CN103704509A - Method for preparing slow release feed for carps by adopting nano materials - Google Patents
Method for preparing slow release feed for carps by adopting nano materials Download PDFInfo
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Abstract
The invention discloses a method for preparing a slow release feed for carps by adopting nano materials. A composite microorganism fish fertilizer specially used for the carps comprises the following components in parts by weight: 2-4 parts of nitrogen-fixing bacteria, 1-3 parts of phosphate solubilizing bacteria, 3-5 parts of enzyme bacteria, 50-60 parts of fish meal, 75-80 parts of bean cakes, 20-30 parts of bran, 70-80 parts of rice bran, 10-14 parts of brown sugar, 8-10 parts of yeast powder, 12-15 parts of edible salt and the like. The composite microorganism fertilizer disclosed by the invention can promote rapid growth of fish and also improve the grade and the quality of the fish, so that diseases of the fish can be reduced; meanwhile, beneficial microorganisms in water can be increased, and the growth of phycophyta in a fishpond is alleviated.
Description
Technical field
The present invention relates to a kind of microbial manure, particularly relate to a kind of complex microorganism fish guano, be specifically related to a kind of carp specific complex microbial fish guano and preparation method thereof, belong to technical field of fertilizers.
Background technology
The protein of carp not only content is high, and quality is also very high, human body digestibility can reach 96%, and contain needed by human body elements such as can supplying with human body essential amino acid, mineral matter, vitamin A and vitamin D, the food that nutritive value is very high, and way is various, very popular.
In the breeding process of carp, need to throw in feed and grow for it, but long-term input feed can grow some harmful bacterias in fishpond and fish pond, these harmful bacterias not only can affect water body environment, are also unfavorable for the growth of carp.And in the breeding process of carp, at present a lot of plants adopt fertilizer, by as throwing in a certain amount of fertilizer in pond, improve the output of carp; Traditional fertilizer has its advantage, but shortcoming function singleness is longer by the process that phytoplankton utilized, and in mineralization process, consumes a large amount of oxygen in water body, this in water to put product in a suitable place to breed as unfavorable in the growth such as fish; In addition, organic fish guano should be made base manure, and is mainly used in Winter-Spring water temperature lower season.And inorganic fertilizer function is comparatively single, although can make fish high yield, use for a long time chemical fertilizer can bring many drawbacks, contaminated environment, destroys the ecological balance.
Except the fertilizer and inorganic fertilizer of simple function, from last century the eighties also start to promote " rational application of fertilizers ", i.e. " composite organic-inorganic fertilizer ", although composite fertilizer has absorbed the advantage of single fertilizer and inorganic fertilizer two aspects, their shortcoming is not fine to be overcome.Existing single type fish guano and compound fish guano also have a common shortcoming, and that can not be killed harmful bacteria exactly, therefore, lack the effectively effect of control of fish disease.The content that can increase beneficial bacterium in fishpond by the compound fish guano of microorganism, effectively reduces the generation of fish diseases, does not also report at present about being exclusively used in the complex microorganism fish guano of carp.
Summary of the invention
The technical problem that the present invention mainly solves is to provide a kind of carp specific complex microbial fish guano and preparation method thereof, comprehensive nutrition is provided can on the one hand the growth of carp, can improve on the other hand the useful content in pond, suppress the breeding growth of pathogen in water body, reduce the generation of disease, improve the yield and quality of carp.
For solving the problems of the technologies described above, the technical scheme that the present invention adopts is:
A kind of employing nano material is prepared carp released fodder, it is characterized in that, its raw material comprises the composition of following weight ratio: nitrogen-fixing bacteria 2-4 part, phosphate solubilizing bacteria 1-3 part, ferment bacterium 3-5 part, fish meal 50-60 part, soya-bean cake 75-80 part, wheat bran 20-30 part, rice bran 70-80 part, brown sugar 10-14 part, dusty yeast 8-10 part, salt 12-15 part, chicken manure 80-85 part, pasture and water 60-65 part, calcium hydroxide 10-13 part, urea 15-20 part, potassium sulfate 3-5 part, ironic citrate 3-5 part, Cobastab
10.2-0.4 part, Cobastab
120.1-0.3 part, kongpo monkshood root 4.5-5.5 part, 4-5 parts of semen momordicaes, Chinese Stellera Root 1-1.5 part, nano controlled-release carrier 20-25 part;
The preparation method of described nano controlled-release carrier is:
(1) silicon hydroxyapatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, in 65 ℃, stir 60 hours, filter, and wash and remove excessive methyl-sulfoxide (DMSO) for 3 times with the hot ethanol of 60 ℃ of temperature, put into vacuum drying chamber, 60 ℃ of temperature, be dried 24 hours, grinding is sieved, and obtains modified composite one time;
(2) 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water are mixed, in temperature 50 C, stir more than 10 hours, in 30 ℃ of temperature, first under ultrasonic electric power 350W condition, disperse 3.5 hours, and then disperse 4 hours under ultrasonic electric power 250W condition.Filter, and wash 3 times with distillation, 80 ℃ of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed to 60min at 600W power ultrasonic, with constant temperature heating device, be heated to 90 ℃, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier complexes.
