CN103583907B - A kind of nano carrier material that utilizes is as shrimp feed of auxiliary material and preparation method thereof - Google Patents
A kind of nano carrier material that utilizes is as shrimp feed of auxiliary material and preparation method thereof Download PDFInfo
- Publication number
- CN103583907B CN103583907B CN201310563673.3A CN201310563673A CN103583907B CN 103583907 B CN103583907 B CN 103583907B CN 201310563673 A CN201310563673 A CN 201310563673A CN 103583907 B CN103583907 B CN 103583907B
- Authority
- CN
- China
- Prior art keywords
- parts
- vitamin
- nano
- promoting agent
- feed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 241000238557 Decapoda Species 0.000 title claims abstract description 45
- 239000000463 material Substances 0.000 title claims abstract description 42
- 239000002539 nanocarrier Substances 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000002131 composite material Substances 0.000 claims abstract description 29
- 238000013270 controlled release Methods 0.000 claims abstract description 27
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 23
- 230000001737 promoting effect Effects 0.000 claims abstract description 23
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 claims abstract description 18
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 claims abstract description 18
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 claims abstract description 18
- 150000003839 salts Chemical class 0.000 claims abstract description 18
- 235000019155 vitamin A Nutrition 0.000 claims abstract description 18
- 239000011719 vitamin A Substances 0.000 claims abstract description 18
- 229940045997 vitamin a Drugs 0.000 claims abstract description 18
- 235000019733 Fish meal Nutrition 0.000 claims abstract description 15
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 claims abstract description 15
- 239000004471 Glycine Substances 0.000 claims abstract description 15
- 244000046052 Phaseolus vulgaris Species 0.000 claims abstract description 15
- 235000010627 Phaseolus vulgaris Nutrition 0.000 claims abstract description 15
- 240000004808 Saccharomyces cerevisiae Species 0.000 claims abstract description 15
- 235000014680 Saccharomyces cerevisiae Nutrition 0.000 claims abstract description 15
- ZPWVASYFFYYZEW-UHFFFAOYSA-L dipotassium hydrogen phosphate Chemical compound [K+].[K+].OP([O-])([O-])=O ZPWVASYFFYYZEW-UHFFFAOYSA-L 0.000 claims abstract description 15
- 239000004467 fishmeal Substances 0.000 claims abstract description 15
- 235000013312 flour Nutrition 0.000 claims abstract description 15
- 235000013922 glutamic acid Nutrition 0.000 claims abstract description 15
- 239000004220 glutamic acid Substances 0.000 claims abstract description 15
- 235000015099 wheat brans Nutrition 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 14
- 238000000227 grinding Methods 0.000 claims abstract description 13
- 238000003756 stirring Methods 0.000 claims abstract description 13
- 206010047700 Vomiting Diseases 0.000 claims abstract description 12
- 235000013379 molasses Nutrition 0.000 claims abstract description 12
- 230000008673 vomiting Effects 0.000 claims abstract description 12
- 239000002994 raw material Substances 0.000 claims abstract description 8
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 claims abstract description 5
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 34
- 150000001875 compounds Chemical class 0.000 claims description 20
- 241000411851 herbal medicine Species 0.000 claims description 18
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 claims description 17
- 229930003268 Vitamin C Natural products 0.000 claims description 17
- 229930003316 Vitamin D Natural products 0.000 claims description 17
- QYSXJUFSXHHAJI-XFEUOLMDSA-N Vitamin D3 Natural products C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C/C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-XFEUOLMDSA-N 0.000 claims description 17
- 235000019154 vitamin C Nutrition 0.000 claims description 17
- 239000011718 vitamin C Substances 0.000 claims description 17
- 235000019166 vitamin D Nutrition 0.000 claims description 17
- 239000011710 vitamin D Substances 0.000 claims description 17
- 150000003710 vitamin D derivatives Chemical class 0.000 claims description 17
- 229940046008 vitamin d Drugs 0.000 claims description 17
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical class CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims description 12
- 238000002156 mixing Methods 0.000 claims description 12
- LOVYCUYJRWLTSU-UHFFFAOYSA-N 2-(3,4-dichlorophenoxy)-n,n-diethylethanamine Chemical compound CCN(CC)CCOC1=CC=C(Cl)C(Cl)=C1 LOVYCUYJRWLTSU-UHFFFAOYSA-N 0.000 claims description 10
- 240000002234 Allium sativum Species 0.000 claims description 10
- 235000003092 Artemisia dracunculus Nutrition 0.000 claims description 10
- 240000001851 Artemisia dracunculus Species 0.000 claims description 10
- 235000000832 Ayote Nutrition 0.000 claims description 10
- 240000004244 Cucurbita moschata Species 0.000 claims description 10
- 235000009854 Cucurbita moschata Nutrition 0.000 claims description 10
- 235000009804 Cucurbita pepo subsp pepo Nutrition 0.000 claims description 10
- 241000735527 Eupatorium Species 0.000 claims description 10
- 244000062748 Eupatorium adenophorum Species 0.000 claims description 10
- 244000192024 Euphorbia helioscopia Species 0.000 claims description 10
- 235000012043 Euphorbia helioscopia Nutrition 0.000 claims description 10
- 235000013717 Houttuynia Nutrition 0.000 claims description 10
- 240000000691 Houttuynia cordata Species 0.000 claims description 10
