CN102260116A - Plant nutrient containing oligosaccharide and organic silicon - Google Patents
Plant nutrient containing oligosaccharide and organic silicon Download PDFInfo
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- CN102260116A CN102260116A CN2011101295656A CN201110129565A CN102260116A CN 102260116 A CN102260116 A CN 102260116A CN 2011101295656 A CN2011101295656 A CN 2011101295656A CN 201110129565 A CN201110129565 A CN 201110129565A CN 102260116 A CN102260116 A CN 102260116A
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- 235000015097 nutrients Nutrition 0.000 title claims abstract description 66
- 239000010703 silicon Substances 0.000 title abstract description 31
- 229910052710 silicon Inorganic materials 0.000 title abstract description 31
- 229920001542 oligosaccharide Polymers 0.000 title abstract description 5
- 150000002482 oligosaccharides Chemical class 0.000 title abstract description 5
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 58
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 33
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 29
- 241000196324 Embryophyta Species 0.000 claims abstract description 27
- 240000007594 Oryza sativa Species 0.000 claims abstract description 23
- 235000007164 Oryza sativa Nutrition 0.000 claims abstract description 22
- 235000009566 rice Nutrition 0.000 claims abstract description 22
- 239000010903 husk Substances 0.000 claims abstract description 17
- 239000005648 plant growth regulator Substances 0.000 claims abstract description 13
- 239000000203 mixture Substances 0.000 claims abstract description 11
- 239000002131 composite material Substances 0.000 claims abstract description 10
- FGIUAXJPYTZDNR-UHFFFAOYSA-N potassium nitrate Chemical compound [K+].[O-][N+]([O-])=O FGIUAXJPYTZDNR-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000004021 humic acid Substances 0.000 claims abstract description 9
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000004202 carbamide Substances 0.000 claims abstract description 8
- 241000193417 Brevibacillus laterosporus Species 0.000 claims abstract description 7
- ZPWVASYFFYYZEW-UHFFFAOYSA-L dipotassium hydrogen phosphate Chemical compound [K+].[K+].OP([O-])([O-])=O ZPWVASYFFYYZEW-UHFFFAOYSA-L 0.000 claims abstract description 7
- 238000000605 extraction Methods 0.000 claims abstract description 7
- 239000004323 potassium nitrate Substances 0.000 claims abstract description 5
- 235000010333 potassium nitrate Nutrition 0.000 claims abstract description 5
- 239000011573 trace mineral Substances 0.000 claims abstract description 5
- 235000013619 trace mineral Nutrition 0.000 claims abstract description 5
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims abstract description 3
- 238000001914 filtration Methods 0.000 claims abstract description 3
- 150000001875 compounds Chemical class 0.000 claims description 16
- 238000000855 fermentation Methods 0.000 claims description 12
- 230000004151 fermentation Effects 0.000 claims description 12
- 229910052700 potassium Inorganic materials 0.000 claims description 12
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 10
- 239000011591 potassium Substances 0.000 claims description 10
- 235000016709 nutrition Nutrition 0.000 claims description 9
- 230000035764 nutrition Effects 0.000 claims description 9
- 244000068988 Glycine max Species 0.000 claims description 7
- 235000010469 Glycine max Nutrition 0.000 claims description 7
- 239000002068 microbial inoculum Substances 0.000 claims description 7
- 125000001181 organosilyl group Chemical group [SiH3]* 0.000 claims description 7
- 229910019142 PO4 Inorganic materials 0.000 claims description 6
- 239000010452 phosphate Substances 0.000 claims description 6
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 6
- HEBKCHPVOIAQTA-NGQZWQHPSA-N d-xylitol Chemical compound OC[C@H](O)C(O)[C@H](O)CO HEBKCHPVOIAQTA-NGQZWQHPSA-N 0.000 claims description 5
- DLRVVLDZNNYCBX-RTPHMHGBSA-N isomaltose Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1OC[C@@H]1[C@@H](O)[C@H](O)[C@@H](O)C(O)O1 DLRVVLDZNNYCBX-RTPHMHGBSA-N 0.000 claims description 4
- AXKBOWBNOCUNJL-UHFFFAOYSA-M sodium;2-nitrophenolate Chemical compound [Na+].[O-]C1=CC=CC=C1[N+]([O-])=O AXKBOWBNOCUNJL-UHFFFAOYSA-M 0.000 claims description 4
- 235000000346 sugar Nutrition 0.000 claims description 4
- 241000233866 Fungi Species 0.000 claims description 2
- 239000002893 slag Substances 0.000 claims description 2
- 150000008163 sugars Chemical class 0.000 claims description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 abstract description 30
- 239000000284 extract Substances 0.000 abstract description 4
- 230000000813 microbial effect Effects 0.000 abstract description 4
- QJZYHAIUNVAGQP-UHFFFAOYSA-N 3-nitrobicyclo[2.2.1]hept-5-ene-2,3-dicarboxylic acid Chemical compound C1C2C=CC1C(C(=O)O)C2(C(O)=O)[N+]([O-])=O QJZYHAIUNVAGQP-UHFFFAOYSA-N 0.000 abstract 1
- 244000063299 Bacillus subtilis Species 0.000 abstract 1
- 235000014469 Bacillus subtilis Nutrition 0.000 abstract 1
- 229910000402 monopotassium phosphate Inorganic materials 0.000 abstract 1
- 235000019796 monopotassium phosphate Nutrition 0.000 abstract 1
- PJNZPQUBCPKICU-UHFFFAOYSA-N phosphoric acid;potassium Chemical compound [K].OP(O)(O)=O PJNZPQUBCPKICU-UHFFFAOYSA-N 0.000 abstract 1
- 239000003337 fertilizer Substances 0.000 description 51
- 239000000243 solution Substances 0.000 description 25
