CN109954396A - A kind of sterilizing deodorization agent of livestock and poultry cultivation - Google Patents

A kind of sterilizing deodorization agent of livestock and poultry cultivation Download PDF

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Publication number
CN109954396A
CN109954396A CN201910223482.XA CN201910223482A CN109954396A CN 109954396 A CN109954396 A CN 109954396A CN 201910223482 A CN201910223482 A CN 201910223482A CN 109954396 A CN109954396 A CN 109954396A
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China
Prior art keywords
deodorization agent
sterilizing deodorization
sterilizing
livestock
mixed liquor
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Pending
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CN201910223482.XA
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Chinese (zh)
Inventor
鞠剑峰
章琴
于亚楠
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Nantong University
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Nantong University
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Priority to CN201910223482.XA priority Critical patent/CN109954396A/en
Publication of CN109954396A publication Critical patent/CN109954396A/en
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    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/34—Chemical or biological purification of waste gases
    • B01D53/74—General processes for purification of waste gases; Apparatus or devices specially adapted therefor
    • B01D53/77—Liquid phase processes
    • B01D53/78—Liquid phase processes with gas-liquid contact
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/72—Treatment of water, waste water, or sewage by oxidation
    • C02F1/722—Oxidation by peroxides
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F11/00—Treatment of sludge; Devices therefor
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2303/00—Specific treatment goals
    • C02F2303/02—Odour removal or prevention of malodour
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2303/00—Specific treatment goals
    • C02F2303/04—Disinfection

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Hydrology & Water Resources (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Dentistry (AREA)
  • Zoology (AREA)
  • Plant Pathology (AREA)
  • Inorganic Chemistry (AREA)
  • Agronomy & Crop Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Pest Control & Pesticides (AREA)
  • Environmental Sciences (AREA)
  • Biomedical Technology (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Disinfection, Sterilisation Or Deodorisation Of Air (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

The present invention provides a kind of sterilizing deodorization agent of livestock and poultry cultivation, the sterilizing deodorization agent is mainly prepared by 0.10%~0.40% Peracetic acid, 0.15%~0.60% hydrogen peroxide, 0.05%~0.10% quaternary ammonium salt cationic surfactant, 0.05%~0.10% benzethonium chloride, 0.10%~0.20% emulsifier and 98.60%~99.40% water, the sterilizing deodorization agent has broad-spectrum sterilization effect, can effectively kill Escherichia coli, Staphylococcus aureus, Pseudomonas aeruginosa, bacterial spore and virus, microorganism etc..The aerial foul smell main source NH of dispersion generated in excrement and feed can be absorbed in bactericidal deodorant injection fog-like3、H2S etc., while being no odour by stink substances oxygenolysis.

