CN103708977A - Fulvic acid water-soluble foliar fertilizer and preparation method thereof - Google Patents
Fulvic acid water-soluble foliar fertilizer and preparation method thereof Download PDFInfo
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- CN103708977A CN103708977A CN201310716392.7A CN201310716392A CN103708977A CN 103708977 A CN103708977 A CN 103708977A CN 201310716392 A CN201310716392 A CN 201310716392A CN 103708977 A CN103708977 A CN 103708977A
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Abstract
The invention discloses a fulvic acid water-soluble foliar fertilizer and a preparation method thereof. The fulvic acid water-soluble foliar fertilizer comprises the following active ingredients in parts by weight: 30-40 parts of sodium fulvate, 40-50 parts of potassium dihydrogen phosphate, 20-30 parts of urea, 10-15 parts of ammonium sulfate, 25-35 parts of waste silk, 15-20 parts of feather meal, 5-10 parts of monosodium glutamate leftovers, 2-3 parts of zinc nitrate, 1-2 parts of manganese sulfate, 1-2 parts of magnesium sulphate, 0.5-1.5 parts of sodium molybrate, 1-2 parts of boric acid, 0.5-1 part of thylenediaminetetraacetic acid disodium, 10-15 parts of kelp residues, 5-10 parts of rape seed cakes, 8-12 parts of soyabean meal, 5-10 parts of brewer's grain, 8-12 parts of waste methane liquid, 2-3 parts of luffa stem, 1.5-2.5 parts of cortex meliae, 1-2 parts of tung tree roots, 2-3 parts of radix sophorae flavescentis, 1-2 parts of thunder god vine, and 2-3 parts of castor plant leaves. The foliar fertilizer is complete and balanced in nutrients, high in fertilizer efficiency, high in fertilizer utilization rate, capable of fast replenishing the nutrition for crops, also has the effects of disease prevention, antibiosis, insect killing, insect expelling, flower retention, fruit retention and the like, is obvious in effects of reducing the plant disease and insect pest of crops, reducing the use of chemical pesticide, promoting fast growth of crops, enhancing the stress tolerance of crops, improving the quality of crops and increasing both production and income, and has tremendous economic benefits.
Description
Technical field
the present invention relates to water-soluble foliage fertilizer of a kind of xanthohumic acid and preparation method thereof, belong to technical field of agricultural fertilizers.
Background technology
Foliage fertilizer is to take Foliage Absorption as object, and the required nutrient of crop is directly used to the fertilizer on blade face, is the important supplement of soil application.Nutrient balance supply is the key of farm crop good quality and high output.The degree that the present crop yield of foliage fertilizer fertilizer efficiency final body increases income.For a long time, China's foliage fertilizer is main mainly with the foliar nutrient of single nutrition, cannot meet the required various nutritive ingredients of crop growth, and therefore, the multiple nutritional components foliage fertilizer that exploitation adapts to the many nutritional needs of the many nutrients of farm crop has important economic benefit.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, a kind of main fertilizer, micro-fertilizer, organic matter, amino acid, humic acid of integrating is provided, comprehensive nutrition is balanced, water-soluble foliage fertilizer of xanthohumic acid that utilization rate of fertilizer is high, fertilizer efficiency is high and preparation method thereof.
For achieving the above object, the technical solution used in the present invention is as follows:
The water-soluble foliage fertilizer of a kind of xanthohumic acid, raw material by following weight part is made: SODLUM FULVATE 30-40, potassium primary phosphate 40-50, urea 20-30, ammonium sulfate 10-15, useless silk 25-35, feather meal 15-20, monosodium glutamate tankage 5-10, zinc nitrate 2-3, manganous sulfate 1-2, magnesium sulfate 1-2, Sodium orthomolybdate 0.5-1.5, boric acid 1-2, disodium ethylene diamine tetraacetate 0.5-1, kelp residue 10-15, rapeseed cake 5-10, dregs of beans 8-12, brewer's grains 5-10, methane waste liquor 8-12, Towel Gourd Stem 2-3, Cortex Meliae 1.5-2.5, Root of Tungoiltree 1-2, kuh-seng 2-3, trypterygine 1-2, Folium Ricini 2-3.
