CN104736666A - 硅酸盐发光材料及其制备方法 - Google Patents

硅酸盐发光材料及其制备方法 Download PDF

Info

Publication number
CN104736666A
CN104736666A CN201280076460.1A CN201280076460A CN104736666A CN 104736666 A CN104736666 A CN 104736666A CN 201280076460 A CN201280076460 A CN 201280076460A CN 104736666 A CN104736666 A CN 104736666A
Authority
CN
China
Prior art keywords
luminescent material
silicate luminescent
preparation
under
silicate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201280076460.1A
Other languages
English (en)
Inventor
周明杰
王荣
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Oceans King Lighting Science and Technology Co Ltd
Shenzhen Oceans King Lighting Engineering Co Ltd
Original Assignee
Oceans King Lighting Science and Technology Co Ltd
Shenzhen Oceans King Lighting Engineering Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Oceans King Lighting Science and Technology Co Ltd, Shenzhen Oceans King Lighting Engineering Co Ltd filed Critical Oceans King Lighting Science and Technology Co Ltd
Publication of CN104736666A publication Critical patent/CN104736666A/zh
Pending legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
    • C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
    • C09K11/87—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing platina group metals
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
    • C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
    • C09K11/87—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing platina group metals
    • C09K11/873—Chalcogenides
    • C—CHEMISTRY; METALLURGY
    • C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
    • C09K11/00—Luminescent, e.g. electroluminescent, chemiluminescent materials
    • C09K11/08—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials
    • C09K11/77—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals
    • C09K11/7743—Luminescent, e.g. electroluminescent, chemiluminescent materials containing inorganic luminescent materials containing rare earth metals containing terbium
    • C09K11/77492—Silicates

Landscapes

  • Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Chemistry (AREA)
  • Luminescent Compositions (AREA)

Abstract

本发明涉及一种硅酸盐发光材料及其制备方法，该硅酸盐发光材料具有化学通式：Li2Ca1-xSiO4:Tbx,My；其中，Tb和M掺杂在Li2Ca1-xSiO4中，且Tb和M为掺杂粒子；M为Ag、Au、Pt、Pd和Cu金属纳米粒子中的至少一种，x的取值范围为0<x≤0.2，y为M与硅酸盐发光材料中Si的摩尔之比，y的取值为0<y≤1×10-2。上述硅酸盐发光材料，通过掺杂金属粒子，使得钛酸盐发光材料在同样激发条件下的发光效率得到极大的提高，发射光的波长没有改变。该硅酸盐发光材料具有良好的稳定性，克服了硫化物和硫氧化物系列发光材料容易分解的缺陷，能替代硫化物和硫氧化物系列发光材料在场发射器件中应用。此外，还提供一种硅酸盐发光材料的制备方法。

Description

PCT国内申请，说明书已公开。

Claims (1)

  1. PCT国内申请，权利要求书已公开。
CN201280076460.1A 2012-10-31 2012-10-31 硅酸盐发光材料及其制备方法 Pending CN104736666A (zh)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PCT/CN2012/083880 WO2014067113A1 (zh) 2012-10-31 2012-10-31 硅酸盐发光材料及其制备方法

Publications (1)

Publication Number Publication Date
CN104736666A true CN104736666A (zh) 2015-06-24

Family

ID=50626337

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201280076460.1A Pending CN104736666A (zh) 2012-10-31 2012-10-31 硅酸盐发光材料及其制备方法

Country Status (5)

Country Link
US (1) US20150284631A1 (zh)
EP (1) EP2915863B1 (zh)
JP (1) JP5965551B2 (zh)
CN (1) CN104736666A (zh)
WO (1) WO2014067113A1 (zh)