Description

A kind of sterilizing deodorization agent of livestock and poultry cultivation
Technical field
The invention belongs to disinfectant fields, and in particular to a kind of livestock and poultry cultivation sterilizing deodorization agent.
Background technique
With livestock and poultry cultivation modernization, intensive, scale development, aquaculture communicable disease also largely occurs, and prevents Disease epidemic prevention and environmental issue also gradually obtain people's attention.Checken pest, swine fever be due to virus, spread of germs, once outburst, it is difficult to Control, causes heavy losses to chicken farm, pig farm, is one of the major issue that livestock and poultry cultivation faces.Odor pollution is livestock and poultry Another major issue in environmental issue is cultivated, not only horizontal, production performance has an impact to animal health, is good for practitioner Health also results in high risks.How effective blocking virus, bacterium route of transmission, reduce checken pest, swine fever outburst risk, reduce NH in foul smell3And H2The material concentrations such as S are of great significance to the development for pushing livestock and poultry breeding industry.
Chicken farm, the common disinfection sanitizer in pig farm have sodium hydroxide, formalin, bromogeramine, peroxide second at present Acid, potassium permanganate, sodium hypochlorite, quick lime etc., but single disinfection sanitizer using effect is not so good as compounding disinfectant, and can only Sterilizing is unable to deodorization.To improve disinfection effect, the Chinese patent of publication number CN108576055A reports a kind of family Fowl cultivates disinfection solution, and main component is Peracetic acid, potassium permanganate, copper sulphate, and phenol etc. is predominantly oxidizing to kill Bacterium and copper sulphate, phenol sterilization, but oxidant concentration is higher, and constituent part is toxic.The China of publication number CN105498494A A kind of wood vinegar of patent report and hydrogen peroxide are the livestock and poultry cultivation disinfection deodorizer of main component, using hydrogen peroxide as disinfectant, Wood vinegar absorbs deodorization, and Peracetic acid, hydrogen peroxide and hydrogen persulfate potassium content are higher in formula, high production cost, in addition, dioxygen Water unstable, easily decompose, hydrogen peroxide once decompose, it is this with hydrogen peroxide be main fungicide disinfection deodorizer Disinfection Effect just It is poor.The Chinese patent of publication number CN109169734A reports a kind of plant source extraction for animal husbandry sterilizing and kills Bacterium deodorant, preparation process is complicated, higher cost.The Chinese patent of 108902145 A of publication number CN reports a kind of sterilization Composition and its preparation and application, sterilization main component are Peracetic acid, hydrogen peroxide and potassium hydrogen persulfate, can effectively kill Portugal Grape coccus, Escherichia coli, Listeria, salmonella, pseudomonas aeruginosa, saccharomycete and S type cholera bacteria, while also can effectively kill The microorganisms such as micrococcus and lactic acid bacteria, but Peracetic acid, hydrogen peroxide and hydrogen persulfate potassium content are higher, and use cost is high.
In conclusion there is also unstable, component is toxic, higher cost for compound sterilizing disinfection deodorizer in the prior art Etc. technical problems.
Summary of the invention
In view of this, the present invention provides the purpose of the present invention is to provide a kind of sterilizing deodorization agent of livestock and poultry cultivation Sterilizing deodorization agent sterilizing deodorization effect it is good and nontoxic, inexpensive, and stability with higher.
The present invention provides a kind of sterilizing deodorization agent of livestock and poultry cultivation, and the composition is by with the following group by weight percentage It is grouped as:
Preferably, quaternary ammonium salt cationic surfactant is selected from cetyl trimethyl bromination in sterilizing deodorization agent Ammonium, hexadecyltrimethylammonium chloride, dodecyl dimethyl benzyl ammonium bromide, dodecyl benzyl dimethyl ammonium chloride, ten One of dialkyl dimethyl ammonium bromide, dodecyl trimethyl ammonium chloride are several.
Preferably, emulsifier is selected from one of OP-10, Tween-20, Triton X-100 in sterilizing deodorization agent Or it is several.
Preferably, sterilizing deodorization agent the preparation method is as follows:
S1. add water into container, then sequentially add quaternary ammonium salt cationic surfactant, benzyl rope under agitation Oronain and emulsifier are dissolved, and the first mixed liquor is obtained；
S2. Peracetic acid and hydrogen peroxide are stirred, obtain the second mixed liquor, the concentration of used Peracetic acid is 15%~20%, the concentration of used hydrogen peroxide is 25%~30%；
S3. then the second mixed liquor obtained in step S2 is added in the first mixed liquor obtained in step S1, is stirred Sterilizing deodorization agent is obtained after mixing uniformly.
The present invention also provides a kind of livestock and poultry cultivation application methods of sterilizing deodorization agent, by sterilizing deodorization agent Direct spraying is on livestock and poultry cultivation region and feces of livestock and poultry.
Compared with prior art, the invention has the following advantages:
1. sterilizing deodorization agent of the invention using Peracetic acid, hydrogen peroxide, quaternary ammonium salt cationic surfactant, Benzethonium chloride compounding, acts synergistically preferably in terms of sterilizing, and it is much super to be sprayed aerial disinfection effect One or two kinds of single disinfection sanitizers are crossed, while quaternary ammonium salt cationic surfactant, benzethonium chloride and emulsifier are multiple Match, there is good osmosis, fall on excrement the microorganism that can effectively kill in excrement after mist sedimentation, it is Peracetic acid, double Stink substances oxygenolysis is effectively no odour by oxygen water energy.Water is very big in misty disinfection sanitizer simultaneously, can effectively inhale Receive the aerial foul smell main source NH of dispersion generated in excrement and feed3、H2S etc., deodorizing effect is preferable.
2. sterilizing deodorization agent energy conservation and environmental protection of the invention, spray amount only need to reach 10mL/m3, can generate relatively strong Sterilizing deodorization effect, nontoxic, pollution-free, noresidue.Noresidue after Peracetic acid, decomposing hydrogen dioxide solution, other several groups It is point nontoxic, and each group is grouped as that content is low in sterilizing deodorization agent prescription, and the content of water is up to 99% or so, is produced into This is low.
3. sterilizing deodorization agent of the invention has broad-spectrum sterilization effect, Escherichia coli, golden yellow grape can be effectively killed Coccus, Pseudomonas aeruginosa, bacterial spore and virus, microorganism etc..
Specific embodiment
Below in conjunction with the embodiment of the present invention, clear, complete description is carried out to technical solution of the present invention, it is clear that institute The embodiment of description is only a part of the embodiments of the present invention, rather than whole embodiments.Based on the embodiments of the present invention, Every other embodiment obtained by those of ordinary skill in the art without making creative efforts, belongs to this hair Bright protection scope.
