CN104364196B - 用于纯化氨气或氮气和氢气的混合物或氮气、氢气和氨气的混合物的方法 - Google Patents

用于纯化氨气或氮气和氢气的混合物或氮气、氢气和氨气的混合物的方法 Download PDF

Info

Publication number
CN104364196B
CN104364196B CN201380030255.6A CN201380030255A CN104364196B CN 104364196 B CN104364196 B CN 104364196B CN 201380030255 A CN201380030255 A CN 201380030255A CN 104364196 B CN104364196 B CN 104364196B
Authority
CN
China
Prior art keywords
ammonia
mixture
hydrogen
gas
column
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201380030255.6A
Other languages
English (en)
Chinese (zh)
Other versions
CN104364196A (zh
Inventor
斯瓦沃米尔·安杰伊·马库莱维奇
维欧莱塔·拉娆格-皮莱克卡
斯瓦沃米尔·波德西亚德罗
达留什·莱恩凯维科茨
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WARSAW UNIVERSITY OF TECHNOLOGY
Original Assignee
WARSAW UNIVERSITY OF TECHNOLOGY
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by WARSAW UNIVERSITY OF TECHNOLOGY filed Critical WARSAW UNIVERSITY OF TECHNOLOGY
Publication of CN104364196A publication Critical patent/CN104364196A/zh
Application granted granted Critical
Publication of CN104364196B publication Critical patent/CN104364196B/zh
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/50—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
    • C01B3/56—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification by contacting with solids; Regeneration of used solids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/04—Purification or separation of nitrogen
    • C01B21/0405—Purification or separation processes
    • C01B21/0433—Physical processing only
    • C01B21/045—Physical processing only by adsorption in solids
    • C01B21/0455—Physical processing only by adsorption in solids characterised by the adsorbent
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/04—Purification or separation of nitrogen
    • C01B21/0405—Purification or separation processes
    • C01B21/0433—Physical processing only
    • C01B21/045—Physical processing only by adsorption in solids
    • C01B21/0455—Physical processing only by adsorption in solids characterised by the adsorbent
    • C01B21/0461—Carbon based materials
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/025—Preparation or purification of gas mixtures for ammonia synthesis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/024—Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/04—Purification or separation of nitrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/042—Purification by adsorption on solids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/048—Composition of the impurity the impurity being an organic compound
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/0495—Composition of the impurity the impurity being water
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/06—Integration with other chemical processes
    • C01B2203/068—Ammonia synthesis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14—Details of the flowsheet
    • C01B2203/146—At least two purification steps in series
    • C01B2203/147—Three or more purification steps in series
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0043—Impurity removed
    • C01B2210/0062—Water
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0043—Impurity removed
    • C01B2210/0068—Organic compounds
    • C01B2210/007—Hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Materials Engineering (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Drying Of Gases (AREA)
  • Catalysts (AREA)
  • Gas Separation By Absorption (AREA)
CN201380030255.6A 2012-06-08 2013-06-07 用于纯化氨气或氮气和氢气的混合物或氮气、氢气和氨气的混合物的方法 Expired - Fee Related CN104364196B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
PL399466 2012-06-08
PL399466A PL224195B1 (pl) 2012-06-08 2012-06-08 Sposób oczyszczania amoniaku, mieszanin azotu i wodoru albo azotu, wodoru i amoniaku
PCT/PL2013/000075 WO2013184012A1 (en) 2012-06-08 2013-06-07 Method for purification of ammonia, mixtures of nitrogen and hydrogen, or nitrogen, hydrogen and ammonia

Publications (2)

Publication Number Publication Date
CN104364196A CN104364196A (zh) 2015-02-18
CN104364196B true CN104364196B (zh) 2017-03-15

Family

ID=49684235

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201380030255.6A Expired - Fee Related CN104364196B (zh) 2012-06-08 2013-06-07 用于纯化氨气或氮气和氢气的混合物或氮气、氢气和氨气的混合物的方法

Country Status (16)

Country Link
US (1) US9272906B2 (enExample)
EP (1) EP2858949B1 (enExample)
JP (1) JP5916949B2 (enExample)
KR (1) KR102140118B1 (enExample)
CN (1) CN104364196B (enExample)
CA (1) CA2875257C (enExample)
DK (1) DK2858949T3 (enExample)
ES (1) ES2666124T3 (enExample)
IL (1) IL235948B (enExample)
IN (1) IN2014MN01652A (enExample)
NO (1) NO2858949T3 (enExample)
PL (1) PL224195B1 (enExample)
RU (1) RU2612686C2 (enExample)
SG (1) SG11201406281XA (enExample)
UA (1) UA111880C2 (enExample)
WO (1) WO2013184012A1 (enExample)

Families Citing this family (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105381785A (zh) * 2015-12-16 2016-03-09 无锡吉进环保科技有限公司 一种氨气净化剂的制备方法
CN106310870A (zh) * 2016-11-15 2017-01-11 苏州金宏气体股份有限公司 逐级吸附提纯氨气的装置及利用该装置提纯氨气的方法
RU2689602C1 (ru) * 2018-12-06 2019-05-28 федеральное государственное бюджетное образовательное учреждение высшего образования "Нижегородский государственный технический университет им. Р.Е. Алексеева" (НГТУ) Способ глубокой очистки хладагента R717
JP7628660B2 (ja) * 2019-05-14 2025-02-12 ジェイオーコスメティックス株式会社 粉体化粧料