- 239000007921 spray Substances 0.000 description 24
- 239000007788 liquid Substances 0.000 description 23
- 240000008067 Cucumis sativus Species 0.000 description 19
- 235000010799 Cucumis sativus var sativus Nutrition 0.000 description 19
- 238000012360 testing method Methods 0.000 description 19
- 235000011430 Malus pumila Nutrition 0.000 description 17
- 235000015103 Malus silvestris Nutrition 0.000 description 17
- 244000070406 Malus silvestris Species 0.000 description 16
- 235000013399 edible fruits Nutrition 0.000 description 13
- 238000012545 processing Methods 0.000 description 12
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 10
- 230000000694 effects Effects 0.000 description 10
- 238000004519 manufacturing process Methods 0.000 description 10
- 239000002689 soil Substances 0.000 description 10
- 238000000034 method Methods 0.000 description 9
- 238000004458 analytical method Methods 0.000 description 7
- 239000000463 material Substances 0.000 description 7
- 239000000047 product Substances 0.000 description 7
- 241000219112 Cucumis Species 0.000 description 6
- 235000015510 Cucumis melo subsp melo Nutrition 0.000 description 6
- FJJCIZWZNKZHII-UHFFFAOYSA-N [4,6-bis(cyanoamino)-1,3,5-triazin-2-yl]cyanamide Chemical compound N#CNC1=NC(NC#N)=NC(NC#N)=N1 FJJCIZWZNKZHII-UHFFFAOYSA-N 0.000 description 6
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 6
- 201000010099 disease Diseases 0.000 description 6
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 6
- 230000000050 nutritive effect Effects 0.000 description 6
- 238000002360 preparation method Methods 0.000 description 6
- 230000000638 stimulation Effects 0.000 description 6
- 230000004720 fertilization Effects 0.000 description 5
- 239000000377 silicon dioxide Substances 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 230000035558 fertility Effects 0.000 description 4
- 230000012010 growth Effects 0.000 description 4
- 229910052698 phosphorus Inorganic materials 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- JVXHQHGWBAHSSF-UHFFFAOYSA-L 2-[2-[bis(carboxylatomethyl)amino]ethyl-(carboxylatomethyl)amino]acetate;hydron;iron(2+) Chemical compound [H+].[H+].[Fe+2].[O-]C(=O)CN(CC([O-])=O)CCN(CC([O-])=O)CC([O-])=O JVXHQHGWBAHSSF-UHFFFAOYSA-L 0.000 description 3
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 3
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 3
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 3
- 238000011161 development Methods 0.000 description 3
- 210000003608 fece Anatomy 0.000 description 3
- 239000000706 filtrate Substances 0.000 description 3
- 239000010871 livestock manure Substances 0.000 description 3
- 238000007726 management method Methods 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 239000000618 nitrogen fertilizer Substances 0.000 description 3
- 239000011574 phosphorus Substances 0.000 description 3
- 229960001866 silicon dioxide Drugs 0.000 description 3
- 235000012239 silicon dioxide Nutrition 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- 239000011701 zinc Substances 0.000 description 3
- 229910052725 zinc Inorganic materials 0.000 description 3
- 235000017060 Arachis glabrata Nutrition 0.000 description 2
- 244000105624 Arachis hypogaea Species 0.000 description 2
- 235000010777 Arachis hypogaea Nutrition 0.000 description 2
- 235000018262 Arachis monticola Nutrition 0.000 description 2
- AYRXSINWFIIFAE-SCLMCMATSA-N Isomaltose Natural products OC[C@H]1O[C@H](OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O)[C@@H](O)[C@@H](O)[C@@H]1O AYRXSINWFIIFAE-SCLMCMATSA-N 0.000 description 2
- 244000046052 Phaseolus vulgaris Species 0.000 description 2
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 2
- 241000607479 Yersinia pestis Species 0.000 description 2
- 239000003513 alkali Substances 0.000 description 2
- 150000001413 amino acids Chemical class 0.000 description 2
- -1 and contain oligose Substances 0.000 description 2
- 229910021538 borax Inorganic materials 0.000 description 2
- ZCCIPPOKBCJFDN-UHFFFAOYSA-N calcium nitrate Chemical compound [Ca+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O ZCCIPPOKBCJFDN-UHFFFAOYSA-N 0.000 description 2
- 238000006243 chemical reaction Methods 0.000 description 2
- 239000000084 colloidal system Substances 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 230000018109 developmental process Effects 0.000 description 2
- UQGFMSUEHSUPRD-UHFFFAOYSA-N disodium;3,7-dioxido-2,4,6,8,9-pentaoxa-1,3,5,7-tetraborabicyclo[3.3.1]nonane Chemical compound [Na+].[Na+].O1B([O-])OB2OB([O-])OB1O2 UQGFMSUEHSUPRD-UHFFFAOYSA-N 0.000 description 2
- 230000008030 elimination Effects 0.000 description 2
- 238000003379 elimination reaction Methods 0.000 description 2
- 244000037666 field crops Species 0.000 description 2
- 239000004615 ingredient Substances 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 235000021374 legumes Nutrition 0.000 description 2
- 231100000957 no side effect Toxicity 0.000 description 2
- 235000020232 peanut Nutrition 0.000 description 2
- 230000029553 photosynthesis Effects 0.000 description 2
- 238000010672 photosynthesis Methods 0.000 description 2
- 230000008635 plant growth Effects 0.000 description 2
- 230000001863 plant nutrition Effects 0.000 description 2
- 230000002265 prevention Effects 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 239000004328 sodium tetraborate Substances 0.000 description 2
