CN103720046B - Tobacco filter tip stick of sugar alcohol sweetening agent and production process thereof - Google Patents
Tobacco filter tip stick of sugar alcohol sweetening agent and production process thereof Download PDFInfo
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- CN103720046B CN103720046B CN201410016774.3A CN201410016774A CN103720046B CN 103720046 B CN103720046 B CN 103720046B CN 201410016774 A CN201410016774 A CN 201410016774A CN 103720046 B CN103720046 B CN 103720046B
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Abstract
A tobacco filter tip stick of a sugar alcohol sweetening agent is composed of a tobacco shred beam, a curing agent, forming paper and lap joint glue, wherein the curing agent comprises a mixture made of water-soluble adhesives, the sugar alcohol sweetening agent and modified materials, the sugar alcohol sweetening agent and the modified materials are mixed to prepare a water solution of 40-50%, then the water-soluble adhesives are added to the water solution while the water solution is stirred, so that a mixed solution is prepared, the mixed solution is sprayed to the tobacco shred beam, and the tobacco filter tip stick is manufactured after the steps of formation, drying and balance. The tobacco filter tip stick is firm in adhesive bonding, each physical index and the appearance of the tobacco filter tip stick are qualified, a cigarette applying the tobacco filter tip stick is small in firing feeling and irritation when a user smokes the cigarette, and the quality and sensory quality of the cigarette are both improved.
Description
Technical field
The present invention relates to a kind of cigarette filter tip rod capable containing glycitols sweetener, belong to filter material of cigarette technical field.
Background technology
In prior art, sweetener is generally applicable to all tobacco products, is specially adapted to the cigarette that sugar content is low, nicotine content is high, flue gas pH value is higher.Traditional sweetener mainly sugar products, as: white sugar, brown sugar, honey, glucose, maltose, fructose etc., general sweetener is all used in cigarette charging, sweetener can participate in burning along with the suction of cigarette in pipe tobacco simultaneously, not only can lose that due increasing is sweet, flavouring effect, the chemical reactions such as cracking also may occur and produce new harmful substance.Be added to by sweetener in filter rod, make it in cigarette smoking process, give the special fragrance of cigarette and jealous, be also a kind of conventional method, application number is the patent of invention of 200910311088.8, discloses a kind of Synthesis and applications of mint type cigarette coolant agent; Application number is the patent of invention of 201010200782.5, discloses a kind of cigarette sweet taste freshener slowly-releasing capsule and pill for filter rod; These researchs are all produce refrigerant sense based on interpolation pennyroyal sweetener, and technical essential is the evaporation rate controlling pennyroyal sweetener, and is applied to filter rod and cigarette product.But, the preparation process of these cold-type yellow (clear) sweeteners and slowly-releasing capsule and pill all more complicated, require higher to the forming process of filter rod, production cost is also higher.
Sugar alcohol is a kind of polyalcohol, containing more than two hydroxyls.Current exploitation have D-sorbite, mannitol, antierythrite, maltitol, lactitol, xylitol etc., these sugar alcohols have higher stability to acid, heat, Maillard reaction is less likely to occur, becomes low calorie foods sweetener, be widely used in low calorie foods formula.External using sugar alcohol as sugar substitute, be widely used in food industry.Claim sugarfree foods with the confectionery that sugar alcohol is produced, sugar alcohol, because not utilized by microorganism in oral cavity, does not make again oral cavity pH reduce, can rise on the contrary, so do not corrode tooth, is anticariogenic good material.Sugar alcohol rises without impact on blood sugar for human body value, and can provide certain heat for diabetes patient, so can be used as the nutritive sweetener that diabetes patient provides heat.Sugar alcohol has become one of security food of the use of need not limiting the quantity of international food and health organization approval now.Sugar alcohol dissolves in water, absorb heat, and entrance has refrigerant sense, is suitable for the food such as the peppermint candy producing refrigerant sense.
Polypropylene fibre filter rod and the acid fiber by polylactic filter rod developed, in filter stick formation process, carry out bonding with water-soluble binder, sugar alcohol can be dissolved in this water-soluble binder, join easily in filter rod, production process is simple, be convenient to implement, filter rod cost is lower.Because using water-soluble binder, polypropylene fibre filter rod and the acid fiber by polylactic filter rod developed, to dry more than 30 minutes at 80 ~ 120 DEG C after shaping, generation Maillard reaction makes filter stick variable color not use by sugar sweetener in the process, and glycitols sweetener has higher stability to acid, heat, Maillard reaction is less likely to occur, the requirement of filter rod hyperthermia drying can be met, simultaneously addition within the specific limits time also can ensure the quality index such as adhesive property, hardness of filter rod.