- 241001495453 Parthenium argentatum Species 0.000 claims description 10
- 235000011609 Pinus massoniana Nutrition 0.000 claims description 10
- 241000018650 Pinus massoniana Species 0.000 claims description 10
- 240000003152 Rhus chinensis Species 0.000 claims description 10
- 235000014220 Rhus chinensis Nutrition 0.000 claims description 10
- 244000057114 Sapium sebiferum Species 0.000 claims description 10
- 235000005128 Sapium sebiferum Nutrition 0.000 claims description 10
- 235000004611 garlic Nutrition 0.000 claims description 10
- 235000015136 pumpkin Nutrition 0.000 claims description 10
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 9
- 229960001760 dimethyl sulfoxide Drugs 0.000 claims description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 6
- 238000001291 vacuum drying Methods 0.000 claims description 6
- 239000005995 Aluminium silicate Substances 0.000 claims description 3
- 229910021532 Calcite Inorganic materials 0.000 claims description 3
- 206010013786 Dry skin Diseases 0.000 claims description 3
- 235000012211 aluminium silicate Nutrition 0.000 claims description 3
- GDVKFRBCXAPAQJ-UHFFFAOYSA-A dialuminum;hexamagnesium;carbonate;hexadecahydroxide Chemical compound [OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[OH-].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Mg+2].[Al+3].[Al+3].[O-]C([O-])=O GDVKFRBCXAPAQJ-UHFFFAOYSA-A 0.000 claims description 3
- CGMRCMMOCQYHAD-UHFFFAOYSA-J dicalcium hydroxide phosphate Chemical compound [OH-].[Ca++].[Ca++].[O-]P([O-])([O-])=O CGMRCMMOCQYHAD-UHFFFAOYSA-J 0.000 claims description 3
- 239000012153 distilled water Substances 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 238000010438 heat treatment Methods 0.000 claims description 3
- 229960001545 hydrotalcite Drugs 0.000 claims description 3
- 229910001701 hydrotalcite Inorganic materials 0.000 claims description 3
- -1 imvite Chemical compound 0.000 claims description 3
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 3
- 239000011259 mixed solution Substances 0.000 claims description 3
- 229920001296 polysiloxane Polymers 0.000 claims description 3
- SCVFZCLFOSHCOH-UHFFFAOYSA-M potassium acetate Chemical class [K+].CC([O-])=O SCVFZCLFOSHCOH-UHFFFAOYSA-M 0.000 claims description 3
- 235000011056 potassium acetate Nutrition 0.000 claims description 3
- 239000004408 titanium dioxide Substances 0.000 claims description 3
- 238000005406 washing Methods 0.000 claims description 3
- 238000001132 ultrasonic dispersion Methods 0.000 claims 1
- 230000007423 decrease Effects 0.000 abstract description 6
- 235000019629 palatability Nutrition 0.000 abstract description 6
- 235000013305 food Nutrition 0.000 abstract description 4
- 239000000843 powder Substances 0.000 abstract description 4
- 239000011782 vitamin Substances 0.000 abstract 2
- 229940088594 vitamin Drugs 0.000 abstract 2
- 229930003231 vitamin Natural products 0.000 abstract 2
- 235000013343 vitamin Nutrition 0.000 abstract 2
- 150000003722 vitamin derivatives Chemical class 0.000 abstract 2
- 238000010298 pulverizing process Methods 0.000 abstract 1
- 239000002245 particle Substances 0.000 description 8
- 239000003337 fertilizer Substances 0.000 description 6
- 229910052588 hydroxylapatite Inorganic materials 0.000 description 6
- XYJRXVWERLGGKC-UHFFFAOYSA-D pentacalcium;hydroxide;triphosphate Chemical compound [OH-].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O XYJRXVWERLGGKC-UHFFFAOYSA-D 0.000 description 6
- 230000008901 benefit Effects 0.000 description 5
- 230000000844 anti-bacterial effect Effects 0.000 description 4
- 201000010099 disease Diseases 0.000 description 4
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 235000016709 nutrition Nutrition 0.000 description 4
- 230000035764 nutrition Effects 0.000 description 4
- 244000045947 parasite Species 0.000 description 4
- 239000000654 additive Substances 0.000 description 3
- 230000000996 additive effect Effects 0.000 description 3
- 244000037640 animal pathogen Species 0.000 description 3
- 239000000284 extract Substances 0.000 description 3
- 210000001035 gastrointestinal tract Anatomy 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000011265 semifinished product Substances 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- 230000001629 suppression Effects 0.000 description 3
- 235000013619 trace mineral Nutrition 0.000 description 3
- 239000011573 trace mineral Substances 0.000 description 3
- RZVAJINKPMORJF-UHFFFAOYSA-N Acetaminophen Chemical group CC(=O)NC1=CC=C(O)C=C1 RZVAJINKPMORJF-UHFFFAOYSA-N 0.000 description 2
- 208000030852 Parasitic disease Diseases 0.000 description 2
- 241000927735 Penaeus Species 0.000 description 2
- 210000001015 abdomen Anatomy 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 230000002141 anti-parasite Effects 0.000 description 2
- 239000003096 antiparasitic agent Substances 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 238000000855 fermentation Methods 0.000 description 2
- 230000004151 fermentation Effects 0.000 description 2
- 230000002045 lasting effect Effects 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000012795 verification Methods 0.000 description 2
- 241000238421 Arthropoda Species 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 241000238550 Penaeidae Species 0.000 description 1
- 238000009360 aquaculture Methods 0.000 description 1
- 244000144974 aquaculture Species 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000012258 culturing Methods 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000021050 feed intake Nutrition 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003387 muscular Effects 0.000 description 1
