CN104403009B - 一种抗性糊精的制备方法 - Google Patents
一种抗性糊精的制备方法 Download PDFInfo
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- CN104403009B CN104403009B CN201410671093.0A CN201410671093A CN104403009B CN 104403009 B CN104403009 B CN 104403009B CN 201410671093 A CN201410671093 A CN 201410671093A CN 104403009 B CN104403009 B CN 104403009B
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- starch
- resistant dextrin
- acid
- crude product
- sea sand
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- 229920001353 Dextrin Polymers 0.000 title claims abstract description 102
- 239000004375 Dextrin Substances 0.000 title claims abstract description 56
- 235000019425 dextrin Nutrition 0.000 title claims abstract description 56
- 238000002360 preparation method Methods 0.000 title claims abstract description 16
- 229920002472 Starch Polymers 0.000 claims abstract description 47
- 235000019698 starch Nutrition 0.000 claims abstract description 47
- 239000008107 starch Substances 0.000 claims abstract description 47
- 239000012043 crude product Substances 0.000 claims abstract description 46
- 239000004576 sand Substances 0.000 claims abstract description 38
- 239000000047 product Substances 0.000 claims abstract description 37
- 238000000034 method Methods 0.000 claims abstract description 18
- 229920000881 Modified starch Polymers 0.000 claims abstract description 7
- 235000019426 modified starch Nutrition 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 5
- 239000004368 Modified starch Substances 0.000 claims abstract description 3
- 238000011033 desalting Methods 0.000 claims description 24
- 239000002253 acid Substances 0.000 claims description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 17
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 15
- 238000001035 drying Methods 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 13
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
- 230000008569 process Effects 0.000 claims description 8
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 6
- 240000003183 Manihot esculenta Species 0.000 claims description 5
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 claims description 5
- 229920001592 potato starch Polymers 0.000 claims description 5
- 230000033228 biological regulation Effects 0.000 claims description 4
- 229910052799 carbon Inorganic materials 0.000 claims description 4
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 3
- 239000003456 ion exchange resin Substances 0.000 claims description 3
- 229920003303 ion-exchange polymer Polymers 0.000 claims description 3
- 229910017604 nitric acid Inorganic materials 0.000 claims description 3
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 2
- 239000001117 sulphuric acid Substances 0.000 claims description 2
- 235000011149 sulphuric acid Nutrition 0.000 claims description 2
- 239000010977 jade Substances 0.000 claims 1
- 239000000843 powder Substances 0.000 claims 1
- 229940100486 rice starch Drugs 0.000 claims 1
- 238000003763 carbonization Methods 0.000 abstract description 4
- 230000004044 response Effects 0.000 abstract description 4
- 238000005265 energy consumption Methods 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 abstract description 3
- 229920002261 Corn starch Polymers 0.000 description 25
- 239000008120 corn starch Substances 0.000 description 25
- 239000003957 anion exchange resin Substances 0.000 description 12
- 239000003729 cation exchange resin Substances 0.000 description 12
- 239000011347 resin Substances 0.000 description 12
- 229920005989 resin Polymers 0.000 description 12
- 239000011260 aqueous acid Substances 0.000 description 11
- 239000007921 spray Substances 0.000 description 11
- 108090000790 Enzymes Proteins 0.000 description 5
- 102000004190 Enzymes Human genes 0.000 description 5
- 229940088598 enzyme Drugs 0.000 description 5
- 235000013305 food Nutrition 0.000 description 5
- 235000013325 dietary fiber Nutrition 0.000 description 4
- 238000005304 joining Methods 0.000 description 4
- 150000003839 salts Chemical class 0.000 description 4
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 3
- 239000008103 glucose Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000010792 warming Methods 0.000 description 3
- DLRVVLDZNNYCBX-UHFFFAOYSA-N Polydextrose Polymers OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(O)O1 DLRVVLDZNNYCBX-UHFFFAOYSA-N 0.000 description 2
- 238000003556 assay Methods 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000004061 bleaching Methods 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 201000006549 dyspepsia Diseases 0.000 description 2
- 230000002255 enzymatic effect Effects 0.000 description 2
- 210000001035 gastrointestinal tract Anatomy 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 230000035790 physiological processes and functions Effects 0.000 description 2
- 239000004575 stone Substances 0.000 description 2
- 239000004382 Amylase Substances 0.000 description 1
- 102000013142 Amylases Human genes 0.000 description 1
- 108010065511 Amylases Proteins 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 241000186016 Bifidobacterium bifidum Species 0.000 description 1
- 206010009944 Colon cancer Diseases 0.000 description 1
- 108010073178 Glucan 1,4-alpha-Glucosidase Proteins 0.000 description 1
- 102100022624 Glucoamylase Human genes 0.000 description 1
- 229920001100 Polydextrose Polymers 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 238000010306 acid treatment Methods 0.000 description 1
- 102000004139 alpha-Amylases Human genes 0.000 description 1
