CN104403009A - 一种抗性糊精的制备方法 - Google Patents
一种抗性糊精的制备方法 Download PDFInfo
- Publication number
- CN104403009A CN104403009A CN201410671093.0A CN201410671093A CN104403009A CN 104403009 A CN104403009 A CN 104403009A CN 201410671093 A CN201410671093 A CN 201410671093A CN 104403009 A CN104403009 A CN 104403009A
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- Prior art keywords
- starch
- resistant dextrin
- preparation
- acid
- crude product
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920001353 Dextrin Polymers 0.000 title claims abstract description 104
- 239000004375 Dextrin Substances 0.000 title claims abstract description 58
- 235000019425 dextrin Nutrition 0.000 title claims abstract description 58
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 229920002472 Starch Polymers 0.000 claims abstract description 56
- 239000008107 starch Substances 0.000 claims abstract description 51
- 235000019698 starch Nutrition 0.000 claims abstract description 51
- 239000012043 crude product Substances 0.000 claims abstract description 46
- 239000004576 sand Substances 0.000 claims abstract description 38
- 239000000047 product Substances 0.000 claims abstract description 37
- 238000006243 chemical reaction Methods 0.000 claims abstract description 29
- 238000000034 method Methods 0.000 claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 238000010306 acid treatment Methods 0.000 claims abstract description 4
- 238000011033 desalting Methods 0.000 claims description 24
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 15
- 238000001035 drying Methods 0.000 claims description 13
- 238000003756 stirring Methods 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 11
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 10
- 239000002253 acid Substances 0.000 claims description 10
- 230000008569 process Effects 0.000 claims description 8
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 6
- 235000013312 flour Nutrition 0.000 claims description 6
- 240000003183 Manihot esculenta Species 0.000 claims description 5
- 235000016735 Manihot esculenta subsp esculenta Nutrition 0.000 claims description 5
- 229940100445 wheat starch Drugs 0.000 claims description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 4
- 229920000881 Modified starch Polymers 0.000 claims description 4
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims description 4
- 235000019426 modified starch Nutrition 0.000 claims description 4
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 claims description 3
- 229910052799 carbon Inorganic materials 0.000 claims description 3
- 239000003456 ion exchange resin Substances 0.000 claims description 3
- 229920003303 ion-exchange polymer Polymers 0.000 claims description 3
- 229910017604 nitric acid Inorganic materials 0.000 claims description 3
- 230000035484 reaction time Effects 0.000 abstract description 4
- 238000005265 energy consumption Methods 0.000 abstract description 3
- 238000005516 engineering process Methods 0.000 abstract description 3
- 238000007670 refining Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 48
- 230000002378 acidificating effect Effects 0.000 description 12
- 239000003957 anion exchange resin Substances 0.000 description 12
- 239000003729 cation exchange resin Substances 0.000 description 12
- 239000011347 resin Substances 0.000 description 12
- 229920005989 resin Polymers 0.000 description 12
- 239000011260 aqueous acid Substances 0.000 description 11
- 239000007921 spray Substances 0.000 description 11
- 235000013305 food Nutrition 0.000 description 7
- 235000005979 Citrus limon Nutrition 0.000 description 5
- 244000131522 Citrus pyriformis Species 0.000 description 5
- 108090000790 Enzymes Proteins 0.000 description 5
- 102000004190 Enzymes Human genes 0.000 description 5
- 229940088598 enzyme Drugs 0.000 description 5
- 150000003839 salts Chemical class 0.000 description 4
- 238000003763 carbonization Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000010792 warming Methods 0.000 description 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- DLRVVLDZNNYCBX-UHFFFAOYSA-N Polydextrose Polymers OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(O)O1 DLRVVLDZNNYCBX-UHFFFAOYSA-N 0.000 description 2