- 235000015097 nutrients Nutrition 0.000 description 1
Abstract
The invention discloses a kind of nano carrier material that utilizes as shrimp feed of auxiliary material and preparation method thereof, utilize nano carrier material as the shrimp feed of auxiliary material, raw material consists of fish meal, fermented bean dregs, wheat bran, brewer's yeast, flour, dipotassium hydrogen phosphate, vitamin, vitamin, vitamin A, nano controlled-release carrier, salt and composite feeding promoting agent.Utilize nano carrier material as the preparation method of the shrimp feed of auxiliary material, comprise following step: glycine, glutamic acid, molasses and vomiting nut are carried out ultramicro grinding by (A), obtain composite feeding promoting agent powder; (B) pulverizing of all the other components of feed is placed in mixer, stirs after adding composite feeding promoting agent; (C) be placed in each one-tenth mixed dry 20-30 minute in drier, finally adopts comminutor to make graininess finished product.The present invention with the addition of phagostimulant in utilizing nano carrier material as the shrimp feed of auxiliary material, improves the palatability of feed, improves the food ration of prawn, and the growth both having facilitated prawn decreases residual bait, is conducive to protecting water body environment.In addition, preparation method of the present invention is simple, easy to operate.
Description
technical field:
The present invention relates to a kind of aquaculture feed and preparation method thereof, be specifically related to a kind of nano carrier material that utilizes as shrimp feed of auxiliary material and preparation method thereof.
background technology:
Prawn (Penacus orientalis), formal name used at school oriental prawn, also known as Chinese prawn, spot joint shrimp.Arthropoda, Crustachia, Decapoda, Penaeidae, Penaeus.Penaeus is individual large, common name prawn.Long general 16 ~ 22 centimetres of female growing individual body, heavily about 50 ~ 80 grams, maximum reaches 30 centimetres, weighs 250 grams; Male less, long 13 ~ 18 centimetres of body, weighs 30 ~ 50 grams.Prawn is wide temperature eurysalinity aquatic/marine animals.Body is long tubular, and left and right is flat-sided, and health is divided into head, chest and belly, is made up of 20 body segments.Belly is longer, muscular, and merogenesis is obvious.
China is prawn culturing big country, and growth momentum was increasingly swift and violent in recent years.Only national cultured prawn total output in 2003 just reaches 780,000 tons, and the foreign exchange earning for China creates huge economic benefit.But many prawn feed palatabilities are bad on the market, feed intake declines, and certainly will affect the total amount of nutrients intake, also can have influence on the effect of feed undoubtedly, affect the output of prawn.
summary of the invention:
The object of the invention is to overcome that the deficiencies in the prior art provide a kind of comprehensive nutrition, good palatability utilizes nano carrier material as shrimp feed of auxiliary material and preparation method thereof.
To achieve these goals, technical scheme of the present invention is as follows:
A kind of nano carrier material that utilizes is as the shrimp feed of auxiliary material, it is characterized in that, raw material consists of fish meal, fermented bean dregs, wheat bran, brewer's yeast, flour, dipotassium hydrogen phosphate, vitamin C, vitamin D, vitamin A, nano controlled-release carrier, salt, Chinese herbal medicine compound thing and composite feeding promoting agent;
With weight parts, fish meal 30-35 part, fermented bean dregs 25-35 part, wheat bran 25-35 part, brewer's yeast 1-3 part, flour 15-20 part, dipotassium hydrogen phosphate 0.5-1.5 part, vitamin C 0.5-1.5 part, vitamin D 0.2-0.5 part, vitamin A 0.5-0.8 part, nano controlled-release carrier 15-20 part, salt 1-5 part, Chinese herbal medicine compound thing is: Pinus massoniana 5-15 part, China tree 12-24 part, garlic 20-30 part, pumpkin 16-27 part, Chinese tallowtree leaf 6-13 part, fragrant eupatorium herb 10-20 part, Eupatorium adenophorum 10-20 part, guayule rubber 10-20 part, kuh-seng 10-20 part, Chinese gall 15-26 part, wolf's milk 1-5 part, cordate houttuynia 20-30 part and tarragon 18-26 part and composite feeding promoting agent 0.2-0.8 part.
Described composite feeding promoting agent comprises glycine, glutamic acid, molasses and vomiting nut;
With weight parts, glycine 15-25 part, glutamic acid 30-40 part, molasses 10-20 part and vomiting nut 25-35 part.The preparation method of described nano controlled-release carrier is:
(1) silicone hydroxyl apatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, stir 60 hours in 65 DEG C, filter, and wash the excessive methyl-sulfoxide (DMSO) of 3 removings with the hot ethanol of 60 DEG C of temperature, put into vacuum drying chamber, 60 DEG C of temperature dryings 24 hours, grinding is sieved, and obtains a modified composite;
(2) by 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water mixing, more than 10 hours are stirred in temperature 50 C, in temperature 30 DEG C, first disperse 3.5 hours under ultrasonic electric power 350W condition, and then disperse 4 hours under ultrasonic electric power 250W condition.To filter, and with distilling washing 3 times, 80 DEG C of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed 60min at 600W power ultrasonic, be heated to 90 DEG C with constant temperature heating device, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier.