- 235000010339 sodium tetraborate Nutrition 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- PRPINYUDVPFIRX-UHFFFAOYSA-N 1-naphthaleneacetic acid Chemical compound C1=CC=C2C(CC(=O)O)=CC=CC2=C1 PRPINYUDVPFIRX-UHFFFAOYSA-N 0.000 description 1
- 240000007087 Apium graveolens Species 0.000 description 1
- 235000015849 Apium graveolens Dulce Group Nutrition 0.000 description 1
- 235000010591 Appio Nutrition 0.000 description 1
- 241001530056 Athelia rolfsii Species 0.000 description 1
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 240000001980 Cucurbita pepo Species 0.000 description 1
- 235000009852 Cucurbita pepo Nutrition 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 1
- 244000141359 Malus pumila Species 0.000 description 1
- 108090000913 Nitrate Reductases Proteins 0.000 description 1
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 1
- 241000918585 Pythium aphanidermatum Species 0.000 description 1
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 description 1
- FKNQFGJONOIPTF-UHFFFAOYSA-N Sodium cation Chemical compound [Na+] FKNQFGJONOIPTF-UHFFFAOYSA-N 0.000 description 1
- 235000021307 Triticum Nutrition 0.000 description 1
- 244000098338 Triticum aestivum Species 0.000 description 1
- 235000010724 Wisteria floribunda Nutrition 0.000 description 1
- 240000008042 Zea mays Species 0.000 description 1
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 description 1
- 235000002017 Zea mays subsp mays Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 description 1
- 235000018660 ammonium molybdate Nutrition 0.000 description 1
- 239000011609 ammonium molybdate Substances 0.000 description 1
- 229940010552 ammonium molybdate Drugs 0.000 description 1
- 238000000540 analysis of variance Methods 0.000 description 1
- 235000021053 average weight gain Nutrition 0.000 description 1
- 230000001580 bacterial effect Effects 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000033558 biomineral tissue development Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 239000011575 calcium Substances 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 235000013339 cereals Nutrition 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 229930002875 chlorophyll Natural products 0.000 description 1
- 235000019804 chlorophyll Nutrition 0.000 description 1
- ATNHDLDRLWWWCB-AENOIHSZSA-M chlorophyll a Chemical compound C1([C@@H](C(=O)OC)C(=O)C2=C3C)=C2N2C3=CC(C(CC)=C3C)=[N+]4C3=CC3=C(C=C)C(C)=C5N3[Mg-2]42[N+]2=C1[C@@H](CCC(=O)OC\C=C(/C)CCC[C@H](C)CCC[C@H](C)CCCC(C)C)[C@H](C)C2=C5 ATNHDLDRLWWWCB-AENOIHSZSA-M 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 235000005822 corn Nutrition 0.000 description 1
- 230000007850 degeneration Effects 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 230000008034 disappearance Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000019634 flavors Nutrition 0.000 description 1
- 230000034659 glycolysis Effects 0.000 description 1
- 235000021384 green leafy vegetables Nutrition 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 239000002932 luster Substances 0.000 description 1
- 239000011777 magnesium Substances 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 150000007523 nucleic acids Chemical class 0.000 description 1
- 102000039446 nucleic acids Human genes 0.000 description 1
- 108020004707 nucleic acids Proteins 0.000 description 1
- 239000002420 orchard Substances 0.000 description 1
- 239000002686 phosphate fertilizer Substances 0.000 description 1
- 229940072033 potash Drugs 0.000 description 1
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 description 1
- 235000015320 potassium carbonate Nutrition 0.000 description 1
- 229910052939 potassium sulfate Inorganic materials 0.000 description 1
- 235000011151 potassium sulphates Nutrition 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 235000021251 pulses Nutrition 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000021749 root development Effects 0.000 description 1
- 230000002786 root growth Effects 0.000 description 1
- 229910001415 sodium ion Inorganic materials 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
- 238000003971 tillage Methods 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
Landscapes
- Fertilizers (AREA)
Abstract
The invention relates to a plant nutrient containing oligosaccharide and organic silicon. The plant nutrient contains the following components based on the weight of the plant nutrient: 0.1-4% of oligosaccharide, 1-10% of humic acid, 0-50% of urea, 0-15% of potassium nitrate, 0-15% of potassium dihydrogen phosphate, 0-30% of dipotassium hydrogen phosphate, 0.1-5% of trace elements, 0.1-5% of plant growth regulator, 10-80% of organic silicon extract and the balance of water, wherein the organic silicon extract is prepared by the following steps: mixing 50-75% of rice husk, 0.5-1.5% of microbial agent and the balance of water based on the weight of the mixture, fermenting the mixture for 72 hours, then adding 20% (W/W) NaOH solution to extract at 95 DEG C for 6 hours, and filtering to remove residues after extraction so as to obtain the organic silicon extract, wherein the mass ratio of the fermented mixture to the NaOH solution is 4.0:1; and the microbial agent is a composite microbial agent of Bacillus subtilis, Bacillus laterosporus, and yeast in a weight ratio of (50-80):(0-50):(0-35).