Families Citing this family (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20150275083A1 (en) * 2012-10-31 2015-10-01 Ocean's King Lighting Science & Technology Co., Ltd Silicate luminescent material and preparation method therefor
CN110452690A (zh) * 2019-08-24 2019-11-15 宝艺新材料股份有限公司 一种用于纸板表面的防伪发光材料的制备方法
CN112408837A (zh) * 2020-11-23 2021-02-26 保利长大工程有限公司 一种基于花岗岩石粉的复合矿物掺合料及其制备方法
CN112408836A (zh) * 2020-11-23 2021-02-26 贵州四方联达科技有限公司 一种复合矿物掺合料及其制备方法
CN116376538B (zh) * 2023-05-11 2024-04-19 广西师范大学 一种掺杂混合价态Eu离子的无机非光致变色荧光可调材料及其制备方法

Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101760195A (zh) * 2010-01-22 2010-06-30 海洋王照明科技股份有限公司 硅酸盐蓝色发光材料及其制备方法
WO2011153692A1 (zh) * 2010-06-09 2011-12-15 海洋王照明科技股份有限公司 氧化物锡酸盐发光材料及其制备方法
CN102337121A (zh) * 2010-07-21 2012-02-01 海洋王照明科技股份有限公司 硅酸盐发光材料及其制备方法
CN102337120A (zh) * 2010-07-15 2012-02-01 海洋王照明科技股份有限公司 荧光材料及其制备方法
CN102337123A (zh) * 2010-07-20 2012-02-01 海洋王照明科技股份有限公司 硅酸盐发光材料及其制备方法
CN102373059A (zh) * 2010-08-13 2012-03-14 海洋王照明科技股份有限公司 硅酸盐荧光材料及其制造方法
CN102703066A (zh) * 2012-06-13 2012-10-03 中国计量学院 一种氟硅酸盐荧光粉及其制备方法
CN104130774A (zh) * 2014-08-15 2014-11-05 昆明学院 一种氯硅酸盐荧光粉及其制备方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5379000A (en) * 1976-12-22 1978-07-12 Agency Of Ind Science & Technol Lithium calcium silicate and production thereof
US5391320A (en) * 1989-08-28 1995-02-21 Lockheed Missiles & Space Company, Inc. Terbium activated silicate luminescent glasses
DE10238399A1 (de) * 2002-08-22 2004-02-26 Philips Intellectual Property & Standards Gmbh Vorrichtung zur Erzeugung von Strahlung
JP2006232906A (ja) * 2005-02-23 2006-09-07 Sumitomo Chemical Co Ltd 蛍光体およびそれを用いた発光装置
JP4899319B2 (ja) * 2005-02-23 2012-03-21 住友化学株式会社 白色ｌｅｄ
JP5380790B2 (ja) * 2007-01-30 2014-01-08 日亜化学工業株式会社 アルカリ土類金属アルミン酸塩蛍光体及びそれを用いた蛍光ランプ
CN101348714A (zh) * 2008-09-12 2009-01-21 东北师范大学 紫光led转换白光用红色稀土发光材料及制备方法
CN102050573B (zh) * 2009-10-30 2013-03-06 海洋王照明科技股份有限公司 发光玻璃及其制造方法
EP2597133B1 (en) * 2010-07-19 2016-12-07 Ocean's King Lighting Science&Technology Co., Ltd. Luminescent material of silicate and preparing method thereof
JP5701383B2 (ja) * 2010-07-28 2015-04-15 オーシャンズ キング ライティング サイエンス アンド テクノロジー シーオー．，エルティーディー ケイ酸塩蛍光物質の製造方法
WO2013166663A1 (zh) * 2012-05-08 2013-11-14 海洋王照明科技股份有限公司 包覆有金属纳米颗粒的硅酸盐发光材料及其制备方法
US20150275083A1 (en) * 2012-10-31 2015-10-01 Ocean's King Lighting Science & Technology Co., Ltd Silicate luminescent material and preparation method therefor