With weight parts, raw material consists of fish meal 25 parts, fermented bean dregs 30 parts, 30 parts, wheat bran, brewer's yeast 3 parts, 20 parts, flour, dipotassium hydrogen phosphate 0.5 part, vitamin C 0.5 part, vitamin D 0.5 part, vitamin A 0.8 part, 1.3 parts, nano controlled-release carrier, salt 5 parts, Chinese herbal medicine compound thing is: Pinus massoniana 15 parts, China tree 24 parts, 30 parts, garlic, pumpkin 27 parts, Chinese tallowtree leaf 13 parts, fragrant eupatorium herb 20 parts, Eupatorium adenophorum 20 parts, guayule rubber 20 parts, kuh-seng 20 parts, 26 parts, Chinese gall, wolf's milk 5 parts, cordate houttuynia 30 parts and tarragon 26 parts and composite feeding promoting agent 0.8 part.
Utilize nano carrier material as a preparation method for the shrimp feed of auxiliary material, it is characterized in that, comprise following step:
(A) glycine 15-25 part and glutamic acid 30-40 part are carried out ultramicro grinding, cross 200 mesh sieves; Vomiting nut 25-35 part extracts 0.5h in 100 DEG C of water, filters, after obtaining clear liquid, add the glycine through ultramicro grinding and glutamic acid, after abundant dissolving, be concentrated by spraying dry and obtain dry powder, stir with molasses 10-20 part afterwards and obtain composite feeding promoting agent;
(B) by fish meal 30-35 part, fermented bean dregs 25-35 part, wheat bran 25-35 part, brewer's yeast 1-3 part, flour 15-20 part, dipotassium hydrogen phosphate 0.5-1.5 part, vitamin C 0.5-1.5 part, vitamin D 0.2-0.5 part, vitamin A 0.5-0.8 part, nano controlled-release carrier 15-20 part, salt 1-5 part, Chinese herbal medicine compound thing is: Pinus massoniana 5-15 part, China tree 12-24 part, garlic 20-30 part, pumpkin 16-27 part, Chinese tallowtree leaf 6-13 part, fragrant eupatorium herb 10-20 part, Eupatorium adenophorum 10-20 part, guayule rubber 10-20 part, kuh-seng 10-20 part, Chinese gall 15-26 part, wolf's milk 1-5 part, cordate houttuynia 20-30 part and tarragon 18-26 part are pulverized respectively and are placed in mixer, start after adding composite feeding promoting agent 0.2-0.8 part in step (A) and salt 1-5 part to stir, mixing speed is 20 turns per minute, mixing time is 30-50 minute,
(C) the feed semi-finished product after mixing in step (B) are placed in the dry 20-30 minute of drier, finally adopt comminutor to make graininess finished product, finished particle particle size 2-3mm.
Beneficial effect of the present invention is as follows:
The present invention with the addition of phagostimulant in utilizing nano carrier material as the shrimp feed of auxiliary material, improves the palatability of feed, improves the food ration of prawn, and the growth both having facilitated prawn decreases residual bait, is conducive to protecting water body environment.The nano carrier material that utilizes of the present invention also added vitamin A, vitamin C and vitamin D, comprehensive nutrition as in the shrimp feed of auxiliary material, meets the demand of prawn growth.In addition, preparation method of the present invention is simple, easy to operate.With the addition of the Chinese herbal medicine with the sick function of anti parasitic in feed, the parasite disease that can fundamentally prevent and treat, through actual verification, the present invention can reduce the generation of parasite disease and reduce the quantity infecting parasitic disease; There is the Chinese herbal medicine particle of bactericidal effect, by fermentation, the effect of various composition fully played, be applied to that water body is rapid-action, action time is lasting, environmental protection and there is bactericidal effect; In addition, the present invention fills a prescription rationally, and preparation method is simple.Utilize hydroxyapatite etc. itself to have the character of loose structure, fertilizer components is adsorbed in the inner mesh of carrier, reach the object of slow releasing.Hydroxyapatite also has biodegradability properties, and gained catabolite is various trace elements ion, and these elements can be gradually resorbed.Nano controlled-release additive has good biocompatibility, gastrointestinal tract mucous compatibility, each component making it load has controlled-release function, all improve a lot through twice-modified nano-complex drugloading rate and adsorbance, fertilizer efficiency time lengthening more than 3 months, the increment of effective suppression animal pathogen, improves the benefit of the producer.
detailed description of the invention:
The technological means realized to make the present invention, creation characteristic, reaching object and effect is easy to understand, below in conjunction with specific embodiment, setting forth the present invention further.