Description
Technical field
The present invention relates to a kind of crop foliage fertilizer, be specifically related to a kind of organosilyl plant nutrient agent of oligose that contains.
Background technology
Rice husk is one of main byproduct of cereal processing, accounts for 20% of paddy quality, is big, wide, the inexpensive renewable resources of a kind of amount.There is at least 3.6 hundred million tons on rice husk every year in China.Rice husk contains multiple element.Main component is SiO in the rice hull ash
2, it mainly is to exist with biomineralization form, metamict.Rice husk basal component after charing is carbon and silicon-dioxide, does not contain heavy metal, and this provides condition for producing agricultural Chemicals and application.Yet current people are to the not enough science of the utilization of rice husk, reasonable, and the beneficiating ingredient in the rice husk can not be fully used, and has caused waste.Occurring in nature, plant absorb some nutrient in the soil again and again, just cause the disappearance of these nutrients; Particularly silicon, calcium, fertiliser containing magnesium never have artificially and replenished, and have so just influenced the development growth of plant, and further high yield.Show that by clay fertilizer institute of the Chinese Academy of Agricultural Sciences test-results siliceous fertilizer is one of necessary nutritive element in paddy rice, legume crop, the growth and development of fruit tree.Executed fruit tree, beans, peanut, paddy rice of siliceous fertilizer or the like, cane is sturdy, and growing way is evenly healthy, and blade is big and compact, straight and upright, plump, color and luster is dark green, chlorophyll content increases greatly, and helps cold-resistantly, resists extraneous germ dip-dye.Siliceous fertilizer has " three anti-three short " effect to the high and stable yields of crop, worm promptly resistant to lodging, disease-resistant, anti-ly does early, promotes to promote root growth and development by photosynthesis, promotes effective utilization of nutrient.Amino acid, humic acids siliceous fertilizer have good synergistic effects, have better effect of increasing production than single nutrient, also can improve crop quality.But because the element silicon chemical property determines that its most compounds are insoluble, so siliceous fertilizer is difficult to be absorbed by crop veritably and utilize.China's ZL98121697.8 patent of invention " a kind of silicon foliage fertilizer and preparation method thereof that contains " is to utilize colloid silica to improve the utilization ratio of crop to siliceous fertilizer.Colloid silica belongs to inorganic silicon, though contain solvend, crop absorption and utilization ratio are still very low, and fertilizer efficiency period is short." seed amino acid, humic acids siliceous fertilizer and the production method thereof " of China CN1467 183A patent application document is as hydrolytic reagent with liquid soluble glass, with discarded albumen is raw material, but the cost of material height, and protein is handled not thorough, it is too much to contain sodium ion, and the nutritive ingredient loss is serious.
Summary of the invention
The present invention will solve and lack the high-efficiency plant nutrition agent at present, and can not make full use of the problem that rice husk is produced the high-efficiency plant nutrition agent, a kind of organosilyl plant nutrient agent of oligose that contains of the present invention is provided for this reason, this nutrition agent is easy to be absorbed by crop, and utilization ratio height, fertilizer efficiency period is long, has no side effect.