The present invention provides a kind of sterilizing deodorization agent of livestock and poultry cultivation, and the composition is by with the following group by weight percentage It is grouped as:
In the present invention, quaternary ammonium salt cationic surfactant is preferably cetyl trimethylammonium bromide, hexadecane Base trimethyl ammonium chloride, dodecyl dimethyl benzyl ammonium bromide, dodecyl benzyl dimethyl ammonium chloride, dimethyl One of base ammonium bromide, dodecyl trimethyl ammonium chloride are several, more preferably cetyl trimethylammonium bromide.This Invention is not particularly limited the source of quaternary ammonium salt cationic surfactant, using well known to those skilled in the art 16 Alkyl trimethyl ammonium bromide, hexadecyltrimethylammonium chloride, dodecyl dimethyl benzyl ammonium bromide, dodecyl dimethyl Benzyl ammonium chloride, Dodecydimethylammonium bronides, dodecyl trimethyl ammonium chloride commercial goods.
In the present invention, emulsifier is preferably one of OP-10, Tween-20, Triton X-100 or several, more Preferably OP-10.The present invention is not particularly limited the source of emulsifier, using OP-10 well known to those skilled in the art, Tween-20, the commercial goods Triton X-100.
The present invention also provides the livestock and poultry cultivation preparation methods of sterilizing deodorization agent, comprising the following steps: root first According to the weight percent of each component in sterilizing deodorization agent calculate needed for use quaternary ammonium salt cationic surfactant, The amount of benzethonium chloride and emulsifier, and the amount of water is added；Suitable water is added into container, then successively adds under agitation The quaternary ammonium salt cationic surfactant, benzethonium chloride and emulsifier for entering calculation amount are dissolved, and the first mixed liquor is obtained；It will The Peracetic acid of calculation amount is stirred with hydrogen peroxide, obtains the second mixed liquor, and the concentration of Peracetic acid is preferably 15%~ 20%, the concentration of hydrogen peroxide is preferably 25%~30%, and the present invention is not particularly limited the source of Peracetic acid and hydrogen peroxide, Using commercial goods well known to those skilled in the art；Finally the second mixed liquor is added in the first mixed liquor, is stirred Sterilizing deodorization agent is obtained after uniformly.
The present invention also provides a kind of livestock and poultry cultivation application methods of sterilizing deodorization agent, by sterilizing deodorization agent In spraying device, Direct spraying is reached and preferably killed on livestock and poultry cultivation region and feces of livestock and poultry by spraying device Bacterium disinfecting, deodorizing purpose.
The present invention is not particularly limited hybrid mode, using mechanical stirring well known to those skilled in the art or manually stirs The technical solution mixed, it is therefore an objective to be uniformly mixed each reaction raw materials.
In order to further illustrate the present invention, it is described in detail below by following embodiment.Following embodiment of the present invention Raw material used is commercial goods.
Embodiment 1
Using cetyl trimethylammonium bromide as quaternary ammonium salt cationic surfactant in the present embodiment, according to table The corresponding each component content of embodiment 1, water is added into container, Xiang Shuizhong sequentially adds cetyl under agitation in 1 Trimethylammonium bromide, benzethonium chloride and OP-10 carry out dissolving to obtain the first mixed liquor；Then it weighs Peracetic acid and hydrogen peroxide stirs Mix the second mixed liquor of mixing；Finally the second mixed liquor is added in the first mixed liquor and is sufficiently dissolved, sterilizing, disinfecting and removing is obtained Smelly dose.
Embodiment 2
Using hexadecyltrimethylammonium chloride as quaternary ammonium salt cationic surfactant in the present embodiment, according to table The corresponding each component content of embodiment 2 repeats to implement 1 method in 1, obtains sterilizing deodorization agent.
Embodiment 3
It is pressed using dodecyl dimethyl benzyl ammonium bromide as quaternary ammonium salt cationic surfactant in the present embodiment According to the method that the corresponding each component content of embodiment 3 in table 1 repeats implementation 1, sterilizing deodorization agent is obtained.
Each embodiment constituent content of table 1
The sterilizing deodorization agent for taking the Examples 1 to 3 of equal quality to prepare carries out sterilization experiment, true using clump count method Determine bactericidal effect.Taking 4 bubble chamber volumes is 320mm*450mm*350mm as close test space, is sprayed with 75% alcohol Original bacterium in removing case body is wiped, it is open to come into full contact with placement for 24 hours with colony house, distinguish the sterilization of Example 1~3 afterwards for 24 hours The interior sprinkling bactericidal deodorant of 3 bubble chambers distinguishes closed 20min to disinfection deodorizer thereto, and closed environment sprinkling dosage is 10mL/m3, then take 12 sterile agar cultures to be placed in 4 bubble chambers, wherein 1 is not sprayed sterilizing deodorization agent It is put into 3 sterile agar cultures in bubble chamber, makees blank control, it is closed to fall bacterium processing.Other 3 sprayed embodiment 1~ In the bubble chamber of the sterilizing deodorization agent of 3 preparations, each bubble chamber is put into 3 sterile agar cultures, closed to fall bacterium processing, Namely blank and each embodiment 3 times experiments.After closed processes 5h, it is put into 37 degrees Celsius of insulating box culture 18h.Compare blank The average colony number of agar medium, the average sterilization rate of Examples 1 to 3 sterilizing deodorization agent is up to 99.9%.
The sterilizing deodorization agent for taking the Examples 1 to 3 of equal quality to prepare carries out Deodorization Experiment, passes through air sampler It is sampled.The bactericidal deodorant of equal quality Examples 1 to 3 is taken to spray to environment, wherein the dosage of bactericidal deodorant is 10mL/m3, sample after 3h, every sub-sampling 3 times, NH measured using spectrophotometry3Content and H2S content calculates average value, removes Smelly effect such as table 2:
Bactericidal deodorant deodorizing effect prepared by table 2
Embodiment NH3Content/mgm-3 H2S content/mgm-3
1 0.76 0.53
2 0.84 0.65
3 0.71 0.45
When through detecting unused deodorant, NH3Content is 3.01mgm-3, H2S content is 2.05mgm-3, as shown in Table 2, Spraying to air sterilizing using atomising device, it is because after mist sedimentation that the concentration of the stink substances in air, which is decreased obviously, Falling on excrement can permeate well and to excrement sterilizing, kill the microorganism in excrement, reduce the generation of foul smell；It is misty Disinfection sanitizer absorbs the aerial foul smell main source NH of dispersion generated in excrement and feed3、H2S etc., while by stink Substance oxygenolysis is no odour.
Better embodiment of the invention is explained in detail above, but the present invention is not limited to above-mentioned embodiment party Formula within the knowledge of one of ordinary skill in the art can also be without departing from the purpose of the present invention Various changes can be made.