With the acetate fiber ［ C being applied to medium and high classes cigarette
6h
7o
2(OCOCH
3)
x(OH)
3-xn, x=2.28 ~ 2.49 filter rods compare, polypropylene fibre [-(CHCH
3cH
2) n-]) filter rod and acid fiber by polylactic [H-(OCHCH
3cOOCHCH
3cO) n-OH] lack hydroxyl (-OH) group in filter rod molecular structure, also slightly poor to the sensory effects when adsorption effect of cigarette smoke and suction, in filter stick formation process, add a certain amount of sugar alcohol and material modified, introduce hydroxyl (-OH) isopolarity group, also will be conducive to smoke filtration, Sensory Quality of Cigarette improves.
Summary of the invention
The object of the present invention is to provide a kind of sugar alcohol contained cigarette filter tip rod capable, particularly sugar alcohol contained polypropylene fibre or acid fiber by polylactic cigarette filter tip rod capable.Filtration adsorption effect and the Sensory Quality of Cigarette of polypropylene fibre or acid fiber by polylactic cigarette filter tip rod capable can be improved, improving product class.
Technical scheme of the present invention is: a kind of sugar alcohol contained cigarette filter tip rod capable, is made up of pipe tobacco, curing agent, forming paper, overlapping glue, and described curing agent is water-soluble binder, glycitols sweetener and material modified mixture.
Described pipe tobacco is polypropylene fibre tow or acid fiber by polylactic tow.
Described water-soluble binder is: the mixture of vinyl copolymer emulsion, acrylic acid ester emulsion, ester gum emulsion, propane diols and water, and its mass fraction is 40 ~ 50%.
Described glycitols sweetener comprises wherein one or more the mixture such as D-sorbite, mannitol, antierythrite, maltitol, lactitol, xylitol.More preferably one or more mixture in antierythrite, xylitol, D-sorbite, mannitol.
Described material modified be one or more in the poly-γ glutamic acid of the degree of polymerization 300 ~ 1000, acetate starch, phosphate ester starch, vinylacetate starch, oxidized starch, acrylate starch, polyvinyl alcohol, polyvinylpyrrolidone, taurine, carboxymethyl cellulose.
Described glycitols sweetener and material modified mass ratio are 50 ~ 95:5 ~ 50, are made into the aqueous solution that mass fraction is 40-50%, and the mass ratio of this aqueous solution and water soluble adhesive is 5 ~ 30:70 ~ 95.
Described forming paper is the common forming paper of filter rod, and preferred specification is 40g/cm
2forming paper; Described overlapping glue is the water base overlapping glue of cigarette.
Another object of the present invention is to the production technology that a kind of sugar alcohol contained cigarette filter tip rod capable is provided, after specifically glycitols sweetener and material modified mixing being made into the aqueous solution of 40 ~ 50%, add under stirring in water soluble adhesive, continue to stir 30-60min, make glycitols sweetener and material modified fully dissolving in water soluble adhesive be made into mixed serum---curing agent; Sprayed to by this curing agent on the pipe tobacco after shredding, the quantity for spray of curing agent accounts for 10 ~ 25% of pipe tobacco quality.Cigarette filter tip rod capable is made after drying 30-90min, balance at shaping, 80-120 DEG C.
The sugar alcohol contained cigarette filter tip rod capable of one provided by the invention, is a differentiation functional product in cigarette filter tip rod capable segmentation field, can improves filtration adsorption effect and the Sensory Quality of Cigarette of polypropylene (or PLA) fiber cigarette filter tip rod capable, improving product class; Simultaneously can give be hinged with cigarette comfortable refrigerant sense, burning sensation when alleviating suction and excitant, meet the particularization demand of part smoker.This filter rod production technology is simple, be convenient to implement, and the filter rod cost of production is lower, be also conducive to application.