For addressing the above problem, its special character of the technical solution used in the present invention is to be that benchmark contains: oligose 0.1～4% with described nutrition agent weight, humic acids 1～10%, urea 0～50%, saltpetre 0～15%, potassium primary phosphate 0～15%, dipotassium hydrogen phosphate 0～30%, trace element accounts for 0.1～5%, plant-growth regulator 0.1～5%, organosilicon extracting solution 10～80%, surplus are water;
Described organosilicon extracting solution is made by following steps: rice husk, microbiobacterial agent, water are mixed into rice husk/microbial inoculum/water mixture, are benchmark with described compound weight, rice husk 50～75%, and microbial inoculum 0.5～1.5%, surplus is a water; Described compound fermentation became fermentation back compound in 72 hours, described fermentation back compound adds the lixiviate of 20% (W/W) NaOH solution, the mass ratio of described fermentation back compound and NaOH solution is 3.5: 1,90 ℃ of extraction temperatures, extraction time 5 hours, the lixiviate after-filtration removes slag (should adopt centrifuging), gets tan organosilicon extracting solution;
Described microbial inoculum is subtilis, bacillus laterosporus and saccharomycetic composite fungus agent, and three's weight ratio is subtilis/bacillus laterosporus/yeast=(50～80)/(0～50)/(0～35).
Described oligose is the composition of two or more (containing two kinds) in xylo-oligosaccharide, oligomeric soya sugars, the poly-isomaltose.
Described plant-growth regulator is the composition of two or more in sodium nitrophenolate, α-Nai Yisuanna, the rape element (containing two kinds).
Described microbiobacterial agent is the composition that (contains two kinds) more than two kinds in subtilis, bacillus laterosporus, the cereuisiae fermentum.
It is 8-9 that fermentation of the present invention back compound is transferred PH through the lixiviate of NaOH solution, filter and remove residue gained filtrate, is described organosilicon extracting solution; Wherein lixiviate is that alkali is excessive slightly, but adding citric acid is transferred PH.
Organosilicon extracting solution of the present invention through adopt " People's Republic of China's agricultural industry criteria. siliceous fertilizer (NY/T 797-2004) " in detection method measure, described organosilicon extracting solution contains silicon-dioxide 20-32.6%.
The most basic chemical fertilizer of plant is nitrogenous fertilizer, phosphate fertilizer and potash fertilizer.Among the present invention, urea is nitrogenous fertilizer; Saltpetre contains element N and K, is nitrogen-K composite fertilizer; Dipotassium hydrogen phosphate and potassium primary phosphate contain element P and K, are phosphorus-K composite fertilizer.
Trace element among the present invention is a trace element fertilizer, is called for short little fertilizer.
The present invention contains plant-growth regulator (Plant growth regulator).Plant-growth regulator is meant. the material with coordinate plant growth growth and other functions contained or synthetic in the plant.
The present invention is dissolved in water after oligose, humic acids, nitrogenous fertilizer, composite microbial fertilizer and plant-growth regulator are mixed in proportion, and adds the water of organosilicon extracting solution and surplus again, makes plant nutrient agent of the present invention.The invention has the advantages that:
1, rice husk is got filtrate through microbiobacterial agent glycolysis, soda boiling (alkali lye heat lixiviate), centrifuging, extracts organosilicon, and pollution-free, the nutritive substance loss is few, and cost is low, and is active high, is easy to plant absorbing, and can improves utilization rate of fertilizer, and fertilizer efficiency period is long, has no side effect.
2, the present invention is except that nitrogenous, phosphorus, potassium and little fertilizer, and contain oligose, humic acids, plant-growth regulator, so complete function, wide spectrum, has the coordination crop growth, improve sugar, protein, nucleic acid content in the plant materials, strengthen the activity of nitrate reductase, increase the accumulation of dry-matter, water balance in the control agent promotes effects such as crop precocity, degeneration-resistant, volume increase.
3, contain the present invention who carries effective substance, siliceous fertilizer and synergistic matter compatibility can improve plant cold resistance and stalk performance resistant to lodging, and be balanced in nutrition, and various nutritive elements can really be absorbed by crop, reaches the quick-acting and long-acting characteristics of taking into account, and amount of increase in production is big.
Embodiment
One, the preparation of organosilicon extracting solution
With rice husk, microbiobacterial agent, water mixes, with compound weight is benchmark, rice husk 65%, microbial inoculum 1.0%, water 34% compound fermentation 72 hours, fermentation back compound adds the lixiviate of 20% (W/W) NaOH solution, the mass ratio of fermentation back compound and NaOH solution is 4.0: 1,95 ℃ of extraction temperatures, extraction time 6 hours, centrifuging waste after the lixiviate, it is 8.2 that the filtrate adding citric acid is transferred PH, the organosilicon extracting solution, adopt " People's Republic of China's agricultural industry criteria. siliceous fertilizer (NY/T 797-2004) " in detection method measure, described organosilicon extracting solution contains silicon-dioxide 32.6%.
Subordinate list one: organosilicon extracting solution preparation method embodiment
Two, preparation Gramineae rice seedling water-soluble fertilizer-a kind of plant nutrient agent of the present invention
With xylo-oligosaccharide 0.4kg, soybean oligosaccharide 0.2kg, potassium humate 8kg, sodium nitrophenolate 0.8kg, Nafusaku 0.3kg, urea 30kg, potassium primary phosphate 4.5kg, dipotassium hydrogen phosphate 5kg, four water, eight Sodium Tetraborate 1kg, EDTA zinc 0.5kg, EDTA iron 0.5kg, the organosilicon extracting solution 40kg of step 1, water 8.8kg be mixed and made into 100kg product of the present invention;
Thin up is 400～600 times during use.
