CN105585386A - Amino acid biological organic water-soluble fertilizer and preparing method thereof - Google Patents
Amino acid biological organic water-soluble fertilizer and preparing method thereof Download PDFInfo
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- CN105585386A CN105585386A CN201610167190.5A CN201610167190A CN105585386A CN 105585386 A CN105585386 A CN 105585386A CN 201610167190 A CN201610167190 A CN 201610167190A CN 105585386 A CN105585386 A CN 105585386A
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
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- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05G—MIXTURES OF FERTILISERS COVERED INDIVIDUALLY BY DIFFERENT SUBCLASSES OF CLASS C05; MIXTURES OF ONE OR MORE FERTILISERS WITH MATERIALS NOT HAVING A SPECIFIC FERTILISING ACTIVITY, e.g. PESTICIDES, SOIL-CONDITIONERS, WETTING AGENTS; FERTILISERS CHARACTERISED BY THEIR FORM
- C05G3/00—Mixtures of one or more fertilisers with additives not having a specially fertilising activity
- C05G3/80—Soil conditioners
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- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Soil Sciences (AREA)
- Fertilizers (AREA)
Abstract
The invention belongs to the technical field of fertilizer, and particularly relates to amino acid biological organic water-soluble fertilizer and a preparing method thereof. The fertilizer is prepared from monosodium glutamate waste liquid, triethanolamine, bean dregs, urea, monopotassium phosphate, traditional Chinese medicine residues, chicken manure, ethyl phenyl polyethylene glycol, a microelement additive, aureobasidium pullulans, bacillus licheniformis, streptomyces microflavus and paecilomyces lilacinus. All nutritional ingredients of the water-soluble fertilizer take effect synergistically, inorganic nutrients and soluble organic matter are provided for crop growth, the capacity for preserving moisture and fertility is good, absorption is fast, the physical characteristics of soil are improved, and the defect of soil caking caused by using fertilizer continuously is overcome.
Description
Technical field
The invention belongs to technical field of fertilizers, be specifically related to a kind of amino acid bio organic water-soluble fertilizer and preparation method thereof.
Background technology
Water soluble fertilizer is a kind of quick action fertilizer, without residue, can directly be absorbed by the root system of crop or blade face, with water band fertilizer, realize water-fertilizer integral, fertilizer efficiency is fast, can solve the nutritional need of high-yield crop fast growing period, and water-soluble fertilizer is as a kind of new-type fertilizer, and its formula is various, and using method is also very flexible. Gourmet powder waste water is in glutamate production process, to extract the mother liquor after glutamic acid, and 1 ton of monosodium glutamate of every production approximately will be discharged the gourmet powder waste water of 10-15 ton. In gourmet powder waste water, contain the required trace element of amino acid, residual sugar and various plants, be the desirable feedstock of producing organic fertilizer, but in gourmet powder waste water, contain the ammonium sulfate of high concentration, use for a long time, cause soil block etc., restricted its development and application aspect fertilizer. The water-soluble fertilizer of existing liquid state can provide sufficient nutrient for the growth of crop, but the fertilizer efficiency time is too short, and preserve moisture and fertility ability causes degradation problem under soil productivity.
Summary of the invention
The problem existing for prior art, the invention provides a kind of amino acid bio organic water-soluble fertilizer, various nutritional labeling synergies in this fertilizer, both for the growth of crop provides inorganic nutrients, SOM is provided simultaneously, preserve moisture and fertility ability is good, absorbs soon, improves the physical behavior of soil.
The present invention also provides a kind of preparation method of amino acid bio organic water-soluble fertilizer.