Detailed description of the invention
The preparation of water-soluble binder: be the vinyl copolymer emulsion of 40 ~ 50% by mass fraction, acrylic acid ester emulsion, ester gum emulsion, mix with the ratio of propane diols in 20:50:28:2, be mixed with water-soluble binder for subsequent use.
embodiment 1
Take 25g xylitol sweetener, the 25g degree of polymerization be 850 poly-γ glutamic acid, join in 50g water, be made into the aqueous solution of 50%, under constantly stirring, the above-mentioned aqueous solution is joined in 900g water-soluble binder, continue to stir 60min, fully mix, stir obtained mixed serum-curing agent; Then on commercially available " ZL21 type " filter-stick forming device, be sprayed onto on the polylactic acid fiber cigarette tows after shredding by the curing agent of polylactic acid tobacco tow weight 10%, after shaping, 90 DEG C of drying and shaping 60min, balance, be prepared from acid fiber by polylactic cigarette filter tip rod capable.Bonding firm, the every physical index of this filter stick and outward appearance all qualified, the cigarette be hinged with this filter rod, aspirate time burning sensation, excitant reduce, cigarette quality, aesthetic quality increase.
embodiment 2
Take 33g mannitol, 10g acetate starch, join in 57g, the hot water of 80 DEG C, after being continuously stirring to the complete gelatinization of acetate starch, be made into the suspension of 43%, under constantly stirring, above-mentioned suspension is joined in 930g water-soluble binder, stir 30min, mannitol is dissolved completely, obtained mixed serum-curing agent; Then on commercially available " ZL21 type " filter-stick forming device, be sprayed onto on the polylactic acid fiber cigarette tows after shredding by the mixed serum of tow weight 15%, after shaping, 80 DEG C of drying and shaping 120min, balance, be prepared from acid fiber cigarette filter tip rod capable.Bonding firm, the every physical index of this filter stick and outward appearance all qualified, the cigarette be hinged with this filter rod, aspirate time burning sensation, excitant reduce, cigarette quality, aesthetic quality increase.
embodiment 3
Take 60g D-sorbite, 20g antierythrite, join in 110g, the hot water of 80 DEG C, be stirred to and dissolve completely, add 10g phosphate ester starch, heating water bath, be continuously stirring to the complete gelatinization of phosphate ester starch, under constantly stirring, aforesaid liquid is joined in 800g water soluble adhesive agent emulsion, stir, mix, obtained mixed serum-curing agent; Then on commercially available " ZL21 type " filter-stick forming device, be sprayed onto on the polylactic acid fiber cigarette tows after shredding by the mixed serum of tow weight 20%, after shaping, 95 DEG C of drying and shaping 50min, balance, be prepared from acid fiber cigarette filter tip rod capable.Bonding firm, the every physical index of this filter stick and outward appearance all qualified, the cigarette be hinged with this filter rod, aspirate time burning sensation, excitant reduce, cigarette quality, aesthetic quality increase.
embodiment 4
Take 32g maltitol, 18g lactitol, 10g polyvinylpyrrolidone, the 10g degree of polymerization are the poly-γ glutamic acid of 500, join in 105g water, be made into the aqueous solution of 40%, under constantly stirring, the above-mentioned aqueous solution is joined in 825g water-soluble binder, abundant stirring, to mix, obtained mixed serum-curing agent; Then on commercially available " ZL21 type " filter-stick forming device, be sprayed onto on the polylactic acid fiber cigarette tows after shredding by the mixed serum of tow weight 25%, after shaping, 100 DEG C of drying and shaping 40min, balance, be prepared from acid fiber cigarette filter tip rod capable.Bonding firm, the every physical index of this filter stick and outward appearance all qualified, the cigarette be hinged with this filter rod, aspirate time burning sensation, excitant reduce, cigarette quality, aesthetic quality increase.
embodiment 5
Take 45g maltitol, 15g mannitol, 30g xylitol join in 174g water, be stirred to and dissolve completely, then 22.5g oxidized starch is added, the starch that 13.5g is acrylate modified, be heated to 80 DEG C, be continuously stirring to acrylate modified starch, the complete gelatinization of oxidized starch, under constantly stirring, aforesaid liquid is joined in 700g water-soluble binder, stir, obtained mixed serum-curing agent; Then on commercially available " ZL21 type " filter-stick forming device, be sprayed onto on the polylactic acid fiber cigarette tows after shredding by the mixed serum of tow weight 12.5%, after shaping, 95 DEG C of drying and shaping 55min, balance, be prepared from acid fiber cigarette filter tip rod capable.Bonding firm, the every physical index of this filter stick and outward appearance all qualified, the cigarette be hinged with this filter rod, aspirate time burning sensation, excitant reduce, cigarette quality, aesthetic quality increase.