Embodiment 1:
A kind of nano carrier material that utilizes is as the shrimp feed of auxiliary material, it is characterized in that, raw material consists of fish meal, fermented bean dregs, wheat bran, brewer's yeast, flour, dipotassium hydrogen phosphate, vitamin C, vitamin D, vitamin A, nano controlled-release carrier, salt, Chinese herbal medicine compound thing and composite feeding promoting agent;
With weight parts, fish meal 30 parts, fermented bean dregs 25 parts, 25 parts, wheat bran, brewer's yeast 1 part, 15 parts, flour, dipotassium hydrogen phosphate 0.5 part, vitamin C 0.5 part, vitamin D 0.2 part, vitamin A 0.5 part, 15 parts, nano controlled-release carrier, salt 1 part, Chinese herbal medicine compound thing are: Pinus massoniana 5 parts, China tree 12 parts, 20 parts, garlic, pumpkin 16 parts, Chinese tallowtree leaf 6 parts, fragrant eupatorium herb 10 parts, Eupatorium adenophorum 10 parts, guayule rubber 10 parts, kuh-seng 10 parts, 15 parts, Chinese gall, wolf's milk 1 part, cordate houttuynia 20 parts and tarragon 18 parts.
Described composite feeding promoting agent comprises glycine, glutamic acid, molasses and vomiting nut; The preparation method of described nano controlled-release carrier is:
(1) silicone hydroxyl apatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, stir 60 hours in 65 DEG C, filter, and wash the excessive methyl-sulfoxide (DMSO) of 3 removings with the hot ethanol of 60 DEG C of temperature, put into vacuum drying chamber, 60 DEG C of temperature dryings 24 hours, grinding is sieved, and obtains a modified composite;
(2) by 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water mixing, more than 10 hours are stirred in temperature 50 C, in temperature 30 DEG C, first disperse 3.5 hours under ultrasonic electric power 350W condition, and then disperse 4 hours under ultrasonic electric power 250W condition.To filter, and with distilling washing 3 times, 80 DEG C of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; (3) above-mentioned 1 part of twice-modified compound is disperseed 60min at 600W power ultrasonic, be heated to 90 DEG C with constant temperature heating device, and stir (1200r/min) 60 minutes with mechanical agitator; Obtain nano controlled-release carrier.
With weight parts, glycine 15 parts, 30 parts, glutamic acid, 10 parts, molasses and vomiting nut 25 parts.
With weight parts, raw material consists of fish meal 25 parts, fermented bean dregs 30 parts, 30 parts, wheat bran, brewer's yeast 3 parts, 20 parts, flour, dipotassium hydrogen phosphate 0.5 part, vitamin C 0.5 part, vitamin D 0.5 part, vitamin A 0.8 part, 15 parts, nano controlled-release carrier, salt 5 parts, Chinese herbal medicine compound thing is: Pinus massoniana 15 parts, China tree 24 parts, 30 parts, garlic, pumpkin 27 parts, Chinese tallowtree leaf 13 parts, fragrant eupatorium herb 20 parts, Eupatorium adenophorum 20 parts, guayule rubber 20 parts, kuh-seng 20 parts, 26 parts, Chinese gall, wolf's milk 5 parts, cordate houttuynia 30 parts and tarragon 26 parts and composite feeding promoting agent 0.8 part.
Utilize nano carrier material as a preparation method for the shrimp feed of auxiliary material, it is characterized in that, comprise following step:
(A) glycine 15 parts and 30 parts, glutamic acid are carried out ultramicro grinding, cross 200 mesh sieves; Vomiting nut 25 parts extracts 0.5h in 100 DEG C of water, filters, after obtaining clear liquid, add the glycine through ultramicro grinding and glutamic acid, after abundant dissolving, be concentrated by spraying dry and obtain dry powder, stir with 10 parts, molasses afterwards and obtain composite feeding promoting agent;
(B) by fish meal 30 parts, fermented bean dregs 25 parts, 25 parts, wheat bran, brewer's yeast 1 part, 15 parts, flour, dipotassium hydrogen phosphate 0.5 part, vitamin C 0.5 part, vitamin D 0.2 part, vitamin A 0.5 part, 15 parts, nano controlled-release carrier, salt 1 part, Chinese herbal medicine compound thing is: Pinus massoniana 5 parts, China tree 12 parts, 20 parts, garlic, pumpkin 16 parts, Chinese tallowtree leaf 6 parts, fragrant eupatorium herb 10 parts, Eupatorium adenophorum 10 parts, guayule rubber 10 parts, kuh-seng 10 parts, 15 parts, Chinese gall, wolf's milk 1 part, cordate houttuynia 20 parts and tarragon 18 parts are pulverized respectively and are placed in mixer, start after adding composite feeding promoting agent 0.2 part in step (A) and salt 1 part to stir, mixing speed is 20 turns per minute, mixing time is 30 minutes,
(C) the feed semi-finished product after mixing in step (B) are placed in drier dry 20 minutes, finally adopt comminutor to make graininess finished product, finished particle particle size 2 mm.
The present invention with the addition of phagostimulant in utilizing nano carrier material as the shrimp feed of auxiliary material, improves the palatability of feed, improves the food ration of prawn, and the growth both having facilitated prawn decreases residual bait, is conducive to protecting water body environment.The nano carrier material that utilizes of the present invention also added vitamin A, vitamin C and vitamin D, comprehensive nutrition as in the shrimp feed of auxiliary material, meets the demand of prawn growth.In addition, preparation method of the present invention is simple, easy to operate.Embodiment 1 is known by actual cultivation, and the speed of growth of the prawn of the present embodiment improves 1.5 times, and the residual bait in water decreases 30%.Utilize hydroxyapatite etc. itself to have the character of loose structure, fertilizer components is adsorbed in the inner mesh of carrier, reach the object of slow releasing.Hydroxyapatite also has biodegradability properties, and gained catabolite is various trace elements ion, and these elements can be gradually resorbed.Nano controlled-release additive has good biocompatibility, gastrointestinal tract mucous compatibility, each component making it load has controlled-release function, all improve a lot through twice-modified nano-complex drugloading rate and adsorbance, fertilizer efficiency time lengthening more than 3 months, the increment of effective suppression animal pathogen, improves the benefit of the producer.