A preparation method for the water-soluble foliage fertilizer of xanthohumic acid, comprises the following steps:
(1) getting useless silk and feather meal mixes, then by 1:3-5 solid-liquid ratio, adding concentration is the sulphuric acid soln of 15-20%, at 105-115 ℃ of temperature, be hydrolyzed 4-6h, then the sodium hydroxide solution neutralizing hydrolysis solution that is 10-15% by concentration is to neutral, in hydrating solution, add monosodium glutamate tankage, zinc nitrate, manganous sulfate, magnesium sulfate, Sodium orthomolybdate, boric acid and disodium ethylene diamine tetraacetate again, be heated to 80-90 ℃, chelatropic reaction 30-40min, be concentrated into appropriate, lyophilize powdered, obtains the micro-fertilizer of rear chelating amino acids;
(2) get Towel Gourd Stem, Cortex Meliae, Root of Tungoiltree, kuh-seng, trypterygine and Folium Ricini and mix, add 4-8 times of water big fire and boil rear medium and small fire decoction 1-2h, filter, filtrate, filter residue are all stand-by;
(3) filter residue kelp residue, rapeseed cake, dregs of beans, brewer's grains, methane waste liquor and step (2) being made mixes, add again appropriate water, moisture controlled is at 50-60%, stir, sealing and fermenting, temperature is controlled at 32-36 ℃, and secondary fermentation in 10-15 days completes, cross leaching fermented liquid, stand-by;
(4) fermented liquid step (3) being made mixes with the filtrate that step (2) makes, and is concentrated in right amount lyophilize powdered;
(5) the micro-fertilizer of chelating amino acids that powder SODLUM FULVATE, potassium primary phosphate, urea, ammonium sulfate and step (4) being made, step (1) make mixes, and packing is finished product.
Beneficial effect of the present invention:
Foliage fertilizer comprehensive nutrition of the present invention is balanced, the Available Amino Acids of existing q.s and high reactivity xanthohumic acid, there are again the appropriate main fertile composition of nitrogen phosphorus potassium and zinc-manganese magnesium molybdenum boron micro-fertilizer composition, meet the required various nutritive ingredients of plant growth completely, foliage fertilizer of the present invention not only fertilizer efficiency is high, utilization rate of fertilizer is high, can supplement rapidly crop nutrition content, also there is diseases prevention, antibacterial, desinsection, expelling parasite, protect flower, the effects such as fruit retention, reduce the disease and pest incidence of crop, reduce the use of chemical pesticide, promote crop Fast Growth, strengthen crop anti-adversity, improve crop quality, the effect of increasing income is obvious, there is huge economic benefit.
Embodiment
the water-soluble foliage fertilizer of xanthohumic acid, is made by the raw material of following weight (kg): SODLUM FULVATE 35, potassium primary phosphate 45, urea 25, ammonium sulfate 12, useless silk 30, feather meal 18, monosodium glutamate tankage 8, zinc nitrate 2, manganous sulfate 1.5, magnesium sulfate 1, Sodium orthomolybdate 1, boric acid 1.5, disodium ethylene diamine tetraacetate 0.7, kelp residue 12, rapeseed cake 8, dregs of beans 10, brewer's grains 7, methane waste liquor 9, Towel Gourd Stem 2.5, Cortex Meliae 2, Root of Tungoiltree 1.5, kuh-seng 2, trypterygine 1, Folium Ricini 2.
A preparation method for the water-soluble foliage fertilizer of xanthohumic acid, comprises the following steps:
(1) getting useless silk and feather meal mixes, then by 1:4 solid-liquid ratio, adding concentration is 18% sulphuric acid soln, at 110 ℃ of temperature, be hydrolyzed 5h, then the sodium hydroxide solution neutralizing hydrolysis solution that is 15% by concentration is extremely neutral, then adds monosodium glutamate tankage, zinc nitrate, manganous sulfate, magnesium sulfate, Sodium orthomolybdate, boric acid and disodium ethylene diamine tetraacetate in hydrating solution, is heated to 85 ℃, chelatropic reaction 30min, be concentrated in right amount, lyophilize powdered, obtains the micro-fertilizer of rear chelating amino acids;
(2) get Towel Gourd Stem, Cortex Meliae, Root of Tungoiltree, kuh-seng, trypterygine and Folium Ricini and mix, add 6 times of water big fire and boil rear medium and small fire decoction 1.5h, filter, filtrate, filter residue are all stand-by;
(3) filter residue kelp residue, rapeseed cake, dregs of beans, brewer's grains, methane waste liquor and step (2) being made mixes, then adds appropriate water, and moisture controlled is 55%, stir, sealing and fermenting, temperature is controlled at 35 ℃, secondary fermentation in 12 days completes, and crosses leaching fermented liquid, stand-by;
(4) fermented liquid step (3) being made mixes with the filtrate that step (2) makes, and is concentrated in right amount lyophilize powdered;
(5) the micro-fertilizer of chelating amino acids that powder SODLUM FULVATE, potassium primary phosphate, urea, ammonium sulfate and step (4) being made, step (1) make mixes, and packing is finished product.
