil is added during use according to every 10 liters of water, takes a shower 12 minutes to pig spraying, is then taken a shower 23 minutes with clear water again, you can.The present invention has the function that sterilization expelling parasite, and its wide sterilization spectrum, anthelminthic effect is good, and excitant is small, can also remove cutin, soft and moist hair.
Description
Technical field
The present invention relates to boar sterilization bath oil, belong to agricultural breeding field.
Background technology
Pig industry is the important industry in China's agricultural.Played an important role to ensureing that meat food safety is supplied, at present China
Pig industry is just changed from traditional pig industry to Pig Industry industry, either aquaculture model, Regional Distribution or the mode of production, production
All significant changes are occurring for ability.
The cultivation of sow always is the key of pig industry, supports good sow, and the purpose for improving sow plant productivity is exactly one
Head sow can provide more, healthy and strong piglets for 1 year.The measure of three aspects is usually taken：1st, sows in lactation and sow are shortened
Wean to the interval time bred again；2nd, the number of live birth of sow is improved；3rd, piglet survival ratio is improved.Above-mentioned measure can carry
The economic benefit of high feeding mother pig.To ensure the survival rate of piglet, enter before sow production from pig house before obstetric table, it is necessary to carry out
Sterilization.To kill the germ carried with sow, cut-out is propagated, and preventing and treating pathogen transmission is to piglet.Effectively improve piglet survival ratio.
It is both at home and abroad to use organophosphor, organochlorine compound etc. in terms of the insecticide of purification animal vermin more, all
There is the shortcomings that some are common, such as different to different parasite killing effects, stability is poor, corrosivity is strong, has very big thorn
Swash property etc..Simultaneously because the continuous variation of infectious disease pathogens and the emergence of drug resistance, the Disinfection Effect of many disinfecting drugs
Also gradually it is deteriorated.And the excitant of most chemosterilants can come smell to lead for animal stress, so as to cause animal uneasy, hot-tempered
Dynamic, unsmooth breath even influences to search for food.Therefore the scientific development of disinfectant and reasonable utilization play pass to plant's purification work
Key acts on.
S- fenvalerates are broad-spectrum highly efficient insecticide, and effect is rapid, and it is strong to knock down power, based on tagging, can prevent and treat multi-cotton
Flower insect, such as bollworm, cotten aphid etc., preventing and treating tobacco, soybean, corn, fruit tree, the insect of vegetables are widely used in, can also be used for preventing
Manage a household poultry and storage etc. insect.The formulation used at present is mostly 0.05%S- fenvalerate missible oils.Because missible oil is long-term
Use easy pollution environment.
Moreover, existing disinfectant only has the function of sterilizing, does not possess the effect of protection animal skin.
The content of the invention
In view of the deficiencies of the prior art, the present invention provides boar sterilization bath oil, tool sterilization expelling parasite, fur is moistened
Effect, its wide sterilization spectrum, anthelminthic effect is good, and excitant is small, can also remove cutin, soft and moist hair.
Technical solution of the present invention is as follows：One boar sterilization bath oil, principle active component are：S- fenvalerates and poly- dimension
Ketone iodine, the wherein weight of S- fenvalerates and PVP-I ratio are 2-2.5:10-12.
Specifically, pig of the present invention sterilization bath oil, including following component：S- fenvalerate original powder 2%-2.5%, gather dimension
Ketone iodine 10%-12%, solvent naphtha 150#20%-25%, emulsifying agent 5%-15%, ethylene glycol 5%-10%, glacial acetic acid 0.01%-
0.05%, deionized water supplies 100%
The emulsifying agent is：Agriculture breast 600#B:, agriculture breast 500#, SPAN-20/60/80 one or more of mixing, preferably
For：Agriculture breast 600#B:SPAN-60：Agriculture breast 500#=2:6:2.
It is as follows to be configured to aqueous emulsion processing method：
(1) S- fenvalerate original powder is dissolved in solvent, mixed, form oil phase；
(2) emulsifying agent is mixed with ethylene glycol and isometric deionized water, forms surfactant phase；
(3) PVP-I, remaining deionized water, glacial acetic acid are added into aqueous phase modulation kettle and is mixed into aqueous phase；
(4) surfactant phase is added into high speed homogenization kettle, is gradually added into oil phase, high speed homogenization stirs 10 minutes；Oil
Phase temperature is preferably 40-60 DEG C.