The plant nutrient agent of present embodiment is applicable to gramineous crop.This plant nutrient agent contains wheat, paddy rice, the needed various nutritive elements of corn growth and abundant organosilicon, can improve resistant to lodging, the resistant to diseases and insects of crop.This nutrition agent can excite the activity of enzyme, accelerate growing process, accelerate chlorophyllous synthetic and conversion, make crop tiller many, take root soon, can strengthen resistance, effectively suppress the generation of diseases such as bacterial wilt, damping-off, banded sclerotial blight and rice blast, some physiological diseases such as low temperature freezing-disaster there are rapid alleviation and restitution, can promote precocious 3-5 days, about volume increase 12-18%, 100-grain weight can increase the 0.3-0.8 gram.
Three, preparation soybean (pulse family) water-soluble fertilizer-another plant nutrient agent of the present invention
To gather isomaltose 1.5kg, xylo-oligosaccharide 0.5kg, humic acids 10kg, the plain 0.1kg of plant-growth regulator rape, α-Nai Yisuanna 0.4kg, urea 20kg, potassium primary phosphate 5kg, dipotassium hydrogen phosphate 10kg, four water, eight Sodium Tetraborate 3kg, EDTA zinc 0.5kg, EDTA iron 1kg, ammonium molybdate 0.2kg, the organosilicon extracting solution 30kg of step 1, water 17.8kg be mixed and made into 100kg product of the present invention.
Thin up is 600～800 times during use.
This nutrition agent is applicable to leguminous crop.This nutrition agent contains the organosilicon that leguminous crop (peanut, soybean, legume vegetable) grows needed various nutritive element and enriches, can increase chlorophyllous synthetic and conversion, strengthen photosynthesis, it is green that beans leaflet, leaf roll, Huang Yeke are alleviated commentaries on classics rapidly, and blade is unfolded, suppress the generation of root rot, the anti continuous and alternative-year effect is remarkable; Can improve soybean and protect flower guarantor pod rate, precocious 3-5 days, volume increase about 10%, 100-grain weight can increase by 2.5 grams.
Four, preparation melon dish water-soluble fertilizer-another plant nutrient agent
To gather isomaltose 0.6kg, soybean oligosaccharide 1kg, xylo-oligosaccharide 0.4kg, plant-growth regulator sodium nitrophenolate 0.6kg, the plain 0.05kg of rape, humic acids 8kg, urea 25kg, saltpetre 7kg, potassium primary phosphate 5kg, dipotassium hydrogen phosphate 5kg, nitrocalcite 3kg, boric acid 1kg, EDTA zinc 0.8kg, EDTA iron 0.5kg, silicon extracting solution 30kg, water 12.5kg is mixed and made into, and dilution is 500～700 times during use.
This nutrition agent is applicable to melon dish, fruit tree.This nutrition agent can make the leaf vegetables blade increase rapidly, and bulb bag hearty cord is real.Melon and solanberry class is bloomed expand morning, percentage of fertile fruit height, fruit fast, painted morning even, local flavor is good, VITAMIN, sugar content height, increases production 15-35%; Can make fruit tree promote bud differentiation, reduce biennial bearing, prevent the Spring frost in early spring, percentage of fertile fruit height, ripen in advance 5-10 days, volume increase 15-30%.
Subordinate list 2: the plant nutrient agent embodiment that only indicates oligose and plant-growth regulator weight percentage
Field test results of the present invention below is described.
One one kinds of plant nutrient agents that contain the oligose liquid silicon of field test results
Manure trial report on cucumber
According to Ministry of Agriculture's " fertilizer management method of registration ", " fertilizer data registration request " and agricultural industry criteria " fertilizer effect is identified the field plot technique rules " (NY/497-2002), be the effect of checking " containing a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " on cucumber produces, special this test of arrangement.
1 materials and methods
1.1 material
Tested in the 5-6 month in 2007 being arranged in the contracted field of Zhuji City Xi Yan township Qian Jiazhuan Qian Hong army, quality is middle earth, and soil fertility is better-than-average, and soil fertility is even.This field piece topsoil soils nutrient is: organic content 12.87g/kg, alkali-hydrolyzable nitrogen content 86.7mg/kg, rapid available phosphorus (P
2O
5) 18.3mg/kg, available potassium (K
2O) 135mg/kg, preceding crop celery, yield level 3800kg.For studying the thing cucumber, kind is Tianjin spring No. four.For examination fertilizer be " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " (name at that time, plant nutrient agent promptly of the present invention, down with) insult the production of agricultural science and technology company limited, provide by the sky, Zhejiang.
1.2 method
Three processing are established in test altogether, adopt district's group arrangement at random, triplicate, sub-district area 25m
2
Handle 1: conventional fertilizer application+every mu of each this fertilizer 50ml that uses converts clear water 30kg, in cucumber seedling stage, initial bloom stage, each spray of fruiting period once, sprays altogether 3 times.