Embodiment 2:
In this enforcement, a kind of nano carrier material that utilizes is as the shrimp feed of auxiliary material, it is characterized in that, raw material consists of fish meal, fermented bean dregs, wheat bran, brewer's yeast, flour, dipotassium hydrogen phosphate, vitamin C, vitamin D, vitamin A, nano controlled-release carrier, salt, Chinese herbal medicine compound thing and composite feeding promoting agent;
With weight parts, by fish meal 35 parts, fermented bean dregs 35 parts, 35 parts, wheat bran, brewer's yeast 3 parts, 20 parts, flour, dipotassium hydrogen phosphate 1.5 parts, vitamin C 1.5 parts, vitamin D 0.5 part, vitamin A 0.8 part, 20 parts, nano controlled-release carrier, salt 5 parts, Chinese herbal medicine compound thing is: Pinus massoniana 15 parts, China tree 24 parts, 30 parts, garlic, pumpkin 27 parts, Chinese tallowtree leaf 13 parts, fragrant eupatorium herb 20 parts, Eupatorium adenophorum 20 parts, guayule rubber 20 parts, kuh-seng 20 parts, 26 parts, Chinese gall, wolf's milk 5 parts, cordate houttuynia 30 parts and tarragon 26 parts and composite feeding promoting agent 0.2-0.8 part.
Described composite feeding promoting agent comprises glycine, glutamic acid, molasses and vomiting nut;
With weight parts, glycine 15-25 part, glutamic acid 30-40 part, molasses 10-20 part and vomiting nut 25-35 part.
With weight parts, raw material consists of fish meal 25 parts, fermented bean dregs 30 parts, 30 parts, wheat bran, brewer's yeast 3 parts, 20 parts, flour, dipotassium hydrogen phosphate 0.5 part, vitamin C 0.5 part, vitamin D 0.5 part, vitamin A 0.8 part, 20 parts, nano controlled-release carrier, salt 5 parts, Chinese herbal medicine compound thing is: Pinus massoniana 15 parts, China tree 24 parts, 30 parts, garlic, pumpkin 27 parts, Chinese tallowtree leaf 13 parts, fragrant eupatorium herb 20 parts, Eupatorium adenophorum 20 parts, guayule rubber 20 parts, kuh-seng 20 parts, 26 parts, Chinese gall, wolf's milk 5 parts, cordate houttuynia 30 parts and tarragon 26 parts and composite feeding promoting agent 0.8 part.
Utilize nano carrier material as a preparation method for the shrimp feed of auxiliary material, it is characterized in that, comprise following step:
(A) glycine 25 parts and 40 parts, glutamic acid are carried out ultramicro grinding, cross 200 mesh sieves; Vomiting nut 35 parts extracts 0.5h in 100 DEG C of water, filters, after obtaining clear liquid, add the glycine through ultramicro grinding and glutamic acid, after abundant dissolving, be concentrated by spraying dry and obtain dry powder, stir with 20 parts, molasses afterwards and obtain composite feeding promoting agent;
(B) by fish meal 35 parts, fermented bean dregs 35 parts, 35 parts, wheat bran, brewer's yeast 3 parts, 20 parts, flour, dipotassium hydrogen phosphate 1.5 parts, vitamin C 1.5 parts, vitamin D 0.5 part, vitamin A 0.8 part, 20 parts, nano controlled-release carrier, salt 5 parts, Chinese herbal medicine compound thing is: Pinus massoniana 15 parts, China tree 24 parts, 30 parts, garlic, pumpkin 27 parts, Chinese tallowtree leaf 13 parts, fragrant eupatorium herb 20 parts, Eupatorium adenophorum 20 parts, guayule rubber 20 parts, kuh-seng 20 parts, 26 parts, Chinese gall, wolf's milk 5 parts, cordate houttuynia 30 parts and tarragon 26 parts are pulverized respectively and are placed in mixer, start after adding composite feeding promoting agent 0.8 part in step (A) and salt 5 parts to stir, mixing speed is 20 turns per minute, mixing time is 50 minutes,
(C) the feed semi-finished product after mixing in step (B) are placed in drier dry 30 minutes, finally adopt comminutor to make graininess finished product, finished particle particle size 3mm.