(5) and then aqueous phase modulation kettle and high speed homogenization kettle are connected, aqueous phase is flowed slowly into high speed homogenization kettle；This process is most
High speed homogenization temperature in the kettle is set to be maintained at 40-60 DEG C well；
(6) after aqueous phase is fully immersed high speed homogenization kettle, high speed homogenization is continued 30 minutes；
(7) stop stirring, be cooled to normal temperature, stirring at low speed is uniform, and sampling analysis is filling.
Aqueous emulsion of the present invention uses D phase emulsion processes, is machined with high speed homogeneous dispersion.By inventive formulation formulated
Aqueous emulsion indices meet the quality requirement of aqueous emulsion.Aqueous emulsion stability of the present invention is good, and in (54 ± 2), DEG C heat is store 14 days,
Resolution ratio is less than 1%.
| Index name | Index |
| Outward appearance | Thick white working fluid |
| pH | 4-6 |
| Stability of emulsion (200 times of dilution) | It is qualified |
| Heat storage stability | It is qualified |
| Cold storage stability | It is qualified |
Bath oil usage of the present invention：The ratio of 0.1 liter of bath oil is added according to every 10 liters of water, to 1-2 points of pig spraying shower
Clock, then again with clear water shower 2-3 minutes, you can.
S- fenvalerates used in the present invention, it is efficient pesticides the most frequently used in current aquaculture.It is to a variety of of livestock and poultry
Vermin and hematophagus such as mite, lice, flea, tick, mosquito, fly, horsefly etc. have good killing effect, and insecticidal power is strong, effect
It is high.Its pharmacological action has stomach toxicity and repellent action concurrently based on tagging.
PVP-I：For disinfection preservative, there is killing action to various bacteria, brood cell, virus, fungi etc..It acts on machine
System is after this product contacts the surface of a wound or affected part, and energy depolymerization discharges free-iodine and plays bactericidal action.Feature be it is small to tissue irritation,
Suitable for skin, mucosa infection.Sterilization available for small area skin, mucous membrane wound.Sterilization speed is fast, most of bacteriums 30 seconds
It is interior to kill, individual bacteria is enough to kill for 5 minutes.To mucocutaneous non-stimulated, available for disappearing for body cavity, mucous membrane and ulcer surface
Poison and treatment.It is non-toxic.It is not easy to make microorganism produce drug resistance, is not susceptible to allergic reaction.Using lasting, stability is good, storage
Deposit term of validity length.It is soluble in water, easy cleaning, do not pollute or damage fabric and other articles.
When aqueous emulsion of the present invention is prepared, add oil phase different from traditional aqueous phase or oil phase adds aqueous phase, but by S-
Fenvalerate and solvent form oil phase；Emulsifying agent mixes with ethylene glycol and appropriate deionized water, forms surfactant phase；It is poly-
Dimension ketone iodine, remaining deionized water, glacial acetic acid are mixed into aqueous phase；Three-phase homogeneous in high speed homogenization kettle.First plus surfactant
Phase, oil phase is gradually added into, after stirring homogeneous, is eventually adding aqueous phase and continues homogeneous.The aqueous emulsion stability of above method production is good,
It will not flocculate, coalesce and be layered bleed.Drug effect is more preferable than S- fenvalerate missible oil.
The present invention has the advantages that：
1st, the present inventor study find by S- fenvalerates with PVP-I compounding after compared with single dose, the preventing and treating to insect
There is obvious synergistic function, hence it is evident that improve prevention effect.
2nd, sterilized for animal body surface, have the function that to drive away epizoon, can quickly kill various viruses, carefully
Bacterium, gemma, mycoplasma, fungi etc..There is very high killing rate to the various parasites of body surface (such as mite, flea, lice etc.).
3rd, it is harmless to people and animals, non-stimulated, safety and environmental protection.Alternative high-toxic pesticide, reduces environmental pollution and residues of pesticides.
Reduce production and use cost.
4th, the present invention has cleaning fur, removes the effect of cuticula.
Embodiment
With reference to embodiment and test example, the present invention will be further described.
