SG11201406281XA - Method for purification of ammonia, mixtures of nitrogen and hydrogen, or nitrogen, hydrogen and ammonia - Google Patents

Method for purification of ammonia, mixtures of nitrogen and hydrogen, or nitrogen, hydrogen and ammonia

Info

Publication number
SG11201406281XA
SG11201406281XA SG11201406281XA SG11201406281XA SG11201406281XA SG 11201406281X A SG11201406281X A SG 11201406281XA SG 11201406281X A SG11201406281X A SG 11201406281XA SG 11201406281X A SG11201406281X A SG 11201406281XA SG 11201406281X A SG11201406281X A SG 11201406281XA
Authority
SG
Singapore
Prior art keywords
ammonia
nitrogen
hydrogen
purification
mixtures
Prior art date
Application number
SG11201406281XA
Inventor
Wioletta Raróg-Pilecka
Sławomir Podsiadło
Sławomir Andrzej Maculewicz
Dariusz Lenkiewicz
Original Assignee
Politechnika Warszawska
Sławomir Andrzej Maculewicz
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Politechnika Warszawska, Sławomir Andrzej Maculewicz filed Critical Politechnika Warszawska
Publication of SG11201406281XA publication Critical patent/SG11201406281XA/en

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/04Purification or separation of nitrogen
    • C01B21/0405Purification or separation processes
    • C01B21/0433Physical processing only
    • C01B21/045Physical processing only by adsorption in solids
    • C01B21/0455Physical processing only by adsorption in solids characterised by the adsorbent
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/04Purification or separation of nitrogen
    • C01B21/0405Purification or separation processes
    • C01B21/0433Physical processing only
    • C01B21/045Physical processing only by adsorption in solids
    • C01B21/0455Physical processing only by adsorption in solids characterised by the adsorbent
    • C01B21/0461Carbon based materials
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/02Production of hydrogen or of gaseous mixtures containing a substantial proportion of hydrogen
    • C01B3/025Preparation or purification of gas mixtures for ammonia synthesis
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B3/00Hydrogen; Gaseous mixtures containing hydrogen; Separation of hydrogen from mixtures containing it; Purification of hydrogen
    • C01B3/50Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification
    • C01B3/56Separation of hydrogen or hydrogen containing gases from gaseous mixtures, e.g. purification by contacting with solids; Regeneration of used solids
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
    • C01C1/024Purification
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/04Purification or separation of nitrogen
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/042Purification by adsorption on solids
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/048Composition of the impurity the impurity being an organic compound
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/04Integrated processes for the production of hydrogen or synthesis gas containing a purification step for the hydrogen or the synthesis gas
    • C01B2203/0465Composition of the impurity
    • C01B2203/0495Composition of the impurity the impurity being water
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/06Integration with other chemical processes
    • C01B2203/068Ammonia synthesis
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2203/00Integrated processes for the production of hydrogen or synthesis gas
    • C01B2203/14Details of the flowsheet
    • C01B2203/146At least two purification steps in series
    • C01B2203/147Three or more purification steps in series
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00Purification or separation of specific gases
    • C01B2210/0043Impurity removed
    • C01B2210/0062Water
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B2210/00Purification or separation of specific gases
    • C01B2210/0043Impurity removed
    • C01B2210/0068Organic compounds
    • C01B2210/007Hydrocarbons
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01CAMMONIA; CYANOGEN; COMPOUNDS THEREOF
    • C01C1/00Ammonia; Compounds thereof
    • C01C1/02Preparation, purification or separation of ammonia
SG11201406281XA 2012-06-08 2013-06-07 Method for purification of ammonia, mixtures of nitrogen and hydrogen, or nitrogen, hydrogen and ammonia SG11201406281XA (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
PL399466A PL224195B1 (en) 2012-06-08 2012-06-08 Method for purifying ammonia, mixtures of nitrogen and hydrogen or nitrogen, hydrogen and ammonia
PCT/PL2013/000075 WO2013184012A1 (en) 2012-06-08 2013-06-07 Method for purification of ammonia, mixtures of nitrogen and hydrogen, or nitrogen, hydrogen and ammonia

Publications (1)

Publication Number Publication Date
SG11201406281XA true SG11201406281XA (en) 2014-11-27

Family

ID=49684235

Family Applications (1)

Application Number Title Priority Date Filing Date
SG11201406281XA SG11201406281XA (en) 2012-06-08 2013-06-07 Method for purification of ammonia, mixtures of nitrogen and hydrogen, or nitrogen, hydrogen and ammonia

Country Status (16)

