PL399466A1 - Sposób oczyszczania amoniaku, mieszanin azotu i wodoru albo azotu, wodoru i amoniaku - Google Patents

Sposób oczyszczania amoniaku, mieszanin azotu i wodoru albo azotu, wodoru i amoniaku

Info

Publication number
PL399466A1
PL399466A1 PL399466A PL39946612A PL399466A1 PL 399466 A1 PL399466 A1 PL 399466A1 PL 399466 A PL399466 A PL 399466A PL 39946612 A PL39946612 A PL 39946612A PL 399466 A1 PL399466 A1 PL 399466A1
Authority
PL
Poland
Prior art keywords
ammonia
nitrogen
hydrogen
mixture
mixtures
Prior art date
Application number
PL399466A
Other languages
English (en)
Other versions
PL224195B1 (pl
Inventor
Wioletta Raróg-Pilecka
Sławomir Podsiadło
Dariusz Lenkiewicz
Sławomir Andrzej Maculewicz
Original Assignee
Politechnika Warszawska
Sławomir Andrzej Maculewicz
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Warszawska, Sławomir Andrzej Maculewicz filed Critical Politechnika Warszawska
Priority to PL399466A priority Critical patent/PL224195B1/pl
Priority to EP13734868.6A priority patent/EP2858949B1/en
Priority to CN201380030255.6A priority patent/CN104364196B/zh
Priority to SG11201406281XA priority patent/SG11201406281XA/en
Priority to IN1652MUN2014 priority patent/IN2014MN01652A/en
Priority to JP2015515979A priority patent/JP5916949B2/ja
Priority to CA2875257A priority patent/CA2875257C/en
Priority to DK13734868.6T priority patent/DK2858949T3/en
Priority to PCT/PL2013/000075 priority patent/WO2013184012A1/en
Priority to KR1020157000112A priority patent/KR102140118B1/ko
Priority to NO13734868A priority patent/NO2858949T3/no
Priority to RU2014133963A priority patent/RU2612686C2/ru
Priority to ES13734868.6T priority patent/ES2666124T3/es
Priority to UAA201409311A priority patent/UA111880C2/uk
Publication of PL399466A1 publication Critical patent/PL399466A1/pl
Priority to IL235948A priority patent/IL235948B/en
Priority to US14/561,677 priority patent/US9272906B2/en
Publication of PL224195B1 publication Critical patent/PL224195B1/pl

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/04—Purification or separation of nitrogen
    • C01B21/0405—Purification or separation processes
    • C01B21/0433—Physical processing only
    • C01B21/045—Physical processing only by adsorption in solids
    • C01B21/0455—Physical processing only by adsorption in solids characterised by the adsorbent
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/04—Purification or separation of nitrogen
    • C01B21/0405—Purification or separation processes
    • C01B21/0433—Physical processing only
    • C01B21/045—Physical processing only by adsorption in solids
    • C01B21/0455—Physical processing only by adsorption in solids characterised by the adsorbent
    • C01B21/0461—Carbon based materials
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02—Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/025—Preparation or purification of gas mixtures for ammonia synthesis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00—Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/50—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
    • C01B3/56—Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification by contacting with solids; Regeneration of used solids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia
    • C01C1/024—Purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/04—Purification or separation of nitrogen
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/042—Purification by adsorption on solids
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/048—Composition of the impurity the impurity being an organic compound
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04—Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465—Composition of the impurity
    • C01B2203/0495—Composition of the impurity the impurity being water
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/06—Integration with other chemical processes
    • C01B2203/068—Ammonia synthesis
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00—Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14—Details of the flowsheet
    • C01B2203/146—At least two purification steps in series
    • C01B2203/147—Three or more purification steps in series
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0043—Impurity removed
    • C01B2210/0062—Water
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00—Purification or separation of specific gases
    • C01B2210/0043—Impurity removed
    • C01B2210/0068—Organic compounds
    • C01B2210/007—Hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01C—AMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00—Ammonia; Compounds thereof
    • C01C1/02—Preparation, purification or separation of ammonia

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Materials Engineering (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Catalysts (AREA)
  • Gas Separation By Absorption (AREA)
  • Drying Of Gases (AREA)