- 235000008452 baby food Nutrition 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 238000004061 bleaching Methods 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 235000013325 dietary fiber Nutrition 0.000 description 2
- 230000001079 digestive effect Effects 0.000 description 2
- 201000006549 dyspepsia Diseases 0.000 description 2
- 230000002255 enzymatic effect Effects 0.000 description 2
- 239000000835 fiber Substances 0.000 description 2
- JVTAAEKCZFNVCJ-UHFFFAOYSA-N lactic acid Chemical compound CC(O)C(O)=O JVTAAEKCZFNVCJ-UHFFFAOYSA-N 0.000 description 2
- 210000002429 large intestine Anatomy 0.000 description 2
- 230000035790 physiological processes and functions Effects 0.000 description 2
- 239000004575 stone Substances 0.000 description 2
- 239000004382 Amylase Substances 0.000 description 1
- 102000013142 Amylases Human genes 0.000 description 1
- 108010065511 Amylases Proteins 0.000 description 1
- 241000193830 Bacillus <bacterium> Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 206010009944 Colon cancer Diseases 0.000 description 1
- 108010073178 Glucan 1,4-alpha-Glucosidase Proteins 0.000 description 1
- 102100022624 Glucoamylase Human genes 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- 229920001100 Polydextrose Polymers 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 102000004139 alpha-Amylases Human genes 0.000 description 1
- 108090000637 alpha-Amylases Proteins 0.000 description 1
- 229940024171 alpha-amylase Drugs 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 235000019418 amylase Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000037396 body weight Effects 0.000 description 1
- 238000009395 breeding Methods 0.000 description 1
- 230000001488 breeding effect Effects 0.000 description 1
- 239000000872 buffer Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000004587 chromatography analysis Methods 0.000 description 1
- 208000029742 colonic neoplasm Diseases 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 210000001035 gastrointestinal tract Anatomy 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000000968 intestinal effect Effects 0.000 description 1
- 235000014655 lactic acid Nutrition 0.000 description 1
- 150000002632 lipids Chemical class 0.000 description 1
- 239000007791 liquid phase Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000013622 meat product Nutrition 0.000 description 1
- 230000000813 microbial effect Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 235000013856 polydextrose Nutrition 0.000 description 1
- 239000001259 polydextrose Substances 0.000 description 1
- 229940035035 polydextrose Drugs 0.000 description 1
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 description 1
- 108010001816 pyranose oxidase Proteins 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 150000004666 short chain fatty acids Chemical class 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Landscapes
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
Description
Claims (9)
Priority Applications (1)
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CN201410671093.0A CN104403009B (zh) | 2014-11-21 | 2014-11-21 | 一种抗性糊精的制备方法 |
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CN201410671093.0A CN104403009B (zh) | 2014-11-21 | 2014-11-21 | 一种抗性糊精的制备方法 |
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CN104403009A true CN104403009A (zh) | 2015-03-11 |
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Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105542019A (zh) * | 2016-01-27 | 2016-05-04 | 山东百龙创园生物科技有限公司 | 抗性糊精及其制备方法 |
CN105693871A (zh) * | 2016-03-10 | 2016-06-22 | 翁源广业清怡食品科技有限公司 | 一种抗性糊精的制备方法 |
CN106117375A (zh) * | 2016-08-02 | 2016-11-16 | 保龄宝生物股份有限公司 | 一种抗性糊精的脱色除杂方法 |
CN107384989A (zh) * | 2017-07-20 | 2017-11-24 | 江南大学 | 一种分支酶及其在抗性糊精制备中的应用 |
CN107674893A (zh) * | 2017-10-19 | 2018-02-09 | 无锡甜丰食品有限公司 | 一种抗性麦芽糊精的制备方法 |
CN109081874A (zh) * | 2018-10-23 | 2018-12-25 | 东莞东美食品有限公司 | 一种抗性糊精的制备方法 |