Described a kind of preparation method who adopts nano material to prepare carp released fodder, is characterized in that, comprises the following steps:
(1) pasture and water are dried, make its water content below 40%, be cut to 2-4cm, then according to described ratio, add fish meal, soya-bean cake, wheat bran, rice bran, brown sugar, dusty yeast, salt, chicken manure, fully stir, mix;
(2) said mixture is fermented, described fermentation is aerobic composting fermentation, and fermentation water accounts for the 20-30% of material gross weight, and be 50-60 hour winter oxygen supply time, and be 20-25 hour summer, and fermentation temperature is 45-60 ℃, and fermentation time is 7-10 days; The aqueous solution that adds the calcium hydroxide melt into of described ratio, to sterilize by conventional method;
(3) organic mixture after fermentation, sterilization is dried, baking temperature is 45-60 ℃, and being dried to water content is 15-25%;
(4) nitrogen-fixing bacteria, phosphate solubilizing bacteria, ferment bacterium are joined in above-mentioned material according to described ratio, fully mix, stir;
(5) by urea, potassium sulfate, ironic citrate, Cobastab
1, Cobastab
12, kongpo monkshood root, semen momordicae, Chinese Stellera Root, nano controlled-release carrier join in mixture according to described ratio, fully mixes, stir;
(6) above-mentioned material is carried out under the condition of 18-45 ℃ to low temperature drying, making its water content is below 10%.
The invention has the beneficial effects as follows:
(1) added fish and produced needed organic matter and inorganic mineral, comprehensive nutrition is provided can to the growth of fish;
(2) nitrogen-fixing bacteria, phosphate solubilizing bacteria, ferment bacterium have been added, can increase the content of N in pond, reduce the gathering of P, thereby reduce attached zoic amount reproduction, be conducive to the growth of carp, add killing the harmful bacteria in fishpond of ferment bacterium, suppress the breeding growth of pathogen in water body, reduce the generation of disease, improve the yield and quality of fish.
(3) in the present invention, added the medicinal herb componentses such as the root of large-flowered skullcap, Radix Isatidis, Radix Glycyrrhizae, can reduce the generation of carp disease, effectively prophylactic spreading.
(4) these mushrooms that add can continue breeding in water body, expand survival rate, to maintaining the balance of microorganisms in water, have a very important role, and can regulate and adjust microecological balance in fish body enteron aisle, can also decomposer in the Harmful Residue, strengthen fingerling premunition.
(5) utilize hydroxyapatite etc. itself to there is the character of loose structure, fertilizer components is adsorbed in the inner mesh of carrier, reach the object of slow release.Hydroxyapatite also has biodegradable characteristic, and gained catabolite is various trace elements ion, and these elements can be absorbed again.Nano controlled-release additive has good biocompatibility, gastrointestinal tract mucous compatibility, each component that makes it load has controlled-release function, through twice-modified nano-complex medicine carrying amount and adsorbance, all improve a lot, fertilizer efficiency time lengthening is more than 3 months, effectively suppress the increment of animal pathogen, improve the producer's benefit.
The specific embodiment
Below preferred embodiment of the present invention is described in detail, thereby so that advantages and features of the invention can be easier to be it will be appreciated by those skilled in the art that, protection scope of the present invention is made to more explicit defining.