field test:
1, test is processed and is arranged
2 processing, test group are established in test altogether: local habits fertilization+spray the water-soluble foliage fertilizer of xanthohumic acid of the present invention, sprays 3 times; Control group: the clear water of local habits fertilization+spray and test group equivalent.3 repetitions, community area 30m are established in each processing
2, random alignment.Tested in paddy rice jointing stage, boot stage and filling stage and spray, totally 3 times, the jointing stage is got foliage fertilizer 100g/hm
2, be watered 400 times and implement foliage-spray; Boot stage and filling stage are got respectively foliage fertilizer 150g/hm
2, be watered 500 times and implement foliage-spray.
2, test basic condition
Tested on May 4th, 2011 to August 12 and carry out in certain Rice Cropping base, experimental field soil type is two to close soil, soil physico-chemical property: pH value is 8.24, organic 18.6g/kg, alkali-hydrolyzable nitrogen 136.9 mg/kg, rapid available phosphorus 17.2mg/kg, available potassium 104.5mg/kg, soil medium fertility level.For examination rice varieties Shen Nong 606.Each processing cultivation and field management measure are in full accord.
3, experimental result:
The impact of table 1 foliage fertilizer of the present invention on Economic Character of Rice
As shown in Table 1, foliage fertilizer of the present invention can promote crop Fast Growth, improves rice yield and improves rice quality, reduces the incidence of disease and pest, has important economic benefit.
Claims (2)
1. the water-soluble foliage fertilizer of xanthohumic acid, it is characterized in that, raw material by following weight part is made: SODLUM FULVATE 30-40, potassium primary phosphate 40-50, urea 20-30, ammonium sulfate 10-15, useless silk 25-35, feather meal 15-20, monosodium glutamate tankage 5-10, zinc nitrate 2-3, manganous sulfate 1-2, magnesium sulfate 1-2, Sodium orthomolybdate 0.5-1.5, boric acid 1-2, disodium ethylene diamine tetraacetate 0.5-1, kelp residue 10-15, rapeseed cake 5-10, dregs of beans 8-12, brewer's grains 5-10, methane waste liquor 8-12, Towel Gourd Stem 2-3, Cortex Meliae 1.5-2.5, Root of Tungoiltree 1-2, kuh-seng 2-3, trypterygine 1-2, Folium Ricini 2-3.
2. the preparation method of the water-soluble foliage fertilizer of xanthohumic acid according to claim 1, is characterized in that comprising the following steps:
(1) getting useless silk and feather meal mixes, then by 1:3-5 solid-liquid ratio, adding concentration is the sulphuric acid soln of 15-20%, at 105-115 ℃ of temperature, be hydrolyzed 4-6h, then the sodium hydroxide solution neutralizing hydrolysis solution that is 10-15% by concentration is to neutral, in hydrating solution, add monosodium glutamate tankage, zinc nitrate, manganous sulfate, magnesium sulfate, Sodium orthomolybdate, boric acid and disodium ethylene diamine tetraacetate again, be heated to 80-90 ℃, chelatropic reaction 30-40min, be concentrated into appropriate, lyophilize powdered, obtains the micro-fertilizer of rear chelating amino acids;
(2) get Towel Gourd Stem, Cortex Meliae, Root of Tungoiltree, kuh-seng, trypterygine and Folium Ricini and mix, add 4-8 times of water big fire and boil rear medium and small fire decoction 1-2h, filter, filtrate, filter residue are all stand-by;
(3) filter residue kelp residue, rapeseed cake, dregs of beans, brewer's grains, methane waste liquor and step (2) being made mixes, add again appropriate water, moisture controlled is at 50-60%, stir, sealing and fermenting, temperature is controlled at 32-36 ℃, and secondary fermentation in 10-15 days completes, cross leaching fermented liquid, stand-by;
(4) fermented liquid step (3) being made mixes with the filtrate that step (2) makes, and is concentrated in right amount lyophilize powdered;
(5) the micro-fertilizer of chelating amino acids that powder SODLUM FULVATE, potassium primary phosphate, urea, ammonium sulfate and step (4) being made, step (1) make mixes, and packing is finished product.