CN110295208A (zh) * | 2019-06-28 | 2019-10-01 | 山东省食品发酵工业研究设计院 | 一种提升抗性糊精抗性和产量的方法 |
CN110862461A (zh) * | 2019-11-12 | 2020-03-06 | 潍坊盛泰药业有限公司 | 一种抗性糊精制备方法 |
JP2021515067A (ja) * | 2018-02-22 | 2021-06-17 | ロケット フレールRoquette Freres | 耐性エンドウデキストリンの製造方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103045701A (zh) * | 2012-12-29 | 2013-04-17 | 保龄宝生物股份有限公司 | 一种高收率联产抗性糊精、β-环糊精及F42果葡糖浆的方法 |
-
2014
- 2014-11-21 CN CN201410671093.0A patent/CN104403009B/zh active Active
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103045701A (zh) * | 2012-12-29 | 2013-04-17 | 保龄宝生物股份有限公司 | 一种高收率联产抗性糊精、β-环糊精及F42果葡糖浆的方法 |
Cited By (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US10479840B2 (en) * | 2016-01-27 | 2019-11-19 | Shandong Bailong Chuangyuan Bio-Tech Co., Ltd | Resistant dextrin and method for preparing the same |
WO2017128984A1 (zh) * | 2016-01-27 | 2017-08-03 | 山东百龙创园生物科技股份有限公司 | 抗性糊精及其制备方法 |
CN105542019B (zh) * | 2016-01-27 | 2017-08-18 | 山东百龙创园生物科技股份有限公司 | 抗性糊精及其制备方法 |
CN105542019A (zh) * | 2016-01-27 | 2016-05-04 | 山东百龙创园生物科技有限公司 | 抗性糊精及其制备方法 |
CN105693871A (zh) * | 2016-03-10 | 2016-06-22 | 翁源广业清怡食品科技有限公司 | 一种抗性糊精的制备方法 |
CN105693871B (zh) * | 2016-03-10 | 2018-08-07 | 翁源广业清怡食品科技有限公司 | 一种抗性糊精的制备方法 |
CN106117375A (zh) * | 2016-08-02 | 2016-11-16 | 保龄宝生物股份有限公司 | 一种抗性糊精的脱色除杂方法 |
CN107384989A (zh) * | 2017-07-20 | 2017-11-24 | 江南大学 | 一种分支酶及其在抗性糊精制备中的应用 |
CN107674893A (zh) * | 2017-10-19 | 2018-02-09 | 无锡甜丰食品有限公司 | 一种抗性麦芽糊精的制备方法 |
JP2021515067A (ja) * | 2018-02-22 | 2021-06-17 | ロケット フレールRoquette Freres | 耐性エンドウデキストリンの製造方法 |
JP7411558B2 (ja) | 2018-02-22 | 2024-01-11 | ロケット フレール | 耐性エンドウデキストリンの製造方法 |
CN109081874A (zh) * | 2018-10-23 | 2018-12-25 | 东莞东美食品有限公司 | 一种抗性糊精的制备方法 |
CN110295208A (zh) * | 2019-06-28 | 2019-10-01 | 山东省食品发酵工业研究设计院 | 一种提升抗性糊精抗性和产量的方法 |
CN110295208B (zh) * | 2019-06-28 | 2023-04-18 | 山东省食品发酵工业研究设计院 | 一种提升抗性糊精抗性和产量的方法 |
CN110862461A (zh) * | 2019-11-12 | 2020-03-06 | 潍坊盛泰药业有限公司 | 一种抗性糊精制备方法 |
CN110862461B (zh) * | 2019-11-12 | 2022-02-22 | 潍坊盛泰药业有限公司 | 一种抗性糊精制备方法 |
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CN104403009B (zh) | 2016-08-17 |
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Address after: 510308 No. 146 East Xingang Road, Guangzhou, Guangdong, Haizhuqu District Patentee after: GUANGDONG FOOD INDUSTRY INSTITUTE CO.,LTD. Address before: 510308 No. 146 East Xingang Road, Guangzhou, Guangdong, Haizhuqu District Patentee before: Guangdong Food Industry Institute Co.,Ltd. |
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Effective date of registration: 20201105 Address after: 512627, Weng Town Industrial Park, Weng Town, Wengyuan County, Guangdong, Shaoguan Patentee after: L&P FOOD INGREDIENT Co.,Ltd. Patentee after: GUANGDONG GUANGYE QINGYI FOOD TECHNOLOGY CO.,LTD. Address before: 510308 No. 146 East Xingang Road, Guangzhou, Guangdong, Haizhuqu District Patentee before: GUANGDONG FOOD INDUSTRY INSTITUTE Co.,Ltd. |
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CP01 | Change in the name or title of a patent holder | ||
CP01 | Change in the name or title of a patent holder |
Address after: 512627 Wengcheng Industrial Park, Wengcheng Town, Wengyuan County, Shaoguan City, Guangdong Province Patentee after: L&P FOOD INGREDIENT Co.,Ltd. Patentee after: Guangdong Guangye Qingyi Food Technology Co.,Ltd. Address before: 512627 Wengcheng Industrial Park, Wengcheng Town, Wengyuan County, Shaoguan City, Guangdong Province Patentee before: L&P FOOD INGREDIENT Co.,Ltd. Patentee before: GUANGDONG GUANGYE QINGYI FOOD TECHNOLOGY CO.,LTD. |
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Effective date of registration: 20230524 Address after: No. 15 Daqing Road, Qinglong Chemical Industry Park, Development Zone, Haimen District, Nantong City, Jiangsu Province, 226466 Patentee after: NANTONG CHANGHAI FOOD ADDITIVE Co.,Ltd. Patentee after: L&P FOOD INGREDIENT Co.,Ltd. Patentee after: Guangdong Guangye Qingyi Food Technology Co.,Ltd. Address before: 512627 Wengcheng Industrial Park, Wengcheng Town, Wengyuan County, Shaoguan City, Guangdong Province Patentee before: L&P FOOD INGREDIENT Co.,Ltd. Patentee before: Guangdong Guangye Qingyi Food Technology Co.,Ltd. |