The technical scheme that the present invention adopted is to achieve these goals:
The invention provides a kind of amino acid bio organic water-soluble fertilizer, be prepared from by following weight portion raw material: gourmet powder waste water 30-40 part, triethanolamine 5-8 part, bean dregs 25-30 part, urea 20-30 part, potassium dihydrogen phosphate 36-38 part, Chinese medicine slag 18-23 part, chicken manure 10-15 part, Nonidet P40 8-10 part, trace mineral supplement 5-8 part, Aureobasidium pullulans 1-3 part, bacillus licheniformis 2-4 part, streptomyces microflavus 2-3 part, Paecilomyces lilacinus 2-3 part.
Further, described trace mineral supplement is made up of according to mass ratio 1:0.6:0.8:1 zinc sulfate, manganese sulfate, EDTA-copper, ammonium molybdate.
Further, the water content of described bean dregs is 65%, and bean dregs used in the present invention are the byproduct of preparing in bean curd process.
The present invention also provides a kind of preparation method of amino acid bio organic water-soluble fertilizer, comprises the following steps:
(1) will in bean dregs, add Aureobasidium pullulans, triethanolamine, after stirring, logical aerobe fermentation 1d, obtains fermenting bean dregs liquid;
(2) urea of 1/3 weight portion will be added in Chinese medicine slag, after stirring, paving is spilt to the leaf of firm after-flame and is built heap, sprinkles chicken manure above Chinese medicine slag, adds water, carry out turning for the first time after 8d building heap, then interval 4d, 3d, the each turning of 2d is once, obtain Chinese medicine slag humus, then add water according to mass ratio 1:1, stir and soak after 12h, filter to obtain humus filtrate;
(3) in gourmet powder waste water, add calcium hydroxide and zeolite, after being warming up to 85 DEG C, stir 30min, then be cooled to 30 DEG C, add above-mentioned fermenting bean dregs liquid, after stirring, leave standstill 1d, filter, extruding filter residue, merges twice liquid, then adds humus filtrate, residue 2/3 weight portion urea, Nonidet P40, trace mineral supplement, potassium dihydrogen phosphate, bacillus licheniformis, streptomyces microflavus, Paecilomyces lilacinus, after stirring.
Further, in step (3), in described every 1kg gourmet powder waste water, add calcium hydroxide and the 30g zeolite of 20g.
First the present invention adds Aureobasidium pullulans to ferment in bean dregs, the appropriate triethanolamine that adds, can change the saturating property of the mould cell of short stalk, reduce fermentation time, in sweat, produce soluble polysaccharide-pulullan polysaccharide, there is the performances such as good film forming, use after the water soluble fertilizer that contains this kind of polysaccharide, can prevent the excess diffusion of fertilizer, improve utilization rate of fertilizer. In gourmet powder waste water by adding calcium hydroxide, can reactive moieties sulphur ammonium, zeolite can adsorb the heavy metal ion in gourmet powder waste water etc., plays catharsis.
Advantage of the present invention is:
(1) the each nutritional labeling synergy of water soluble fertilizer provided by the invention both, for the growth of crop provides inorganic nutrients, provided SOM simultaneously, preserve moisture and fertility ability is good, absorb soon, improve the physical behavior of soil, overcome the soil block that continuous Fertilizer application causes.
(2) can produce by fermentation the humus, amino acid and other polysaccharide that promote plant root growth, promote plant growth, the antipathogenic composition containing in Chinese medicine slag, can reduce disease, improves the resistance against diseases of crop.
(3) by preparation method provided by the invention, improve the stability of fertilizer, between each bacterial classification, act synergistically, strengthen soil enzyme activities, fertilizer efficiency period increases.
Detailed description of the invention
Below by embodiment, the present invention will be further elaborated, should be understood that, following explanation is only in order to explain the present invention, its content is not limited.