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101760195A (zh) * 2010-01-22 2010-06-30 海洋王照明科技股份有限公司 硅酸盐蓝色发光材料及其制备方法
WO2011153692A1 (zh) * 2010-06-09 2011-12-15 海洋王照明科技股份有限公司 氧化物锡酸盐发光材料及其制备方法
CN102337120A (zh) * 2010-07-15 2012-02-01 海洋王照明科技股份有限公司 荧光材料及其制备方法
CN102337123A (zh) * 2010-07-20 2012-02-01 海洋王照明科技股份有限公司 硅酸盐发光材料及其制备方法
CN102337121A (zh) * 2010-07-21 2012-02-01 海洋王照明科技股份有限公司 硅酸盐发光材料及其制备方法
CN102373059A (zh) * 2010-08-13 2012-03-14 海洋王照明科技股份有限公司 硅酸盐荧光材料及其制造方法
CN102703066A (zh) * 2012-06-13 2012-10-03 中国计量学院 一种氟硅酸盐荧光粉及其制备方法
CN104130774A (zh) * 2014-08-15 2014-11-05 昆明学院 一种氯硅酸盐荧光粉及其制备方法

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
X. XU ET AL.，: ""High luminescent Li2CaSiO4:Eu2+ cyan phosphor film for wide color gamut field emission display"", 《OPTICS EXPRESS》 *
中国标准出版社: "《中国国家标准汇编 64 GB 5824-5897》", 31 March 1991 *
卓芳平等，: ""Na2CaSiO4∶RE3+(RE=Ce3+，Tb3+，Eu3+)的制备及发光特性"", 《发光学报》 *

Also Published As

Publication number Publication date
JP5965551B2 (ja) 2016-08-10
US20150284631A1 (en) 2015-10-08
EP2915863A1 (en) 2015-09-09
JP2015532938A (ja) 2015-11-16
WO2014067113A1 (zh) 2014-05-08
EP2915863A4 (en) 2016-06-08
EP2915863B1 (en) 2019-11-06

Similar Documents

Publication Publication Date Title
CN101760195B (zh) 硅酸盐蓝色发光材料及其制备方法
CN101899308B (zh) 掺杂金属纳米粒子的稀土铝酸镧发光材料及其制备方法
CN102382646B (zh) 一种硅酸钇钠绿光发光材料及其制备方法
CN104736666A (zh) 硅酸盐发光材料及其制备方法
CN105419799B (zh) 近紫外光转换发射红色荧光的材料的制备方法及其应用
US9115309B2 (en) Zinc manganese silicate containing metal particles luminescent materials and preparation methods thereof
CN102134482A (zh) 掺杂金属纳米粒子的掺锰硅酸锌发光材料及其制备方法
CN101338188A (zh) 一种具有高初始荧光强度的长余辉发光材料的制备方法
JP5655141B2 (ja) 珪酸塩発光材料及びその調製方法
JP5913730B2 (ja) 金属ナノ粒子含有の珪酸塩発光材料及びその調製方法
CN106905962A (zh) 以Zn位及O位缺陷为发光中心的绿色长余辉发光材料
CN103849383B (zh) 铝酸锌锰发光材料及其制备方法
WO2013166663A1 (zh) 包覆有金属纳米颗粒的硅酸盐发光材料及其制备方法
US20120068117A1 (en) Green luminescent materials and their preparing methods
CN103773362A (zh) 偏硅酸钙发光材料及其制备方法
JP6009091B2 (ja) アルミン酸塩発光材料及びその製造方法
CN102341478A (zh) 三价铥激活的氧化物发光材料及其制备方法
US20150275083A1 (en) Silicate luminescent material and preparation method therefor
CN103773370A (zh) 稀土-铝酸盐发光材料及其制备方法
CN103849378A (zh) 偏硅酸钙红色发光材料及其制备方法
CN103788949A (zh) 稀土铝酸镧发光材料及其制备方法
CN104119877A (zh) 一种铝酸锶铽发光材料及其制备方法
CN104119878A (zh) 一种铝酸锶发光材料及其制备方法

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
RJ01 Rejection of invention patent application after publication
RJ01 Rejection of invention patent application after publication

Application publication date: 20150624