The present invention with the addition of phagostimulant in utilizing nano carrier material as the shrimp feed of auxiliary material, improves the palatability of feed, improves the food ration of prawn, and the growth both having facilitated prawn decreases residual bait, is conducive to protecting water body environment.The nano carrier material that utilizes of the present invention also added vitamin A, vitamin C and vitamin D, comprehensive nutrition as in the shrimp feed of auxiliary material, meets the demand of prawn growth.In addition, preparation method of the present invention is simple, easy to operate.Embodiment 2 is known by actual cultivation, and the speed of growth of the prawn of the present embodiment improves 1.4 times, and the residual bait in water decreases 33%.With the addition of the Chinese herbal medicine with the sick function of anti parasitic in feed, the parasite disease that can fundamentally prevent and treat, through actual verification, the present invention can reduce the generation of parasite disease and reduce the quantity infecting parasitic disease; There is the Chinese herbal medicine particle of bactericidal effect, by fermentation, the effect of various composition fully played, be applied to that water body is rapid-action, action time is lasting, environmental protection and there is bactericidal effect; In addition, the present invention fills a prescription rationally, and preparation method is simple.Utilize hydroxyapatite etc. itself to have the character of loose structure, fertilizer components is adsorbed in the inner mesh of carrier, reach the object of slow releasing.Hydroxyapatite also has biodegradability properties, and gained catabolite is various trace elements ion, and these elements can be gradually resorbed.Nano controlled-release additive has good biocompatibility, gastrointestinal tract mucous compatibility, each component making it load has controlled-release function, all improve a lot through twice-modified nano-complex drugloading rate and adsorbance, fertilizer efficiency time lengthening more than 3 months, the increment of effective suppression animal pathogen, improves the benefit of the producer.
More than show and describe general principle of the present invention and principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and description just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.
Claims (1)
1. one kind utilizes nano carrier material as the shrimp feed of auxiliary material, it is characterized in that, raw material consists of fish meal, fermented bean dregs, wheat bran, brewer's yeast, flour, dipotassium hydrogen phosphate, vitamin C, vitamin D, vitamin A, nano controlled-release carrier, salt, Chinese herbal medicine compound thing and composite feeding promoting agent;
With weight parts, fish meal 30-35 part, fermented bean dregs 25-35 part, wheat bran 25-35 part, brewer's yeast 1-3 part, flour 15-20 part, dipotassium hydrogen phosphate 0.5-1.5 part, vitamin C 0.5-1.5 part, vitamin D 0.2-0.5 part, vitamin A 0.5-0.8 part, nano controlled-release carrier 15-20 part, salt 1-5 part, Chinese herbal medicine compound thing is: Pinus massoniana 5-15 part, China tree 12-24 part, garlic 20-30 part, pumpkin 16-27 part, Chinese tallowtree leaf 6-13 part, fragrant eupatorium herb 10-20 part, Eupatorium adenophorum 10-20 part, guayule rubber 10-20 part, kuh-seng 10-20 part, Chinese gall 15-26 part, wolf's milk 1-5 part, cordate houttuynia 20-30 part and tarragon 18-26 part and composite feeding promoting agent 0.2-0.8 part, described composite feeding promoting agent comprises glycine, glutamic acid, molasses and vomiting nut, with weight parts, glycine 15-25 part, glutamic acid 30-40 part, molasses 10-20 part and vomiting nut 25-35 part, the preparation method of described nano controlled-release carrier is:
(1) silicone hydroxyl apatite, concave convex rod, hydrotalcite, imvite, titanium dioxide, calcite, kaolin are mixed according to the mass fraction proportioning of 35-45:10-15: 10-15:8-10:8-10:7-8:5-7, join in the mixed solution of 230 parts of methyl-sulfoxides (DMSO) and 50 parts of methyl alcohol, stir 60 hours in 65 DEG C, filter, and wash the excessive methyl-sulfoxide (DMSO) of 3 removings with the hot ethanol of 60 DEG C of temperature, put into vacuum drying chamber, 60 DEG C of temperature dryings 24 hours, grinding is sieved, and obtains a modified composite;
(2) by 1 part of modified composite, 15 parts of potassium acetates and 25 parts of distilled water mixing, more than 10 hours are stirred in temperature 50 C, in temperature 30 DEG C, first disperse 3.5 hours under ultrasonic electric power 350W condition, and then disperse 4 hours under ultrasonic electric power 250W condition;
(3) to filter, and with distilling washing 3 times, 80 DEG C of vacuum drying 24 hours, grinding is sieved, and obtains twice-modified compound; By above-mentioned 1 part of twice-modified compound at 600W power ultrasonic dispersion 60min, be heated to 90 DEG C with constant temperature heating device, and stir 60 minutes with mechanical agitator with 1200r/min; Obtain nano controlled-release carrier.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310563673.3A CN103583907B (en) | 2013-11-14 | 2013-11-14 | A kind of nano carrier material that utilizes is as shrimp feed of auxiliary material and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310563673.3A CN103583907B (en) | 2013-11-14 | 2013-11-14 | A kind of nano carrier material that utilizes is as shrimp feed of auxiliary material and preparation method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN103583907A CN103583907A (en) | 2014-02-19 |