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104098405A (en) * | 2014-08-09 | 2014-10-15 | 桂林劲胜生物科技有限公司 | Chelating state micronutrient fertilizer with insecticidal function and production method thereof |
| CN104876755A (en) * | 2015-05-13 | 2015-09-02 | 安徽农业大学 | Special water-soluble fertilizer for seedlings, and preparation method and application thereof |
| CN104945168A (en) * | 2015-07-14 | 2015-09-30 | 甘肃省昕农福农业科技有限责任公司 | Activity compound leaf fertilizer special for potatoes |
| CN105523822A (en) * | 2014-09-29 | 2016-04-27 | 安庆华辉生物科技有限公司 | Compound type amino-acid water-soluble fertilizer for mulberry leaves and preparation method therefor |
| CN105585386A (en) * | 2016-03-23 | 2016-05-18 | 山东绿亨生物工程有限公司 | Amino acid biological organic water-soluble fertilizer and preparing method thereof |
| CN106490069A (en) * | 2016-10-19 | 2017-03-15 | 罗友祥 | Chinese herbal medicine synthetic drug fertilizer and its preparation method and application |
| CN106748099A (en) * | 2016-12-14 | 2017-05-31 | 杨攀 | Celery special insect-proof foliar fertilizer and preparation method thereof |
| CN106800479A (en) * | 2016-12-09 | 2017-06-06 | 河池市技术开发中心 | Crop foliage fertilizer |
| CN108373378A (en) * | 2018-02-28 | 2018-08-07 | 武汉中碳御农生物科技有限公司 | A kind of preparation method of photosynthetic accelerator |
| CN108610150A (en) * | 2018-07-27 | 2018-10-02 | 普定县冠辉种养殖专业合作社 | A kind of grape Liquid Fertilizer and preparation method thereof |
| CN109988004A (en) * | 2017-12-30 | 2019-07-09 | 陕西基训中草药研发有限公司 | A kind of Chinese traditional medicine composition fertilizer and preparation method thereof |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104098405A (en) * | 2014-08-09 | 2014-10-15 | 桂林劲胜生物科技有限公司 | Chelating state micronutrient fertilizer with insecticidal function and production method thereof |
| CN105523822A (en) * | 2014-09-29 | 2016-04-27 | 安庆华辉生物科技有限公司 | Compound type amino-acid water-soluble fertilizer for mulberry leaves and preparation method therefor |
| CN104876755A (en) * | 2015-05-13 | 2015-09-02 | 安徽农业大学 | Special water-soluble fertilizer for seedlings, and preparation method and application thereof |
| CN104945168A (en) * | 2015-07-14 | 2015-09-30 | 甘肃省昕农福农业科技有限责任公司 | Activity compound leaf fertilizer special for potatoes |
| CN105585386A (en) * | 2016-03-23 | 2016-05-18 | 山东绿亨生物工程有限公司 | Amino acid biological organic water-soluble fertilizer and preparing method thereof |
| CN106490069A (en) * | 2016-10-19 | 2017-03-15 | 罗友祥 | Chinese herbal medicine synthetic drug fertilizer and its preparation method and application |
| CN106800479A (en) * | 2016-12-09 | 2017-06-06 | 河池市技术开发中心 | Crop foliage fertilizer |
| CN106748099A (en) * | 2016-12-14 | 2017-05-31 | 杨攀 | Celery special insect-proof foliar fertilizer and preparation method thereof |
| CN109988004A (en) * | 2017-12-30 | 2019-07-09 | 陕西基训中草药研发有限公司 | A kind of Chinese traditional medicine composition fertilizer and preparation method thereof |
| CN108373378A (en) * | 2018-02-28 | 2018-08-07 | 武汉中碳御农生物科技有限公司 | A kind of preparation method of photosynthetic accelerator |
| CN108610150A (en) * | 2018-07-27 | 2018-10-02 | 普定县冠辉种养殖专业合作社 | A kind of grape Liquid Fertilizer and preparation method thereof |
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Application publication date: 20140409 |