Embodiment 1
In 1.1 bean dregs that are 65% by 30 parts of water content, add 3 parts of Aureobasidium pullulans, 8 parts of triethanolamines, after stirring, logical aerobe fermentation 1d, obtains fermenting bean dregs liquid;
1.2 by the urea that adds 9 parts in 23 parts of Chinese medicine slags, after stirring, paving is spilt to the leaf of firm after-flame and is built heap, and the thickness of Chinese medicine slag is 15-18cm, above Chinese medicine slag, 13 parts of chicken manures is spread and is spilt out uniformly, after building heap 8d, carry out turning for the first time, then interval 4d, 3d, the each turning of 2d is once, obtain Chinese medicine slag humus, then add water according to mass ratio 1:1, stir and soak after 12h, filter to obtain humus filtrate;
1.336 in part gourmet powder waste water, in every kg gourmet powder waste water, add 20g calcium hydroxide and 30g zeolite, after being warming up to 85 DEG C, stir 30min, then be cooled to 30 DEG C, add above-mentioned fermenting bean dregs liquid, after stirring, leave standstill 1d, filter, extruding filter residue, filtrate is merged with twice liquid of extruding gained, then add humus filtrate, 18 parts of urea of residue, 9 parts of Nonidet P40s, 7 portions of trace mineral supplements, 37 parts of potassium dihydrogen phosphates, 2 parts of bacillus licheniformis, 3 parts of streptomyces microflavus, 3 parts of Paecilomyces lilacinus, after stirring;
Described trace mineral supplement is made up of according to mass ratio 1:0.6:0.8:1 zinc sulfate, manganese sulfate, EDTA-copper, ammonium molybdate.
Embodiment 2
In 2.1 bean dregs that are 65% by 28 parts of water content, add 2 parts of Aureobasidium pullulans, 5 parts of triethanolamines, after stirring, logical aerobe fermentation 1d, obtains fermenting bean dregs liquid;
2.2 by the urea that adds 10 parts in 20 parts of Chinese medicine slags, after stirring, paving is spilt to the leaf of firm after-flame and is built heap, and the thickness of Chinese medicine slag is 15-18cm, above Chinese medicine slag, 10 parts of chicken manures is spread and is spilt out uniformly, after building heap 8d, carry out turning for the first time, then interval 4d, 3d, the each turning of 2d is once, obtain Chinese medicine slag humus, then add water according to mass ratio 1:1, stir and soak after 12h, filter to obtain humus filtrate;
2.330 in part gourmet powder waste water, in every kg gourmet powder waste water, add 20g calcium hydroxide and 30g zeolite, after being warming up to 85 DEG C, stir 30min, then be cooled to 30 DEG C, add above-mentioned fermenting bean dregs liquid, after stirring, leave standstill 1d, filter, extruding filter residue, filtrate is merged with twice liquid of extruding gained, then add humus filtrate, remain 20 parts of urea, 8 parts of Nonidet P40s, 5 portions of trace mineral supplements (composition is with embodiment 1), 36 parts of potassium dihydrogen phosphates, 3 parts of bacillus licheniformis, 3 parts of streptomyces microflavus, 3 parts of Paecilomyces lilacinus, after stirring.
Embodiment 3
In 3.1 bean dregs that are 65% by 25 parts of water content, add 1 part of Aureobasidium pullulans, 7 parts of triethanolamines, after stirring, logical aerobe fermentation 1d, obtains fermenting bean dregs liquid;
3.2 by the urea that adds 6.7 parts in 18 parts of Chinese medicine slags, after stirring, paving is spilt to the leaf of firm after-flame and is built heap, and the thickness of Chinese medicine slag is 15-18cm, above Chinese medicine slag, 12 parts of chicken manures is spread and is spilt out uniformly, after building heap 8d, carry out turning for the first time, then interval 4d, 3d, the each turning of 2d is once, obtain Chinese medicine slag humus, then add water according to mass ratio 1:1, stir and soak after 12h, filter to obtain humus filtrate;
3.340 in part gourmet powder waste water, in every kg gourmet powder waste water, add 20g calcium hydroxide and 30g zeolite, after being warming up to 85 DEG C, stir 30min, then be cooled to 30 DEG C, add above-mentioned fermenting bean dregs liquid, after stirring, leave standstill 1d, filter, extruding filter residue, filtrate is merged with twice liquid of extruding gained, then add humus filtrate, remain 13.3 parts of urea, 10 parts of Nonidet P40s, 8 portions of trace mineral supplements (composition is with embodiment 1), 38 parts of potassium dihydrogen phosphates, 4 parts of bacillus licheniformis, 3 parts of streptomyces microflavus, 2 parts of Paecilomyces lilacinus, after stirring.