Country Link
US (1) US9272906B2 (en)
EP (1) EP2858949B1 (en)
JP (1) JP5916949B2 (en)
KR (1) KR102140118B1 (en)
CN (1) CN104364196B (en)
CA (1) CA2875257C (en)
DK (1) DK2858949T3 (en)
ES (1) ES2666124T3 (en)
IL (1) IL235948B (en)
IN (1) IN2014MN01652A (en)
NO (1) NO2858949T3 (en)
PL (1) PL224195B1 (en)
RU (1) RU2612686C2 (en)
SG (1) SG11201406281XA (en)
UA (1) UA111880C2 (en)
WO (1) WO2013184012A1 (en)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105381785A (en) * 2015-12-16 2016-03-09 无锡吉进环保科技有限公司 Method for preparing ammonia cleaning agent
CN106310870A (en) * 2016-11-15 2017-01-11 苏州金宏气体股份有限公司 Device for gradually adsorbing and purifying ammonia gas and method for utilizing device to purify ammonia gas
RU2689602C1 (en) * 2018-12-06 2019-05-28 федеральное государственное бюджетное образовательное учреждение высшего образования "Нижегородский государственный технический университет им. Р.Е. Алексеева" (НГТУ) Deep cleaning method of coolant r717

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3432265A (en) * 1967-04-13 1969-03-11 Foster Wheeler Corp Ammonia production process
JPS5278800A (en) 1975-12-26 1977-07-02 Japan Atom Energy Res Inst Drying of ammonia gas flow
SU1530228A1 (en) * 1988-01-11 1989-12-23 Государственный научно-исследовательский и проектный институт азотной промышленности и продуктов органического синтеза Method of cleaning nitrogen-hydrogen mixture
CA2094763A1 (en) * 1992-08-05 1994-02-06 William Hertl System and method for removing hydrocarbons from gaseous mixtures
IT1277458B1 (en) * 1995-08-07 1997-11-10 Getters Spa PROCESS FOR THE REMOVAL OF OXYGEN FROM AMMONIA AT ROOM TEMPERATURE
DE10004311A1 (en) 2000-02-01 2001-08-02 Basf Ag Purification of ammonia by distillation
US6461411B1 (en) * 2000-12-04 2002-10-08 Matheson Tri-Gas Method and materials for purifying hydride gases, inert gases, and non-reactive gases
FR2832141B1 (en) * 2001-11-14 2004-10-01 Ceca Sa SYNTHESIS GAS PURIFICATION PROCESS
DE10261817A1 (en) 2002-12-19 2004-07-01 INSTITUT FüR ANGEWANDTE CHEMIE BERLIN-ADLERSHOF E.V. Selective catalytic reduction of nitrogen oxides with ammonia and oxygen, useful for purifying stationary or mobile engine exhaust gas and waste gas from nitric acid manufacture, uses added hydrogen and catalyst containing silver
US7160360B2 (en) * 2003-12-08 2007-01-09 Air Products And Chemicals, Inc. Purification of hydride gases
US6892473B1 (en) * 2003-12-08 2005-05-17 Air Products And Chemicals, Inc. Process for removing water from ammonia
EP1607371A1 (en) * 2004-06-18 2005-12-21 Ammonia Casale S.A. Process for producing ammonia on the basis of nitrogen and hydrogen obtained from natural gas
US7297181B2 (en) * 2004-07-07 2007-11-20 Air Liquide America L.P. Purification and transfilling of ammonia
UA101527C2 (en) * 2008-10-17 2013-04-10 Юнилевер Нв Carbon block filtler
US9011809B2 (en) 2011-03-31 2015-04-21 N.E. Chemcat Corporation Ammonia oxidation catalyst, exhaust gas purification device using same, and exhaust gas purification method

Also Published As

Publication number Publication date
IL235948A0 (en) 2015-01-29
WO2013184012A1 (en) 2013-12-12
NO2858949T3 (en) 2018-07-21
ES2666124T3 (en) 2018-05-03
EP2858949A1 (en) 2015-04-15
RU2014133963A (en) 2016-03-20
IN2014MN01652A (en) 2015-07-03
PL224195B1 (en) 2016-11-30
EP2858949B1 (en) 2018-02-21
JP5916949B2 (en) 2016-05-11
CN104364196B (en) 2017-03-15
CA2875257A1 (en) 2013-12-12
RU2612686C2 (en) 2017-03-13
CN104364196A (en) 2015-02-18
JP2015525195A (en) 2015-09-03
CA2875257C (en) 2017-11-07
DK2858949T3 (en) 2018-05-07
IL235948B (en) 2018-01-31
US20150083972A1 (en) 2015-03-26
WO2013184012A4 (en) 2014-03-13
US9272906B2 (en) 2016-03-01
KR102140118B1 (en) 2020-08-03
KR20150028800A (en) 2015-03-16
PL399466A1 (en) 2013-12-09
UA111880C2 (en) 2016-06-24

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