Embodiment 1, boar sterilization bath oil, including following component：S- fenvalerate originals powder 2%, PVP-I
10%, solvent naphtha 150#20%, emulsifying agent 10%, ethylene glycol 5%, glacial acetic acid 0.01, deionized water supplies 100%.
The emulsifying agent is：Agriculture breast 600#B:SPAN-60：Agriculture breast 500#=2:6:2
It is as follows to be configured to aqueous emulsion processing method：
(1) S- fenvalerate original powder is dissolved in solvent, mixed, form oil phase；
(2) emulsifying agent is mixed with ethylene glycol and isometric deionized water, forms surfactant phase；
(3) PVP-I, remaining deionized water, glacial acetic acid are added into aqueous phase modulation kettle and is mixed into aqueous phase；
(4) surfactant phase is added into high speed homogenization kettle, is gradually added into oil phase, oil phase temperature is 50 DEG C, at a high speed
Matter stirs 10 minutes；
(5) and then aqueous phase modulation kettle and high speed homogenization kettle are connected, aqueous phase is flowed slowly into high speed homogenization kettle；This process,
High speed homogenization temperature in the kettle is maintained at 50 DEG C；
(6) after aqueous phase is fully immersed high speed homogenization kettle, high speed homogenization is continued 30 minutes；
(7) stop stirring, be cooled to normal temperature, stirring at low speed is uniform, and sampling analysis is filling.
Embodiment 2, boar sterilization bath oil, including following component：S- fenvalerate originals powder 2.5%, PVP-I
12%, solvent naphtha 150#25%, emulsifying agent 15%, ethylene glycol 10%, glacial acetic acid 0.05%, deionized water supplies 100%.
The emulsifying agent is：Agriculture breast 600#B:Agriculture breast 500#=1:1.
It is as follows to be configured to aqueous emulsion processing method：
(1) S- fenvalerate original powder is dissolved in solvent, mixed, form oil phase；
(2) emulsifying agent is mixed with ethylene glycol and isometric deionized water, forms surfactant phase；
(3) PVP-I, remaining deionized water, glacial acetic acid are added into aqueous phase modulation kettle and is mixed into aqueous phase；
(4) surfactant phase is added into high speed homogenization kettle, is gradually added into oil phase, oil phase temperature is 45 DEG C, at a high speed
Matter stirs 12 minutes；
(5) and then aqueous phase modulation kettle and high speed homogenization kettle are connected, aqueous phase is flowed slowly into high speed homogenization kettle；This process,
High speed homogenization temperature in the kettle is maintained at 50 DEG C；
(6) after aqueous phase is fully immersed high speed homogenization kettle, high speed homogenization is continued 25 minutes；
(7) stop stirring, be cooled to normal temperature, stirring at low speed is uniform, and sampling analysis is filling.
Embodiment 3, boar sterilization bath oil, including following component：S- fenvalerate originals powder 2%, PVP-I
10%, solvent naphtha 150#22%, emulsifying agent 10%, ethylene glycol 8%, glacial acetic acid 0.03%, deionized water supplies 100%.
Emulsifying agent is：SPAN-20：SPAN-60：SPAN-80=1:1:1.
It is as follows to be configured to aqueous emulsion processing method：
(1) S- fenvalerate original powder is dissolved in solvent, mixed, form oil phase；
(2) emulsifying agent is mixed with ethylene glycol and isometric deionized water, forms surfactant phase；
(3) PVP-I, remaining deionized water, glacial acetic acid are added into aqueous phase modulation kettle and is mixed into aqueous phase；
(4) surfactant phase is added into high speed homogenization kettle, is gradually added into oil phase, oil phase temperature is 60 DEG C, at a high speed
Matter stirs 15 minutes；
(5) and then aqueous phase modulation kettle and high speed homogenization kettle are connected, aqueous phase is flowed slowly into high speed homogenization kettle；This process,
High speed homogenization temperature in the kettle is maintained at 60 DEG C；
(6) after aqueous phase is fully immersed high speed homogenization kettle, high speed homogenization is continued 35 minutes；
(7) stop stirring, be cooled to normal temperature, stirring at low speed is uniform, and sampling analysis is filling.
Embodiment 4, boar sterilization bath oil, including following component：S- fenvalerate originals powder 2.2%, PVP-I
11, solvent naphtha 150#23%, emulsifying agent 12%, ethylene glycol 7%, glacial acetic acid 0.04%, deionized water supplies 100%.