Comparative example 1
1.1 by the urea that adds 9 parts in 23 parts of Chinese medicine slags, after stirring, paving is spilt to the leaf of firm after-flame and is built heap, and the thickness of Chinese medicine slag is 15-18cm, above Chinese medicine slag, 13 parts of chicken manures is spread and is spilt out uniformly, after building heap 8d, carry out turning for the first time, then interval 4d, 3d, the each turning of 2d is once, obtain Chinese medicine slag humus, then add water according to mass ratio 1:1, stir and soak after 12h, filter to obtain humus filtrate;
1.236 in part gourmet powder waste water, every kg adds 20g calcium hydroxide and 30g zeolite, after being warming up to 85 DEG C, stir 30min, then be cooled to 30 DEG C, filter, extruding filter residue, filtrate is merged with twice liquid of extruding gained, then add humus filtrate, 18 parts of urea of residue, 9 parts of Nonidet P40s, 7 portions of trace mineral supplements, 37 parts of potassium dihydrogen phosphates, 3 parts of Aureobasidium pullulans, 2 parts of bacillus licheniformis, 3 parts of streptomyces microflavus, 3 parts of Paecilomyces lilacinus, after stirring.
Comparative example 2
In 36 parts of gourmet powder waste waters, every kg adds 20g calcium hydroxide and 30g zeolite, after being warming up to 85 DEG C, stir 30min, then be cooled to 30 DEG C, filter, extruding filter residue, filtrate is merged with twice liquid of extruding gained, add 27 parts of urea, 9 parts of Nonidet P40s, 7 portions of trace mineral supplements, 37 parts of potassium dihydrogen phosphates, 3 parts of Aureobasidium pullulans, 2 parts of bacillus licheniformis, 3 parts of streptomyces microflavus, 3 parts of Paecilomyces lilacinus, after stirring.
Compliance test result:
1, the water-soluble fertilizer of amino acid that utilizes the embodiment of the present invention 1 to prepare carries out result of use checking to greenhouse strawberry: inventor opens in Jinan City and test in strawberry cultivating base, strawberry cultivars is Feng Xiang, choose the booth of identical cultivated area, numbering S1-S4, S1 organizes the water-soluble fertilizer that only uses the embodiment of the present invention 1 to prepare; The water-soluble fertilizer that S2 group is used comparative example 1 to prepare; The water-soluble fertilizer that S3 group is used comparative example 2 to prepare; S4 is control group, the fertilizer that adopts traditional plantation strawberry to use; According to every mu of consumption 3-4 kilogram, use after diluting 800 times. All identical with growing period daily management in plantation. Total output to each test group strawberry, soluble sugar content, sugar-acid ratio, Determination of Vitamin C detect, and concrete outcome is in table 1.
Table 1
Use water-soluble fertilizer provided by the invention, the Strawberry ripening phase shifts to an earlier date listing in 5-8 days, and the hyperchromic speed of strawberry is fast, and color and luster is vivid, fruit size homogeneous, and fruit type is good.
2, by the experimental plot of above-mentioned plantation strawberry, carefully extract after Strawberry Seedlings, the earth 200g that fetches earth, averages soil enzyme activities and detects, and concrete outcome is in table 2.
Table 2
The disease probability of happening such as the output of the water-soluble fertilizer of 3, being prepared by embodiment 1-3 and comparative example 1-2 to tomato, droop, bacterial wilt are added up; Each group dose is 6kg/ mu. Concrete statistics is in table 3.