| CN103583907B true CN103583907B (en) | 2015-11-04 |
Family
ID=50074394
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201310563673.3A Active CN103583907B (en) | 2013-11-14 | 2013-11-14 | A kind of nano carrier material that utilizes is as shrimp feed of auxiliary material and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN103583907B (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107242394A (en) * | 2016-12-30 | 2017-10-13 | 定远县仓镇恒润养殖专业合作社 | A kind of high lobster special feed of Se content |
| CN106509503A (en) * | 2016-12-30 | 2017-03-22 | 定远县仓镇恒润养殖专业合作社 | Selenium-enriched lobster feed |
| CN107535692B (en) * | 2017-09-18 | 2021-07-02 | 江苏瑞牧生物科技有限公司 | Feeding vitamin carrier and preparation method thereof |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1853498A (en) * | 2005-04-27 | 2006-11-01 | 南通巴大饲料有限公司 | Incommensurable ecological nutrient mixed forage for aquatic production |
| CN102002141A (en) * | 2010-11-19 | 2011-04-06 | 安徽大学 | Preparation method of polyurethane-nano kaolin composite material |
| CN102845589A (en) * | 2012-08-31 | 2013-01-02 | 杨高林 | Feed for juvenile prawns and preparation method thereof |
| CN103250877A (en) * | 2013-05-17 | 2013-08-21 | 兰州天峰生物科技有限责任公司 | Natural Chinese herbal medicine animal feed additive and application thereof |
-
2013
- 2013-11-14 CN CN201310563673.3A patent/CN103583907B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1853498A (en) * | 2005-04-27 | 2006-11-01 | 南通巴大饲料有限公司 | Incommensurable ecological nutrient mixed forage for aquatic production |
| CN102002141A (en) * | 2010-11-19 | 2011-04-06 | 安徽大学 | Preparation method of polyurethane-nano kaolin composite material |
| CN102845589A (en) * | 2012-08-31 | 2013-01-02 | 杨高林 | Feed for juvenile prawns and preparation method thereof |
| CN103250877A (en) * | 2013-05-17 | 2013-08-21 | 兰州天峰生物科技有限责任公司 | Natural Chinese herbal medicine animal feed additive and application thereof |
Non-Patent Citations (2)
| Title |
|---|
| 中草药在水产健康养殖中的应用;黄玉柳等;《安徽农业科学》;20101130;第38卷(第11期);第5726页第2.1节 * |
| 蒙脱石有机化插层改性及应用研究;余丽秀等;《中国非金属矿工业导刊》;20030831(第4期);第22－25页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103583907A (en) | 2014-02-19 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103549213B (en) | A kind of pollution-free slowly-releasing fertilizer efficiency carp fertilizer and preparation method thereof | |
| CN104026365A (en) | Digestible pig feed and preparation method thereof | |
| CN107467351A (en) | A kind of compound microbial fermented fodder | |
| CN103461715B (en) | Aquatic feed utilizing nano-carrier material as auxiliary material and preparing method for aquatic feed | |
| CN102813084B (en) | Pig feed for feeding farm pigs | |
| CN107683969A (en) | One broad sow microbial fermentation organic feed | |
| CN103519009A (en) | Healthcare sand for pigeons | |
| CN104621390A (en) | Breast-feeding sow feed and preparation method thereof | |
| CN105941923A (en) | Pork pig feed and preparation method thereof | |
| CN103583907B (en) | A kind of nano carrier material that utilizes is as shrimp feed of auxiliary material and preparation method thereof | |
| CN109362983A (en) | A kind of selenium-rich chicken feed and preparation method thereof | |
| CN109043166A (en) | A kind of seven-star tea grounds fermented feed and preparation method thereof for improving fermentation bed cultivation pig quality | |
| CN107373035A (en) | A kind of chicken manure stalk soya-bean cake pig feed and preparation method thereof | |
| CN105815595A (en) | Green high-protein chicken feed formula for improving immunity of chicken body | |
| CN103535563B (en) | A kind of high-efficiency sustained-release fertilizer efficiency silver carp fertilizer and preparation method thereof | |
| CN103704509A (en) | Method for preparing slow release feed for carps by adopting nano materials | |
| CN109430176A (en) | Earthworm high yield healthy aquaculture method | |
| CN108936038A (en) | A kind of method for breeding of ferment meat goose feed and preparation method thereof and meat goose | |
| CN103583906B (en) | Compound induced slow-release aquaculture fertilizer and preparation method thereof | |
| CN107897511A (en) | Improve the egg feedstuff of chicken and egg quality | |
| CN104171540B (en) | A kind of weanling pig anti-diarrhea growth-promoting changqiang immunity compound Chinese herbal medicinal feed additive and preparation method thereof | |
| CN103583860B (en) | A kind of fleshy duck fodder containing fresh flower | |
| CN103859199A (en) | Chinese herbal medicine antibiotic-free biological feed additive used for duck | |
| CN106858067A (en) | Livestock and poultry nonreactive growth promotion compound preparation and its production and use | |
| CN105995164A (en) | Poultry feed and preparation method thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CB03 | Change of inventor or designer information | ||
| CB03 | Change of inventor or designer information |
Inventor after: Zhao Xiao Inventor after: Zhu Lin Inventor before: Du Weilin |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20171020 Address after: 201500 Shanghai Jinshan District 6988 Town Gallery Road No. Patentee after: SHANGHAI HARMONY FEED Co.,Ltd. Address before: 215133 Jiangsu city of Suzhou province and Xiangcheng District Yuan Zhen Zhu Jing Cun Patentee before: SUZHOU CITY XIANGCHENG DISTRICT NEW ERA SPECIAL AQUATIC FARM |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20231220 Address after: 433000 xinlirenkou Industrial Park, Zhanggou Town, Xiantao City, Hubei Province Patentee after: Hubei Zhaoliang Biotechnology Co.,Ltd. Address before: No. 6988 Caoling Highway, Langxia Town, Jinshan District, Shanghai, 201500 Patentee before: SHANGHAI HARMONY FEED Co.,Ltd. |