The emulsifying agent is agriculture breast 500#：SPAN-20：SPAN60=1:2:3.
It is as follows to be configured to aqueous emulsion processing method：
(1) S- fenvalerate original powder is dissolved in solvent, mixed, form oil phase；
(2) emulsifying agent is mixed with ethylene glycol and isometric deionized water, forms surfactant phase；
(3) PVP-I, remaining deionized water, glacial acetic acid are added into aqueous phase modulation kettle and is mixed into aqueous phase；
(4) surfactant phase is added into high speed homogenization kettle, is gradually added into oil phase, oil phase temperature is 55 DEG C, at a high speed
Matter stirs 12 minutes；
(5) and then aqueous phase modulation kettle and high speed homogenization kettle are connected, aqueous phase is flowed slowly into high speed homogenization kettle；This process,
High speed homogenization temperature in the kettle is maintained at 55 DEG C；
(6) after aqueous phase is fully immersed high speed homogenization kettle, high speed homogenization is continued 28 minutes；
(7) stop stirring, be cooled to normal temperature, stirring at low speed is uniform, and sampling analysis is filling.
Experiment one, disinfection Effect test of the present invention experiment
1st, experimental method
Reference《Disinfectant for animals identification experiment technical specification》(Ministry of Agriculture) method is tested, and is quantified using bacterial suspension
Method, test strain are Escherichia coli, staphylococcus aureus.Specific experiment step is as follows：
(1) after the bacterium solution count plate prepared, it is diluted to 0.3M phosphate buffer containing bacterium 106-107Individual/milliliter
Test bacterium solution.
(2) test group：0.1 milliliter of bacterium solution is drawn to mix for 0.9 milliliter with test disinfectant solution.It is placed in 20 DEG C of water-baths and makees
With to the stipulated time.Above-mentioned bacterium medicine mixed liquor 0.1ml is drawn, the mixing of 0.9ml nertralizers is added and is used as test sample.
(3) control group：Disinfectant solution is replaced with 0.03M phosphate buffers, it is identical with step 2 processing method.
(4) by test group and control group and after 10 minutes, count plate is carried out, calculates sterilizing rate.
Sterilizing rate=(control group bacterium number-test group bacterium number)/control group bacterium number × 100%.
2nd, result of the test
Disinfectant of the present invention kills result of the test to Escherichia coli, staphylococcus aureus and is shown in Table 1.It was found from the data of table 1,
For Escherichia coli, disinfectant of the present invention is for Escherichia coli, and 1:500 are diluted in 1 minute sterilizing rate 99.99%, with regard to that can reach
Sterilization requires.Control group bacterium number 1.61 × 107cfu/ml。
For staphylococcus aureus, 1:100 are diluted in 1 minute sterilizing rate 99.99%, are required with regard to that can reach sterilization.It is right
According to group bacterium number 9.7 × 107cfu/ml。
1 disinfectant of the present invention of table kills result of the test to Escherichia coli, staphylococcus aureus
Experiment two, insecticidal effect testing experiment of the present invention
1st, test method
By disinfectant of the present invention, contrast sterilization test is carried out with two kinds of commercial insecticides.Two kinds of commercial insecticides are respectively：
Ivermectin, S- fenvalerates.
(1) experimental animal
Female KM mouse, 25-30g, standard microscopy turn out to be the positive kunming mice 40 of epizoite louse, at random
It is divided into ivermectin group, S- fenvalerate groups, disinfectant high dose group and low dose group of the present invention.A blank control group separately is set,
To be uninfected by the female KM mouse of louse.Every group of 10 mouse.
(2) processing method
0.5% ivermectin of ivermectin group, S- fenvalerates group carry out spray use with 0.05%S- fenvalerates；This hair
Bright high dose group is with 1：100 dilutions carry out spray-dips, and low dose group of the present invention is with 1：200 dilutions carry out spray-dip.Four groups of the above was with 2 days
It is spaced continuous dipping 3 times, secondary daily inspection insecticidal effect.Observation 30 days.Control group distilled water spray-dip.
Each group test mice fed standard chow, free diet, cage tool, bedding and padding etc. are disinfected, and each group prevents intersection sense
Dye.