Abstract

Przedmiotem wynalazku jest sposób oczyszczania amoniaku albo mieszanin azotu i wodoru albo mieszanin azotu, wodoru i amoniaku, zgodnie z którym: amoniak lub mieszanine gazów pod cisnieniem od 0,1 do 25 MPa przepuszcza sie przez kolumne wypelniona tlenkiem glinu o wysokiej powierzchni wlasciwej; nastepnie amoniak lub mieszanine gazów przepuszcza sie przez kolumne wypelniona CaO, NaOH, KaOH lub stopem NaOH/KOH, pojedynczo lub w mieszaninie, w temperaturze od 20 do 70°C i pod cisnieniem od 0,1 do 25 MPa; po czym przepuszcza sie amoniak lub mieszanine gazów przez kolumne wypelniona weglem aktywnym o powierzchni wlasciwej 100-3000 m2/g, z naniesionymi na jego powierzchnie: azotanami(V) lub azotanami(III) sodu, potasu, cezu, magnezu, wapnia, strontu, baru lub ceru, pojedynczo lub w mieszaninie, przy czym wymienione etapy realizuje sie w procesie szeregowym, przy przeplywie strumienia gazu w zakresie od 100 dm3/h do 1000 m3/h.
PL399466A 2012-06-08 2012-06-08 Sposób oczyszczania amoniaku, mieszanin azotu i wodoru albo azotu, wodoru i amoniaku PL224195B1 (pl)

Priority Applications (16)

Application Number Priority Date Filing Date Title
PL399466A PL224195B1 (pl) 2012-06-08 2012-06-08 Sposób oczyszczania amoniaku, mieszanin azotu i wodoru albo azotu, wodoru i amoniaku
DK13734868.6T DK2858949T3 (en) 2012-06-08 2013-06-07 PROCEDURE FOR PURIFICATION OF AMMONIAK, NITROGEN AND HYDROGEN MIXTURES, OR NITROGEN, HYDROGEN AND AMMONIAK
NO13734868A NO2858949T3 (pl) 2012-06-08 2013-06-07
SG11201406281XA SG11201406281XA (en) 2012-06-08 2013-06-07 Method for purification of ammonia, mixtures of nitrogen and hydrogen, or nitrogen, hydrogen and ammonia
IN1652MUN2014 IN2014MN01652A (pl) 2012-06-08 2013-06-07
JP2015515979A JP5916949B2 (ja) 2012-06-08 2013-06-07 アンモニア、窒素と水素の混合物、または窒素と水素とアンモニアの混合物を精製する方法
CA2875257A CA2875257C (en) 2012-06-08 2013-06-07 Method for purification of ammonia, mixtures of nitrogen and hydrogen, or nitrogen, hydrogen and ammonia
EP13734868.6A EP2858949B1 (en) 2012-06-08 2013-06-07 Method for purification of ammonia, mixtures of nitrogen and hydrogen, or nitrogen, hydrogen and ammonia
PCT/PL2013/000075 WO2013184012A1 (en) 2012-06-08 2013-06-07 Method for purification of ammonia, mixtures of nitrogen and hydrogen, or nitrogen, hydrogen and ammonia
KR1020157000112A KR102140118B1 (ko) 2012-06-08 2013-06-07 암모니아, 질소 및 수소 또는 질소, 수소 및 암모니아의 혼합물들의 정제 방법
CN201380030255.6A CN104364196B (zh) 2012-06-08 2013-06-07 用于纯化氨气或氮气和氢气的混合物或氮气、氢气和氨气的混合物的方法
RU2014133963A RU2612686C2 (ru) 2012-06-08 2013-06-07 Способ очистки аммиака, смесей азота и водорода, или азота, водорода и аммиака
ES13734868.6T ES2666124T3 (es) 2012-06-08 2013-06-07 Método para la purificación de amoniaco, mezclas de nitrógeno e hidrógeno, o nitrógeno, hidrógeno y amoniaco
UAA201409311A UA111880C2 (uk) 2012-06-08 2013-07-06 Спосіб очищення аміаку, суміші азоту й водню, або азоту, водню й аміаку
IL235948A IL235948B (en) 2012-06-08 2014-11-27 A method for cleaning ammonia and nitrogen and hydrogen mixtures or nitrogen, hydrogen and ammonia
US14/561,677 US9272906B2 (en) 2012-06-08 2014-12-05 Method for purification of ammonia, mixtures of nitrogen and hydrogen, or nitrogen, hydrogen and ammonia

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
PL399466A PL224195B1 (pl) 2012-06-08 2012-06-08 Sposób oczyszczania amoniaku, mieszanin azotu i wodoru albo azotu, wodoru i amoniaku

Publications (2)

Publication Number Publication Date
PL399466A1 true PL399466A1 (pl) 2013-12-09
PL224195B1 PL224195B1 (pl) 2016-11-30

Family

ID=49684235

Family Applications (1)

Application Number Title Priority Date Filing Date
PL399466A PL224195B1 (pl) 2012-06-08 2012-06-08 Sposób oczyszczania amoniaku, mieszanin azotu i wodoru albo azotu, wodoru i amoniaku

Country Status (16)