embodiment 6
Take 19g antierythrite, 30g maltitol, 33g lactitol, 5g polyvinyl alcohol, after 3g carboxymethyl cellulose mixes, under stirring, join in 100g water, be stirred to and dissolve completely, then, aforesaid liquid is joined in 1000g water-soluble binder, stir, obtained mixed serum-curing agent; Then on commercially available " ZL21 type " filter-stick forming device, be sprayed onto on the polypropylene fibre pipe tobacco after shredding by the mixed serum of tow weight 10.8%, after shaping, 95 DEG C of drying and shaping 70min, balance, be prepared from polypropylene fibre cigarette filter tip rod capable.Bonding firm, the every physical index of this filter stick and outward appearance all qualified, the cigarette be hinged with this filter rod, aspirate time burning sensation, excitant reduce, cigarette quality, aesthetic quality increase.
embodiment 7
Take 52g lactitol, 33g D-sorbite, 10.6 polyvinylpyrrolidones, the 12.8g degree of polymerization be that 400 poly-γ glutamic acid join in 150g water, be stirred to and dissolve completely, then under constantly stirring, aforesaid liquid is joined in 846g water-soluble binder, stir, obtained mixed serum-curing agent; Then on commercially available " ZL21 type " filter-stick forming device, be sprayed onto on the polypropylene fibre pipe tobacco after shredding by the mixed serum of tow weight 22.3%, after shaping, 110 DEG C of drying and shaping 50min, balance, be prepared from polypropylene fibre cigarette filter tip rod capable.Bonding firm, the every physical index of this filter stick and outward appearance all qualified, the cigarette be hinged with this filter rod, aspirate time burning sensation, excitant reduce, cigarette quality, aesthetic quality increase.
embodiment 8
Take 20g D-sorbite, 6.5g mannitol, 25g lactitol, 5.5g taurine join in 100g water, be stirred to and dissolve completely, then 20g phosphate ester starch is added, be heated to 80 DEG C, be continuously stirring to the complete gelatinization of phosphate ester starch, under constantly stirring, aforesaid liquid is joined in 823g water-soluble binder, stir, obtained mixed serum-curing agent; Then on commercially available " ZL21 type " filter-stick forming device, be sprayed onto on the polypropylene fibre pipe tobacco after shredding by the mixed serum of tow weight 25%, after shaping, 115 DEG C of drying and shaping 45min, balance, be prepared from polypropylene fibre cigarette filter tip rod capable.Bonding firm, the every physical index of this filter stick and outward appearance all qualified, the cigarette be hinged with this filter rod, aspirate time burning sensation, excitant reduce, cigarette quality, aesthetic quality increase.
embodiment 9
Take 45g maltitol, 30g xylitol joins in 120g water, be stirred to and dissolve completely, then the starch that 9g is acrylate modified is added, 13.5g vinylacetate starch, be heated to 80 DEG C, be continuously stirring to acrylate modified starch, the complete gelatinization of vinylacetate starch, under constantly stirring, aforesaid liquid is joined in 820g water-soluble binder, stir, obtained mixed serum-curing agent; Then on commercially available " ZL21 type " filter-stick forming device, be sprayed onto on the polypropylene fibre pipe tobacco after shredding by the mixed serum of tow weight 18.8%, after shaping, 120 DEG C of drying and shaping 30min, balance, be prepared from polypropylene fibre cigarette filter tip rod capable.Bonding firm, the every physical index of this filter stick and outward appearance all qualified, the cigarette be hinged with this filter rod, aspirate time burning sensation, excitant reduce, cigarette quality, aesthetic quality increase.
embodiment 10
Take 14g mannitol, 27g D-sorbite, 22g maltitol, 5g polyvinyl alcohol, 8.5g taurine join in 100g water, be stirred to and dissolve completely, under constantly stirring, aforesaid liquid is joined in 920g water-soluble binder, stir, obtained mixed serum-curing agent; Then on commercially available " ZL21 type " filter-stick forming device, be sprayed onto on the polypropylene fibre pipe tobacco after shredding by the mixed serum of tow weight 10%, after shaping, 105 DEG C of drying and shaping 50min, balance, be prepared from polypropylene fibre cigarette filter tip rod capable.Bonding firm, the every physical index of this filter stick and outward appearance all qualified, the cigarette be hinged with this filter rod, aspirate time burning sensation, excitant reduce, cigarette quality, aesthetic quality increase.