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020100366A1 (en) * 2000-12-04 2002-08-01 Tadaharu Watanabe Method and materials for purifying hydride gases, inert gases, and non-reactive gases
CN1644501A (zh) * 2003-12-08 2005-07-27 气体产品与化学公司 从氨中除去水的方法
CN1657138A (zh) * 2003-12-08 2005-08-24 气体产品与化学公司 氢化物气体的净化

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3432265A (en) * 1967-04-13 1969-03-11 Foster Wheeler Corp Ammonia production process
JPS5278800A (en) 1975-12-26 1977-07-02 Japan Atom Energy Res Inst Drying of ammonia gas flow
SU1530228A1 (ru) * 1988-01-11 1989-12-23 Государственный научно-исследовательский и проектный институт азотной промышленности и продуктов органического синтеза Способ очистки азотоводородной смеси
CA2094763A1 (en) * 1992-08-05 1994-02-06 William Hertl System and method for removing hydrocarbons from gaseous mixtures
IT1277458B1 (it) * 1995-08-07 1997-11-10 Getters Spa Processo per la rimozione di ossigeno da ammoniaca a temperatura ambiente
DE10004311A1 (de) 2000-02-01 2001-08-02 Basf Ag Destillative Reinigung von Ammoniak
FR2832141B1 (fr) * 2001-11-14 2004-10-01 Ceca Sa Procede de purification de gaz de synthese
DE10261817A1 (de) 2002-12-19 2004-07-01 INSTITUT FüR ANGEWANDTE CHEMIE BERLIN-ADLERSHOF E.V. Verfahren zur katalytischen Umwandlung von Stickoxiden in Stickstoff
EP1607371A1 (en) * 2004-06-18 2005-12-21 Ammonia Casale S.A. Process for producing ammonia on the basis of nitrogen and hydrogen obtained from natural gas
US7297181B2 (en) * 2004-07-07 2007-11-20 Air Liquide America L.P. Purification and transfilling of ammonia
WO2010043472A1 (en) * 2008-10-17 2010-04-22 Unilever Nv Carbon block filter
EP2692437B1 (en) 2011-03-31 2023-09-20 N.E. Chemcat Corporation Ammonia oxidation catalyst, exhaust gas purification device using same, and exhaust gas purification method

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20020100366A1 (en) * 2000-12-04 2002-08-01 Tadaharu Watanabe Method and materials for purifying hydride gases, inert gases, and non-reactive gases
CN1644501A (zh) * 2003-12-08 2005-07-27 气体产品与化学公司 从氨中除去水的方法
CN1657138A (zh) * 2003-12-08 2005-08-24 气体产品与化学公司 氢化物气体的净化

Also Published As

Publication number Publication date
RU2014133963A (ru) 2016-03-20
KR20150028800A (ko) 2015-03-16
SG11201406281XA (en) 2014-11-27
EP2858949A1 (en) 2015-04-15
US20150083972A1 (en) 2015-03-26
RU2612686C2 (ru) 2017-03-13
WO2013184012A1 (en) 2013-12-12
NO2858949T3 (enExample) 2018-07-21
IL235948B (en) 2018-01-31
ES2666124T3 (es) 2018-05-03
CA2875257C (en) 2017-11-07
WO2013184012A4 (en) 2014-03-13
PL224195B1 (pl) 2016-11-30
IL235948A0 (en) 2015-01-29
EP2858949B1 (en) 2018-02-21
JP2015525195A (ja) 2015-09-03
JP5916949B2 (ja) 2016-05-11
KR102140118B1 (ko) 2020-08-03
UA111880C2 (uk) 2016-06-24
CN104364196A (zh) 2015-02-18
PL399466A1 (pl) 2013-12-09
DK2858949T3 (en) 2018-05-07
CA2875257A1 (en) 2013-12-12
US9272906B2 (en) 2016-03-01
IN2014MN01652A (enExample) 2015-07-03

Similar Documents

Publication Publication Date Title
KR940006239B1 (ko) 일산화탄소 생성을 위한 통합적 방법
Khunpolgrang et al. Alternative PSA process cycle with combined vacuum regeneration and nitrogen purging for CH4/CO2 separation
CN104364196B (zh) 用于纯化氨气或氮气和氢气的混合物或氮气、氢气和氨气的混合物的方法
JP2016147766A (ja) 亜酸化窒素の精製方法
WO2008151913A1 (en) Psa process suitable for recovering specific compounds
CN106132508B (zh) 制备和纯化合成气体的方法
TWI537214B (zh) 藉由連續或半連續製程製造高純度鍺烷的方法
KR102033456B1 (ko) 일산화탄소 분리방법 및 일산화탄소 분리시스템
JP6935282B2 (ja) 酸素同位体置換方法及び酸素同位体置換装置
TW201016607A (en) Process for producing high-purity chlorine
JP2015182927A (ja) 塩化水素精製方法および塩化水素精製装置
CN101597069A (zh) 一种氨气的纯化方法
CA2872273C (en) Process and apparatus for producing synthesis gas
JPS6265919A (ja) Ｃｏ分離回収用吸着剤、その製造法およびそれを用いてｃｏを分離回収する方法
JPS6011202A (ja) 水素ガスの選択的濃縮方法
JPH0221285B2 (enExample)
JPH0149643B2 (enExample)
JPS61236896A (ja) コ−クス炉ガスから高純度水素及び合成天然ガスを製造する方法
KR20170039509A (ko) 클러스레이트 화합물을 이용한 올레핀-파라핀 분리 장치 및 방법

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170315