CN104093729B - 防止多亚磷酸酯配体生产中的溶剂结晶 - Google Patents

防止多亚磷酸酯配体生产中的溶剂结晶 Download PDF

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Publication number
CN104093729B
CN104093729B CN201280053359.4A CN201280053359A CN104093729B CN 104093729 B CN104093729 B CN 104093729B CN 201280053359 A CN201280053359 A CN 201280053359A CN 104093729 B CN104093729 B CN 104093729B
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polyphosphite
crystal
solvent
group
cleaning solvent
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CN104093729A (zh
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G·A·米勒
P·达尔维
R·N·拉瓦尔
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Dow Technology Investments LLC
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Dow Technology Investments LLC
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
    • C07F9/02—Phosphorus compounds
    • C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
    • C07F9/6564—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
    • C07F9/6571—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus and oxygen atoms as the only ring hetero atoms
    • C07F9/6574—Esters of oxyacids of phosphorus
    • C07F9/65746—Esters of oxyacids of phosphorus the molecule containing more than one cyclic phosphorus atom

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Molecular Biology (AREA)
CN201280053359.4A 2011-10-31 2012-10-25 防止多亚磷酸酯配体生产中的溶剂结晶 Active CN104093729B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
IN3721CH2011 2011-10-31
IN3721/CHE/2011 2011-10-31
PCT/US2012/061874 WO2013066712A1 (en) 2011-10-31 2012-10-25 Preventing solvent of crystallization in production of polyphosphite ligands

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CN104093729A CN104093729A (zh) 2014-10-08
CN104093729B true CN104093729B (zh) 2016-09-07

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US (1) US10227365B2 (enExample)
EP (1) EP2773649B1 (enExample)
JP (2) JP6170059B2 (enExample)
CN (1) CN104093729B (enExample)
IN (1) IN2014CN03131A (enExample)
WO (1) WO2013066712A1 (enExample)

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CN104144935B (zh) * 2011-12-30 2016-07-06 巴斯夫欧洲公司 6，6’-[[3，3’，5，5’-四(1，1-二甲基乙基)-[1，1’-联苯]-2，2’-二基]双(氧基)]双-二苯并[d，f][1，3，2]-二氧杂磷杂庚因的结晶溶剂化物和非溶剂化形式
US8796481B2 (en) 2011-12-30 2014-08-05 Basf Se Crystalline solvate and non-solvated forms of 6,6′-[[3,3′,5,5′-tetrakis(1,1-dimethylethyl)-[1,1′biphenyl]-2,2′-diyl]bis(oxy)]bis-dibenzo [d,f] [1,3,2]-dioxaphosphepine
US9108988B2 (en) 2011-12-30 2015-08-18 Basf Se Method of purifying organic diphosphite compounds
CN106660915B (zh) 2014-05-14 2020-08-14 陶氏技术投资有限责任公司 稳定的有机磷化合物
CN107690435A (zh) * 2015-06-19 2018-02-13 陶氏技术投资有限责任公司 结晶配体6，6’‑[[3，3’，5，5’‑四(1，1‑二甲基乙基)‑[1，1’‑联苯]‑2，2’‑二基]双(氧基)]双二苯并[d，f][1，3，2]‑二氧杂磷杂庚英(dioxaphosphepin)
TWI709566B (zh) * 2015-09-30 2020-11-11 美商陶氏科技投資公司 用於製造有機磷化合物的方法
TWI709568B (zh) 2015-09-30 2020-11-11 美商陶氏科技投資公司 用於製造有機磷化合物的方法
RU2770753C2 (ru) * 2017-06-19 2022-04-21 Дау Текнолоджи Инвестментс Ллк Способы очистки лигандов
KR20230087523A (ko) 2020-10-13 2023-06-16 다우 실리콘즈 코포레이션 알데히드 작용기를 갖는 유기규소 화합물의 제조
JP2025512331A (ja) 2022-04-13 2025-04-17 ダウ グローバル テクノロジーズ エルエルシー ポリエーテル官能性有機ケイ素化合物の製造