embodiment 1
A kind of employing nano material is prepared carp released fodder, it is characterized in that, its raw material comprises the composition of following weight ratio: nitrogen-fixing bacteria 2-4 part, phosphate solubilizing bacteria 1-3 part, ferment bacterium 3-5 part, fish meal 50-60 part, soya-bean cake 75-80 part, wheat bran 20-30 part, rice bran 70-80 part, brown sugar 10-14 part, dusty yeast 8-10 part, salt 12-15 part, chicken manure 80-85 part, pasture and water 60-65 part, calcium hydroxide 10-13 part, urea 15-20 part, potassium sulfate 3-5 part, ironic citrate 3-5 part, Cobastab
10.2-0.4 part, Cobastab
120.1-0.3 part, kongpo monkshood root 4.5-5.5 part, 4-5 parts of semen momordicaes, Chinese Stellera Root 1-1.5 part, nano controlled-release carrier 20-25 part;
The preparation method of described nano controlled-release carrier is:
(1) silicon hydroxyapatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, in 65 ℃, stir 60 hours, filter, and wash and remove excessive methyl-sulfoxide (DMSO) for 3 times with the hot ethanol of 60 ℃ of temperature, put into vacuum drying chamber, 60 ℃ of temperature, be dried 24 hours, grinding is sieved, and obtains modified composite one time;
(2) 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water are mixed, in temperature 50 C, stir more than 10 hours, in 30 ℃ of temperature, first under ultrasonic electric power 350W condition, disperse 3.5 hours, and then disperse 4 hours under ultrasonic electric power 250W condition.Filter, and wash 3 times with distillation, 80 ℃ of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed to 60min at 600W power ultrasonic, with constant temperature heating device, be heated to 90 ℃, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier complexes.
Described a kind of preparation method who adopts nano material to prepare carp released fodder, is characterized in that, comprises the following steps:
(1) pasture and water are dried, make its water content below 40%, be cut to 2-4cm, then according to described ratio, add fish meal, soya-bean cake, wheat bran, rice bran, brown sugar, dusty yeast, salt, chicken manure, fully stir, mix;
(2) said mixture is fermented, described fermentation is aerobic composting fermentation, and fermentation water accounts for the 20-30% of material gross weight, and be 50-60 hour winter oxygen supply time, and be 20-25 hour summer, and fermentation temperature is 45-60 ℃, and fermentation time is 7-10 days; The aqueous solution that adds the calcium hydroxide melt into of described ratio, to sterilize by conventional method;
(3) organic mixture after fermentation, sterilization is dried, baking temperature is 45-60 ℃, and being dried to water content is 15-25%;
(4) nitrogen-fixing bacteria, phosphate solubilizing bacteria, ferment bacterium are joined in above-mentioned material according to described ratio, fully mix, stir;
(5) by urea, potassium sulfate, ironic citrate, Cobastab
1, Cobastab
12, kongpo monkshood root, semen momordicae, Chinese Stellera Root, nano controlled-release carrier join in mixture according to described ratio, fully mixes, stir;
(6) above-mentioned material is carried out under the condition of 18-45 ℃ to low temperature drying, making its water content is below 10%.
Juvenile stage at carp growth, fish is pulled out, divide and support in the middle of five ponds, 300, every pond, in four ponds, according to the injected volume of every mu of 200kg, throw in respectively microbial fish guano and the (contrast 1 of common fish guano of embodiment of the present invention 1-3, originate from Beijing Century AMMS Biotechnology Co., Ltd.), fish guano (contrast 2) is not thrown in another one pond, but throw in the common fish food of same amount, remaining feeding amount is identical, culture environment is identical, cultivation through 2-3 month, add composite microbe fertilizer of the present invention and not only can promote the Fast Growth of fish, can also improve quality and the quality of fish, reduce the generation of fish disease, thereby the fish that makes to die of illness reduces, also make the beneficial microbe in water body increase simultaneously, reduce the growth of algae in fishpond, thereby reduce the waste of fish feed, it is a kind of cost-effective method.Utilize hydroxyapatite etc. itself to there is the character of loose structure, fertilizer components is adsorbed in the inner mesh of carrier, reach the object of slow release.Hydroxyapatite also has biodegradable characteristic, and gained catabolite is various trace elements ion, and these elements can be absorbed again.Nano controlled-release additive has good biocompatibility, gastrointestinal tract mucous compatibility, each component that makes it load has controlled-release function, through twice-modified nano-complex medicine carrying amount and adsorbance, all improve a lot, fertilizer efficiency time lengthening is more than 3 months, effectively suppress the increment of animal pathogen, improve the producer's benefit.
The foregoing is only embodiments of the invention; not thereby limit the scope of the claims of the present invention; every equivalent structure or conversion of equivalent flow process that utilizes description of the present invention to do; or be directly or indirectly used in other relevant technical fields, be all in like manner included in scope of patent protection of the present invention.