Claims (5)

1. a kind of sterilizing deodorization agent of livestock and poultry cultivation, which is characterized in that be made of the raw material of following weight percent:
2. sterilizing deodorization agent according to claim 1, which is characterized in that the quaternary ammonium salt type cationic surface active Agent is cetyl trimethylammonium bromide, hexadecyltrimethylammonium chloride, dodecyl dimethyl benzyl ammonium bromide, dodecane One of base dimethyl benzyl ammonium chloride, Dodecydimethylammonium bronides, dodecyl trimethyl ammonium chloride are several.
3. sterilizing deodorization agent according to claim 1, which is characterized in that the emulsifier is OP-10, Tween- 20, one of Triton X-100 or several.
4. sterilizing deodorization agent according to claim 1, which is characterized in that the preparation side of the sterilizing deodorization agent Method is as follows:
S1. add water into container, then sequentially add quaternary ammonium salt cationic surfactant, benzethonium chloride under agitation It is dissolved with emulsifier, obtains the first mixed liquor；
S2. Peracetic acid and hydrogen peroxide are stirred, obtain the second mixed liquor, wherein the concentration of the Peracetic acid is 15%~20%, the concentration of the hydrogen peroxide is 25%~30%；
S3. then the second mixed liquor obtained in step S2 is added in the first mixed liquor obtained in step S1, stirring is equal Sterilizing deodorization agent is obtained after even.
5. a kind of application method of any one of Claims 1 to 4 sterilizing deodorization agent, it is characterised in that: killed described Bacterium disinfection deodorizer Direct spraying is on livestock and poultry cultivation region and feces of livestock and poultry.
CN201910223482.XA 2019-03-22 2019-03-22 A kind of sterilizing deodorization agent of livestock and poultry cultivation Pending CN109954396A (en)