Country Link
US (1) US9272906B2 (pl)
EP (1) EP2858949B1 (pl)
JP (1) JP5916949B2 (pl)
KR (1) KR102140118B1 (pl)
CN (1) CN104364196B (pl)
CA (1) CA2875257C (pl)
DK (1) DK2858949T3 (pl)
ES (1) ES2666124T3 (pl)
IL (1) IL235948B (pl)
IN (1) IN2014MN01652A (pl)
NO (1) NO2858949T3 (pl)
PL (1) PL224195B1 (pl)
RU (1) RU2612686C2 (pl)
SG (1) SG11201406281XA (pl)
UA (1) UA111880C2 (pl)
WO (1) WO2013184012A1 (pl)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105381785A (zh) * 2015-12-16 2016-03-09 无锡吉进环保科技有限公司 一种氨气净化剂的制备方法
CN106310870A (zh) * 2016-11-15 2017-01-11 苏州金宏气体股份有限公司 逐级吸附提纯氨气的装置及利用该装置提纯氨气的方法
RU2689602C1 (ru) * 2018-12-06 2019-05-28 федеральное государственное бюджетное образовательное учреждение высшего образования "Нижегородский государственный технический университет им. Р.Е. Алексеева" (НГТУ) Способ глубокой очистки хладагента R717

Family Cites Families (15)

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Publication number Priority date Publication date Assignee Title
US3432265A (en) * 1967-04-13 1969-03-11 Foster Wheeler Corp Ammonia production process
JPS5278800A (en) 1975-12-26 1977-07-02 Japan Atom Energy Res Inst Drying of ammonia gas flow
SU1530228A1 (ru) * 1988-01-11 1989-12-23 Государственный научно-исследовательский и проектный институт азотной промышленности и продуктов органического синтеза Способ очистки азотоводородной смеси
CA2094763A1 (en) * 1992-08-05 1994-02-06 William Hertl System and method for removing hydrocarbons from gaseous mixtures
IT1277458B1 (it) * 1995-08-07 1997-11-10 Getters Spa Processo per la rimozione di ossigeno da ammoniaca a temperatura ambiente
DE10004311A1 (de) 2000-02-01 2001-08-02 Basf Ag Destillative Reinigung von Ammoniak
US6461411B1 (en) * 2000-12-04 2002-10-08 Matheson Tri-Gas Method and materials for purifying hydride gases, inert gases, and non-reactive gases
FR2832141B1 (fr) * 2001-11-14 2004-10-01 Ceca Sa Procede de purification de gaz de synthese
DE10261817A1 (de) 2002-12-19 2004-07-01 INSTITUT FüR ANGEWANDTE CHEMIE BERLIN-ADLERSHOF E.V. Verfahren zur katalytischen Umwandlung von Stickoxiden in Stickstoff
US7160360B2 (en) * 2003-12-08 2007-01-09 Air Products And Chemicals, Inc. Purification of hydride gases
US6892473B1 (en) * 2003-12-08 2005-05-17 Air Products And Chemicals, Inc. Process for removing water from ammonia
EP1607371A1 (en) * 2004-06-18 2005-12-21 Ammonia Casale S.A. Process for producing ammonia on the basis of nitrogen and hydrogen obtained from natural gas
US7297181B2 (en) * 2004-07-07 2007-11-20 Air Liquide America L.P. Purification and transfilling of ammonia
CN102186552B (zh) * 2008-10-17 2015-05-06 荷兰联合利华有限公司 碳块过滤器
WO2012132678A1 (ja) 2011-03-31 2012-10-04 エヌ・イー ケムキャット株式会社 アンモニア酸化触媒、およびそれを用いた排気ガス浄化装置並びに排気ガス浄化方法

Also Published As

Publication number Publication date
CN104364196A (zh) 2015-02-18
JP2015525195A (ja) 2015-09-03
EP2858949A1 (en) 2015-04-15
US9272906B2 (en) 2016-03-01
PL224195B1 (pl) 2016-11-30
JP5916949B2 (ja) 2016-05-11
WO2013184012A4 (en) 2014-03-13
US20150083972A1 (en) 2015-03-26
UA111880C2 (uk) 2016-06-24
CA2875257A1 (en) 2013-12-12
KR20150028800A (ko) 2015-03-16
DK2858949T3 (en) 2018-05-07
ES2666124T3 (es) 2018-05-03
RU2612686C2 (ru) 2017-03-13
NO2858949T3 (pl) 2018-07-21
IL235948A0 (en) 2015-01-29
CN104364196B (zh) 2017-03-15
CA2875257C (en) 2017-11-07
WO2013184012A1 (en) 2013-12-12
SG11201406281XA (en) 2014-11-27
KR102140118B1 (ko) 2020-08-03
IN2014MN01652A (pl) 2015-07-03
RU2014133963A (ru) 2016-03-20
EP2858949B1 (en) 2018-02-21
IL235948B (en) 2018-01-31

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