Handle 2: conventional fertilizer application+spray is with handling dosage clear water such as 1 same period.
Handle 3: conventional fertilizer application.
Experimental field grow seedlings field planting on April 21 on March 20th, 2007.Every mu of bottom application fertilizer 5000kg before the whole ground, composite fertilizer 60kg (15-15-15).Topdress 2 times, every mu imposes compound potassium sulfate fertilizer 30kg (15-15-15) at every turn, urea 15kg, and whole growing is watered 4 times, prevention and elimination of disease and pests 8 times, test is respectively on May 24th, 2007, June 11, June 28 spraying solution or clear water 3 times.Experimental field cucumber is gathered and plucks single product respectively that claims in the sub-district for the unit list, adds up to output at last.Test is except that by the spraying solution or the clear water of fertilising scheme requirement, and other control measures are with general land for growing field crops.
2 results and analysis
2.1 spray " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " becomes the product factor to cucumber influence
Spray " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " and improved cucumber one-tenth product factor.As known from Table 1: individual plant knot melon number is inconsistent.Handle 1 and how handled 2 average individual plant knot melon numbers 0.5, handle the long average 1.8cm of increasing of 2 average single sugar-preserved gourd, the heavy 13.8g that on average increases of single melon handles 3 average weight gain 17.7g.This has illustrated and has sprayed the single fruit weight that " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " increased cucumber, for the high yield of cucumber has been laid certain basis.
Table 3 cucumber field investigation record information slip
(annotate: data are three multiple mean numbers in the table)
2.2 spray " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " influence to cucumber yield
Spray " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " and can significantly increase cucumber yield.As shown in Table 2, handle 1 and handle 2 average every mu of increase 581.2kg, stimulation ratio is 13.6%, and processing 1 is compared with processing 3 and increased production 611.4kg, and stimulation ratio is 14.4%.In order to verify whether there is significant difference between processing, cucumber is respectively handled yield result carry out variance analysis (seeing Table 3), reached utmost point conspicuous level between processing.Adopt the PLSD method to carry out multiple comparisons (seeing Table 4), handle as can be seen 1 with handle 2 and handle 3 volume variances and all reach conspicuous level.This shows, spray the output that " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " can increase cucumber.
Table 4 is respectively handled the cucumber yield cartogram
Table 5 variance analysis
Table 6 multiple comparisons
3 brief summaries
3.1 the test in a season shows, on the basis of conventional fertilizer application, begin spray " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " every mu seedling stage from cucumber and convert clear water 30kg with this fertilizer 50ml at every turn, in seedling stage, initial bloom stage and fruiting period, spray altogether 3 times, the one-tenth that can improve cucumber produces factor, increases cucumber yield.Spray this liquid fertilizer and compare average mu volume increase cucumber 581.2kg with the spray clear water, stimulation ratio is 13.6%, reaches utmost point conspicuous level through variance analysis check volume variance.
3.2 this test-results is only to being responsible for for examination fertilizer.
The test unit of finishing: agricultural science and technology company limited is insulted in the sky, Zhejiang
Test transactor: Zhou Jingjie
Reported date: 2010-08-07
Field test results two
" a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " manure trial report on apple
According to Ministry of Agriculture's " fertilizer management method of registration ", " the fertilizer data registration request is " with " fertilizer effect identify field plot technique rules " requirement (NY/497-2002), be checking " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " effect on Henan Province's apple production, special this test of arrangement.
1 materials and methods
1.1 material
Test arrangement is at Henan Province's Shangqiu City
XiayiThe county
Hu QiaoThe township
Hu QiaoThe village
Lee Generation armyThe orchard in.Great soil group is a moisture soil, and soil fertility is medium, and soil fertility is even.This field piece topsoil soils nutrient is organic content 11.2g/kg, cracks nitrogen 80mg/kg, rapid available phosphorus 16.4mg/kg, available potassium 120mg/kg.For studying the thing apple, kind is " Fuji apple ", the age of tree 13 years, and the tree vigo(u)r neat and consistent, level of management are higher.Insulting agricultural science and technology company limited for examination fertilizer " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " by the sky, Zhejiang produces, provides.
1.2 method
3 processing are established in this test altogether, and district's group is arranged at random, repeats 5 trees in every sub-district 3 times.
Handle 1: habits fertilization+convert water 30kg with this fertilizer 80g, respectively spray once at apple young fruit period and expanding stage respectively;
Handle 2: habits fertilization+spray the equivalent clear water 1 same period with processing;
Handle 3: habits fertilization.