Table 3
In addition, the more traditional water-soluble fertilizer stability of the amino sour water dissolubility of liquid state fertilizer prepared by the present invention improves, and the shelf-life extends 1-2 month.
Claims (5)
1. an amino acid bio organic water-soluble fertilizer, is characterized in that, is prepared from by following weight portion raw material: monosodium glutamate waste liquid 30-40 part, triethanolamine 5-8 part, bean dregs 25-30 part, urea 20-30 part, potassium dihydrogen phosphate 36-38 part, Chinese medicine slag 18-23 part, chicken manure 10-15 part, Nonidet P40 8-10 part, trace mineral supplement 5-8 part, Aureobasidium pullulans 1-3 part, bacillus licheniformis 2-4 part, streptomyces microflavus 2-3 part, Paecilomyces lilacinus 2-3 part.
2. amino acid bio organic water-soluble fertilizer according to claim 1, is characterized in that, described trace mineral supplement is made up of according to mass ratio 1:0.6:0.8:1 zinc sulfate, manganese sulfate, EDTA-copper, ammonium molybdate.
3. amino acid bio organic water-soluble fertilizer according to claim 1, is characterized in that, the water content of described bean dregs is 65%.
4. a preparation method for the amino acid bio organic water-soluble fertilizer as described in claim 1-3 any one, is characterized in that, comprises the following steps:
(1) will in bean dregs, add Aureobasidium pullulans, triethanolamine, after stirring, logical aerobe fermentation 1d, obtains fermenting bean dregs liquid;
(2) urea of 1/3 weight portion will be added in Chinese medicine slag, after stirring, paving is spilt to the leaf of firm after-flame and is built heap, sprinkles chicken manure above Chinese medicine slag, adds water, carry out turning for the first time after 8d building heap, then interval 4d, 3d, the each turning of 2d is once, obtain Chinese medicine slag humus, then add water according to mass ratio 1:1, stir and soak after 12h, filter to obtain humus filtrate;
(3) in gourmet powder waste water, add calcium hydroxide and zeolite, after being warming up to 85 DEG C, stir 30min, then be cooled to 30 DEG C, add above-mentioned fermenting bean dregs liquid, after stirring, leave standstill 1d, filter, extruding filter residue, merges twice liquid, then adds humus filtrate, residue 2/3 weight portion urea, Nonidet P40, trace mineral supplement, potassium dihydrogen phosphate, bacillus licheniformis, streptomyces microflavus, Paecilomyces lilacinus, after stirring.
5. preparation method according to claim 4, is characterized in that, in step (3), adds calcium hydroxide and the 30g zeolite of 20g in described every 1kg gourmet powder waste water.
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106187387A (en) * | 2016-07-21 | 2016-12-07 | 何颖 | A kind of preparation method of kafir lily culture fluid |
| CN109220543A (en) * | 2018-09-08 | 2019-01-18 | 佛山市森昂生物科技有限公司 | A method of lentinus edodes strain stick is prepared using Amino Acid Fermentation Wastewater |
| CN113493355A (en) * | 2020-04-07 | 2021-10-12 | 钦州市凤源泉生物科技有限公司 | Preparation method of organic compound fertilizer capable of increasing content of calcium and magnesium elements |
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| CN106187387A (en) * | 2016-07-21 | 2016-12-07 | 何颖 | A kind of preparation method of kafir lily culture fluid |
| CN109220543A (en) * | 2018-09-08 | 2019-01-18 | 佛山市森昂生物科技有限公司 | A method of lentinus edodes strain stick is prepared using Amino Acid Fermentation Wastewater |
| CN113493355A (en) * | 2020-04-07 | 2021-10-12 | 钦州市凤源泉生物科技有限公司 | Preparation method of organic compound fertilizer capable of increasing content of calcium and magnesium elements |
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Application publication date: 20160518 |