- 108090000637 alpha-Amylases Proteins 0.000 description 1
- 229940024171 alpha-amylase Drugs 0.000 description 1
- 235000019418 amylase Nutrition 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 235000008452 baby food Nutrition 0.000 description 1
- 230000037396 body weight Effects 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 208000029742 colonic neoplasm Diseases 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 102000038379 digestive enzymes Human genes 0.000 description 1
- 108091007734 digestive enzymes Proteins 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000000855 fermentation Methods 0.000 description 1
- 230000004151 fermentation Effects 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 235000013373 food additive Nutrition 0.000 description 1
- 239000002778 food additive Substances 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 239000004310 lactic acid Substances 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 210000002429 large intestine Anatomy 0.000 description 1
- 238000004811 liquid chromatography Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000013622 meat product Nutrition 0.000 description 1
- 244000005700 microbiome Species 0.000 description 1
- 235000013336 milk Nutrition 0.000 description 1
- 239000008267 milk Substances 0.000 description 1
- 210000004080 milk Anatomy 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 239000008363 phosphate buffer Substances 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 235000013856 polydextrose Nutrition 0.000 description 1
- 239000001259 polydextrose Substances 0.000 description 1
- 229940035035 polydextrose Drugs 0.000 description 1
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 1
- 108010001816 pyranose oxidase Proteins 0.000 description 1
- 150000004666 short chain fatty acids Chemical class 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
Landscapes
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
Description
Claims (7)
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CN201410671093.0A CN104403009B (zh) | 2014-11-21 | 2014-11-21 | 一种抗性糊精的制备方法 |
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CN201410671093.0A CN104403009B (zh) | 2014-11-21 | 2014-11-21 | 一种抗性糊精的制备方法 |
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CN104403009A CN104403009A (zh) | 2015-03-11 |
CN104403009B true CN104403009B (zh) | 2016-08-17 |
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Families Citing this family (9)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105542019B (zh) * | 2016-01-27 | 2017-08-18 | 山东百龙创园生物科技股份有限公司 | 抗性糊精及其制备方法 |
CN105693871B (zh) * | 2016-03-10 | 2018-08-07 | 翁源广业清怡食品科技有限公司 | 一种抗性糊精的制备方法 |
CN106117375A (zh) * | 2016-08-02 | 2016-11-16 | 保龄宝生物股份有限公司 | 一种抗性糊精的脱色除杂方法 |
CN107384989A (zh) * | 2017-07-20 | 2017-11-24 | 江南大学 | 一种分支酶及其在抗性糊精制备中的应用 |
CN107674893A (zh) * | 2017-10-19 | 2018-02-09 | 无锡甜丰食品有限公司 | 一种抗性麦芽糊精的制备方法 |
FR3077959B1 (fr) * | 2018-02-22 | 2021-09-24 | Roquette Freres | Procede de fabrication de dextrine de pois resistante |
CN109081874A (zh) * | 2018-10-23 | 2018-12-25 | 东莞东美食品有限公司 | 一种抗性糊精的制备方法 |
CN110295208B (zh) * | 2019-06-28 | 2023-04-18 | 山东省食品发酵工业研究设计院 | 一种提升抗性糊精抗性和产量的方法 |
CN110862461B (zh) * | 2019-11-12 | 2022-02-22 | 潍坊盛泰药业有限公司 | 一种抗性糊精制备方法 |
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CN103045701A (zh) * | 2012-12-29 | 2013-04-17 | 保龄宝生物股份有限公司 | 一种高收率联产抗性糊精、β-环糊精及F42果葡糖浆的方法 |
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Address after: 510308 No. 146 East Xingang Road, Guangzhou, Guangdong, Haizhuqu District Patentee after: GUANGDONG FOOD INDUSTRY INSTITUTE CO.,LTD. Address before: 510308 No. 146 East Xingang Road, Guangzhou, Guangdong, Haizhuqu District Patentee before: Guangdong Food Industry Institute Co.,Ltd. |
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TR01 | Transfer of patent right |
Effective date of registration: 20201105 Address after: 512627, Weng Town Industrial Park, Weng Town, Wengyuan County, Guangdong, Shaoguan Patentee after: L&P FOOD INGREDIENT Co.,Ltd. Patentee after: GUANGDONG GUANGYE QINGYI FOOD TECHNOLOGY CO.,LTD. Address before: 510308 No. 146 East Xingang Road, Guangzhou, Guangdong, Haizhuqu District Patentee before: GUANGDONG FOOD INDUSTRY INSTITUTE Co.,Ltd. |
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TR01 | Transfer of patent right | ||
CP01 | Change in the name or title of a patent holder |
Address after: 512627 Wengcheng Industrial Park, Wengcheng Town, Wengyuan County, Shaoguan City, Guangdong Province Patentee after: L&P FOOD INGREDIENT Co.,Ltd. Patentee after: Guangdong Guangye Qingyi Food Technology Co.,Ltd. Address before: 512627 Wengcheng Industrial Park, Wengcheng Town, Wengyuan County, Shaoguan City, Guangdong Province Patentee before: L&P FOOD INGREDIENT Co.,Ltd. Patentee before: GUANGDONG GUANGYE QINGYI FOOD TECHNOLOGY CO.,LTD. |
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CP01 | Change in the name or title of a patent holder | ||
TR01 | Transfer of patent right |
Effective date of registration: 20230524 Address after: No. 15 Daqing Road, Qinglong Chemical Industry Park, Development Zone, Haimen District, Nantong City, Jiangsu Province, 226466 Patentee after: NANTONG CHANGHAI FOOD ADDITIVE Co.,Ltd. Patentee after: L&P FOOD INGREDIENT Co.,Ltd. Patentee after: Guangdong Guangye Qingyi Food Technology Co.,Ltd. Address before: 512627 Wengcheng Industrial Park, Wengcheng Town, Wengyuan County, Shaoguan City, Guangdong Province Patentee before: L&P FOOD INGREDIENT Co.,Ltd. Patentee before: Guangdong Guangye Qingyi Food Technology Co.,Ltd. |
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