(3) method of inspection
Carry out inspection insecticidal effect after each medication, with pincet to the groin of mouse, face both sides, forelimb on the inside of,
Pulled off the feather of after ear, being placed on drop has microscopy work lice on the slide of physiological saline.
2nd, experimental result
Effect is shown in Table 2 after each group medication.
Compared with the present invention of table 2 kills lice effect with ivermectin, lambda-cyhalothrin
From table 2 it can be seen that in above-mentioned experiment, 0.5% ivermectin delousing is ineffective, is in still after spray-dip twice
Moderate or low invasion and attack.0.05%S- fenvalerates treatment pediculosis is curative for effect, and delousing rate just reaches 84.6% after a spray-dip.
Continuous observation has no movable louse in 30 days after spray-dip twice.The present invention 1:Insecticidal effect of low dose group medication of 200 dilutions
Preferably, for rear killing rate up to 100%, effect is better than 0.5% ivermectin twice.Killing rate of high dose group medication of the present invention is just
Up to more than 92%, effect is better than 0.5% ivermectin and 0.05%S- fenvalerates, and mouse skin do not occur depilation, ulcer,
Incrustation, sclerosis of the skin etc..The present invention also has no animal dead and intoxicating phenomenon with high concentration.Blank control group is uninfected by lice all the time
Son, meet expected results.The active constituent content S- fenvalerates of high dose group of the present invention are 0.02%, less than 0.05%S- cyanogen
Valerate, effect are better than 0.05%S- fenvalerates.It is probably due to after S- fenvalerates and PVP-I compounding, being sent out between component
Raw synergistic function.
Claims (5)
1. boar sterilization bath oil, it is characterized in that, principle active component is：S- fenvalerates and PVP-I, wherein S-
The weight of fenvalerate and PVP-I ratio is 2-2.5:10-12.
2. pig as claimed in claim 1 sterilization bath oil, it is characterized in that, including following component：S- fenvalerate original powder
2%-2.5%, PVP-I 10%-12%, solvent naphtha 150#20%-25%, emulsifying agent 5%-15%, ethylene glycol 5%-
10%, glacial acetic acid 0.01%-0.05%, deionized water supplies 100%.
3. pig as claimed in claim 2 sterilization bath oil, it is characterized in that, the emulsifying agent is：Agriculture breast 600#B, agriculture breast
500#, SPAN-20/60/80 one or more of mixing.
4. pig as claimed in claim 3 sterilization bath oil, it is characterized in that, the emulsifying agent is：Agriculture breast 600#B:SPAN-60：
Agriculture breast 500#=2:6:2.
5. claim 1-4 any described pig sterilization bath oils, it is characterized in that, formulated method is as follows：
(1) S- fenvalerate original powder is dissolved in solvent, mixed, form oil phase；
(2) emulsifying agent is mixed with ethylene glycol and isometric deionized water, forms surfactant phase；
(3) PVP-I, remaining deionized water, glacial acetic acid are added into aqueous phase modulation kettle and is mixed into aqueous phase；
(4) surfactant phase is added into high speed homogenization kettle, is gradually added into oil phase, high speed homogenization stirring；
(5) and then aqueous phase modulation kettle and high speed homogenization kettle are connected, aqueous phase is flowed slowly into high speed homogenization kettle；
(6) after aqueous phase is fully immersed high speed homogenization kettle, high speed homogenization stirring is continued；
(7) stirring is stopped, sampling analysis is filling.
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|---|---|---|---|
| CN201510945407.6A CN105362287B (en) | 2015-12-17 | 2015-12-17 | One boar sterilization bath oil |
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| CN105362287B true CN105362287B (en) | 2017-12-29 |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102935082A (en) * | 2012-11-19 | 2013-02-20 | 穆永才 | Drug for external use for preventing and treating scabies |
| CN104523748A (en) * | 2015-01-05 | 2015-04-22 | 四川悦康源通药业有限公司 | Compound iodine disinfectant and preparation method and application thereof |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102935082A (en) * | 2012-11-19 | 2013-02-20 | 穆永才 | Drug for external use for preventing and treating scabies |
| CN104523748A (en) * | 2015-01-05 | 2015-04-22 | 四川悦康源通药业有限公司 | Compound iodine disinfectant and preparation method and application thereof |
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