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US5334739A (en) * 1992-11-30 1994-08-02 Ciba-Geigy Corporation Process an alpha monoclinic crystalline modification of 2,2',2"-nitrilo[triethyl-tris-(3,3',5,5'-tetra-tert-butyl-1,1'-biphenyl-2,2'-diyl)phosphite]

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US4351759A (en) * 1978-01-03 1982-09-28 Ciba-Geigy Corporation Alkylated 2,2'-biphenylene phosphites and stabilized compositions
US4196117A (en) * 1978-01-03 1980-04-01 Ciba-Geigy Corporation Alkylated 1,1'-biphenyl-2,2'-diyl phosphites and stabilized compositions
DE2940548A1 (de) 1979-10-06 1981-04-16 Hoechst Ag, 6000 Frankfurt Kristallisiertes tris-(2-tert.-butylphenyl)-phosphit und verfahren zu seiner herstellung
JPS58103537A (ja) * 1981-12-15 1983-06-20 Adeka Argus Chem Co Ltd 安定化された合成樹脂組成物
US4668651A (en) 1985-09-05 1987-05-26 Union Carbide Corporation Transition metal complex catalyzed processes
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JPH01121368A (ja) * 1987-11-06 1989-05-15 Adeka Argus Chem Co Ltd 安定化された合成樹脂組成物
WO1991009040A1 (en) * 1989-12-08 1991-06-27 Uniroyal Chemical Company, Inc. Method for preparing sterically hindered aryl phosphites
TW213465B (enExample) 1991-06-11 1993-09-21 Mitsubishi Chemicals Co Ltd
JP3416956B2 (ja) * 1991-06-11 2003-06-16 三菱化学株式会社 ヒドロホルミル化法およびビスホスファイト化合物
US5360938A (en) 1991-08-21 1994-11-01 Union Carbide Chemicals & Plastics Technology Corporation Asymmetric syntheses
US5288918A (en) 1992-09-29 1994-02-22 Union Carbide Chemicals & Plastics Technology Corporation Hydroformylation process
DE4238567A1 (de) * 1992-11-16 1994-05-19 Henkel Kgaa Stabilisatormischungen für Polymerisate mit Granaten
DE69412635T2 (de) 1993-11-23 1999-04-15 E.I. Du Pont De Nemours And Co., Wilmington, Del. Verfahren und katalysator-zusammensetzungen für die anlagerung von cyanwassenstoff an monoolefine
JPH07309884A (ja) * 1994-05-18 1995-11-28 Yotsukaichi Gosei Kk トリスアルキルフェニルホスファイトの製造方法
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JPH1053595A (ja) * 1996-05-10 1998-02-24 Sumitomo Chem Co Ltd アリールホスファイト類及びその製造方法
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DE102011002640B4 (de) 2011-01-13 2021-10-07 Evonik Operations Gmbh Verfahren zur Aufreinigung von Biphephos

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US4318845A (en) * 1980-11-24 1982-03-09 Ciba-Geigy Corporation Alkanolamine esters of 1,1'-biphenyl-2,2'-diyl-and alkylidene-1,1'-biphenyl-2,2'-diyl-cyclic phosphites
US5334739A (en) * 1992-11-30 1994-08-02 Ciba-Geigy Corporation Process an alpha monoclinic crystalline modification of 2,2',2"-nitrilo[triethyl-tris-(3,3',5,5'-tetra-tert-butyl-1,1'-biphenyl-2,2'-diyl)phosphite]

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JP6420385B2 (ja) 2018-11-07
EP2773649B1 (en) 2017-07-12
US20140288322A1 (en) 2014-09-25
IN2014CN03131A (enExample) 2015-07-03
EP2773649A1 (en) 2014-09-10
JP6170059B2 (ja) 2017-07-26
CN104093729A (zh) 2014-10-08
US10227365B2 (en) 2019-03-12
JP2017114881A (ja) 2017-06-29
JP2014532653A (ja) 2014-12-08
WO2013066712A1 (en) 2013-05-10

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