Claims (4)
1., containing a cigarette filter tip rod capable for glycitols sweetener, be made up of pipe tobacco, curing agent, forming paper, overlapping glue, it is characterized in that, described curing agent is water-soluble binder, glycitols sweetener and material modified mixture;
Described water soluble adhesive is the mixture of vinyl copolymer emulsion, acrylic acid ester emulsion, ester gum emulsion, propane diols and water, and its mass fraction is 40 ~ 50%;
Described glycitols sweetener is D-sorbite, mannitol, antierythrite, maltitol, lactitol, xylitol wherein one or more mixture;
Described material modified be one or more in the poly-γ glutamic acid of the degree of polymerization 300 ~ 1000, acetate starch, phosphate ester starch, vinylacetate starch, oxidized starch, acrylate starch, polyvinylpyrrolidone, taurine, carboxymethyl cellulose;
Described glycitols sweetener and material modified mass ratio are 50 ~ 95:5 ~ 50, are made into the aqueous solution that mass fraction is 40-50% after being mixed, and the mass ratio of this aqueous solution and water soluble adhesive is 5 ~ 30:70 ~ 95.
2., according to the cigarette filter tip rod capable containing glycitols sweetener described in claim 1, it is characterized in that, described pipe tobacco is polypropylene fibre tow or acid fiber by polylactic tow.
3. according to described in claim 1 containing the cigarette filter tip rod capable of glycitols sweetener, it is characterized in that, described glycitols sweetener is one or more mixture in antierythrite, xylitol, D-sorbite, mannitol.
4. according to the production technology of the cigarette filter tip rod capable containing glycitols sweetener described in claim 1, it is characterized in that, be added to the water after glycitols sweetener and material modified mixing, be warming up to 25 ~ 80 DEG C, stirring makes it dissolve or gelatinization, then join in water-soluble binder, continue to stir 30-60min, make glycitols sweetener and material modified fully dissolving in water-soluble binder be made into mixed serum curing agent; This curing agent is sprayed on the pipe tobacco after shredding, after drying 30-90min, balance at shaping, 80-120 DEG C, make cigarette filter tip rod capable.
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| CN201410016774.3A CN103720046B (en) | 2014-01-15 | 2014-01-15 | Tobacco filter tip stick of sugar alcohol sweetening agent and production process thereof |
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| CN201410016774.3A CN103720046B (en) | 2014-01-15 | 2014-01-15 | Tobacco filter tip stick of sugar alcohol sweetening agent and production process thereof |
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| CN103720046A CN103720046A (en) | 2014-04-16 |
| CN103720046B true CN103720046B (en) | 2015-04-08 |
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Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104095288A (en) * | 2014-07-04 | 2014-10-15 | 中国烟草总公司郑州烟草研究院 | Additive for preparing cigarette paper for paper filter tip |
| CN104312497B (en) * | 2014-10-13 | 2016-09-21 | 湖北中烟工业有限责任公司 | The spigot joint glue of Medicated cigarette of a kind of efficient loading Mint Essence and preparation technology thereof |
| CN108835712B (en) * | 2018-03-21 | 2021-02-02 | 云南中烟工业有限责任公司 | Compound additive for reducing release amount of crotonaldehyde in smoke and preparation method and application thereof |
| CN108685192A (en) * | 2018-06-27 | 2018-10-23 | 常州龙途新材料科技有限公司 | A kind of degradable smell generating element and smoking article for non-combustion-cigarette |
| CA3028427A1 (en) * | 2018-12-21 | 2020-06-21 | Christian L. Cyr | Bong stem filter |
| CN111466613B (en) * | 2020-04-09 | 2022-04-08 | 上海华宝生物科技有限公司 | Flavoring particle for filter stick, preparation method thereof and filter stick |
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| CN1933744A (en) * | 2004-02-19 | 2007-03-21 | 三荣源有限公司 | Nicotine-reducing agent and nicotine reduction method |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| GB201112402D0 (en) * | 2011-07-19 | 2011-08-31 | British American Tobacco Co | Cellulose acetate compositions |
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| GB1043412A (en) * | 1962-04-09 | 1966-09-21 | Eastman Kodak Co | Tobacco smoke filter |
| CN1933744A (en) * | 2004-02-19 | 2007-03-21 | 三荣源有限公司 | Nicotine-reducing agent and nicotine reduction method |
| CN101693819A (en) * | 2009-09-01 | 2010-04-14 | 常德芙蓉大亚化纤有限公司 | Polypropylene wire-beam forming water-based emulsion bond for cigarettes and production method thereof |
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Effective date of registration: 20200922 Address after: 444100 No. 336, mayor ban Road, Dangyang, Yichang, Hubei Patentee after: HUBEI JINYE YUYANG CHEMICAL FIBRE Co.,Ltd. Patentee after: Shenzhen Ruifeng New Material Technology Group Co., Ltd Address before: 444100 Guangzhou Road, Hubei city of Yichang Province Dangyang city No. 77 Patentee before: HUBEI JINYE YUYANG CHEMICAL FIBRE Co.,Ltd. |
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