Test is carried out on the basis of local habits fertilization, and concrete fertilising is every mu of bottom application farm manure 6000kg; Growing period topdresses 3 times, for the first time every mu impose composite fertilizer 80kg, for the second time every mu impose composite fertilizer 100kg, for the third time every mu impose composite fertilizer 100kg.5～August is sprayed the medicine prevention and elimination of disease and pests 6 times in the test garden, intertill and clean tillage 3 times, and pour water once early stage.Experimental field apple sprays solution or clear water respectively on June 13rd, 2009, July 10 carrying out 2 times.Receive single product respectively that claims in the sub-district for the unit list during results.Test is except that by the spraying solution or the clear water of fertilising scheme requirement, and other control measures are with general land for growing field crops.
2 test results and analysis
2.1 spray " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " becomes the product factor to apple influence
Spray " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " and improved the factor that apple becomes to produce.As can be seen from Table 1: the single fruit weight in average that sprays " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " is handled the 2 average 7.5g of increasing; Handle the 3 average 7.6g of increasing; Illustrate to spray the single fruit weight that " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " increased apple, laid good basis for apple production improves.
Table 1 apple field investigation record information slip
(annotate: data are three multiple mean numbers in the table)
2.2 spray " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " influence to apple production
Spray " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " and improved apple production.As can be seen from Table 2: handle 1 and handle 2 average every mu of volume increase 434.4kg, stimulation ratio is 13.8%; Compare every mu of volume increase 475.0kg with processing 3, stimulation ratio is 15.2%.Each is handled yield result carry out variance analysis (seeing Table 3), volume variance reaches conspicuous level.Adopt the PLSD method to carry out multiple comparisons (seeing Table 4), processing 1 reaches conspicuous level with processing 2, processing 3 volume variances.This shows, on the basis of habits fertilization, on apple, spray " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " and can improve output.
Table 2 is respectively handled apple test output statistics table
Table 3 analysis of variance table
Table 4 multiple comparisons table
3 brief summaries
3.1 show by experiment, on the basis of locality fertilising, respectively spray once " a kind of oligose liquid silicon organic nutrient aganic nutrient agent that contains " 80g in apple tree young fruit period, swollen fruit phase and convert water 30kg solution, with spray the equivalent clear water same period and compare, can improve economic characters, the raising output of apple, average every mu of volume increase 434.4kg, stimulation ratio is 13.8%, the variance analysis volume variance reaches utmost point conspicuous level.
3.2 this test-results only is responsible for the fertilizer sample of supply examination.
Test carrier: Henan Province's soil and fertilizer station
Test base unit: agrotechnical center, Xiayi County, Henan Province
Test transactor: Zhou Hongmei
Reported date: on October 30th, 2009
Claims (4)
1. one kind contains the organosilyl plant nutrient agent of oligose, it is characterized in that with described nutrition agent weight being that benchmark contains: oligose 0.1～4%, humic acids 1～10%, urea 0～50%, saltpetre 0～15%, potassium primary phosphate 0～15%, dipotassium hydrogen phosphate 0～30%, trace element accounts for 0.1～5%, plant-growth regulator 0.1～5%, organosilicon extracting solution 10～80%, surplus are water;
Described organosilicon extracting solution is made by following steps: rice husk, microbiobacterial agent, water are mixed into rice husk/microbial inoculum/water mixture, are benchmark with described compound weight, rice husk 50～75%, and microbial inoculum 0.5～1.5%, surplus is a water; Described compound fermentation became fermentation back compound in 72 hours, described fermentation back compound adds the lixiviate of 20% (W/W) NaOH solution, the mass ratio of described fermentation back compound and NaOH solution is 4.0: 1,95 ℃ of extraction temperatures, extraction time 6 hours, the lixiviate after-filtration removes slag, and obtains organosilicon brown extracting solution;
Described microbial inoculum is subtilis, bacillus laterosporus and saccharomycetic composite fungus agent, and three's weight ratio is subtilis/bacillus laterosporus/yeast=(50～80)/(0～50)/(0～35).
2. a kind of organosilyl plant nutrient agent of oligose that contains as claimed in claim 1 is characterized in that described oligose is the composition of two or more (containing two kinds) in xylo-oligosaccharide, oligomeric soya sugars, the poly-isomaltose.
3. a kind of organosilyl plant nutrient agent of oligose that contains as claimed in claim 1 is characterized in that described plant-growth regulator is the composition of two or more in sodium nitrophenolate, α-Nai Yisuanna, the rape element (containing two kinds).
4. a kind of organosilyl plant nutrient agent of oligose that contains as claimed in claim 1 is characterized in that described microbiobacterial agent is the composition that (contains two kinds) more than two kinds in subtilis, bacillus laterosporus, the cereuisiae fermentum.
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| CN102924179A (en) * | 2012-11-22 | 2013-02-13 | 海南正业中农高科股份有限公司 | Application of chitosan-oligosaccharide containing composition to production of edible fungi |
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| CN105924274A (en) * | 2016-04-27 | 2016-09-07 | 庐江县天地禾生物技术有限公司 | Preparation method of Dendrobium officinale organic foliar fertilizer |
| CN107417390A (en) * | 2017-07-25 | 2017-12-01 | 特锐菲克生物科技(福建)有限公司 | A kind of edible and medical fungi activity improver and application thereof |
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