Claims (2)
1. one kind adopts nano material to prepare carp released fodder, it is characterized in that, its raw material comprises the composition of following weight ratio: nitrogen-fixing bacteria 2-4 part, phosphate solubilizing bacteria 1-3 part, ferment bacterium 3-5 part, fish meal 50-60 part, soya-bean cake 75-80 part, wheat bran 20-30 part, rice bran 70-80 part, brown sugar 10-14 part, dusty yeast 8-10 part, salt 12-15 part, chicken manure 80-85 part, pasture and water 60-65 part, calcium hydroxide 10-13 part, urea 15-20 part, potassium sulfate 3-5 part, ironic citrate 3-5 part, Cobastab
10.2-0.4 part, Cobastab
120.1-0.3 part, kongpo monkshood root 4.5-5.5 part, 4-5 parts of semen momordicaes, Chinese Stellera Root 1-1.5 part, nano controlled-release carrier 20-25 part;
The preparation method of described nano controlled-release carrier is:
(1) silicon hydroxyapatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, in 65 ℃, stir 60 hours, filter, and wash and remove excessive methyl-sulfoxide (DMSO) for 3 times with the hot ethanol of 60 ℃ of temperature, put into vacuum drying chamber, 60 ℃ of temperature, be dried 24 hours, grinding is sieved, and obtains modified composite one time;
(2) 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water are mixed, in temperature 50 C, stir more than 10 hours, in 30 ℃ of temperature, first under ultrasonic electric power 350W condition, disperse 3.5 hours, and then disperse 4 hours under ultrasonic electric power 250W condition; Filter, and wash 3 times with distillation, 80 ℃ of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed to 60min at 600W power ultrasonic, with constant temperature heating device, be heated to 90 ℃, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier complexes.
2. a kind of preparation method who adopts nano material to prepare carp released fodder as claimed in claim 1, is characterized in that, comprises the following steps:
(1) pasture and water are dried, make its water content below 40%, be cut to 2-4cm, then according to described ratio, add fish meal, soya-bean cake, wheat bran, rice bran, brown sugar, dusty yeast, salt, chicken manure, fully stir, mix;
(2) said mixture is fermented, described fermentation is aerobic composting fermentation, and fermentation water accounts for the 20-30% of material gross weight, and be 50-60 hour winter oxygen supply time, and be 20-25 hour summer, and fermentation temperature is 45-60 ℃, and fermentation time is 7-10 days; The aqueous solution that adds the calcium hydroxide melt into of described ratio, to sterilize by conventional method;
(3) organic mixture after fermentation, sterilization is dried, baking temperature is 45-60 ℃, and being dried to water content is 15-25%;
(4) nitrogen-fixing bacteria, phosphate solubilizing bacteria, ferment bacterium are joined in above-mentioned material according to described ratio, fully mix, stir;
(5) by urea, potassium sulfate, ironic citrate, Cobastab
1, Cobastab
12, kongpo monkshood root, semen momordicae, Chinese Stellera Root, nano controlled-release carrier join in mixture according to described ratio, fully mixes, stir;
(6) above-mentioned material is carried out under the condition of 18-45 ℃ to low temperature drying, making its water content is below 10%.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
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CN108157672A (en) * | 2017-12-12 | 2018-06-15 | 安徽希普生物科技有限公司 | A kind of production method of nonreactive fermentation fresh water fish material for having an antibacterial action and application |
CN108192847A (en) * | 2018-02-06 | 2018-06-22 | 浦江县协盈动物饲料技术开发有限公司 | The preparation method of Composite microbe inocula for aquatic product culture |
CN113383873A (en) * | 2021-06-30 | 2021-09-14 | 烟台开发区天源水产有限公司 | Aquaculture fertilizer and preparation method thereof |
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CN103340301A (en) * | 2013-06-17 | 2013-10-09 | 苏州市阳澄湖现代农业发展有限公司 | Special compound microorganism fish fertilizer for carp and preparation method thereof |
CN103392642A (en) * | 2013-07-23 | 2013-11-20 | 苏州市阳澄湖现代农业产业园特种水产养殖有限公司 | Method for breeding mandarin fish by utilizing microorganic feed |
CN103444799A (en) * | 2013-09-10 | 2013-12-18 | 苏州莲花岛生态农业专业合作社 | Kongpo monkshood root plant based nano slow-release suspending agent |
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JPS56118480A (en) * | 1980-02-26 | 1981-09-17 | Asahi Denka Kogyo Kk | Slow release composition |
FR2561071A1 (en) * | 1984-03-19 | 1985-09-20 | Morlet Yvette | Fishing bait |
CN102002141A (en) * | 2010-11-19 | 2011-04-06 | 安徽大学 | Preparation method of polyurethane-nano kaolin composite material |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN108157672A (en) * | 2017-12-12 | 2018-06-15 | 安徽希普生物科技有限公司 | A kind of production method of nonreactive fermentation fresh water fish material for having an antibacterial action and application |
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CN113383873A (en) * | 2021-06-30 | 2021-09-14 | 烟台开发区天源水产有限公司 | Aquaculture fertilizer and preparation method thereof |
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