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110897072A (en) * 2019-10-30 2020-03-24 湖北大学 Inorganic ecological breeding feed sterilizing agent and preparation method thereof
CN111165478A (en) * 2020-02-11 2020-05-19 南通大学 Foam type sterilization, disinfection and air purification agent and preparation method and application thereof
CN111202095A (en) * 2020-03-10 2020-05-29 广东省农业科学院植物保护研究所 Composition for preventing and treating bacterial leaf streak of rice as well as preparation method and application thereof

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US20120164699A1 (en) * 2010-12-22 2012-06-28 Empire Technology Development Llc Economical, food-safe extraction of bisphenols
US20130245272A1 (en) * 2010-11-15 2013-09-19 Virdev Intermediates Pvt. Ltd. Process for cyclooxygenase-2 selective inhibitor
CN103704264A (en) * 2014-01-09 2014-04-09 南通思锐生物科技有限公司 Disinfecting detergent
CN105010379A (en) * 2014-04-30 2015-11-04 宁波润增医疗科技有限公司 Bactericide and application thereof
CN105494339A (en) * 2016-02-02 2016-04-20 成都科宏达科技有限公司 Disinfectant for disinfection of livestock and poultry farms, as well as application thereof
US20170215415A1 (en) * 2016-01-29 2017-08-03 David Reay Oxidizing disinfectant formulation and methods of use
CN107374998A (en) * 2017-07-18 2017-11-24 南通优护优家卫生用品有限公司 The preparation technology of hand-cleaning liquid
CN108990979A (en) * 2018-08-14 2018-12-14 广州超威日化股份有限公司 It a kind of cationic germicide and reduces cationic germicide irritation and extends the method for antibacterial time

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20130245272A1 (en) * 2010-11-15 2013-09-19 Virdev Intermediates Pvt. Ltd. Process for cyclooxygenase-2 selective inhibitor
US20120164699A1 (en) * 2010-12-22 2012-06-28 Empire Technology Development Llc Economical, food-safe extraction of bisphenols
CN103704264A (en) * 2014-01-09 2014-04-09 南通思锐生物科技有限公司 Disinfecting detergent
CN105010379A (en) * 2014-04-30 2015-11-04 宁波润增医疗科技有限公司 Bactericide and application thereof
US20170215415A1 (en) * 2016-01-29 2017-08-03 David Reay Oxidizing disinfectant formulation and methods of use
CN105494339A (en) * 2016-02-02 2016-04-20 成都科宏达科技有限公司 Disinfectant for disinfection of livestock and poultry farms, as well as application thereof
CN107374998A (en) * 2017-07-18 2017-11-24 南通优护优家卫生用品有限公司 The preparation technology of hand-cleaning liquid
CN108990979A (en) * 2018-08-14 2018-12-14 广州超威日化股份有限公司 It a kind of cationic germicide and reduces cationic germicide irritation and extends the method for antibacterial time

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110897072A (en) * 2019-10-30 2020-03-24 湖北大学 Inorganic ecological breeding feed sterilizing agent and preparation method thereof
CN111165478A (en) * 2020-02-11 2020-05-19 南通大学 Foam type sterilization, disinfection and air purification agent and preparation method and application thereof
CN111202095A (en) * 2020-03-10 2020-05-29 广东省农业科学院植物保护研究所 Composition for preventing and treating bacterial leaf streak of rice as well as preparation method and application thereof
CN111202095B (en) * 2020-03-10 2021-04-06 广东省农业科学院植物保护研究所 Composition for preventing and treating bacterial leaf streak of rice as well as preparation method and application thereof

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